CN105815353A - Herbicide special for wheat and preparation method of herbicide - Google Patents
Herbicide special for wheat and preparation method of herbicide Download PDFInfo
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- CN105815353A CN105815353A CN201610288287.1A CN201610288287A CN105815353A CN 105815353 A CN105815353 A CN 105815353A CN 201610288287 A CN201610288287 A CN 201610288287A CN 105815353 A CN105815353 A CN 105815353A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/20—N-Aryl derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/30—Derivatives containing the group >N—CO—N aryl or >N—CS—N—aryl
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/36—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/46—Stemonaceae [Stemona family], e.g. croomia
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Abstract
The invention discloses herbicide special for wheat and a preparation method of the herbicide. The herbicide is prepared from ethylene oxide, chlorimuron-methyl, metsulfuron-methyl, tribenuron-methyl, sodium polyacrylate, diuron, isopropyl N-(3-chlorophenyl)carbamate, fluazifop-butyl, fluorine cyanide, paraquat, kaolin, a surface active agent, fungicide, a herba leonuri extraction solution, a rhizoma pinelliae extraction solution, rhizoma atractylodis macrocephalae leach liquor, Chinese yam leach liquor, radix scrophulariae leach liquor, licorice root leach liquor, radix saposhnikoviae leach liquor, radix astragali leach liquor, radix bupleuri leach liquor, radix salviae miltiorrhizae leach liquor, rhizoma anemarrhenae leach liquor, carbonate, tripterygium wilfordii and radix stemonae. The raw materials are reasonable in matching and easy to obtain and are all harmless non-chemical components, the herbicide is pure natural and free of pollution, can prevent and treat various types of weeds, and is good in weeding effect, wide in weeding spectrum, free of harms to the environment and humans and suitable for being applied and popularized, cost is low, and thus the herbicide does not influence plantation of organic food and is good in absorption and convenient to use and popularize.
Description
Technical field
The present invention relates to preparation technique of pesticide field, specifically a kind of Semen Tritici aestivi herbicides special and preparation method thereof.
Background technology
Semen Tritici aestivi is a kind of very important cereal crops of China, Semen Tritici aestivi often suffers various Weed infestation from after planting to results, chemical agent is except the maximally effective means of wheat weeds, the herbicide of the management of weeds that wheat paddock is main is 2.4 d butyl esters, florasulam etc. at present, due to life-time service, resistance improves, cause dosage big, environmental pollution, also add peasant's dispenser cost, in order to solve above-mentioned drawback, the present invention have selected several has preventing and treating and the newtype drug composition of herbicidal effect, develops a kind of wheat field herbicide and preparation method thereof.
Summary of the invention
It is an object of the invention to provide and a kind of prepare simple, herbicidal effect is good Semen Tritici aestivi herbicides special and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
nullA kind of Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: oxirane 6-8 part、Chlorimuron-ethyl 4-6 part、Metsulfuron-methyl 3-5 part、Tribenuron-methyl 2-4 part、Sodium polyacrylate 6-8 part、Diuron 7-9 part、Chlorpropham 6-8 part、Fluazifop 8-10 part、Fluorine worm cyanogen 4-6 part、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 3-5 part、Kaolin 5-7 part、Surfactant 1-3 part、Antibacterial 1-2 part、Herba Leonuri extracting solution 13-17 part、Rhizoma Pinelliae extracting solution 10-14 part、Rhizoma Atractylodis Macrocephalae lixiviating solution 6-8 part、Rhizoma Dioscoreae lixiviating solution 6-8 part、Radix Scrophulariae lixiviating solution 6-10 part、Licorice extract 5-7 part、Radix Saposhnikoviae lixiviating solution 10-14 part、Radix Astragali lixiviating solution 6-10 part、Radix Bupleuri lixiviating solution 8-10 part、Radix Salviae Miltiorrhizae lixiviating solution 8-12 part、RHIZOMA ANEMARRHENAE with peet lixiviating solution 8-12 part、Carbonate 20-40 part、Radix Tripterygii Wilfordii 20-40 part、Radix Stemonae 30-50 part、Fructus Quisqualis 10-20 part、Rhizoma Gastrodiae 10-20 part、Semen Cuscutae 15-25 part、Radix Sophorae Flavescentis 15-25 part、Radix Saposhnikoviae 8-12 part、Folium Artemisiae Argyi 10-30 part、Chinaberry seeds 10-30 part、Semen Pharbitidis 20-40 part、Bulbus Allii 15-25 part、Pericarpium Zanthoxyli 15-25 part、Rhizoma Osmundae 15-35 part、Radix Astragali 20-30 part.
