CN106116147B - A kind of oil-spot glaze and preparation method thereof containing shraff - Google Patents

A kind of oil-spot glaze and preparation method thereof containing shraff Download PDF

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Publication number
CN106116147B
CN106116147B CN201610461313.6A CN201610461313A CN106116147B CN 106116147 B CN106116147 B CN 106116147B CN 201610461313 A CN201610461313 A CN 201610461313A CN 106116147 B CN106116147 B CN 106116147B
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Prior art keywords
parts
shraff
oil
oxide
glaze
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CN201610461313.6A
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Chinese (zh)
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CN106116147A (en
Inventor
林锦明
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DEHUA HENGHAN ARTS Co Ltd
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DEHUA HENGHAN ARTS Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes

Abstract

The invention discloses a kind of oil-spot glaze and preparation method thereof containing shraff, the oil-spot glaze is made of the raw material below according to parts by weight: 115-135 parts of nepheline syenite, 15-28 parts of calcium carbonate, 30-50 parts of coarse whiting, 3-15 parts of zinc oxide, 5-15 parts of barium carbonate, 18-32 parts of kaolin, 70-90 parts of quartz, 0.5-3 parts of copper oxide, 5-18 parts of cobalt oxide, 20-40 parts of shraff.Nepheline syenite, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are weighed according to parts by weight, obtained mixed material is ground up, sieved after mixing, mixed material is applied to the dry billet surface of ceramics, after drying 1230-1280 DEG C at a temperature of and oxygen atmosphere under fire to obtain the final product.Present invention process control is simple, good process repeatability, is applicable in various ceramic bodies, glaze is insensitive to temperature, firing atmosphere and glazing thickness, has the pattern of black oil drop-wise in the ceramic product glaze paint made with the glaze, glaze paint is smooth, good decorating effect.

