CN106070393A - A kind of bactericide and preparation method thereof - Google Patents
A kind of bactericide and preparation method thereof Download PDFInfo
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- CN106070393A CN106070393A CN201610422122.9A CN201610422122A CN106070393A CN 106070393 A CN106070393 A CN 106070393A CN 201610422122 A CN201610422122 A CN 201610422122A CN 106070393 A CN106070393 A CN 106070393A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/04—Nitrogen directly attached to aliphatic or cycloaliphatic carbon atoms
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/34—Nitriles
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/24—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
- A01N43/26—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings
- A01N43/28—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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Abstract
nullThe invention discloses a kind of bactericide and preparation method thereof，Relate to pesticide field，A kind of bactericide，By weight，Described bactericide includes: the root of Chinese wild ginger 2～6 parts，3～7 parts of turmeric，Kuh-seng 5～7 parts、2～4 parts of Radix Glycyrrhizae、The rhizome of Chinese monkshood 1～5 part、0.5～2 part of sulphur、Rosin 3.5～5 parts、5～10 parts of calcium oxide、Bravo 2～5.5 parts、Big raw 5～10 parts、Spray gram 1～5 part、Safe and sound life 7～10 parts、Lime sulfur 10～12 parts、Iprodione 4～10 parts、Hymexazol-matulaxyl 3～6 parts、Agricultural streptavidin 6～9 parts、Blue or green withered clever 2～5 parts、Octyl trichlamide 4～8 parts，Remaining is water or tar，Use technical scheme，Production efficiency is high、Step is simple and low cost，Easily implement，Raw material easily obtains，Also it is capable of the growth of cover crop while strengthening sterilizing，It is not likely to produce the resistance to the action of a drug simultaneously.
Description
Technical field
The present invention relates to pesticide field, be specifically related to a kind of bactericide and preparation method thereof.
Background technology
Chemical agent plays a significant role in terms of crop pest control, but, due to chemical agent Long-Time Service,
Causing most area pest and disease damage fastness frequency more than 50%, resistance level is up to more than ten thousand times, and single use chemical agent is
Lose preventive effect completely.Further, as resistant strain constantly strengthens, spraying times increases year by year, and formulation rate is also doubled and redoubled, and gives anti-
Control and bring immense pressure with surrounding environment.Its drawback also becomes increasingly conspicuous, ferocious again such as medicament residue, environmental pollution and harmful organism
Rampant etc..
Patent No. CN 104012529 B provides a kind of bactericide, including protective agent and therapeutic agent；Described guarantor
Protect agent include Da Kening, Bravo, big raw, spray gram, safe and sound life, lime sulfur, iprodione, can kill, Cupravit；Described treatment
Agent includes: Hymexazol-matulaxyl, hymexazol, agricultural streptavidin, blue or green withered spirit, kasugarnycin, octyl trichlamide；Formula in the present invention is applicable to greatly
The interference of most crops suffered insect pest, bacteriums in growth course, and especially protective agent and therapeutic agent are melted in filling a prescription for
Integrally, it is also capable of the growth of cover crop while strengthening sterilizing, but its Long-Time Service is easily generated resistance.
Patent No. CN 101744010 B discloses a kind of botanical fungicide and preparation method thereof, relates to a kind of bactericide
And preparation method thereof.The present invention solves existing bactericide and has that environmental pollution is serious and Long-Time Service produces lacking of resistance
Point.Botanical fungicide of the present invention is made up of Chinese Stellera Root, Radix Glycyrrhizae, the rhizome of Chinese monkshood and kuh-seng.The method of the present invention is as follows: the first, weigh
Mix after Chinese Stellera Root, Radix Glycyrrhizae, the rhizome of Chinese monkshood and kuh-seng；2nd, alcohol steep；3rd, filter；4th, distill；5th, moist heat sterilization.This
Invention botanical fungicide have nontoxic, low-residual, medicament usage amount are little, pollution-free, without drug-fast advantage, but its cost is relatively
High.
