CN106070396A - A kind of bactericide and preparation method thereof - Google Patents
A kind of bactericide and preparation method thereof Download PDFInfo
- Publication number
- CN106070396A CN106070396A CN201610475752.2A CN201610475752A CN106070396A CN 106070396 A CN106070396 A CN 106070396A CN 201610475752 A CN201610475752 A CN 201610475752A CN 106070396 A CN106070396 A CN 106070396A
- Authority
- CN
- China
- Prior art keywords
- parts
- bactericide
- sulfur
- bravo
- streptavidin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/04—Nitrogen directly attached to aliphatic or cycloaliphatic carbon atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/34—Nitriles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/46—N-acyl derivatives
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/24—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
- A01N43/26—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings
- A01N43/28—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
- A01N47/14—Di-thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
nullThe invention discloses a kind of bactericide and preparation method thereof，Relate to pesticide field，A kind of bactericide，By weight，Described bactericide includes: Herba Asari 2～6 parts，Rhizoma Curcumae Longae 3～7 parts，Radix Sophorae Flavescentis 5～7 parts、Radix Glycyrrhizae 2～4 parts、Aconitum carmichjaelii Debx. 1～5 parts、Sulfur 0.5～2 parts、Colophonium 3.5～5 parts、Calcium oxide 5～10 parts、Bravo 2～5.5 parts、Big raw 5～10 parts、Spray gram 1～5 part、Safe and sound life 7～10 parts、Lime sulfur 10～12 parts、RP-26019 4～10 parts、Hymexazol-matulaxyl 3～6 parts、Agricultural streptavidin 6～9 parts、Blue or green withered clever 2～5 parts、Octyl trichlamide 4～8 parts，Remaining is water or tar，Use technical scheme，Production efficiency is high、Step is simple and low cost，Easily implement，Raw material easily obtains，The growth of cover crop it also is able to while strengthening sterilizing，It is not likely to produce Drug resistance simultaneously.
Description
Technical field
The present invention relates to pesticide field, be specifically related to a kind of bactericide and preparation method thereof.
Background technology
Chemical agent plays a significant role in terms of crop pest control, but, due to chemical agent life-time service,
Causing most area pest and disease damage fastness frequency more than 50%, resistance level is up to more than ten thousand times, and single use chemical agent is
Lose preventive effect completely.Further, along with resistant strain constantly strengthens, spraying times increases year by year, and formulation rate is also doubled and redoubled, and gives anti-
Control and bring immense pressure with surrounding.Its drawback also becomes increasingly conspicuous, the most ferocious such as drug residue, environmental pollution and harmful organism
Rampant etc..
Patent No. CN 104012529 B provides a kind of bactericide, including protective agent and therapeutic agent；Described guarantor
Protect agent include Da Kening, Bravo, big raw, spray gram, safe and sound life, lime sulfur, RP-26019, can kill, Cupravit；Described treatment
Agent includes: Hymexazol-matulaxyl, hymexazol, agricultural streptavidin, blue or green withered spirit, kasugarnycin, octyl trichlamide；Formula in the present invention is applicable to greatly
Most crops are suffered insect pest, the interference of antibacterial in growth course, and protective agent and therapeutic agent are melted by formula especially for
Integrally, it also is able to the growth of cover crop while strengthening sterilizing, but its life-time service is easily generated resistance.
Patent No. CN 101744010 B discloses a kind of botanical fungicide and preparation method thereof, relates to a kind of antibacterial
And preparation method thereof.The present invention solves existing antibacterial and has that environmental pollution is serious and life-time service produces lacking of resistance
Point.Botanical fungicide of the present invention is made up of Stellera chamaejasme L., Radix Glycyrrhizae, Aconitum carmichjaelii Debx. and Radix Sophorae Flavescentis.The method of the present invention is as follows: one, weigh
Mix after Stellera chamaejasme L., Radix Glycyrrhizae, Aconitum carmichjaelii Debx. and Radix Sophorae Flavescentis；Two, alcohol steep；Three, filter；Four, distillation；Five, moist heat sterilization.This
Invention botanical fungicide have nontoxic, low-residual, medicament usage amount are little, pollution-free, without drug-fast advantage, but its cost is relatively
High.
