CN106116147B - A kind of oil-spot glaze and preparation method thereof containing shraff - Google Patents
A kind of oil-spot glaze and preparation method thereof containing shraff Download PDFInfo
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- CN106116147B CN106116147B CN201610461313.6A CN201610461313A CN106116147B CN 106116147 B CN106116147 B CN 106116147B CN 201610461313 A CN201610461313 A CN 201610461313A CN 106116147 B CN106116147 B CN 106116147B
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- shraff
- oil
- oxide
- glaze
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of oil-spot glaze and preparation method thereof containing shraff, the oil-spot glaze is made of the raw material below according to parts by weight: 115-135 parts of nepheline syenite, 15-28 parts of calcium carbonate, 30-50 parts of coarse whiting, 3-15 parts of zinc oxide, 5-15 parts of barium carbonate, 18-32 parts of kaolin, 70-90 parts of quartz, 0.5-3 parts of copper oxide, 5-18 parts of cobalt oxide, 20-40 parts of shraff.Nepheline syenite, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are weighed according to parts by weight, obtained mixed material is ground up, sieved after mixing, mixed material is applied to the dry billet surface of ceramics, after drying 1230-1280 DEG C at a temperature of and oxygen atmosphere under fire to obtain the final product.Present invention process control is simple, good process repeatability, is applicable in various ceramic bodies, glaze is insensitive to temperature, firing atmosphere and glazing thickness, has the pattern of black oil drop-wise in the ceramic product glaze paint made with the glaze, glaze paint is smooth, good decorating effect.
Description
Technical field
The present invention relates to ceramic glaze technical field, specifically a kind of oil-spot glaze and preparation method thereof containing shraff.
Background technique
Oil-spot glaze, black glaze special kinds belong to crystalline glaze.It is created in the Song Dynasty, there is typical case to put up a kiln characteristic.Generally matched with lime stone
Glaze, iron are photoghraphic coupler.Green compact rest enters kiln roasting to certain temperature, and the iron in glaze forms crystalline solid, and aggregates into black oil
New shape is dripped, after cooling is extinguished, crystalline particle is retained in glaze layer, there is unique decorative effect.Because the uniqueness of manufacturing technology is profound,
Very rare and become traditional name glaze of all times, the target that ceramics industry of all times is pursued is produced with it
Porcelain feature is steady, beautiful, and is full of variety and becomes the gem of art in ceramics, and current fine piece of writing handed down from ancient times is actually rare.
But the method control of prepared oil-spot glaze is relatively difficult at present, especially oil droplet effect is to very quick to atmosphere and glazing thickness
Sense.
Summary of the invention
That the purpose of the present invention is to provide a kind of simple processes is easy to control, reproducible, to temperature, firing atmosphere and glazing
Thickness is insensitive, the oil-spot glaze containing shraff and preparation method thereof, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of oil-spot glaze containing shraff, is made of the raw material below according to parts by weight:
115-135 parts of nepheline syenite
15-28 parts of calcium carbonate
30-50 parts of coarse whiting
3-15 parts of zinc oxide
5-15 parts of barium carbonate
18-32 parts of kaolin
It is 70-90 parts quartzy
0.5-3 parts of copper oxide
5-18 parts of cobalt oxide
20-40 parts of shraff.
As a further solution of the present invention: the oil-spot glaze containing shraff, by below according to the original of parts by weight
Material composition:
118-130 parts of nepheline syenite
18-25 parts of calcium carbonate
35-45 parts of coarse whiting
3-15 parts of zinc oxide
7-12 parts of barium carbonate
20-30 parts of kaolin
It is 75-85 parts quartzy
0.8-2.5 parts of copper oxide
7-15 parts of cobalt oxide
25-35 parts of shraff.
As a further solution of the present invention: the oil-spot glaze containing shraff, by below according to the original of parts by weight
Material composition:
120-125 parts of nepheline syenite
20-23 parts of calcium carbonate
38-42 parts of coarse whiting
5-10 parts of zinc oxide
8-10 parts of barium carbonate
22-28 parts of kaolin
It is 80-85 parts quartzy
1-2 parts of copper oxide
8-12 parts of cobalt oxide
28-32 parts of shraff.
