CN106542736A - A kind of bright red glaze and preparation method thereof and glazing method - Google Patents
A kind of bright red glaze and preparation method thereof and glazing method Download PDFInfo
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- CN106542736A CN106542736A CN201610917868.7A CN201610917868A CN106542736A CN 106542736 A CN106542736 A CN 106542736A CN 201610917868 A CN201610917868 A CN 201610917868A CN 106542736 A CN106542736 A CN 106542736A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- Chemical Kinetics & Catalysis (AREA)
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Abstract
The present invention relates to ceramic technology field, and in particular to a kind of bright red glaze and preparation method thereof and glazing method.Which adopts rational glaze formula and firing process so as to reach the gorgeous effect of color and luster light of bright red.A kind of bright red glaze is composed of the following raw materials by weight:13 ~ 17 parts of feldspar in powder, 18 ~ 22 parts of albite in powder, 15 ~ 18 parts of calcite in powder, 4 ~ 6 parts of talcum powder, 21 ~ 25 parts of quartz sand, 1 ~ 4 part of zinc oxide, 3 ~ 8 parts of 2# frits, 3 ~ 6 parts of brium carbonate powder, 3 ~ 6 parts of zirconium silicate powder, 10 ~ 15 parts of erie Congo base, 7 ~ 11 parts of clay are prepared into glaze using certain preparation method and then carry out glazing.
Description
First, technical field:
The present invention relates to ceramic technology field, and in particular to a kind of bright red glaze and preparation method thereof and glazing method.
2nd, background technology:
At present the species of Production of Ceramics red pigment is a lot, and the pigment for Production of Ceramics is inorganic pigment, it with it is organic
Pigment ratio have self performance it is stable, it is not aging the features such as, but red pigment highly volatile in high temperature sintering process moves back colour fading,
Bright red effect, therefore the production technology of conventional 800 DEG C or so firing temperature can not be formed ceramic bright red effect is obtained to reach
Meet the market demand, but the ceramic product of this technique productions is present that glaze splits, delayed crazing, complex process are difficult quality control, into
The deficiency such as this height, Lead and cadmium be big.
3rd, the content of the invention
A kind of bright red glaze of offer of the present invention and preparation method thereof and glazing method, which adopts rational glaze formula and burns till
Technique so as to reach the gorgeous effect of color and luster light of bright red.
For achieving the above object, the technical solution used in the present invention is:A kind of bright red glaze, it is characterised in that:Described
Bright red glaze is composed of the following raw materials by weight:13 ~ 17 parts of feldspar in powder, 18 ~ 22 parts of albite in powder, 15 ~ 18 parts of calcite in powder,
4 ~ 6 parts of talcum powder, 21 ~ 25 parts of quartz sand, 1 ~ 4 part of zinc oxide, 3 ~ 8 parts of 2# frits, 3 ~ 6 parts of brium carbonate powder, zirconium silicate powder 3 ~ 6
Part, 10 ~ 15 parts of erie Congo base, 7 ~ 11 parts of clay.
Described method and step is:Above-mentioned raw materials are carried out into ball milling processing, according to glaze:Ballstone:Water weight ratio is=1:
1.3~1.5:1.3 ~ 1.5 ratio, ball milling 20 ~ 28 hours are crossed 100 ~ 140 target screen clothes and remove iron, complete glaze after ball milling is good
It is prepared by material.
Described glaze:Ballstone:Water weight ratio preferably 1:1.4:1.4 ratio, Ball-milling Time preferably 24 hours.