Content of the invention
Problem to be solved by this invention is to provide a kind of bactericide and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of bactericide, by weight, described bactericide includes: the root of Chinese wild ginger 2～6 parts, 3～7 parts of turmeric, kuh-seng 5
～7 parts, 2～4 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 1～5 part, 0.5～2 part of sulphur, rosin 3.5～5 parts, 5～10 parts of calcium oxide, Bravo 2～
5.5 parts, greatly give birth to 5～10 parts, spray gram 1～5 part, safe and sound life 7～10 parts, lime sulfur 10～12 parts, iprodione 4～10 parts, wide
Withered clever 3～6 parts, agricultural streptavidin 6～9 parts, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water or tar.
Preferably, by weight, described bactericide includes: the root of Chinese wild ginger 4 parts, 5 parts of turmeric, kuh-seng 6 parts, 3 parts of Radix Glycyrrhizae,
The rhizome of Chinese monkshood 3 parts, 1 part of sulphur, rosin 4 parts, 8 parts of calcium oxide, Bravo 4 parts, big life 8 parts, spray gram 3 parts, safe and sound life 8 parts, stone sulphur close
Agent 11 parts, iprodione 8 parts, Hymexazol-matulaxyl 4 parts, agricultural streptavidin 7 parts, blue or green withered clever 3 parts, octyl trichlamide 6 parts, remaining is water or tar.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, and prepares the root of Chinese wild ginger 2～6 parts, 3～7 parts of turmeric, kuh-seng 5～7 parts, 2～4 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 1～5
Part, 0.5～2 part of sulphur, rosin 3.5～5 parts, 5～10 parts of calcium oxide, Bravo 2～5.5 parts, greatly give birth to 5～10 parts, spray gram 1～
5 parts, safe and sound life 7～10 parts, lime sulfur 10～12 parts, iprodione 4～10 parts, Hymexazol-matulaxyl 3～6 parts, agricultural streptavidin 6～9
Part, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water or tar.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, iprodione, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: the root of Chinese wild ginger that will be dried, turmeric, kuh-seng, Radix Glycyrrhizae, the rhizome of Chinese monkshood, sulphur, rosin, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction that step 3 is obtained, wherein the mixing speed in leaching process is 100～250r/min,
Twice, 1 hour every time, extraction temperature was 65～70 DEG C in extraction；
Step 5: the product obtaining step 4 filters；
Step 6: product that the mixed liquor obtaining step 2 and step 5 obtain adds in reactor, temperature at 50～90 DEG C,
Stir, then add water in proportion or add tar, stir 12～18 minutes, obtain reflecting liquid；
Step 7: under the conditions of 100～120 DEG C, reactant liquor is distilled, 125～130 DEG C, under the conditions of 0.05MPa, will reaction
Liquid carries out moist heat sterilization 15～25min, i.e. obtains bactericide；
Step 8: the stoste of bactericide is diluted 100-150 times and can spray use.
Preferably, in the solution after the stoste dilution of bactericide described in step 8, water accounts for the 75%-85% of gross weight.
Preferably, the extraction temperature described in step 4 is 68 DEG C.
Preferably, the leaching liquor extracting use in described step 4 is the ethanol that volume ratio is 70%.
Using technical scheme, production efficiency is high, step is simple and low cost, easily implements, and raw material easily obtains
Take, be also capable of the growth of cover crop while strengthening sterilizing, be not likely to produce the resistance to the action of a drug simultaneously.
Detailed description of the invention
For make the present invention realize technological means, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with
Detailed description of the invention, is expanded on further the present invention.
