CN106116147A - A kind of oil-spot glaze containing shraff and preparation method thereof - Google Patents
A kind of oil-spot glaze containing shraff and preparation method thereof Download PDFInfo
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- CN106116147A CN106116147A CN201610461313.6A CN201610461313A CN106116147A CN 106116147 A CN106116147 A CN 106116147A CN 201610461313 A CN201610461313 A CN 201610461313A CN 106116147 A CN106116147 A CN 106116147A
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- parts
- shraff
- oil
- oxide
- quartz
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of oil-spot glaze containing shraff and preparation method thereof, this oil-spot glaze, is made up of according to the raw material of weight portion following: nepheline syenite 115 135 parts, calcium carbonate 15 28 parts, triple superphosphate 30 50 parts, zinc oxide 3 15 parts, brium carbonate 5 15 parts, Kaolin 18 32 parts, 70 90 parts of quartz, copper oxide 0.5 3 parts, cobalt oxide 5 18 parts, shraff 20 40 parts.Nepheline syenite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff is weighed according to weight portion, after mixing, ground sieve series obtains mixed material, mixed material is applied to pottery dry body surface, fires at a temperature of 1,230 1280 DEG C and under oxygen atmosphere after drying and get final product.Present invention process controls simple, good process repeatability, and the most applicable to various ceramic bodies, glaze is insensitive to temperature, firing atmosphere and glazing thickness, and the ceramic product glaze made with this glaze has the pattern of black oil drop-wise, and glaze smooths, good decorating effect.
Description
Technical field
The present invention relates to ceramic glaze technical field, a kind of oil-spot glaze containing shraff and preparation method thereof.
Background technology
Oil-spot glaze, black glaze special kinds, belong to crystalline glaze.Created in the Song dynasty, have typical case to put up a kiln characteristic.General limestone joins glaze, ferrum
For photoghraphic coupler.Green compact rest, enters kiln roasting to uniform temperature, and the ferrum in glaze forms crystalline solid, and it is new to aggregate into black oil droplet
Shape, after cooling is extinguished, crystalline particle is retained in glaze layer, has the decorative effect of uniqueness.Because the uniqueness of manufacturing technology is profound, thousand loads
Difficulty is met and is become traditional name glaze of all times, the target that pottery industry of all times is pursued, the porcelain produced with it
Feature is steady, attractive in appearance, and is full of variety and the gem of art that becomes in ceramics, and current fine piece of writing handed down from ancient times is actually rare.But
The method of the most prepared oil-spot glaze controls relatively difficult, and particularly oil droplet effect is to very sensitive to atmosphere and glazing thickness.
Summary of the invention
It is an object of the invention to provide a kind of technique simple and easy to control, reproducible, to temperature, firing atmosphere and glazing
Thickness is insensitive, oil-spot glaze containing shraff and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of oil-spot glaze containing shraff, is made up of according to the raw material of weight portion following:
Nepheline syenite 115-135 part
Calcium carbonate 15-28 part
Triple superphosphate 30-50 part
Zinc oxide 3-15 part
Brium carbonate 5-15 part
Kaolin 18-32 part
Quartz 70-90 part
Copper oxide 0.5-3 part
Cobalt oxide 5-18 part
Shraff 20-40 part.
As the further scheme of the present invention: the described oil-spot glaze containing shraff, by following former according to weight portion
Material composition:
Nepheline syenite 118-130 part
Calcium carbonate 18-25 part
Triple superphosphate 35-45 part
Zinc oxide 3-15 part
Brium carbonate 7-12 part
Kaolin 20-30 part
Quartz 75-85 part
Copper oxide 0.8-2.5 part
Cobalt oxide 7-15 part
Shraff 25-35 part.
As the further scheme of the present invention: the described oil-spot glaze containing shraff, by following former according to weight portion
Material composition:
Nepheline syenite 120-125 part
Calcium carbonate 20-23 part
Triple superphosphate 38-42 part
Zinc oxide 5-10 part
Brium carbonate 8-10 part
Kaolin 22-28 part
Quartz 80-85 part
Copper oxide 1-2 part
Cobalt oxide 8-12 part
Shraff 28-32 part.
As the further scheme of the present invention: the described oil-spot glaze containing shraff, by following former according to weight portion
Material composition:
Nepheline syenite 123.6 parts
Calcium carbonate 21 parts
Triple superphosphate 40 parts
Zinc oxide 8.1 parts
Brium carbonate 9.8 parts
Kaolin 25.8 parts
83.5 parts of quartz
Copper oxide 1.6 parts
Cobalt oxide 10 parts
Shraff 30 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff, grind after mixing
Cross 200 mesh sieves and prepare mixed material, mixed material is applied to pottery dry body surface, the temperature of 1230-1280 DEG C after drying
Down and fire and get final product under oxygen atmosphere.