Summary of the invention
Problem to be solved by this invention is to provide a kind of bactericide and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of bactericide, by weight, described bactericide includes: Herba Asari 2～6 parts, Rhizoma Curcumae Longae 3～7 parts, Radix Sophorae Flavescentis 5
～7 parts, Radix Glycyrrhizae 2～4 parts, Aconitum carmichjaelii Debx. 1～5 parts, sulfur 0.5～2 parts, Colophonium 3.5～5 parts, calcium oxide 5～10 parts, Bravo 2～
5.5 parts, big raw 5～10 parts, spray gram 1～5 part, safe and sound life 7～10 parts, lime sulfur 10～12 parts, RP-26019 4～10 parts, wide
Withered clever 3～6 parts, agricultural streptavidin 6～9 parts, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water or tar.
Preferably, by weight, described bactericide includes: Herba Asari 4 parts, 5 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 6 parts, 3 parts of Radix Glycyrrhizae,
Aconitum carmichjaelii Debx. 3 parts, 1 part of sulfur, Colophonium 4 parts, calcium oxide 8 parts, Bravo 4 parts, big raw 8 parts, spray gram 3 parts, safe and sound life 8 parts, stone thio
Agent 11 parts, RP-26019 8 parts, Hymexazol-matulaxyl 4 parts, agricultural streptavidin 7 parts, blue or green withered clever 3 parts, octyl trichlamide 6 parts, remaining is water or tar.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, prepares Herba Asari 2～6 parts, Rhizoma Curcumae Longae 3～7 parts, Radix Sophorae Flavescentis 5～7 parts, Radix Glycyrrhizae 2～4 parts, Aconitum carmichjaelii Debx. 1～5
Part, sulfur 0.5～2 parts, Colophonium 3.5～5 parts, calcium oxide 5～10 parts, Bravo 2～5.5 parts, big raw 5～10 parts, spray gram 1～
5 parts, safe and sound life 7～10 parts, lime sulfur 10～12 parts, RP-26019 4～10 parts, Hymexazol-matulaxyl 3～6 parts, agricultural streptavidin 6～9
Part, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water or tar.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, RP-26019, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: by dry Herba Asari, Rhizoma Curcumae Longae, Radix Sophorae Flavescentis, Radix Glycyrrhizae, Aconitum carmichjaelii Debx., sulfur, Colophonium, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction that step 3 is obtained, wherein the mixing speed in leaching process is 100～250r/min,
Extracting twice, each 1 hour, extraction temperature is 65～70 DEG C；
Step 5: product step 4 obtained filters；
Step 6: product that mixed liquor step 2 obtained and step 5 obtain adds in reactor, temperature at 50～90 DEG C,
Stir, then add water in proportion or add tar, stir 12～18 minutes, obtain reflecting liquid；
Step 7: under the conditions of 100～120 DEG C, reactant liquor is distilled, 125～130 DEG C, under the conditions of 0.05MPa, will reaction
Liquid carries out moist heat sterilization 15～25min, i.e. obtains bactericide；
Step 8: the stock solution of bactericide is diluted 100-150 times and can spray use.
Preferably, in the solution after the stock solution dilution of bactericide described in step 8, water accounts for the 75%-85% of gross weight.
Preferably, the extraction temperature described in step 4 is 68 DEG C.
Preferably, described step 4 extracts the lixiviating solution of use be volume ratio be the ethanol of 70%.
Using technical scheme, production efficiency is high, step is simple and low cost, easily implements, and raw material easily obtains
Take, also be able to the growth of cover crop while strengthening sterilizing, be not likely to produce Drug resistance simultaneously.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with
Detailed description of the invention, is expanded on further the present invention.
