CN106074353B - A kind of toner and its production technology - Google Patents
A kind of toner and its production technology Download PDFInfo
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- CN106074353B CN106074353B CN201610479181.XA CN201610479181A CN106074353B CN 106074353 B CN106074353 B CN 106074353B CN 201610479181 A CN201610479181 A CN 201610479181A CN 106074353 B CN106074353 B CN 106074353B
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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Abstract
The present invention relates to a kind of toner and its production technologies, belong to cosmetic technical field.A kind of toner is made of following substance: solvent, moisturizer, chelating agent, skin conditioning agent, thickener/emulsifier, emollient and preservative；A kind of production technology of toner includes the following steps: 1. to be grouped；2. solvent is handled；3. emulsifying；4. mixing；5. standing.Toner moistening effect is good, timeliness is long, performance is stable, and has good antiseptic property, highly-safe without the substance for generating injury to human body；A kind of production craft step of toner is simple, production is easy.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of toner and its production technology.
Background technique
In recent years, cosmetics are increasing in the sales quota of China, have exceeded hundred billion yuan, have been only second to beauty in the world
State and Japan, some well-known household chemicals companies in the world try hard to be vast all in the dynamics of investment for continuing to increase scientific research
Consumer provides the daily cosmetics for being more suitable for oneself, and the toner as conventional dosage forms is in cosmetic field always in occupation of strong
The big market share, toner, smoothing toner, astringent lotion, moisture retention water etc. are referred to as toner, are a kind of transparent in traditional sense
The cosmetics of liquid are applied to the surface of skin, for the health for cleaning skin, keeping skin.Toner has both cleaning skin
With keep the skin wet, to protect the function of skin.In recent years, toner, which is more focused on, keeps moisture of skin equilibrium, control grease product
Poly-, skin nutrition removes skin surface lipid peroxide and activity lipase, makes that skin is refrigerant, it is clean to feel well.
It maintains the barrier function of skin complete in addition to the health of its skin texture, largely depends on the hydration of skin
Moisture-keeping functions；Moisture major storage in skin, the 18%-20% of skin moisture storage capacity point whole body.Infant's moisture content of skin is up to
40%, so soft flexible；Female skin water content is higher than male, so seeming finer and smoother, beautiful.It is therefore prevented that skin
Water loss, for keeping skin barrier function and the beautiful degree of skin appearance extremely important, the general ingredient of liquid toner
Are as follows: water, polysaccharide moisturizer, chelating agent, preservative, solubilizer, assigns fragrant ingredient, other related notion ingredients at polyalcohol；Application
Publication No. is that the Chinese invention patent of 102113966 A of CN discloses a kind of cosmetic lotion containing micro clustered water, dissolving power, diffusion
Power, penetration etc. are faster and better；Authorization Notice No. is that the Chinese invention patent of 103830119 B of CN discloses one kind with natural
Sericin is the preparation method of the toner of matrix, is that matrix prepares high-grade toner using natural sericin.But
It is liquid toner is all some water-soluble substances, closure moisturizing ingredient lacks, dry chap skin, in chill external environment
Under, it is not easy to lock moisture of skin, to more effectively moisture of skin cannot be kept to balance.
Summary of the invention
The purpose of the present invention is to solve the above-mentioned problems, to provide a kind of toner and its production technology.
Technical proposal that the invention solves the above-mentioned problems is as follows:
A kind of toner is made of following substance: solvent, moisturizer, chelating agent, skin conditioning agent, thickener/emulsifier, profit
Skin agent and preservative；Wherein the solvent is water, and the moisturizer is to mention including at least glycerol, propylene glycol, spirulina maxim
Take object, trimethylglycine, trehalose, biological carbohydrate gum -1, algae extract and panthenol mixture, the chelating agent is EDTA-
2Na, the skin conditioning agent are the mixture including at least allantoin and compound amino acid, and the thickener/emulsifier is acryloyl
The cross-linked polymer of -25 methacrylate of dimethyltaurine ammonium and docosyl alcohol polyethers, the emollient are including at least white
The mixture of pond flower seed oil and ring five dimethyl silicone polymer, the preservative are Bis(hydroxymethyl)imidazolidinyl urea and iodine propine
The mixture of alcohol butyl mephenesin Carbamate.
Toner combines the characteristics of general flowing liquid toner, existing occlusive moisturizer, such as glycerol, by skin
The supplement of skin cuticula lipid material forms the additional lubricant film layer in surface, cuticula is wrapped up, and is made by closing
With the loss of moist stopped in skin, the water content of cuticula is kept；Have wetability or hygroscopicity moisturizer again, as propylene glycol,
Spirulina maxim extract, trimethylglycine, trehalose, biological carbohydrate gum -1, algae extract and mixture of panthenol etc..Solid
Shape toner can provide moisture supplement body, and when moisture of skin is lost, such moisturizer carries hydrone, or will be in skin
Hydrone latching loses it no longer；To keep cuticula water.