Embodiment 1:
A kind of bactericide, by weight, described bactericide includes: the root of Chinese wild ginger 2 parts, 3 parts of turmeric, kuh-seng 5 parts, Radix Glycyrrhizae
2 parts, the rhizome of Chinese monkshood 1 part, 0.5 part of sulphur, rosin 3.5 parts, 5 parts of calcium oxide, Bravo 2 parts, big raw 5 parts, spray gram 1 part, safe and sound life 7
Part, lime sulfur 10 parts, iprodione 4 parts, Hymexazol-matulaxyl 3 parts, agricultural streptavidin 6 parts, blue or green withered clever 2 parts, octyl trichlamide 4 parts, remaining is
Water.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, the root of Chinese wild ginger 2 parts, 3 parts of turmeric, kuh-seng 5 parts, 2 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 1 part, 0.5 part of sulphur, rosin 3.5
Part, 5 parts of calcium oxide, Bravo 2 parts, big raw 5 parts, spray gram 1 part, safe and sound life 7 parts, lime sulfur 10 parts, iprodione 4 parts, extensively withered
Spirit 3 parts, agricultural streptavidin 6 parts, blue or green withered clever 2 parts, octyl trichlamide 4 parts, remaining is water.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, iprodione, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: the root of Chinese wild ginger that will be dried, turmeric, kuh-seng, Radix Glycyrrhizae, the rhizome of Chinese monkshood, sulphur, rosin, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction obtaining step 3, wherein the mixing speed in leaching process is 100r/min, extracts two
Secondary, 1 hour every time, extraction temperature was 65 DEG C；
Step 5: the product obtaining step 4 filters；
Step 6: the product that the mixed liquor obtaining step 2 and step 5 obtain adds in reactor, temperature, at 50 DEG C, stirs
Uniformly, more in proportion add water or add tar, stirring 12 minutes, obtaining reflecting liquid；
Step 7: under the conditions of 100 DEG C, reactant liquor is distilled, 125 DEG C, under the conditions of 0.05MPa, reactant liquor is carried out damp and hot
Sterilizing 15min, i.e. obtains bactericide；
Step 8: the stoste of bactericide is diluted 100 times and can spray use.
Wherein, in the solution after the stoste dilution of bactericide described in step 8, water accounts for the 75% of gross weight.
Wherein, the leaching liquor extracting use in described step 4 is the ethanol that volume ratio is 70%.
Embodiment 2:
A kind of bactericide, by weight, described bactericide includes: the root of Chinese wild ginger 6 parts, 7 parts of turmeric, kuh-seng 7 parts, Radix Glycyrrhizae
4 parts, the rhizome of Chinese monkshood 5 parts, 2 parts of sulphur, rosin 5 parts, 10 parts of calcium oxide, Bravo 5.5 parts, big raw 10 parts, spray gram 5 parts, safe and sound life 10
Part, lime sulfur 12 parts, iprodione 10 parts, Hymexazol-matulaxyl 6 parts, agricultural streptavidin 9 parts, blue or green withered clever 5 parts, octyl trichlamide 8 parts, remaining is
Water.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, and prepares the root of Chinese wild ginger 6 parts, 7 parts of turmeric, kuh-seng 7 parts, 4 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 5 parts, 2 parts of sulphur, rosin 5
Part, 10 parts of calcium oxide, Bravo 5.5 parts, big life 10 parts, spray gram 5 parts, safe and sound life 10 parts, lime sulfur 12 parts, iprodione 10
Part, Hymexazol-matulaxyl 6 parts, agricultural streptavidin 9 parts, blue or green withered clever 5 parts, octyl trichlamide 8 parts, remaining is water.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, iprodione, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: the root of Chinese wild ginger that will be dried, turmeric, kuh-seng, Radix Glycyrrhizae, the rhizome of Chinese monkshood, sulphur, rosin, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction obtaining step 3, wherein the mixing speed in leaching process is 250r/min, extraction
Twice, every time 1 hour, extraction temperature was 70 DEG C；
Step 5: the product obtaining step 4 filters；
Step 6: the product that the mixed liquor obtaining step 2 and step 5 obtain adds in reactor, temperature, at 90 DEG C, stirs
Uniformly, more in proportion add water or add tar, stirring 18 minutes, obtaining reflecting liquid；
Step 7: under the conditions of 120 DEG C, reactant liquor is distilled, 130 DEG C, under the conditions of 0.05MPa, reactant liquor is carried out damp and hot
Sterilizing 25min, i.e. obtains bactericide；
Step 8: the stoste of bactericide is diluted 150 times and can spray use.