Embodiment 1:
A kind of bactericide, by weight, described bactericide includes: Herba Asari 2 parts, 3 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 5 parts, Radix Glycyrrhizae
2 parts, Aconitum carmichjaelii Debx. 1 part, 0.5 part of sulfur, Colophonium 3.5 parts, calcium oxide 5 parts, Bravo 2 parts, big raw 5 parts, spray gram 1 part, safe and sound life 7
Part, lime sulfur 10 parts, RP-26019 4 parts, Hymexazol-matulaxyl 3 parts, agricultural streptavidin 6 parts, blue or green withered clever 2 parts, octyl trichlamide 4 parts, remaining is
Water.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, Herba Asari 2 parts, 3 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 5 parts, 2 parts of Radix Glycyrrhizae, Aconitum carmichjaelii Debx. 1 part, 0.5 part of sulfur, Colophonium 3.5
Part, calcium oxide 5 parts, Bravo 2 parts, big raw 5 parts, spray gram 1 part, safe and sound life 7 parts, lime sulfur 10 parts, RP-26019 4 parts, the most withered
Spirit 3 parts, agricultural streptavidin 6 parts, blue or green withered clever 2 parts, octyl trichlamide 4 parts, remaining is water.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, RP-26019, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: by dry Herba Asari, Rhizoma Curcumae Longae, Radix Sophorae Flavescentis, Radix Glycyrrhizae, Aconitum carmichjaelii Debx., sulfur, Colophonium, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: mixture extraction step 3 obtained, wherein the mixing speed in leaching process is 100r/min, extracts two
Secondary, each 1 hour, extraction temperature was 65 DEG C；
Step 5: product step 4 obtained filters；
Step 6: the product that mixed liquor step 2 obtained and step 5 obtain adds in reactor, temperature, at 50 DEG C, stirs
Uniformly, then add water in proportion or add tar, stirring 12 minutes, obtaining reflecting liquid；
Step 7: under the conditions of 100 DEG C, reactant liquor is distilled, 125 DEG C, under the conditions of 0.05MPa, reactant liquor is carried out damp and hot
Sterilizing 15min, i.e. obtains bactericide；
Step 8: the stock solution of bactericide is diluted 100 times and can spray use.
Wherein, in the solution after the stock solution dilution of bactericide described in step 8, water accounts for the 75% of gross weight.
Wherein, described step 4 extracts the lixiviating solution of use be volume ratio be the ethanol of 70%.
Embodiment 2:
A kind of bactericide, by weight, described bactericide includes: Herba Asari 6 parts, 7 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 7 parts, Radix Glycyrrhizae
4 parts, Aconitum carmichjaelii Debx. 5 parts, 2 parts of sulfur, Colophonium 5 parts, calcium oxide 10 parts, Bravo 5.5 parts, big raw 10 parts, spray gram 5 parts, safe and sound life 10
Part, lime sulfur 12 parts, RP-26019 10 parts, Hymexazol-matulaxyl 6 parts, agricultural streptavidin 9 parts, blue or green withered clever 5 parts, octyl trichlamide 8 parts, remaining is
Water.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, and prepares Herba Asari 6 parts, 7 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 7 parts, 4 parts of Radix Glycyrrhizae, Aconitum carmichjaelii Debx. 5 parts, 2 parts of sulfur, Colophonium 5
Part, calcium oxide 10 parts, Bravo 5.5 parts, big life 10 parts, spray gram 5 parts, safe and sound life 10 parts, lime sulfur 12 parts, RP-26019 10
Part, Hymexazol-matulaxyl 6 parts, agricultural streptavidin 9 parts, blue or green withered clever 5 parts, octyl trichlamide 8 parts, remaining is water.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, RP-26019, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: by dry Herba Asari, Rhizoma Curcumae Longae, Radix Sophorae Flavescentis, Radix Glycyrrhizae, Aconitum carmichjaelii Debx., sulfur, Colophonium, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: mixture extraction step 3 obtained, wherein the mixing speed in leaching process is 250r/min, extraction
Twice, each 1 hour, extraction temperature was 70 DEG C；
Step 5: product step 4 obtained filters；
Step 6: the product that mixed liquor step 2 obtained and step 5 obtain adds in reactor, temperature, at 90 DEG C, stirs
Uniformly, then add water in proportion or add tar, stirring 18 minutes, obtaining reflecting liquid；
Step 7: under the conditions of 120 DEG C, reactant liquor is distilled, 130 DEG C, under the conditions of 0.05MPa, reactant liquor is carried out damp and hot
Sterilizing 25min, i.e. obtains bactericide；
Step 8: the stock solution of bactericide is diluted 150 times and can spray use.
Wherein, in the solution after the stock solution dilution of bactericide described in step 8, water accounts for the 85% of gross weight.
Wherein, described step 4 extracts the lixiviating solution of use be volume ratio be the ethanol of 70%.