Spirulina maxim is a kind of low value object, belongs to Cyanophyta, Oscillariaceae, and Spirullina is one kind of spirulina, by
Relatively high in spirulina maxim protein content, content of phycocyanin is most, and contains high activity SOD(superoxide dismutase
Enzyme), oxygen radical can be converted to hydrogen peroxide, and then resolve into water；Biological carbohydrate gum -1 is also known as fucosan or brown alga
Carbohydrate gum is a kind of biological polyoses, plays the role of moisturizer in cosmetics；Contain algin, agar-agar, OK a karaoke club in algae extract
Glue and part SOD；EDTA-2Na is called disodium ethylene diamine tetraacetate, and it to be good compounding agent that there are six coordination atoms.
As a preferred embodiment of the above technical solution, each substance in mass fraction ratio are as follows: 70-70.05 parts of water, 3 parts of glycerol,
3 parts of propylene glycol, 3 parts of spirulina maxim extract, 1 part of trimethylglycine, 1.5 parts of trehalose, 5 parts of (biological carbohydrate gum -1), algae
2 parts of extract, 0.1 part of panthenol, EDTA-2Na0.05 parts, 0.15 part of allantoin, 2 parts of compound amino acid, acryloyldimethyl ox
1 part of cross-linked polymer, 1 part of white pond flower seed oil, the five poly dimethyl silicon of ring of -25 methacrylate of ichthyodin and docosyl alcohol polyethers
2 parts of oxygen alkane, 0.1188 part of Bis(hydroxymethyl)imidazolidinyl urea, 0.0012 part of mephenesin Carbamate of iodine propilolic alcohol butyl.
As a preferred embodiment of the above technical solution, the moisturizer further includes the hyaluronic acid that mass fraction is 0.03-0.05
Sodium；The dormant oil that the emollient further includes the saualane that mass fraction is 3 or mass fraction is 3；The skin conditioning agent also wraps
The mixture of glycosyl sphingolipid and digalactosyl double glyceride that mass fraction is 2 is included, or, the raw H of dimension and phosphide that mass fraction is 2
Mixture, or, the mixed vitamin H that mixing glycosyl sphingolipid and digalactosyl double glyceride that mass fraction is 1 and mass fraction are 1
With the mixture of phosphatide.
As a preferred embodiment of the above technical solution, the moisturizer further includes the Sodium Hyaluronate that mass fraction is 0.05；Institute
Stating emollient further includes the saualane that mass fraction is 3；The skin conditioning agent further includes the mixing glycosyl sphingolipid that mass fraction is 1
The mixture of the mixed vitamin H and phosphatide that are 1 with digalactosyl double glyceride and mass fraction.
Sodium Hyaluronate (SODIUM HYALURONATE) is the substance extracted from cockscomb, can also be sent out by Lactococcus
Ferment is made, for white or off-white color particle or powder, odorless, and when dry, nitrogen content 2.8%-4.0%, glucuronic acid content
For 37.0%-51.0%.Using more in cosmetic field, there is moisture-keeping function.
It as a preferred embodiment of the above technical solution, further include odorant, the odorant is the essence that mass fraction is 0.03.
A kind of production technology of toner, includes the following steps:
1. grouping: a kind of component of toner described in claim 1 being grouped, is respectively as follows:
A phase, including water, glycerol, propylene glycol, EDTA-2Na, allantoin, spirulina maxim extract, trimethylglycine
And trehalose；
B phase, the cross-linked polymer including -25 methacrylate of ammonium acryloyldime-thyltaurate and docosyl alcohol polyethers；
C phase, including white pond flower seed oil and ring five dimethyl silicone polymer；
D phase, including biological carbohydrate gum -1, algae extract, panthenol and compound amino acid；
E phase, including Bis(hydroxymethyl)imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate；
2. solvent is handled: adding water to vessel in heating to 93-97 DEG C, keep the temperature 30 minutes, stirring is cooled to 80 later
℃；
3. emulsification: the substance in A phase than water being added in the container, 0.5-1.5 minutes homogeneous, insulated and stirred
Until A phase substance dissolves, the substance of B phase is added, 1.5-2.5 minutes homogeneous, the material in insulated and stirred to the container is uniform,
The substance of C phase is added, stirs 8-12 minutes, then 2-4 minutes homogeneous, is cooled to 45 DEG C；
4. mixing: the substance of D phase is added in the above-mentioned material for being cooled to 45 DEG C, it is 0.5-1.5 minutes homogeneous, stir 4-6
Minute, the substance of E phase is added, it is 0.5-1.5 minutes homogeneous, it is stirred for 4-6 minutes, is cooled to 38 DEG C of dischargings；
5. standing: the material that mixing step is completed stands 10 hours or more,.
