CN106120160A - 一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法 - Google Patents

一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法 Download PDF

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CN106120160A
CN106120160A CN201610709515.8A CN201610709515A CN106120160A CN 106120160 A CN106120160 A CN 106120160A CN 201610709515 A CN201610709515 A CN 201610709515A CN 106120160 A CN106120160 A CN 106120160A
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张泽成
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Anhui Province Taihu Ze Hong Plastic Co Ltd
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Abstract

本发明公开了一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，是由以下重量份的原料制成：生态棉纤维3‑5，竹丝纤维粉3‑7，三聚氰胺1‑2，纳米电气石粉4‑8，PAMAM溶液4‑9，聚乳酸5‑10，聚乙二醇200 1‑2，硅烷偶联剂KH560 3‑7，活性炭3‑5，薄荷香精4‑8，高碘酸钠溶液10‑15，等规聚丙烯50‑70，硅藻土3‑6，十二烷基磺酸钠1‑2，羟甲基纤维素钠适量，水适量；在无纺布中添加纳米电气石粉，可以达到连续释放负氧离子的效果，应用于服装内衬时，具有镇静、镇痛、镇咳、止痒、增食欲、降血压之效；配合添加生态棉纤维使目标材料具有生物降解、环保生态等特点。

Description

一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其 制备方法
技术领域
本发明涉及一种无纺布及其制备方法，具体涉及一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法。
背景技术
无纺布是一种非织造布，它是直接利用高聚物切片、短纤维或长丝将纤维通过气流或机械成网，然后经过水刺，针刺，或热轧加固，最后经过后整理形成的无编织的布料。具有柔软、透气和平面结构的新型纤维制品，优点是不产生纤维屑，强韧、耐用、丝般柔软，而且还有棉质的感觉，已被广泛用于服装领域。随着人们对“生态、健康、环保”理念的不断追求，纺织品和时尚、健康环保已紧密联系在一起，这种时尚折射出的是人类对自身的关爱和对生存环境的关注，同时由于生态纺织品概念在全球范围内的推广，以及人们追求天然舒适、回归自然、返璞归真的心理，绿色纺织品已经成为未来纺织品发展的主要趋向。
蒋颖刚在《含竹炭粉内衬布制备与吸附性能研究》中，利用竹炭粉和非织造布，通过涂层、浸轧等方法，制成多种含竹炭粉非织造衬布。然而，还存在着不能提供负氧离子、不能释放提神清凉的芳香等有利于人的身体健康、提神抗疲劳的不足之处。
发明内容
综合以上的考虑，本发明提供一种无纺布及其配方，目的在于解决当无纺布应用于汽车内饰时，不能连续释放负氧离子，提供更好的车内空间的缺陷。
为实现上述目的， 本发明的技术方案如下：
一种保温的、可连续释放负氧离子的含竹丝纤维无纺布，其特征在于，由以下重量份的原料制成：
生态棉纤维3-5，竹丝纤维粉3-7，三聚氰胺1-2，纳米电气石粉4-8，PAMAM溶液4-9，聚乳酸5-10，聚乙二醇200 1-2，硅烷偶联剂KH560 3-7，活性炭3-5，薄荷香精4-8，高碘酸钠溶液10-15，等规聚丙烯50-70，硅藻土3-6，十二烷基磺酸钠1-2，羟甲基纤维素钠适量，水适量；
所述高碘酸钠溶液的浓度为0.1-10g/L；PAMAM溶液浓度为1-10g/L。
所述的一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，由以下步骤制成：
a. 在150-200℃下，将纳米电气石粉加入到聚乳酸中，再加入聚乙二醇200、硅烷偶联剂KH560，搅拌均匀，使纳米电气石粉均匀分散到聚乳酸中，形成微球，过滤并烘干；