As a further solution of the present invention: the oil-spot glaze containing shraff, by below according to the original of parts by weight
Material composition:
123.6 parts of nepheline syenite
21 parts of calcium carbonate
40 parts of coarse whiting
8.1 parts of zinc oxide
9.8 parts of barium carbonate
25.8 parts of kaolin
83.5 parts of quartz
1.6 parts of copper oxide
10 parts of cobalt oxide
30 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are ground after mixing
It crosses 200 meshes and mixed material is made, mixed material is applied to the dry billet surface of ceramics, in 1230-1280 DEG C of temperature after drying
It is fired under lower and oxygen atmosphere to obtain the final product.
As a further solution of the present invention: process of lapping: pressing mixture: mill ball: water=1:1-3:0.5-2 quality
It is ground than being added in grinder, then crosses 200 meshes and mixed material is made.
Compared with prior art, the beneficial effects of the present invention are:
Present invention process control is simple, good process repeatability, is applicable in various ceramic bodies, glaze is to temperature, firing
Atmosphere and glazing thickness are insensitive, are easy to control, and are distributed spottiness in the ceramic product glaze paint made with the glaze, and have
The pattern of black oil drop-wise, it is abnormal exquisite, and in glaze paint oil droplet size be evenly distributed, glaze paint is smooth, good decorating effect.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
115 parts of nepheline syenite
15 parts of calcium carbonate
30 parts of coarse whiting
3 parts of zinc oxide
5 parts of barium carbonate
18 parts of kaolin
70 parts of quartz
0.5 part of copper oxide
5 parts of cobalt oxide
20 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are ground after mixing
Cross 200 meshes and mixed material be made, mixed material is applied to the dry billet surface of ceramics, after drying 1230 DEG C at a temperature of and
It is fired under oxygen atmosphere to obtain the final product.
Embodiment 2
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
135 parts of nepheline syenite
28 parts of calcium carbonate
50 parts of coarse whiting
15 parts of zinc oxide
15 parts of barium carbonate
32 parts of kaolin
90 parts of quartz
3 parts of copper oxide
18 parts of cobalt oxide
40 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are ground after mixing
Cross 200 meshes and mixed material be made, mixed material is applied to the dry billet surface of ceramics, after drying 1280 DEG C at a temperature of and
It is fired under oxygen atmosphere to obtain the final product.
Embodiment 3
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
118 parts of nepheline syenite
18 parts of calcium carbonate
35 parts of coarse whiting
3 parts of zinc oxide
7 parts of barium carbonate
20 parts of kaolin
75 parts of quartz
0.8 part of copper oxide
7 parts of cobalt oxide
25 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground
Journey: by mixture: mill ball: water=1:1:0.5 mass ratio is added in grinder and is ground, and then 200 meshes excessively are made mixed
Close material.Mixed material is applied to the dry billet surface of ceramics, after drying 1230 DEG C at a temperature of and oxygen atmosphere under fire
To obtain the final product.
Embodiment 4
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
130 parts of nepheline syenite
25 parts of calcium carbonate
45 parts of coarse whiting
15 parts of zinc oxide
12 parts of barium carbonate
30 parts of kaolin
85 parts of quartz
2.5 parts of copper oxide
15 parts of cobalt oxide
35 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground
Journey: by mixture: mill ball: water=1:3:2 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made
Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1280 DEG C at a temperature of and oxygen atmosphere under fire and be
?.
Embodiment 5
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
120 parts of nepheline syenite
20 parts of calcium carbonate
38 parts of coarse whiting
5 parts of zinc oxide
8 parts of barium carbonate
22 parts of kaolin
80 parts of quartz
1 part of copper oxide
8 parts of cobalt oxide
28 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground
Journey: by mixture: mill ball: water=1:1:1 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made
Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1250 DEG C at a temperature of and oxygen atmosphere under fire and be
?.
Embodiment 6
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
125 parts of nepheline syenite
23 parts of calcium carbonate
42 parts of coarse whiting
10 parts of zinc oxide
10 parts of barium carbonate
28 parts of kaolin
85 parts of quartz
2 parts of copper oxide
12 parts of cobalt oxide
32 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground
Journey: by mixture: mill ball: water=1:2:2 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made
Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1260 DEG C at a temperature of and oxygen atmosphere under fire and be
?.