As a preferred embodiment of the above technical solution, the A phase further includes Sodium Hyaluronate；The C phase further include saualane or
Dormant oil；The D phase further includes the mixture of glycosyl sphingolipid and digalactosyl double glyceride, or, the mixture of raw H and phosphide are tieed up, or,
Mix the mixture of glycosyl sphingolipid and digalactosyl double glyceride and mixed vitamin H and phosphatide；The E phase further includes essence.
As a preferred embodiment of the above technical solution, the A phase further includes Sodium Hyaluronate；The C phase further includes saualane；Institute
Stating D phase further includes the mixture for mixing glycosyl sphingolipid and digalactosyl double glyceride and mixed vitamin H and phosphatide；The E phase is also
Including essence.
As a preferred embodiment of the above technical solution, described homogeneous homogeneous for middling speed, i.e., the slewing rate of shear axis is when homogeneous
2500-3500 revs/min.
As a preferred embodiment of the above technical solution, the step 2. in water first pass through reverse osmosis membrane filtration deionization, then
It is added in the container.
In conclusion the invention has the following advantages:
A kind of toner moistening effect of the present invention is good, timeliness is long, performance is stable, and has good anti-corrosive properties
Can, it is highly-safe without the substance for generating injury to human body；A kind of production craft step of toner is simple, produces
It is easy.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Embodiment in the present invention, ordinary skill
Personnel's all other embodiment obtained under the premise of not doing creative work, shall fall within the protection scope of the present invention.
With embodiment, the present invention is described in detail below.
Embodiment 1- embodiment 3 is the three kinds of substances composition and content of a kind of toner, is specifically shown in Table 1:
Toner material composition and content described in 1 embodiment 1-3 of table
The moistening effect trend of changing with time of toner described in embodiment 1-3 is shown in Table 2:
The moistening effect of toner described in 2 embodiment 1-3 of table changes with time trend
As shown in Table 2, behind toner 3 hours of coating embodiment 1, the measured value of the relative humidity RH of skin is up to 77
More than；Behind toner 3 hours of coating embodiment 2, the measured value of the relative humidity RH of skin is up to 77 or so, slightly below in fact
Apply the moistening effect of toner described in example 1；Behind toner 3 hours of coating embodiment 3, the survey of the relative humidity RH of skin
For magnitude up to 78 or more, moistening effect is relatively best.
The toner described in embodiment 1-3 carries out stability test, places 60 under conditions of 48 DEG C and -10 DEG C respectively
It, through detecting, the characteristics such as appearance, pH value, smell, viscosity are unchanged, also without breeding pathogenic bacteria, yeast and mold.
The toner described in embodiment 1-3 carries out corrosion-resistanting test, carries out being inoculated with once on every Mondays, carries out eight microorganisms
Inoculation test is stored in climatic chamber and carries out microbial reproduction, carries out the inspection of a Microbial survival rate every three days,
As a result bacterium < 10cfu/g；Mould and saccharomycete: it is not detected；Other colibacillus of excrement, staphylococcus aureus, Pseudomonas aeruginosa
Be not detected, thus illustrate the protective system be completely can by.
Embodiment 4-6 is related to the production technology of toner, and technological parameter is shown in Table 3, homogeneous and stirring the label in table 3
It is carried out according to the sequence in claims.
The processing parameter of toner in table 3- embodiment 4-6
Specific step is as follows:
Embodiment 4: a kind of production technology of toner includes the following steps:
1. grouping: a kind of component of toner described in claim 1 being grouped, is respectively as follows:
A phase, including water, glycerol, propylene glycol, EDTA-2Na, allantoin, spirulina maxim extract, Sodium Hyaluronate, three
Methylglycine and trehalose；
B phase, the cross-linked polymer including -25 methacrylate of ammonium acryloyldime-thyltaurate and docosyl alcohol polyethers；
C phase, including white pond flower seed oil, dormant oil, ring five dimethyl silicone polymer；
D phase, mixture, algae extract, panthenol and compound amino acid including biological carbohydrate gum -1, dimension raw H and phosphide；
E phase, including Bis(hydroxymethyl)imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate；
2. solvent is handled: adding water to vessel in heating to 95 DEG C, keep the temperature 30 minutes, stirring is cooled to 80 DEG C later；
3. emulsification: the substance in A phase than water being added in the container, homogeneous 1 minute, insulated and stirred is until A
The substance of B phase is added in the dissolution of phase substance, and homogeneous 2 minutes, the material in insulated and stirred to the container was uniform, added C phase
Substance stirs 10 minutes, then homogeneous 3 minutes, is cooled to 45 DEG C；
4. mixing: the substance of D phase is added in the above-mentioned material for being cooled to 45 DEG C, homogeneous 1 minute, stirs 3 minutes, then plus
Enter the substance of E phase, homogeneous 1 minute, be stirred for 3 minutes, be cooled to 38 DEG C of dischargings, it is described it is homogeneous for middling speed it is homogeneous, i.e., when homogeneous
The slewing rate of shear axis is 3000 revs/min；
5. standing: the material that mixing step is completed stands 12 hours,.