Description

A kind of oil-spot glaze and preparation method thereof containing shraff
Technical field
The present invention relates to ceramic glaze technical field, specifically a kind of oil-spot glaze and preparation method thereof containing shraff.
Background technique
Oil-spot glaze, black glaze special kinds belong to crystalline glaze.It is created in the Song Dynasty, there is typical case to put up a kiln characteristic.Generally matched with lime stone Glaze, iron are photoghraphic coupler.Green compact rest enters kiln roasting to certain temperature, and the iron in glaze forms crystalline solid, and aggregates into black oil New shape is dripped, after cooling is extinguished, crystalline particle is retained in glaze layer, there is unique decorative effect.Because the uniqueness of manufacturing technology is profound, Very rare and become traditional name glaze of all times, the target that ceramics industry of all times is pursued is produced with it Porcelain feature is steady, beautiful, and is full of variety and becomes the gem of art in ceramics, and current fine piece of writing handed down from ancient times is actually rare. But the method control of prepared oil-spot glaze is relatively difficult at present, especially oil droplet effect is to very quick to atmosphere and glazing thickness Sense.
Summary of the invention
That the purpose of the present invention is to provide a kind of simple processes is easy to control, reproducible, to temperature, firing atmosphere and glazing Thickness is insensitive, the oil-spot glaze containing shraff and preparation method thereof, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of oil-spot glaze containing shraff, is made of the raw material below according to parts by weight:
115-135 parts of nepheline syenite
15-28 parts of calcium carbonate
30-50 parts of coarse whiting
3-15 parts of zinc oxide
5-15 parts of barium carbonate
18-32 parts of kaolin
It is 70-90 parts quartzy
0.5-3 parts of copper oxide
5-18 parts of cobalt oxide
20-40 parts of shraff.
As a further solution of the present invention: the oil-spot glaze containing shraff, by below according to the original of parts by weight Material composition:
118-130 parts of nepheline syenite
18-25 parts of calcium carbonate
35-45 parts of coarse whiting
3-15 parts of zinc oxide
7-12 parts of barium carbonate
20-30 parts of kaolin
It is 75-85 parts quartzy
0.8-2.5 parts of copper oxide
7-15 parts of cobalt oxide
25-35 parts of shraff.
As a further solution of the present invention: the oil-spot glaze containing shraff, by below according to the original of parts by weight Material composition:
120-125 parts of nepheline syenite
20-23 parts of calcium carbonate
38-42 parts of coarse whiting
5-10 parts of zinc oxide
8-10 parts of barium carbonate
22-28 parts of kaolin
It is 80-85 parts quartzy
1-2 parts of copper oxide
8-12 parts of cobalt oxide
28-32 parts of shraff.
As a further solution of the present invention: the oil-spot glaze containing shraff, by below according to the original of parts by weight Material composition:
123.6 parts of nepheline syenite
21 parts of calcium carbonate
40 parts of coarse whiting
8.1 parts of zinc oxide
9.8 parts of barium carbonate
25.8 parts of kaolin
83.5 parts of quartz
1.6 parts of copper oxide
10 parts of cobalt oxide
30 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are ground after mixing It crosses 200 meshes and mixed material is made, mixed material is applied to the dry billet surface of ceramics, in 1230-1280 DEG C of temperature after drying It is fired under lower and oxygen atmosphere to obtain the final product.
As a further solution of the present invention: process of lapping: pressing mixture: mill ball: water=1:1-3:0.5-2 quality It is ground than being added in grinder, then crosses 200 meshes and mixed material is made.
Compared with prior art, the beneficial effects of the present invention are:
Present invention process control is simple, good process repeatability, is applicable in various ceramic bodies, glaze is to temperature, firing Atmosphere and glazing thickness are insensitive, are easy to control, and are distributed spottiness in the ceramic product glaze paint made with the glaze, and have The pattern of black oil drop-wise, it is abnormal exquisite, and in glaze paint oil droplet size be evenly distributed, glaze paint is smooth, good decorating effect.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
115 parts of nepheline syenite
15 parts of calcium carbonate
30 parts of coarse whiting
3 parts of zinc oxide
5 parts of barium carbonate
18 parts of kaolin
70 parts of quartz
0.5 part of copper oxide
5 parts of cobalt oxide
20 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are ground after mixing Cross 200 meshes and mixed material be made, mixed material is applied to the dry billet surface of ceramics, after drying 1230 DEG C at a temperature of and It is fired under oxygen atmosphere to obtain the final product.
Embodiment 2
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
135 parts of nepheline syenite
28 parts of calcium carbonate
50 parts of coarse whiting
15 parts of zinc oxide
15 parts of barium carbonate
32 parts of kaolin
90 parts of quartz
3 parts of copper oxide
18 parts of cobalt oxide
40 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff are ground after mixing Cross 200 meshes and mixed material be made, mixed material is applied to the dry billet surface of ceramics, after drying 1280 DEG C at a temperature of and It is fired under oxygen atmosphere to obtain the final product.
Embodiment 3
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
118 parts of nepheline syenite
18 parts of calcium carbonate
35 parts of coarse whiting
3 parts of zinc oxide
7 parts of barium carbonate
20 parts of kaolin
75 parts of quartz
0.8 part of copper oxide
7 parts of cobalt oxide
25 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground Journey: by mixture: mill ball: water=1:1:0.5 mass ratio is added in grinder and is ground, and then 200 meshes excessively are made mixed Close material.Mixed material is applied to the dry billet surface of ceramics, after drying 1230 DEG C at a temperature of and oxygen atmosphere under fire To obtain the final product.
Embodiment 4
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
130 parts of nepheline syenite
25 parts of calcium carbonate
45 parts of coarse whiting
15 parts of zinc oxide
12 parts of barium carbonate
30 parts of kaolin
85 parts of quartz
2.5 parts of copper oxide
15 parts of cobalt oxide
35 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground Journey: by mixture: mill ball: water=1:3:2 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1280 DEG C at a temperature of and oxygen atmosphere under fire and be ?.
Embodiment 5
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
120 parts of nepheline syenite
20 parts of calcium carbonate
38 parts of coarse whiting
5 parts of zinc oxide
8 parts of barium carbonate
22 parts of kaolin
80 parts of quartz
1 part of copper oxide
8 parts of cobalt oxide
28 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground Journey: by mixture: mill ball: water=1:1:1 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1250 DEG C at a temperature of and oxygen atmosphere under fire and be ?.
Embodiment 6
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
125 parts of nepheline syenite
23 parts of calcium carbonate
42 parts of coarse whiting
10 parts of zinc oxide
10 parts of barium carbonate
28 parts of kaolin
85 parts of quartz
2 parts of copper oxide
12 parts of cobalt oxide
32 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground Journey: by mixture: mill ball: water=1:2:2 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1260 DEG C at a temperature of and oxygen atmosphere under fire and be ?.
Embodiment 7
In the embodiment of the present invention, a kind of oil-spot glaze containing shraff is made of the raw material below according to parts by weight:
123.6 parts of nepheline syenite
21 parts of calcium carbonate
40 parts of coarse whiting
8.1 parts of zinc oxide
9.8 parts of barium carbonate
25.8 parts of kaolin
83.5 parts of quartz
1.6 parts of copper oxide
10 parts of cobalt oxide
30 parts of shraff.
The preparation method of the oil-spot glaze containing shraff, comprising the following steps: weighing nepheline just according to parts by weight Feldspar, calcium carbonate, coarse whiting, zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff mixing, it is ground Journey: by mixture: mill ball: water=1:2:1 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixing is made Material.Mixed material is applied to the dry billet surface of ceramics, after drying 1240 DEG C at a temperature of and oxygen atmosphere under fire and be ?.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (5)