nullAs the further scheme of the present invention: described Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: oxirane 6.5-7.5 part、Chlorimuron-ethyl 4.5-5.5 part、Metsulfuron-methyl 3.5-4.5 part、Tribenuron-methyl 2.5-3.5 part、Sodium polyacrylate 6.5-7.5 part、Diuron 7.5-8.5 part、Chlorpropham 6.5-7.5 part、Fluazifop 8.5-9.5 part、Fluorine worm cyanogen 4.5-5.5 part、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 3.5-4.5 part、Kaolin 5.5-6.5 part、Surfactant 1.5-2.5 part、Antibacterial 1.2-1.8 part、Herba Leonuri extracting solution 14-16 part、Rhizoma Pinelliae extracting solution 11-13 part、Rhizoma Atractylodis Macrocephalae lixiviating solution 6.5-7.5 part、Rhizoma Dioscoreae lixiviating solution 6.5-7.5 part、Radix Scrophulariae lixiviating solution 7-9 part、Licorice extract 5.5-6.5 part、Radix Saposhnikoviae lixiviating solution 11-13 part、Radix Astragali lixiviating solution 7-9 part、Radix Bupleuri lixiviating solution 8.5-9.5 part、Radix Salviae Miltiorrhizae lixiviating solution 9-11 part、RHIZOMA ANEMARRHENAE with peet lixiviating solution 9-11 part、Carbonate 25-35 part、Radix Tripterygii Wilfordii 25-35 part、Radix Stemonae 35-45 part、Fructus Quisqualis 12-18 part、Rhizoma Gastrodiae 12-18 part、Semen Cuscutae 18-22 part、Radix Sophorae Flavescentis 18-22 part、Radix Saposhnikoviae 9-11 part、Folium Artemisiae Argyi 15-25 part、Chinaberry seeds 15-25 part、Semen Pharbitidis 25-35 part、Bulbus Allii 18-22 part、Pericarpium Zanthoxyli 18-22 part、Rhizoma Osmundae 18-22 part、Radix Astragali 22-28 part.
nullAs the present invention further scheme: described Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: 7 parts of oxirane、Chlorimuron-ethyl 5 parts、Metsulfuron-methyl 4 parts、Tribenuron-methyl 3 parts、Sodium polyacrylate 7 parts、Diuron 8 parts、Chlorpropham 7 parts、Fluazifop 9 parts、5 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 4 parts、Kaolin 6 parts、2 parts of surfactant、Antibacterial 1.5 parts、Herba Leonuri extracting solution 15 parts、Rhizoma Pinelliae extracting solution 12 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 7 parts、Rhizoma Dioscoreae lixiviating solution 7 parts、Radix Scrophulariae lixiviating solution 8 parts、Licorice extract 6 parts、Radix Saposhnikoviae lixiviating solution 12 parts、Radix Astragali lixiviating solution 8 parts、Radix Bupleuri lixiviating solution 9 parts、Radix Salviae Miltiorrhizae lixiviating solution 10 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 10 parts、30 parts of carbonate、Radix Tripterygii Wilfordii 30 parts、The Radix Stemonae 40 parts、Fructus Quisqualis 15 parts、15 parts of Rhizoma Gastrodiae、Semen Cuscutae 20 parts、Radix Sophorae Flavescentis 20 parts、Radix Saposhnikoviae 10 parts、Folium Artemisiae Argyi 20 parts、Chinaberry seeds 20 parts、Semen Pharbitidis 30 parts、20 parts of Bulbus Allii、20 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 20 parts、The Radix Astragali 25 parts.
The preparation method of described Semen Tritici aestivi herbicides special, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion;
(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 10-14 times, decoct 3-5h, filter, obtain filtrate;
(3) filtrate is concentrated into the 0.5-0.7% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 75-85%, reflux, extract, 20-40min;
(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;
(5) adding in agitator to the product of step (4) and the water of 15-25 part, control rotating speed is 200-400r/min, and mechanical agitation 30-50min adds sodium polyacrylate while stirring;
(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 20-30min obtains admixing medical solutions;
(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
Compared with prior art, the invention has the beneficial effects as follows:
Reasonable raw material proportioning of the present invention, with low cost, raw material is easy to get, and raw material is non-harmful non-chemically composition, pure natural is pollution-free, can prevent and treat multiple weeds, herbicidal effect is good, weeding is general extensively, is all safe from harm environment and the mankind, be suitable to popularization and application, therefore the plantation on Organic food does not has any impact, good absorbing, it is simple to promotes and uses.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the technical scheme of this patent is described in more detail.