Wherein, in the solution after the stoste dilution of bactericide described in step 8, water accounts for the 85% of gross weight.
Wherein, the leaching liquor extracting use in described step 4 is the ethanol that volume ratio is 70%.
Embodiment 3: a kind of bactericide, by weight, described bactericide includes: the root of Chinese wild ginger 4 parts, 5 parts of turmeric,
Kuh-seng 6 parts, 3 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 3 parts, 1 part of sulphur, rosin 4 parts, 8 parts of calcium oxide, Bravo 4 parts, big raw 8 parts, spray gram 3 parts,
Safe and sound life 8 parts, lime sulfur 11 parts, iprodione 8 parts, Hymexazol-matulaxyl 4 parts, agricultural streptavidin 7 parts, blue or green withered clever 3 parts, octyl trichlamide 6 parts,
Remaining is tar.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, and prepares the root of Chinese wild ginger 4 parts, 5 parts of turmeric, kuh-seng 6 parts, 3 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 3 parts, 1 part of sulphur, rosin 4
Part, 8 parts of calcium oxide, Bravo 4 parts, big raw 8 parts, spray gram 3 parts, safe and sound life 8 parts, lime sulfur 11 parts, iprodione 8 parts, extensively withered
Spirit 4 parts, agricultural streptavidin 7 parts, blue or green withered clever 3 parts, octyl trichlamide 6 parts, remaining is tar.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, iprodione, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: the root of Chinese wild ginger that will be dried, turmeric, kuh-seng, Radix Glycyrrhizae, the rhizome of Chinese monkshood, sulphur, rosin, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction obtaining step 3, wherein the mixing speed in leaching process is 200r/min, extraction
Twice, every time 1 hour, extraction temperature was 68 DEG C；
Step 5: the product obtaining step 4 filters；
Step 6: the product that the mixed liquor obtaining step 2 and step 5 obtain adds in reactor, temperature, at 70 DEG C, stirs
Uniformly, more in proportion add water or add tar, stirring 15 minutes, obtaining reflecting liquid；
Step 7: under the conditions of 110 DEG C, reactant liquor is distilled, 128 DEG C, under the conditions of 0.05MPa, reactant liquor is carried out damp and hot going out
Bacterium 20min, i.e. obtains bactericide；
Step 8: the stoste of bactericide is diluted 120 times and can spray use.
Wherein, in the solution after the stoste dilution of bactericide described in step 8, water accounts for the 80% of gross weight.
Wherein, the leaching liquor extracting use in described step 4 is the ethanol that volume ratio is 70%.
Based on above-mentioned, using technical scheme, production efficiency is high, step is simple and low cost, easily implements, former
Material easily obtains, and is also capable of the growth of cover crop, is not likely to produce the resistance to the action of a drug simultaneously while strengthening sterilizing.
The obvious present invention implements and is not subject to the restrictions described above, as long as have employed method design and the skill of the present invention
The improvement of the various unsubstantialities that art scheme is carried out, or the not improved design by the present invention and technical scheme directly apply to it
Its occasion, all within protection scope of the present invention.
Claims (6)
1. a bactericide, it is characterised in that by weight, described bactericide includes: the root of Chinese wild ginger 2～6 parts, turmeric
3～7 parts, kuh-seng 5～7 parts, 2～4 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 1～5 part, 0.5～2 part of sulphur, rosin 3.5～5 parts, calcium oxide 5～10
Part, Bravo 2～5.5 parts, greatly raw 5～10 parts, spray gram 1～5 part, safe and sound life 7～10 parts, lime sulfur 10～12 parts, different bacterium
Urea 4～10 parts, Hymexazol-matulaxyl 3～6 parts, agricultural streptavidin 6～9 parts, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water
Or tar.