A kind of glazing method of bright red glaze is:Glazing is completed using traditional leaching glaze method, glazed thickness is 0.3 ~
0.6mm, then carries out glaze firing, and glaze firing is burnt till using rolling tunnel kiln oxidizing atmosphere, and maximum temperature is 1190 ~ 1250 DEG C, firing period
For 4 ~ 6 hours, sintering curve was:1000 DEG C are at the uniform velocity warming up to by room temperature and take 1 ~ 2 hour, then it is time-consuming by 1000 DEG C to 1250 DEG C
1 ~ 2 hour, 1250 DEG C of temperature retention times were 10 ~ 30 minutes, then time-consuming about 10 ~ 30 minutes by 1250 DEG C ~ 1000 DEG C fast coolings,
At the uniform velocity it is down to room temperature for 1000 DEG C and takes about 1 ~ 2 hour, product burns till.
Compared with prior art, the invention has the advantages that and effect:The present invention is by improving preparation technology first
And the present invention is according to colouration mechanism and material micro molecule structural theory, that is, want to improve the performance of glaze, it is necessary to be allowed to be formed
Stable molecular structure, therefore the red pigment for selecting preparation condition qualified is important factor, it is first determined heat endurance is high
Red pigment molecular structure model, the composition, design feature further according to different elements goes to prepare such ceramic glaze original auxiliary
Material, makes the research of high-temperature red ceramic glaze reach a new height, and special technical measures are reducing the poison of pigment
Property, heat endurance is improved, formation high temperature resistant, glaze light, lovely luster, steady quality, Lead and cadmium are qualified, cost is relatively low
High temperature bright red glaze ceramic product.
4th, specific embodiment
Technical scheme is further limited with reference to specific embodiment:
Embodiment one:
A kind of bright red glaze is composed of the following raw materials by weight:13 parts of feldspar in powder, 18 parts of albite in powder, 15 parts of calcite in powder,
4 parts of talcum powder, 21 parts of quartz sand, 1 part of zinc oxide, 3 parts of 2# frits, 3 parts of brium carbonate powder, 3 parts of zirconium silicate powder, erie Congo base 10
Part, 7 parts of clay.
A kind of preparation method step of described bright red glaze is:Above-mentioned raw materials are carried out into ball milling processing, according to glaze:Ball
Stone:Water weight ratio is=1:1.3:1.3 ratio, ball milling 20 hours are crossed 100 target screen clothes and remove iron, complete glaze after ball milling is good
It is prepared by material.
A kind of glazing method of bright red glaze:Glazing is completed using traditional leaching glaze method, glazed thickness is 0.3mm, so
After carry out glaze firing, glaze firing is burnt till using rolling tunnel kiln oxidizing atmosphere, maximum temperature be 1190 DEG C, firing period be 4 hours, burn till song
Line is:1000 DEG C are at the uniform velocity warming up to by room temperature and take 1 hour, then it is time-consuming 1 hour by 1000 DEG C to 1250 DEG C, during 1250 DEG C of insulations
Between be 10 minutes, then time-consuming about 10 minutes by 1250 DEG C ~ 1000 DEG C fast coolings, 1000 DEG C to be at the uniform velocity down to room temperature time-consuming about 1 little
When, product burns till.
Embodiment two:
A kind of bright red glaze is composed of the following raw materials by weight:14 parts of feldspar in powder, 20 parts of albite in powder, 17 parts of calcite in powder,
5 parts of talcum powder, 23 parts of quartz sand, 3 parts of zinc oxide, 5 parts of 2# frits, 5 parts of brium carbonate powder, 4 parts of zirconium silicate powder, erie Congo base 13
Part, 9 parts of clay.
A kind of preparation method step of described bright red glaze is:Above-mentioned raw materials are carried out into ball milling processing, according to glaze:Ball
Stone:Water weight ratio is 1:1.4:1.4 ratio, ball milling 25 hours are crossed 130 target screen clothes and remove iron, complete glaze after ball milling is good
It is prepared by material.