Embodiment 1
nullA kind of Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: 6 parts of oxirane、Chlorimuron-ethyl 4 parts、Metsulfuron-methyl 3 parts、Tribenuron-methyl 2 parts、Sodium polyacrylate 6 parts、Diuron 7 parts、Chlorpropham 6 parts、Fluazifop 8 parts、4 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 3 parts、Kaolin 5 parts、1 part of surfactant、Antibacterial 1 part、Herba Leonuri extracting solution 13 parts、Rhizoma Pinelliae extracting solution 10 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 6 parts、Rhizoma Dioscoreae lixiviating solution 6 parts、Radix Scrophulariae lixiviating solution 6 parts、Licorice extract 5 parts、Radix Saposhnikoviae lixiviating solution 10 parts、Radix Astragali lixiviating solution 6 parts、Radix Bupleuri lixiviating solution 8 parts、Radix Salviae Miltiorrhizae lixiviating solution 8 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 8 parts、20 parts of carbonate、Radix Tripterygii Wilfordii 20 parts、The Radix Stemonae 30 parts、Fructus Quisqualis 10 parts、10 parts of Rhizoma Gastrodiae、Semen Cuscutae 15 parts、Radix Sophorae Flavescentis 15 parts、Radix Saposhnikoviae 8 parts、Folium Artemisiae Argyi 10 parts、Chinaberry seeds 10 parts、Semen Pharbitidis 20 parts、15 parts of Bulbus Allii、15 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 15 parts、The Radix Astragali 20 parts.
The preparation method of described Semen Tritici aestivi herbicides special, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion;
(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 10 times, decoct 3h, filter, obtain filtrate;
(3) filtrate is concentrated into the 0.5% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 75%, reflux, extract, 20min;
(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;
(5) adding in agitator to the product of step (4) and the water of 15 parts, control rotating speed is 200r/min, and mechanical agitation 30min adds sodium polyacrylate while stirring;
(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 20min obtains admixing medical solutions;
(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
Embodiment 2
nullA kind of Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: 6.5 parts of oxirane、Chlorimuron-ethyl 4.5 parts、Metsulfuron-methyl 3.5 parts、Tribenuron-methyl 2.5 parts、Sodium polyacrylate 6.5 parts、Diuron 7.5 parts、Chlorpropham 6.5 parts、Fluazifop 8.5 parts、4.5 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 3.5 parts、Kaolin 5.5 parts、1.5 parts of surfactant、Antibacterial 1.2 parts、Herba Leonuri extracting solution 14 parts、Rhizoma Pinelliae extracting solution 11 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 6.5 parts、Rhizoma Dioscoreae lixiviating solution 6.5 parts、Radix Scrophulariae lixiviating solution 7 parts、Licorice extract 5.5 parts、Radix Saposhnikoviae lixiviating solution 11 parts、Radix Astragali lixiviating solution 7 parts、Radix Bupleuri lixiviating solution 8.5 parts、Radix Salviae Miltiorrhizae lixiviating solution 9 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 9 parts、25 parts of carbonate、Radix Tripterygii Wilfordii 25 parts、The Radix Stemonae 35 parts、Fructus Quisqualis 12 parts、12 parts of Rhizoma Gastrodiae、Semen Cuscutae 18 parts、Radix Sophorae Flavescentis 18 parts、Radix Saposhnikoviae 9 parts、Folium Artemisiae Argyi 15 parts、Chinaberry seeds 15 parts、Semen Pharbitidis 25 parts、18 parts of Bulbus Allii、18 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 18 parts、The Radix Astragali 22 parts.