2. a kind of bactericide according to claim 1, it is characterised in that: by weight, described bactericide
Including: the root of Chinese wild ginger 4 parts, 5 parts of turmeric, kuh-seng 6 parts, 3 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 3 parts, 1 part of sulphur, rosin 4 parts, 8 parts of calcium oxide, Bravo
4 parts, big raw 8 parts, spray gram 3 parts, safe and sound life 8 parts, lime sulfur 11 parts, iprodione 8 parts, Hymexazol-matulaxyl 4 parts, agricultural streptavidin 7 parts,
Blue or green withered clever 3 parts, octyl trichlamide 6 parts, remaining is water or tar.
3. the method for the bactericide prepared described in claim 1-2 any one, it is characterised in that described preparation side
Method specifically includes following steps:
Step one: raw material prepares, and prepares the root of Chinese wild ginger 2～6 parts, 3～7 parts of turmeric, kuh-seng 5～7 parts, 2～4 parts of Radix Glycyrrhizae, the rhizome of Chinese monkshood 1～5
Part, 0.5～2 part of sulphur, rosin 3.5～5 parts, 5～10 parts of calcium oxide, Bravo 2～5.5 parts, greatly give birth to 5～10 parts, spray gram 1～
5 parts, safe and sound life 7～10 parts, lime sulfur 10～12 parts, iprodione 4～10 parts, Hymexazol-matulaxyl 3～6 parts, agricultural streptavidin 6～9
Part, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water or tar；
Step 2: by Bravo, big raw, spray gram, safe and sound life, lime sulfur, iprodione, Hymexazol-matulaxyl, agricultural streptavidin, blue or green withered
Spirit, octyl trichlamide smash into respectively last pours in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight, obtains
Mixed liquor；
Step 3: the root of Chinese wild ginger that will be dried, turmeric, kuh-seng, Radix Glycyrrhizae, the rhizome of Chinese monkshood, sulphur, rosin, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction that step 3 is obtained, wherein the mixing speed in leaching process is 100～250r/min,
Twice, 1 hour every time, extraction temperature was 65～70 DEG C in extraction；
Step 5: the product obtaining step 4 filters；
Step 6: product that the mixed liquor obtaining step 2 and step 5 obtain adds in reactor, temperature at 50～90 DEG C,
Stir, then add water in proportion or add tar, stir 12～18 minutes, obtain reflecting liquid；
Step 7: under the conditions of 100～120 DEG C, reactant liquor is distilled, 125～130 DEG C, under the conditions of 0.05MPa, will reaction
Liquid carries out moist heat sterilization 15～25min, i.e. obtains bactericide；
Step 8: the stoste of bactericide is diluted 100-150 times and can spray use.
4. the preparation method of a kind of bactericide according to claim 3, it is characterised in that: plant described in step 8
In solution after the stoste dilution of bactericide, water accounts for the 75%-85% of gross weight.
5. the preparation method of a kind of bactericide according to claim 3, it is characterised in that: the extraction described in step 4
Temperature is 68 DEG C.
6. the preparation method of a kind of bactericide according to claim 3, it is characterised in that: described step 4 extracts
The leaching liquor using is the ethanol that volume ratio is 70%.
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| CN106035430A (en) * | 2016-06-30 | 2016-10-26 | 安徽金培因科技有限公司 | Plant fungicide and preparation method thereof |
| CN106070396A (en) * | 2016-06-27 | 2016-11-09 | 安徽梅兰园林景观工程有限公司 | A kind of bactericide and preparation method thereof |
| CN108299088A (en) * | 2018-02-11 | 2018-07-20 | 平南县德湖种养农民专业合作社 | A kind of Monstera deliciosa dedicated fertilizer and preparation method thereof |
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Address after: 230000 Anhui city of Hefei province Hefei Economic Development Zone Director Gu Lu Peach Industrial Avenue intersection and innovation of Anhui Hengxin plastic products limited company office building Applicant after: Anhui phenanthrene new materials Co., Ltd. Address before: 230000 Anhui Province, Hefei city of Anhui province Hefei Economic Development Zone Director Gu Lu Peach Industrial Avenue intersection and innovation of Anhui Hengxin plastic products limited company office building Applicant before: Anhui Feiyang Agricultural Technology Co., Ltd. |
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Application publication date: 20161109 |