Embodiment 3: a kind of bactericide, by weight, described bactericide includes: Herba Asari 4 parts, 5 parts of Rhizoma Curcumae Longae,
Radix Sophorae Flavescentis 6 parts, 3 parts of Radix Glycyrrhizae, Aconitum carmichjaelii Debx. 3 parts, 1 part of sulfur, Colophonium 4 parts, calcium oxide 8 parts, Bravo 4 parts, big raw 8 parts, spray gram 3 parts,
Safe and sound life 8 parts, lime sulfur 11 parts, RP-26019 8 parts, Hymexazol-matulaxyl 4 parts, agricultural streptavidin 7 parts, blue or green withered clever 3 parts, octyl trichlamide 6 parts,
Remaining is tar.
A kind of preparation method of bactericide, described preparation method specifically includes following steps:
Step one: raw material prepares, and prepares Herba Asari 4 parts, 5 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 6 parts, 3 parts of Radix Glycyrrhizae, Aconitum carmichjaelii Debx. 3 parts, 1 part of sulfur, Colophonium 4
Part, calcium oxide 8 parts, Bravo 4 parts, big raw 8 parts, spray gram 3 parts, safe and sound life 8 parts, lime sulfur 11 parts, RP-26019 8 parts, the most withered
Spirit 4 parts, agricultural streptavidin 7 parts, blue or green withered clever 3 parts, octyl trichlamide 6 parts, remaining is tar.
Step 2: by Bravo, big life, spray gram, safe and sound life, lime sulfur, RP-26019, Hymexazol-matulaxyl, agricultural streptavidin, green grass or young crops
Withered spirit, octyl trichlamide smash into respectively last to be poured in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight,
To mixed liquor；
Step 3: by dry Herba Asari, Rhizoma Curcumae Longae, Radix Sophorae Flavescentis, Radix Glycyrrhizae, Aconitum carmichjaelii Debx., sulfur, Colophonium, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: mixture extraction step 3 obtained, wherein the mixing speed in leaching process is 200r/min, extraction
Twice, each 1 hour, extraction temperature was 68 DEG C；
Step 5: product step 4 obtained filters；
Step 6: the product that mixed liquor step 2 obtained and step 5 obtain adds in reactor, temperature, at 70 DEG C, stirs
Uniformly, then add water in proportion or add tar, stirring 15 minutes, obtaining reflecting liquid；
Step 7: under the conditions of 110 DEG C, reactant liquor is distilled, 128 DEG C, under the conditions of 0.05MPa, reactant liquor is carried out damp and hot going out
Bacterium 20min, i.e. obtains bactericide；
Step 8: the stock solution of bactericide is diluted 120 times and can spray use.
Wherein, in the solution after the stock solution dilution of bactericide described in step 8, water accounts for the 80% of gross weight.
Wherein, described step 4 extracts the lixiviating solution of use be volume ratio be the ethanol of 70%.
Based on above-mentioned, using technical scheme, production efficiency is high, step is simple and low cost, easily implements, former
Material easily obtains, and also is able to the growth of cover crop, is not likely to produce Drug resistance simultaneously while strengthening sterilizing.
Obviously the present invention implements and is not subject to the restrictions described above, as long as have employed method design and the skill of the present invention
The improvement of the various unsubstantialities that art scheme is carried out, or the most improved design by the present invention and technical scheme directly apply to it
Its occasion, all within protection scope of the present invention.
Claims (6)
1. a bactericide, it is characterised in that by weight, described bactericide includes: Herba Asari 2～6 parts, Rhizoma Curcumae Longae
3～7 parts, Radix Sophorae Flavescentis 5～7 parts, Radix Glycyrrhizae 2～4 parts, Aconitum carmichjaelii Debx. 1～5 parts, sulfur 0.5～2 parts, Colophonium 3.5～5 parts, calcium oxide 5～10
Part, Bravo 2～5.5 parts, big raw 5～10 parts, spray gram 1～5 part, safe and sound life 7～10 parts, lime sulfur 10～12 parts, different bacterium
Urea 4～10 parts, Hymexazol-matulaxyl 3～6 parts, agricultural streptavidin 6～9 parts, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water
Or tar.