Embodiment 5: a kind of production technology of toner includes the following steps:
1. grouping: a kind of component of toner described in claim 1 being grouped, is respectively as follows:
A phase, including water, glycerol, propylene glycol, EDTA-2Na, allantoin, spirulina maxim extract, trimethylglycine
And trehalose；
B phase, the cross-linked polymer including -25 methacrylate of ammonium acryloyldime-thyltaurate and docosyl alcohol polyethers；
C phase, including white pond flower seed oil and ring five dimethyl silicone polymer；
D phase, mixture, panthenol including biological carbohydrate gum -1, algae extract, glycosyl sphingolipid and digalactosyl double glyceride and multiple
Close amino acid；
E phase, including Bis(hydroxymethyl)imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate；
2. solvent is handled: adding water to vessel in heating to 93 DEG C, keep the temperature 30 minutes, stirring is cooled to 80 DEG C later；
3. emulsification: the substance in A phase than water is added in the container, homogeneous 0.5 minute, insulated and stirred until
The substance of B phase is added in the dissolution of A phase substance, and homogeneous 1.5 minutes, the material in insulated and stirred to the container was uniform, added C
The substance of phase stirs 8 minutes, then homogeneous 2 minutes, is cooled to 45 DEG C；
4. mixing: the substance of D phase is added in the above-mentioned material for being cooled to 45 DEG C, homogeneous 0.5 minute, stirs 4 minutes, then
The substance of E phase is added, homogeneous 0.5 minute, is stirred for 4 minutes, is cooled to 38 DEG C of dischargings, it is described it is homogeneous be that middling speed is homogeneous, i.e., it is even
The slewing rate of shear axis is 3500 revs/min when matter；
5. standing: the material that mixing step is completed stands 10 hours,.
Embodiment 6: a kind of production technology of toner includes the following steps:
1. grouping: a kind of component of toner described in claim 1 being grouped, is respectively as follows:
A phase, including water, glycerol, propylene glycol, EDTA-2Na, allantoin, spirulina maxim extract, trimethylglycine
And trehalose；
B phase, the cross-linked polymer including -25 methacrylate of ammonium acryloyldime-thyltaurate and docosyl alcohol polyethers；
C phase, including white pond flower seed oil, saualane, ring five dimethyl silicone polymer；
D phase, including biological carbohydrate gum -1, algae extract, mixing glycosyl sphingolipid and digalactosyl double glyceride and mixed vitamin H
With the mixture, panthenol and compound amino acid of phosphatide；
E phase, including Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate and essence；
2. solvent is handled: water is by reverse osmosis membrane filtration deionization, then the water of deionization is added into container and is added
Heat keeps the temperature 30 minutes to 97 DEG C, and stirring is cooled to 80 DEG C later；
3. emulsification: the substance in A phase than water is added in the container, homogeneous 1.5 minutes, insulated and stirred until
The substance of B phase is added in the dissolution of A phase substance, and homogeneous 2.5 minutes, the material in insulated and stirred to the container was uniform, added C
The substance of phase stirs 12 minutes, then homogeneous 4 minutes, is cooled to 45 DEG C；
4. mixing: the substance of D phase is added in the above-mentioned material for being cooled to 45 DEG C, homogeneous 1.5 minutes, stirs 6 minutes, then
The substance of E phase is added, homogeneous 1.5 minutes, is stirred for 6 minutes, is cooled to 38 DEG C of dischargings, it is described it is homogeneous be that middling speed is homogeneous, i.e., it is even
The slewing rate of shear axis is 2500 revs/min when matter；
5. standing: the material that mixing step is completed stands 11 hours,.