A kind of glazing method of bright red glaze:Glazing is completed using traditional leaching glaze method, glazed thickness is 0.5mm, so
After carry out glaze firing, glaze firing is burnt till using rolling tunnel kiln oxidizing atmosphere, maximum temperature be 1200 DEG C, firing period be 5 hours, burn till song
Line is:1000 DEG C of time-consuming 1.5 hours then time-consuming 1.5 hours by 1000 DEG C to 1250 DEG C, 1250 DEG C of guarantors are at the uniform velocity warming up to by room temperature
The warm time is 20 minutes, then time-consuming about 20 minutes by 1250 DEG C ~ 1000 DEG C fast coolings, is at the uniform velocity down to room temperature for 1000 DEG C and takes about
1.5 hours, product burnt till.
Embodiment three:
A kind of bright red glaze is composed of the following raw materials by weight:17 parts of feldspar in powder, 22 parts of albite in powder, 18 parts of calcite in powder,
6 parts of talcum powder, 25 parts of quartz sand, 4 parts of zinc oxide, 8 parts of 2# frits, 6 parts of brium carbonate powder, 6 parts of zirconium silicate powder, erie Congo base 15
Part, 11 parts of clay.
A kind of preparation method step of described bright red glaze is:Above-mentioned raw materials are carried out into ball milling processing, according to glaze:Ball
Stone:Water weight ratio is=1: 1.5:1.5 ratio, ball milling 28 hours are crossed 140 target screen clothes and remove iron, complete after ball milling is good
It is prepared by glaze.
A kind of glazing method of bright red glaze:Glazing is completed using traditional leaching glaze method, glazed thickness is 0.6mm, so
After carry out glaze firing, glaze firing is burnt till using rolling tunnel kiln oxidizing atmosphere, maximum temperature be 1250 DEG C, firing period be 6 hours, burn till song
Line is:1000 DEG C are at the uniform velocity warming up to by room temperature and take 2 hours, then it is time-consuming 2 hours by 1000 DEG C to 1250 DEG C, during 1250 DEG C of insulations
Between be 30 minutes, then time-consuming about 30 minutes by 1250 DEG C ~ 1000 DEG C fast coolings, 1000 DEG C to be at the uniform velocity down to room temperature time-consuming about 2 little
When, product burns till.
Described traditional leaching glaze method:Base substrate is carried out after removing surface body refuse or dust, with hand or fixture by base substrate
At the uniform velocity it is put in glaze liquid slurry according to technological requirement method of operating, makes glaze slip uniformly be attached on billet surface, glazed thickness
About 0.3 ~ 0.5mm, base substrate is at the uniform velocity removed glaze slip, treats that billet surface glaze slip is dried.
Claims (4)
1. a kind of bright red glaze, it is characterised in that:Described bright red glaze is composed of the following raw materials by weight:Feldspar in powder 13 ~
17 parts, 18 ~ 22 parts of albite in powder, 15 ~ 18 parts of calcite in powder, 4 ~ 6 parts of talcum powder, 21 ~ 25 parts of quartz sand, 1 ~ 4 part of zinc oxide, 2#
3 ~ 8 parts of frit, 3 ~ 6 parts of brium carbonate powder, 3 ~ 6 parts of zirconium silicate powder, 10 ~ 15 parts of erie Congo base, 7 ~ 11 parts of clay.
2. the preparation method of a kind of bright red glaze according to claim 1, it is characterised in that:Described method and step is:
Above-mentioned raw materials are carried out into ball milling processing, according to glaze:Ballstone:Water weight ratio is=1:1.3~1.5:1.3 ~ 1.5 ratio, ball milling
20 ~ 28 hours, 100 ~ 140 target screen clothes are crossed after ball milling is good and iron is removed, glaze preparation is completed.
3. the preparation method of a kind of bright red glaze according to claim 2, it is characterised in that:Described glaze:Ballstone:Water
Weight ratio preferably 1:1.4:1.4 ratio, Ball-milling Time preferably 24 hours.