A kind of bactericide the most according to claim 1, it is characterised in that: by weight, described bactericide
Including: Herba Asari 4 parts, 5 parts of Rhizoma Curcumae Longae, Radix Sophorae Flavescentis 6 parts, 3 parts of Radix Glycyrrhizae, Aconitum carmichjaelii Debx. 3 parts, 1 part of sulfur, Colophonium 4 parts, calcium oxide 8 parts, Bravo
4 parts, big raw 8 parts, spray gram 3 parts, safe and sound life 8 parts, lime sulfur 11 parts, RP-26019 8 parts, Hymexazol-matulaxyl 4 parts, agricultural streptavidin 7 parts,
Blue or green withered clever 3 parts, octyl trichlamide 6 parts, remaining is water or tar.
3. the method for the bactericide prepared described in claim 1-2 any one, it is characterised in that described preparation side
Method specifically includes following steps:
Step one: raw material prepares, prepares Herba Asari 2～6 parts, Rhizoma Curcumae Longae 3～7 parts, Radix Sophorae Flavescentis 5～7 parts, Radix Glycyrrhizae 2～4 parts, Aconitum carmichjaelii Debx. 1～5
Part, sulfur 0.5～2 parts, Colophonium 3.5～5 parts, calcium oxide 5～10 parts, Bravo 2～5.5 parts, big raw 5～10 parts, spray gram 1～
5 parts, safe and sound life 7～10 parts, lime sulfur 10～12 parts, RP-26019 4～10 parts, Hymexazol-matulaxyl 3～6 parts, agricultural streptavidin 6～9
Part, blue or green withered clever 2～5 parts, octyl trichlamide 4～8 parts, remaining is water or tar；
Step 2: by Bravo, big raw, spray gram, safe and sound life, lime sulfur, RP-26019, Hymexazol-matulaxyl, agricultural streptavidin, blue or green withered
Spirit, octyl trichlamide smash into respectively last pours in graduated cylinder, adds deionized water, and described deionized water accounts for the 50% of gross weight, obtains
Mixed liquor；
Step 3: by dry Herba Asari, Rhizoma Curcumae Longae, Radix Sophorae Flavescentis, Radix Glycyrrhizae, Aconitum carmichjaelii Debx., sulfur, Colophonium, calcium oxide are pulverized, and cross 50 mesh sieves；
Step 4: the mixture extraction that step 3 is obtained, wherein the mixing speed in leaching process is 100～250r/min,
Extracting twice, each 1 hour, extraction temperature is 65～70 DEG C；
Step 5: product step 4 obtained filters；
Step 6: product that mixed liquor step 2 obtained and step 5 obtain adds in reactor, temperature at 50～90 DEG C,
Stir, then add water in proportion or add tar, stir 12～18 minutes, obtain reflecting liquid；
Step 7: under the conditions of 100～120 DEG C, reactant liquor is distilled, 125～130 DEG C, under the conditions of 0.05MPa, will reaction
Liquid carries out moist heat sterilization 15～25min, i.e. obtains bactericide；
Step 8: the stock solution of bactericide is diluted 100-150 times and can spray use.
The preparation method of a kind of bactericide the most according to claim 3, it is characterised in that: plant described in step 8
In solution after the stock solution dilution of antibacterial, water accounts for the 75%-85% of gross weight.
The preparation method of a kind of bactericide the most according to claim 3, it is characterised in that: the extraction described in step 4
Temperature is 68 DEG C.