b. 将活性炭、生态棉纤维添加到水中分散均匀，然后向其中添加薄荷香精，继续分散，分散均匀后转入抽真空条件下静置3-5h，后经离心、干燥、研磨处理得到负载有薄荷香精的活性炭粉；
c. 将竹丝纤维粉置于高碘酸钠溶液中避光氧化反应3-5h，反应温度为40-110℃，过滤、水洗、烘干，得到氧化竹纤维；将氧化竹纤维浸渍在PAMAM 溶液中3-6h，反应温度25-85℃，过滤烘干并研磨，得到PAMAM 接枝竹丝纤维粉；
d. 将等规聚丙烯、步骤a所得微球、步骤b所得负载薄荷香精的活性炭粉、步骤c所得PAMAM接枝竹丝纤维粉、三聚氰胺添加到螺杆挤压机进行熔融，再经纺丝、牵伸、成网、热轧后制得无纺布；
e. 将硅藻土加入到水中，搅拌均匀后加入十二烷基磺酸钠，搅拌均匀后加入羟甲基纤维素钠、三聚氰胺，调整粘度适中，制得浆液；将步骤d所得无纺布完全浸没于浆液，并放入超声波振荡器中超声 5-10min，取出，采用“二浸二轧”的方法，即充分浸没，用浸轧机轧液，再一次浸没，然后用浸轧机轧液后，放入焙烘机，烘焙2-5min，取出。
所述的一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，步骤b中所述烘焙机烘焙温度为70-110℃。
本发明的有益效果是：在无纺布中添加纳米电气石粉，可以达到连续释放负氧离子的效果，应用于服装内衬时，具有镇静、镇痛、镇咳、止痒、增食欲、降血压之效，搭配薄荷香精，可以使人神清气爽，抗疲劳；利用聚乳酸来包裹纳米电气石粉，不仅防止了纳米电气石粉的破碎和脱落，并且促进了电气石粉与聚丙烯基底的容合与分散，同时聚乳酸具有优良的透气性、透氧性，以及抑菌及抗霉特性，提高了无纺布的抗霉性，延长使用年限；用活性炭来负载薄荷香精，增加了薄荷香精的载入量及空气接触面积，达到更加持久的释放效果，同时引入了活性炭的吸附特性，增加无纺布吸附异味的功能；竹丝纤维经高碘酸钠氧化后，其表面的羟基基团被氧化为醛基甚至羧基，与PAMAM 表面的氨基发生交联反应，从而将PAMAM 接枝到竹丝纤维上，不仅可以使竹丝纤维更加柔软蓬松，而且增强了竹丝纤维与等规聚丙烯基底的融合；配合添加生态棉纤维使目标材料具有生物降解、节能改排、环保生态等特点。
具体实施方式
下面结合实施例， 对本发明的具体实施方式作进一步描述。
实施例
一种保温的、可连续释放负氧离子的含竹丝纤维无纺布，其特征在于，由以下重量份的原料制成：
生态棉纤维5，竹丝纤维粉7，三聚氰胺2，纳米电气石粉8，PAMAM溶液9，聚乳酸10，聚乙二醇200 2，硅烷偶联剂KH560 7，活性炭5，薄荷香精8，高碘酸钠溶液15，等规聚丙烯70，硅藻土6，十二烷基磺酸钠2，羟甲基纤维素钠适量，水适量；
所述高碘酸钠溶液的浓度为0.1-10g/L；PAMAM溶液浓度为1-10g/L。
所述的一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，由以下步骤制成：
a. 在150-200℃下，将纳米电气石粉加入到聚乳酸中，再加入聚乙二醇200、硅烷偶联剂KH560，搅拌均匀，使纳米电气石粉均匀分散到聚乳酸中，形成微球，过滤并烘干；
b. 将活性炭、生态棉纤维添加到水中分散均匀，然后向其中添加薄荷香精，继续分散，分散均匀后转入抽真空条件下静置3-5h，后经离心、干燥、研磨处理得到负载有薄荷香精的活性炭粉；
c. 将竹丝纤维粉置于高碘酸钠溶液中避光氧化反应3-5h，反应温度为40-110℃，过滤、水洗、烘干，得到氧化竹纤维；将氧化竹纤维浸渍在PAMAM 溶液中3-6h，反应温度25-85℃，过滤烘干并研磨，得到PAMAM 接枝竹丝纤维粉；
d. 将等规聚丙烯、步骤a所得微球、步骤b所得负载薄荷香精的活性炭粉、步骤c所得PAMAM接枝竹丝纤维粉、三聚氰胺添加到螺杆挤压机进行熔融，再经纺丝、牵伸、成网、热轧后制得无纺布；
e. 将硅藻土加入到水中，搅拌均匀后加入十二烷基磺酸钠，搅拌均匀后加入羟甲基纤维素钠、三聚氰胺，调整粘度适中，制得浆液；将步骤d所得无纺布完全浸没于浆液，并放入超声波振荡器中超声 5-10min，取出，采用“二浸二轧”的方法，即充分浸没，用浸轧机轧液，再一次浸没，然后用浸轧机轧液后，放入焙烘机，烘焙2-5min，取出。
所述的一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，步骤b中所述烘焙机烘焙温度为70-110℃。
本发明的技术参数为：
单位重量无纺布的甲醛吸附率≥11.09%，苯吸附率≥14.83%，TVOC吸附率≥13.42%。