1. a kind of oil-spot glaze containing shraff, which is characterized in that be made of the raw material below according to parts by weight:
115-135 parts of nepheline syenite
15-28 parts of calcium carbonate
30-50 parts of coarse whiting
3-15 parts of zinc oxide
5-15 parts of barium carbonate
18-32 parts of kaolin
It is 70-90 parts quartzy
0.5-3 parts of copper oxide
5-18 parts of cobalt oxide
20-40 parts of shraff;
The preparation method of the oil-spot glaze specifically includes the following steps: according to parts by weight weigh nepheline syenite, calcium carbonate, coarse whiting, Zinc oxide, barium carbonate, kaolin, quartz, copper oxide, cobalt oxide, shraff, mixing is made in ground 200 mesh after mixing Mixed material is applied to the dry billet surface of ceramics by material, after drying 1230-1280 DEG C at a temperature of and oxygen atmosphere under burn It makes to obtain the final product.
2. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that by below according to the original of parts by weight Material composition:
118-130 parts of nepheline syenite
18-25 parts of calcium carbonate
35-45 parts of coarse whiting
3-15 parts of zinc oxide
7-12 parts of barium carbonate
20-30 parts of kaolin
It is 75-85 parts quartzy
0.8-2.5 parts of copper oxide
7-15 parts of cobalt oxide
25-35 parts of shraff.
3. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that by below according to the original of parts by weight Material composition:
120-125 parts of nepheline syenite
20-23 parts of calcium carbonate
38-42 parts of coarse whiting
5-10 parts of zinc oxide
8-10 parts of barium carbonate
22-28 parts of kaolin
It is 80-85 parts quartzy
1-2 parts of copper oxide
8-12 parts of cobalt oxide
28-32 parts of shraff.
4. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that by below according to the original of parts by weight Material composition:
123.6 parts of nepheline syenite
21 parts of calcium carbonate
40 parts of coarse whiting
8.1 parts of zinc oxide
9.8 parts of barium carbonate
25.8 parts of kaolin
83.5 parts of quartz
1.6 parts of copper oxide
10 parts of cobalt oxide
30 parts of shraff.
5. the oil-spot glaze according to claim 1 containing shraff, which is characterized in that process of lapping: by mixture: grinding Abrading-ball: water=1:1-3:0.5-2 mass ratio is added in grinder and is ground, and then crosses 200 meshes and mixed material is made.
CN201610461313.6A 2016-06-23 2016-06-23 A kind of oil-spot glaze and preparation method thereof containing shraff Active CN106116147B (en)

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CN106116147B true CN106116147B (en) 2019-02-22

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111253777A (en) * 2020-01-20 2020-06-09 大连交通大学 Ceramic pigment composition, black glass ceramic pigment, glass ceramic and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101805209A (en) * 2010-04-21 2010-08-18 伟业陶瓷有限公司 Matt porcelain glaze prepared by using waste porcelains and production method thereof
CN104496558A (en) * 2014-12-04 2015-04-08 王泽彬 Black oil-drop temmoku glaze
CN105272376A (en) * 2015-11-09 2016-01-27 醴陵陶润实业发展有限公司 Fambe temmoku glaze and preparation method thereof
CN105272150A (en) * 2015-10-14 2016-01-27 德化恒忆陶瓷艺术股份有限公司 Tenmoku glaze procelain

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101805209A (en) * 2010-04-21 2010-08-18 伟业陶瓷有限公司 Matt porcelain glaze prepared by using waste porcelains and production method thereof
CN104496558A (en) * 2014-12-04 2015-04-08 王泽彬 Black oil-drop temmoku glaze
CN105272150A (en) * 2015-10-14 2016-01-27 德化恒忆陶瓷艺术股份有限公司 Tenmoku glaze procelain
CN105272376A (en) * 2015-11-09 2016-01-27 醴陵陶润实业发展有限公司 Fambe temmoku glaze and preparation method thereof

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