The preparation method of a kind of bactericide the most according to claim 3, it is characterised in that: described step 4 extracts
Use lixiviating solution be volume ratio be the ethanol of 70%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610475752.2A CN106070396A (en) | 2016-06-27 | 2016-06-27 | A kind of bactericide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610475752.2A CN106070396A (en) | 2016-06-27 | 2016-06-27 | A kind of bactericide and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106070396A true CN106070396A (en) | 2016-11-09 |
Family
ID=57252882
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610475752.2A Withdrawn CN106070396A (en) | 2016-06-27 | 2016-06-27 | A kind of bactericide and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106070396A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106035430A (en) * | 2016-06-30 | 2016-10-26 | 安徽金培因科技有限公司 | Plant fungicide and preparation method thereof |
| WO2019019416A1 (en) * | 2017-07-28 | 2019-01-31 | 温妙云 | Medical fertilizer containing plant tissue extract and preparation method therefor |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002045512A2 (en) * | 2000-12-05 | 2002-06-13 | S.I.P.C.A.M. Societa' Italiana Prodotti Chimici E Per L'agricoltura Milano S.P.A. | Polyphosphate microbicide for pre- and postharvest crop protecion |
| CN105941513A (en) * | 2016-06-26 | 2016-09-21 | 合肥慧谷农业科技有限公司 | Plant bactericide and preparation method thereof |
| CN106070393A (en) * | 2016-06-15 | 2016-11-09 | 安徽菲扬农业科技有限公司 | A kind of bactericide and preparation method thereof |
| CN106106588A (en) * | 2016-06-25 | 2016-11-16 | 合肥隆扬农业科技有限公司 | A kind of bactericide and preparation method thereof |
-
2016
- 2016-06-27 CN CN201610475752.2A patent/CN106070396A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002045512A2 (en) * | 2000-12-05 | 2002-06-13 | S.I.P.C.A.M. Societa' Italiana Prodotti Chimici E Per L'agricoltura Milano S.P.A. | Polyphosphate microbicide for pre- and postharvest crop protecion |
| CN106070393A (en) * | 2016-06-15 | 2016-11-09 | 安徽菲扬农业科技有限公司 | A kind of bactericide and preparation method thereof |
| CN106106588A (en) * | 2016-06-25 | 2016-11-16 | 合肥隆扬农业科技有限公司 | A kind of bactericide and preparation method thereof |
| CN105941513A (en) * | 2016-06-26 | 2016-09-21 | 合肥慧谷农业科技有限公司 | Plant bactericide and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106035430A (en) * | 2016-06-30 | 2016-10-26 | 安徽金培因科技有限公司 | Plant fungicide and preparation method thereof |
| WO2019019416A1 (en) * | 2017-07-28 | 2019-01-31 | 温妙云 | Medical fertilizer containing plant tissue extract and preparation method therefor |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103265366B (en) | Seed dressing agent | |
| CN105941513A (en) | Plant bactericide and preparation method thereof | |
| CN102640765B (en) | Green and novel crop pest repellent | |
| CN106278756A (en) | One planting fruit-trees insect-prevention, increasing-production bio-feritlizer and preparation method thereof | |
| CN101744010B (en) | Botanical fungicide and the preparation method thereof | |
| CN103864512A (en) | Nanometer biological environment-friendly multifunctional organic bamboo vinegar medicine fertilizer | |
| CN106234431A (en) | A kind of multi-functional plant source bactericide is for preventing and treating the purposes of Folium Hibisci pinta | |
| CN106070393A (en) | A kind of bactericide and preparation method thereof | |
| CN106577891A (en) | Chinese herbal medicine preventing and controlling agent for crop root diseases and insect pests and preparation method thereof | |
| CN105994403A (en) | Medicaments for preventing and treating plant diseases and insect pests and application thereof | |
| CN106106588A (en) | A kind of bactericide and preparation method thereof | |
| CN106070396A (en) | A kind of bactericide and preparation method thereof | |
| CN105815353A (en) | Herbicide special for wheat and preparation method of herbicide | |
| CN103404543A (en) | Pear tree insect repellent agent and preparation and application methods of pear tree insect repellent agent | |
| CN107333795B (en) | Annual preventing and removing method for weeds in sugarcane orchard | |
| CN105794867A (en) | Compound botanical pesticide and preparing method thereof | |
| CN109258726A (en) | A kind of Pesticide with Chinese medicinal material and preparation method thereof | |
| CN104058900B (en) | A kind of no-tillage slowly-releasing purple willow special fertilizer and preparation method thereof | |
| CN101233866A (en) | Matrine agent plant pesticide special for killing cabbage worm and preparation thereof | |
| CN106035430A (en) | Plant fungicide and preparation method thereof | |
| CN106259527B (en) | A kind of formula of biological agent and preparation method thereof of Synthetical prevention peanut disease pest and weed | |
| CN105994441A (en) | Non-toxic pesticide synthetizing technology | |
| CN109953051A (en) | A kind of pure natural environment protection type plant deinsectization diseases prevention ferment and preparation method thereof | |
| CN103828830A (en) | Pesticide containing thiamethoxam and chlorothalonil and production process of pesticide | |
| CN106689224A (en) | Osmanthus tree disease and insect pest preventing and controlling pesticide |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20161109 |