As the further scheme of the present invention: process of lapping: by mixture: mill ball: the quality of water=1:1-3:0.5-2
It is ground than adding in grinder, then crosses 200 mesh sieves and make mixed material.
Compared with prior art, the invention has the beneficial effects as follows:
Present invention process controls simple, and good process repeatability, the most applicable to various ceramic bodies, glaze is to temperature, firing atmosphere
Insensitive with glazing thickness, it is easily controlled, speckle is distributed on the ceramic product glaze made with this glaze, and has black
The pattern of oil droplet shape, abnormal the most exquisite, and on glaze oil droplet size be evenly distributed, glaze smooths, good decorating effect.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 115 parts
Calcium carbonate 15 parts
Triple superphosphate 30 parts
Zinc oxide 3 parts
Brium carbonate 5 parts
Kaolin 18 parts
70 parts of quartz
Copper oxide 0.5 part
Cobalt oxide 5 parts
Shraff 20 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff, grind after mixing
Cross 200 mesh sieves and prepare mixed material, mixed material is applied to pottery dry body surface, after drying at a temperature of 1230 DEG C and
Fire under oxygen atmosphere and get final product.
Embodiment 2
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 135 parts
Calcium carbonate 28 parts
Triple superphosphate 50 parts
Zinc oxide 15 parts
Brium carbonate 15 parts
Kaolin 32 parts
90 parts of quartz
Copper oxide 3 parts
Cobalt oxide 18 parts
Shraff 40 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff, grind after mixing
Cross 200 mesh sieves and prepare mixed material, mixed material is applied to pottery dry body surface, after drying at a temperature of 1280 DEG C and
Fire under oxygen atmosphere and get final product.
Embodiment 3
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 118 parts
Calcium carbonate 18 parts
Triple superphosphate 35 parts
Zinc oxide 3 parts
Brium carbonate 7 parts
Kaolin 20 parts
75 parts of quartz
Copper oxide 0.8 part
Cobalt oxide 7 parts
Shraff 25 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff mix, ground
Journey: by mixture: mill ball: be ground in the mass ratio addition grinder of water=1:1:0.5, then cross 200 mesh sieves and make mixed
Compound material.Mixed material is applied to pottery dry body surface, fires at a temperature of 1230 DEG C and under oxygen atmosphere after drying
Obtain.
Embodiment 4
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 130 parts
Calcium carbonate 25 parts
Triple superphosphate 45 parts
Zinc oxide 15 parts
Brium carbonate 12 parts
Kaolin 30 parts
85 parts of quartz
Copper oxide 2.5 parts
Cobalt oxide 15 parts
Shraff 35 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff mix, ground
Journey: by mixture: mill ball: be ground in the mass ratio addition grinder of water=1:3:2, then cross 200 mesh sieves and make mixing
Material.Mixed material is applied to pottery dry body surface, fires i.e. at a temperature of 1280 DEG C and under oxygen atmosphere after drying
?.
Embodiment 5
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 120 parts
Calcium carbonate 20 parts
Triple superphosphate 38 parts
Zinc oxide 5 parts
Brium carbonate 8 parts
Kaolin 22 parts
80 parts of quartz
Copper oxide 1 part
Cobalt oxide 8 parts
Shraff 28 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff mix, ground
Journey: by mixture: mill ball: be ground in the mass ratio addition grinder of water=1:1:1, then cross 200 mesh sieves and make mixing
Material.Mixed material is applied to pottery dry body surface, fires i.e. at a temperature of 1250 DEG C and under oxygen atmosphere after drying
?.
Embodiment 6
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 125 parts
Calcium carbonate 23 parts
Triple superphosphate 42 parts
Zinc oxide 10 parts
Brium carbonate 10 parts
Kaolin 28 parts
85 parts of quartz
Copper oxide 2 parts
Cobalt oxide 12 parts
Shraff 32 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff mix, ground
Journey: by mixture: mill ball: be ground in the mass ratio addition grinder of water=1:2:2, then cross 200 mesh sieves and make mixing
Material.Mixed material is applied to pottery dry body surface, fires i.e. at a temperature of 1260 DEG C and under oxygen atmosphere after drying
?.
Embodiment 7
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff, it is made up of according to the raw material of weight portion following:
Nepheline syenite 123.6 parts
Calcium carbonate 21 parts
Triple superphosphate 40 parts
Zinc oxide 8.1 parts
Brium carbonate 9.8 parts
Kaolin 25.8 parts
83.5 parts of quartz
Copper oxide 1.6 parts
Cobalt oxide 10 parts
Shraff 30 parts.