Claims (4)
1. a kind of toner, which is characterized in that be made of following substance: solvent, moisturizer, chelating agent, skin conditioning agent, thickening
Emulsifier, emollient, preservative and essence, the mass fraction of the essence are 0.03 part；Wherein the solvent is water, quality
Number is 70 parts；The moisturizer by glycerol, propylene glycol, Sodium Hyaluronate, spirulina maxim extract, trimethylglycine,
Trehalose, biological carbohydrate gum -1, algae extract and panthenol are constituted, and mass fraction is respectively 3 parts, 3 parts, 0.05 part, 3 parts, 1 part, 1.5
Part, 5 parts, 2 parts, 0.1 part；The chelating agent is EDTA-2Na, and mass fraction is 0.05 part；The skin conditioning agent is by allantois
Element, glycosyl sphingolipid and the mixture of digalactosyl double glyceride, the mixture of biotin and phosphide, compound amino acid are constituted, quality
Number is respectively 0.15 part, 1 part, 1 part, 2 parts；The thickener/emulsifier is that ammonium acryloyldime-thyltaurate and docosyl alcohol are poly-
The cross-linked polymer of -25 methacrylate of ether, mass fraction are 1 part；The emollient is by white pond flower seed oil, saualane and ring
Five dimethyl silicone polymers are constituted, and mass fraction is respectively 1 part, 3 parts, 2 parts；The preservative is by bis- (methylol) imidazolidinyls
Urea and iodine propilolic alcohol butyl mephenesin Carbamate are constituted, and mass fraction is respectively 0.1188 part and 0.0012 part.
2. a kind of production technology of toner, which comprises the steps of:
1. grouping: a kind of component of toner described in claim 1 being grouped, is respectively as follows:
A phase, including water, glycerol, propylene glycol, Sodium Hyaluronate, EDTA-2Na, allantoin, spirulina maxim extract, trimethyl
Glycine and trehalose；
B phase, the cross-linked polymer including -25 methacrylate of ammonium acryloyldime-thyltaurate and docosyl alcohol polyethers；
C phase, including saualane, white pond flower seed oil and ring five dimethyl silicone polymer；
D phase, including biological carbohydrate gum -1, algae extract, panthenol, glycosyl sphingolipid, digalactosyl double glyceride, biotin, phosphatide and multiple
Close amino acid；
E phase, including Bis(hydroxymethyl)imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate and essence；
2. solvent is handled: adding water to vessel in heating to 93-97 DEG C, keep the temperature 30 minutes, stirring is cooled to 80 DEG C later；
3. emulsification: the substance in A phase than water is added in the container, it is 0.5-1.5 minute homogeneous, insulated and stirred up to
The dissolution of A phase substance, is added the substance of B phase, and 1.5-2.5 minutes homogeneous, the material in insulated and stirred to the container is uniform, then plus
Enter the substance of C phase, stirs 8-12 minutes, then 2-4 minutes homogeneous, be cooled to 45 DEG C；
4. mixing: the substance of D phase is added in the above-mentioned material for being cooled to 45 DEG C, it is 0.5-1.5 minutes homogeneous, it stirs 4-6 minutes,
The substance of E phase is added, it is 0.5-1.5 minutes homogeneous, it is stirred for 4-6 minutes, is cooled to 38 DEG C of dischargings；
5. standing: the material that mixing step is completed stands 10 hours or more,.
3. a kind of production technology of toner according to claim 2, it is characterised in that: it is described it is homogeneous for middling speed it is homogeneous,
The slewing rate of shear axis is 2500-3500 revs/min when i.e. homogeneous.
4. a kind of production technology of toner according to claim 2, it is characterised in that: the step 2. in water first pass through
Reverse osmosis membrane filtration deionization is crossed, is then added in the container.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102370605A (en) * | 2011-09-27 | 2012-03-14 | 沈志荣 | Smoothening and moisturizing lotion composition and preparation method thereof |
| CN105232438A (en) * | 2015-10-10 | 2016-01-13 | 严建明 | Moisturizing and repairing facial mask and preparation method thereof |
| CN105380870A (en) * | 2015-12-30 | 2016-03-09 | 广州环亚化妆品科技有限公司 | Toning lotion with efficacy of repairing cuticle and a preparation method of toning lotion |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102370605A (en) * | 2011-09-27 | 2012-03-14 | 沈志荣 | Smoothening and moisturizing lotion composition and preparation method thereof |
| CN105232438A (en) * | 2015-10-10 | 2016-01-13 | 严建明 | Moisturizing and repairing facial mask and preparation method thereof |
| CN105380870A (en) * | 2015-12-30 | 2016-03-09 | 广州环亚化妆品科技有限公司 | Toning lotion with efficacy of repairing cuticle and a preparation method of toning lotion |
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