Embodiment 7
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
123.6 parts of nepheline syenite
21 parts of calcium carbonate
40 parts of coarse whiting
8.1 parts of zinc oxide
9.8 parts of barium carbonate
25.8 parts of kaolin
83.5 parts of quartz
1.6 parts of copper oxide
10 parts of cobalt oxide
30 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight
Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground
Journey: by mixture: mill ball: water=1:2:1 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made
Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1240 DEG C at a temperature of and oxygen atmosphere under fire and be
?.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (5)
1. a kind of oil-spot glaze containing shraff, which is characterized in that be made of the raw material below according to parts by weight:
115-135 parts of nepheline syenite
15-28 parts of calcium carbonate
30-50 parts of coarse whiting
3-15 parts of zinc oxide
5-15 parts of barium carbonate
18-32 parts of kaolin
It is 70-90 parts quartzy
0.5-3 parts of copper oxide
5-18 parts of cobalt oxide
20-40 parts of shraff；
The preparation method of the oil-spot glaze specifically includes the following steps: according to parts by weight weigh nepheline syenite, calcium carbonate, coarse whiting,
Zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff, mixing is made in ground 200 mesh after mixing
Mixed material is applied to the dry billet surface of ceramics by material, after drying 1230-1280 DEG C at a temperature of and oxygen atmosphere under burn
It makes to obtain the final product.
2. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that by below according to the original of parts by weight
Material composition:
118-130 parts of nepheline syenite
18-25 parts of calcium carbonate
35-45 parts of coarse whiting
3-15 parts of zinc oxide
7-12 parts of barium carbonate
20-30 parts of kaolin
It is 75-85 parts quartzy
0.8-2.5 parts of copper oxide
7-15 parts of cobalt oxide
25-35 parts of shraff.
3. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that by below according to the original of parts by weight
Material composition:
120-125 parts of nepheline syenite
20-23 parts of calcium carbonate
38-42 parts of coarse whiting
5-10 parts of zinc oxide
8-10 parts of barium carbonate
22-28 parts of kaolin
It is 80-85 parts quartzy
1-2 parts of copper oxide
8-12 parts of cobalt oxide
28-32 parts of shraff.
4. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that by below according to the original of parts by weight
Material composition:
123.6 parts of nepheline syenite
21 parts of calcium carbonate
40 parts of coarse whiting
8.1 parts of zinc oxide
9.8 parts of barium carbonate
25.8 parts of kaolin
83.5 parts of quartz
1.6 parts of copper oxide
10 parts of cobalt oxide
30 parts of shraff.
5. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that process of lapping: by mixture: grinding
Abrading-ball: water=1:1-3:0.5-2 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixed material is made.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610461313.6A CN106116147B (en) | 2016-06-23 | 2016-06-23 | A kind of oil-spot glaze and preparation method thereof containing shraff |
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| CN201610461313.6A CN106116147B (en) | 2016-06-23 | 2016-06-23 | A kind of oil-spot glaze and preparation method thereof containing shraff |
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| CN106116147A CN106116147A (en) | 2016-11-16 |
| CN106116147B true CN106116147B (en) | 2019-02-22 |
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| CN111253777A (en) * | 2020-01-20 | 2020-06-09 | 大连交通大学 | Ceramic pigment composition, black glass ceramic pigment, glass ceramic and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101805209A (en) * | 2010-04-21 | 2010-08-18 | 伟业陶瓷有限公司 | Matt porcelain glaze prepared by using waste porcelains and production method thereof |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN105272150A (en) * | 2015-10-14 | 2016-01-27 | 德化恒忆陶瓷艺术股份有限公司 | Tenmoku glaze procelain |
| CN105272376A (en) * | 2015-11-09 | 2016-01-27 | 醴陵陶润实业发展有限公司 | Fambe temmoku glaze and preparation method thereof |
-
2016
- 2016-06-23 CN CN201610461313.6A patent/CN106116147B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101805209A (en) * | 2010-04-21 | 2010-08-18 | 伟业陶瓷有限公司 | Matt porcelain glaze prepared by using waste porcelains and production method thereof |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN105272150A (en) * | 2015-10-14 | 2016-01-27 | 德化恒忆陶瓷艺术股份有限公司 | Tenmoku glaze procelain |
| CN105272376A (en) * | 2015-11-09 | 2016-01-27 | 醴陵陶润实业发展有限公司 | Fambe temmoku glaze and preparation method thereof |
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| CN106116147A (en) | 2016-11-16 |
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