4. the glazing method of a kind of bright red glaze according to claim 1, it is characterised in that:Described glazing method is:
Glazing is completed using traditional leaching glaze method, glazed thickness is 0.3 ~ 0.6mm, then carry out glaze firing, glaze firing adopts rolling tunnel kiln oxygen
Change atmosphere to burn till, maximum temperature is 1190 ~ 1250 DEG C, firing period is 4 ~ 6 hours, sintering curve is:At the uniform velocity heated up by room temperature
Time-consuming 1 ~ 2 hour to 1000 DEG C then time-consuming 1 ~ 2 hour by 1000 DEG C to 1250 DEG C, 1250 DEG C of temperature retention times are 10 ~ 30 minutes,
It is time-consuming about 10 ~ 30 minutes by 1250 DEG C ~ 1000 DEG C fast coolings again, at the uniform velocity it is down to room temperature for 1000 DEG C and takes about 1 ~ 2 hour, product
Burn till.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107721385A (en) * | 2017-08-28 | 2018-02-23 | 湖南银和瓷业有限公司 | A kind of ceramic bugle formula and manufacture craft |
CN111410425A (en) * | 2020-03-31 | 2020-07-14 | 景德镇市乐陶陶瓷原料有限公司 | Medium-temperature bright red glaze and preparation method thereof |
CN111517647A (en) * | 2020-05-08 | 2020-08-11 | 广西南山瓷器有限公司 | Glaze material for moistening glaze and preparation method thereof |
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CN102101794A (en) * | 2011-01-20 | 2011-06-22 | 潮州市波士发陶瓷制作有限公司 | Glazed low-temperature bright-red glaze and production process for ceramic products thereof |
CN102491794A (en) * | 2011-12-12 | 2012-06-13 | 潮州市庆发陶瓷有限公司 | Scarlet glaze material for ceramics and preparation method thereof |
CN103030430A (en) * | 2012-12-12 | 2013-04-10 | 醴陵陶润实业发展有限公司 | Method for preparing gorgeous space-time glaze |
CN104211444A (en) * | 2014-09-03 | 2014-12-17 | 江苏省宜兴彩陶工艺厂 | Preparation method of furnace transmutation sorghum red-flower glaze |
CN104591790A (en) * | 2014-12-25 | 2015-05-06 | 醴陵陶润实业发展有限公司 | High-temperature iron-red glaze and preparation method thereof |
CN105565901A (en) * | 2014-10-08 | 2016-05-11 | 陈能谟 | Red glaze and preparation process thereof |
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2016
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Patent Citations (7)
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CN102101794A (en) * | 2011-01-20 | 2011-06-22 | 潮州市波士发陶瓷制作有限公司 | Glazed low-temperature bright-red glaze and production process for ceramic products thereof |
CN102491794A (en) * | 2011-12-12 | 2012-06-13 | 潮州市庆发陶瓷有限公司 | Scarlet glaze material for ceramics and preparation method thereof |
CN103030430A (en) * | 2012-12-12 | 2013-04-10 | 醴陵陶润实业发展有限公司 | Method for preparing gorgeous space-time glaze |
CN104211444A (en) * | 2014-09-03 | 2014-12-17 | 江苏省宜兴彩陶工艺厂 | Preparation method of furnace transmutation sorghum red-flower glaze |
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CN104591790A (en) * | 2014-12-25 | 2015-05-06 | 醴陵陶润实业发展有限公司 | High-temperature iron-red glaze and preparation method thereof |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107721385A (en) * | 2017-08-28 | 2018-02-23 | 湖南银和瓷业有限公司 | A kind of ceramic bugle formula and manufacture craft |
CN111410425A (en) * | 2020-03-31 | 2020-07-14 | 景德镇市乐陶陶瓷原料有限公司 | Medium-temperature bright red glaze and preparation method thereof |
CN111517647A (en) * | 2020-05-08 | 2020-08-11 | 广西南山瓷器有限公司 | Glaze material for moistening glaze and preparation method thereof |
CN111517647B (en) * | 2020-05-08 | 2022-08-16 | 广西南山瓷器有限公司 | Glaze material for moistening glaze and preparation method thereof |
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