The preparation method of the described oil-spot glaze containing shraff, comprises the following steps: just weighing nepheline according to weight portion
Anhydrite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, copper oxide, cobalt oxide, shraff mix, ground
Journey: by mixture: mill ball: be ground in the mass ratio addition grinder of water=1:2:1, then cross 200 mesh sieves and make mixing
Material.Mixed material is applied to pottery dry body surface, fires i.e. at a temperature of 1240 DEG C and under oxygen atmosphere after drying
?.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only wraps
Containing an independent technical scheme, this narrating mode of description is only that for clarity sake those skilled in the art should
Description can also be formed those skilled in the art through appropriately combined as an entirety, the technical scheme in each embodiment
May be appreciated other embodiments.
Claims (6)
1. the oil-spot glaze containing shraff, it is characterised in that be made up of according to the raw material of weight portion following:
Nepheline syenite 115-135 part
Calcium carbonate 15-28 part
Triple superphosphate 30-50 part
Zinc oxide 3-15 part
Brium carbonate 5-15 part
Kaolin 18-32 part
Quartz 70-90 part
Copper oxide 0.5-3 part
Cobalt oxide 5-18 part
Shraff 20-40 part.
Oil-spot glaze containing shraff the most according to claim 1, it is characterised in that by following former according to weight portion
Material composition:
Nepheline syenite 118-130 part
Calcium carbonate 18-25 part
Triple superphosphate 35-45 part
Zinc oxide 3-15 part
Brium carbonate 7-12 part
Kaolin 20-30 part
Quartz 75-85 part
Copper oxide 0.8-2.5 part
Cobalt oxide 7-15 part
Shraff 25-35 part.
Oil-spot glaze containing shraff the most according to claim 1, it is characterised in that by following former according to weight portion
Material composition:
Nepheline syenite 120-125 part
Calcium carbonate 20-23 part
Triple superphosphate 38-42 part
Zinc oxide 5-10 part
Brium carbonate 8-10 part
Kaolin 22-28 part
Quartz 80-85 part
Copper oxide 1-2 part
Cobalt oxide 8-12 part
Shraff 28-32 part.
Oil-spot glaze containing shraff the most according to claim 1, it is characterised in that by following former according to weight portion
Material composition:
Nepheline syenite 123.6 parts
Calcium carbonate 21 parts
Triple superphosphate 40 parts
Zinc oxide 8.1 parts
Brium carbonate 9.8 parts
Kaolin 25.8 parts
83.5 parts of quartz
Copper oxide 1.6 parts
Cobalt oxide 10 parts
Shraff 30 parts.
5. the preparation method of the oil-spot glaze containing shraff as described in claim 1-4 is arbitrary, it is characterised in that bag
Include following steps: weigh nepheline syenite, calcium carbonate, triple superphosphate, zinc oxide, brium carbonate, Kaolin, quartz, oxygen according to weight portion
Changing copper, cobalt oxide, shraff, after mixing, ground 200 mesh sieves prepare mixed material, and mixed material is applied to pottery dry body body
Surface, fires at a temperature of 1230-1280 DEG C and under oxygen atmosphere after drying and get final product.
The preparation method of the oil-spot glaze containing shraff the most according to claim 5, it is characterised in that process of lapping:
By mixture: mill ball: the mass ratio addition grinder of water=1:1-3:0.5-2 is ground, then crosses 200 mesh sieves and make
Mixed material.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610461313.6A CN106116147B (en) | 2016-06-23 | 2016-06-23 | A kind of oil-spot glaze and preparation method thereof containing shraff |
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| CN201610461313.6A CN106116147B (en) | 2016-06-23 | 2016-06-23 | A kind of oil-spot glaze and preparation method thereof containing shraff |
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| CN106116147A true CN106116147A (en) | 2016-11-16 |
| CN106116147B CN106116147B (en) | 2019-02-22 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111253777A (en) * | 2020-01-20 | 2020-06-09 | 大连交通大学 | Ceramic pigment composition, black glass ceramic pigment, glass ceramic and preparation method thereof |
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| CN105272376A (en) * | 2015-11-09 | 2016-01-27 | 醴陵陶润实业发展有限公司 | Fambe temmoku glaze and preparation method thereof |
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2016
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| CN101805209A (en) * | 2010-04-21 | 2010-08-18 | 伟业陶瓷有限公司 | Matt porcelain glaze prepared by using waste porcelains and production method thereof |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN105272150A (en) * | 2015-10-14 | 2016-01-27 | 德化恒忆陶瓷艺术股份有限公司 | Tenmoku glaze procelain |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111253777A (en) * | 2020-01-20 | 2020-06-09 | 大连交通大学 | Ceramic pigment composition, black glass ceramic pigment, glass ceramic and preparation method thereof |
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| CN106116147B (en) | 2019-02-22 |
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