The preparation method of described Semen Tritici aestivi herbicides special, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion;
(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 11 times, decoct 3.5h, filter, obtain filtrate;
(3) filtrate is concentrated into the 0.55% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 78%, reflux, extract, 25min;
(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;
(5) adding in agitator to the product of step (4) and the water of 18 parts, control rotating speed is 250r/min, and mechanical agitation 35min adds sodium polyacrylate while stirring;
(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 22min obtains admixing medical solutions;
(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
Embodiment 3
nullA kind of Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: 7 parts of oxirane、Chlorimuron-ethyl 5 parts、Metsulfuron-methyl 4 parts、Tribenuron-methyl 3 parts、Sodium polyacrylate 7 parts、Diuron 8 parts、Chlorpropham 7 parts、Fluazifop 9 parts、5 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 4 parts、Kaolin 6 parts、2 parts of surfactant、Antibacterial 1.5 parts、Herba Leonuri extracting solution 15 parts、Rhizoma Pinelliae extracting solution 12 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 7 parts、Rhizoma Dioscoreae lixiviating solution 7 parts、Radix Scrophulariae lixiviating solution 8 parts、Licorice extract 6 parts、Radix Saposhnikoviae lixiviating solution 12 parts、Radix Astragali lixiviating solution 8 parts、Radix Bupleuri lixiviating solution 9 parts、Radix Salviae Miltiorrhizae lixiviating solution 10 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 10 parts、30 parts of carbonate、Radix Tripterygii Wilfordii 30 parts、The Radix Stemonae 40 parts、Fructus Quisqualis 15 parts、15 parts of Rhizoma Gastrodiae、Semen Cuscutae 20 parts、Radix Sophorae Flavescentis 20 parts、Radix Saposhnikoviae 10 parts、Folium Artemisiae Argyi 20 parts、Chinaberry seeds 20 parts、Semen Pharbitidis 30 parts、20 parts of Bulbus Allii、20 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 20 parts、The Radix Astragali 25 parts.
The preparation method of described Semen Tritici aestivi herbicides special, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion;
(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 12 times, decoct 4h, filter, obtain filtrate;
(3) filtrate is concentrated into the 0.6% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 80%, reflux, extract, 30min;
(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;
(5) adding in agitator to the product of step (4) and the water of 20 parts, control rotating speed is 300r/min, and mechanical agitation 40min adds sodium polyacrylate while stirring;
(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 25min obtains admixing medical solutions;
(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
Embodiment 4
nullA kind of Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: 7.5 parts of oxirane、Chlorimuron-ethyl 5.5 parts、Metsulfuron-methyl 4.5 parts、Tribenuron-methyl 3.5 parts、Sodium polyacrylate 7.5 parts、Diuron 8.5 parts、Chlorpropham 7.5 parts、Fluazifop 9.5 parts、5.5 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 4.5 parts、Kaolin 6.5 parts、2.5 parts of surfactant、Antibacterial 1.8 parts、Herba Leonuri extracting solution 16 parts、Rhizoma Pinelliae extracting solution 13 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 7.5 parts、Rhizoma Dioscoreae lixiviating solution 7.5 parts、Radix Scrophulariae lixiviating solution 9 parts、Licorice extract 6.5 parts、Radix Saposhnikoviae lixiviating solution 13 parts、Radix Astragali lixiviating solution 9 parts、Radix Bupleuri lixiviating solution 9.5 parts、Radix Salviae Miltiorrhizae lixiviating solution 11 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 11 parts、35 parts of carbonate、Radix Tripterygii Wilfordii 35 parts、The Radix Stemonae 45 parts、Fructus Quisqualis 18 parts、18 parts of Rhizoma Gastrodiae、Semen Cuscutae 22 parts、Radix Sophorae Flavescentis 22 parts、Radix Saposhnikoviae 11 parts、Folium Artemisiae Argyi 25 parts、Chinaberry seeds 25 parts、Semen Pharbitidis 35 parts、22 parts of Bulbus Allii、22 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 22 parts、The Radix Astragali 28 parts.