Claims (3)

1.一种保温的、可连续释放负氧离子的含竹丝纤维无纺布，其特征在于，由以下重量份的原料制成：
生态棉纤维3-5，竹丝纤维粉3-7，三聚氰胺1-2，纳米电气石粉4-8，PAMAM溶液4-9，聚乳酸5-10，聚乙二醇200 1-2，硅烷偶联剂KH560 3-7，活性炭3-5，薄荷香精4-8，高碘酸钠溶液10-15，等规聚丙烯50-70，硅藻土3-6，十二烷基磺酸钠1-2，羟甲基纤维素钠适量，水适量；
所述高碘酸钠溶液的浓度为0.1-10g/L；PAMAM溶液浓度为1-10g/L。
2.根据权利要求1所述的一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，由以下步骤制成：
a. 在150-200℃下，将纳米电气石粉加入到聚乳酸中，再加入聚乙二醇200、硅烷偶联剂KH560，搅拌均匀，使纳米电气石粉均匀分散到聚乳酸中，形成微球，过滤并烘干；
b. 将活性炭、生态棉纤维添加到水中分散均匀，然后向其中添加薄荷香精，继续分散，分散均匀后转入抽真空条件下静置3-5h，后经离心、干燥、研磨处理得到负载有薄荷香精的活性炭粉；
c. 将竹丝纤维粉置于高碘酸钠溶液中避光氧化反应3-5h，反应温度为40-110℃，过滤、水洗、烘干，得到氧化竹纤维；将氧化竹纤维浸渍在PAMAM 溶液中3-6h，反应温度25-85℃，过滤烘干并研磨，得到PAMAM 接枝竹丝纤维粉；
d. 将等规聚丙烯、步骤a所得微球、步骤b所得负载薄荷香精的活性炭粉、步骤c所得PAMAM接枝竹丝纤维粉、三聚氰胺添加到螺杆挤压机进行熔融，再经纺丝、牵伸、成网、热轧后制得无纺布；
e. 将硅藻土加入到水中，搅拌均匀后加入十二烷基磺酸钠，搅拌均匀后加入羟甲基纤维素钠、三聚氰胺，调整粘度适中，制得浆液；将步骤d所得无纺布完全浸没于浆液，并放入超声波振荡器中超声 5-10min，取出，采用“二浸二轧”的方法，即充分浸没，用浸轧机轧液，再一次浸没，然后用浸轧机轧液后，放入焙烘机，烘焙2-5min，取出。
3.根据权利要求2所述的一种保温的、可连续释放负氧离子的含竹丝纤维无纺布及其制备方法，其特征在于，步骤b中所述烘焙机烘焙温度为70-110℃。
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