The preparation method of described Semen Tritici aestivi herbicides special, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion;
(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 13 times, decoct 4.5h, filter, obtain filtrate;
(3) filtrate is concentrated into the 0.65% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 82%, reflux, extract, 35min;
(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;
(5) adding in agitator to the product of step (4) and the water of 22 parts, control rotating speed is 350r/min, and mechanical agitation 45min adds sodium polyacrylate while stirring;
(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 28min obtains admixing medical solutions;
(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
Embodiment 5
nullA kind of Semen Tritici aestivi herbicides special,Include according to the raw material of weight portion: 8 parts of oxirane、Chlorimuron-ethyl 6 parts、Metsulfuron-methyl 5 parts、Tribenuron-methyl 4 parts、Sodium polyacrylate 8 parts、Diuron 9 parts、Chlorpropham 8 parts、Fluazifop 10 parts、6 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 5 parts、Kaolin 7 parts、3 parts of surfactant、Antibacterial 2 parts、Herba Leonuri extracting solution 17 parts、Rhizoma Pinelliae extracting solution 14 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 8 parts、Rhizoma Dioscoreae lixiviating solution 8 parts、Radix Scrophulariae lixiviating solution 10 parts、Licorice extract 7 parts、Radix Saposhnikoviae lixiviating solution 14 parts、Radix Astragali lixiviating solution 10 parts、Radix Bupleuri lixiviating solution 10 parts、Radix Salviae Miltiorrhizae lixiviating solution 12 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 12 parts、40 parts of carbonate、Radix Tripterygii Wilfordii 40 parts、The Radix Stemonae 50 parts、Fructus Quisqualis 20 parts、20 parts of Rhizoma Gastrodiae、Semen Cuscutae 25 parts、Radix Sophorae Flavescentis 25 parts、Radix Saposhnikoviae 12 parts、Folium Artemisiae Argyi 30 parts、Chinaberry seeds 30 parts、Semen Pharbitidis 40 parts、25 parts of Bulbus Allii、25 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 35 parts、The Radix Astragali 30 parts.
The preparation method of described Semen Tritici aestivi herbicides special, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion;
(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 14 times, decoct 5h, filter, obtain filtrate;
(3) filtrate is concentrated into the 0.7% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 85%, reflux, extract, 40min;
(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;
(5) adding in agitator to the product of step (4) and the water of 25 parts, control rotating speed is 400r/min, and mechanical agitation 50min adds sodium polyacrylate while stirring;
(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 30min obtains admixing medical solutions;
(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
Reasonable raw material proportioning of the present invention, with low cost, raw material is easy to get, and raw material is non-harmful non-chemically composition, pure natural is pollution-free, can prevent and treat multiple weeds, herbicidal effect is good, weeding is general extensively, is all safe from harm environment and the mankind, be suitable to popularization and application, therefore the plantation on Organic food does not has any impact, good absorbing, it is simple to promotes and uses.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art is possessed, it is also possible to various changes can be made on the premise of without departing from this patent objective.
Claims (4)
- null1. a Semen Tritici aestivi herbicides special,It is characterized in that,Include according to the raw material of weight portion: oxirane 6-8 part、Chlorimuron-ethyl 4-6 part、Metsulfuron-methyl 3-5 part、Tribenuron-methyl 2-4 part、Sodium polyacrylate 6-8 part、Diuron 7-9 part、Chlorpropham 6-8 part、Fluazifop 8-10 part、Fluorine worm cyanogen 4-6 part、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 3-5 part、Kaolin 5-7 part、Surfactant 1-3 part、Antibacterial 1-2 part、Herba Leonuri extracting solution 13-17 part、Rhizoma Pinelliae extracting solution 10-14 part、Rhizoma Atractylodis Macrocephalae lixiviating solution 6-8 part、Rhizoma Dioscoreae lixiviating solution 6-8 part、Radix Scrophulariae lixiviating solution 6-10 part、Licorice extract 5-7 part、Radix Saposhnikoviae lixiviating solution 10-14 part、Radix Astragali lixiviating solution 6-10 part、Radix Bupleuri lixiviating solution 8-10 part、Radix Salviae Miltiorrhizae lixiviating solution 8-12 part、RHIZOMA ANEMARRHENAE with peet lixiviating solution 8-12 part、Carbonate 20-40 part、Radix Tripterygii Wilfordii 20-40 part、Radix Stemonae 30-50 part、Fructus Quisqualis 10-20 part、Rhizoma Gastrodiae 10-20 part、Semen Cuscutae 15-25 part、Radix Sophorae Flavescentis 15-25 part、Radix Saposhnikoviae 8-12 part、Folium Artemisiae Argyi 10-30 part、Chinaberry seeds 10-30 part、Semen Pharbitidis 20-40 part、Bulbus Allii 15-25 part、Pericarpium Zanthoxyli 15-25 part、Rhizoma Osmundae 15-35 part、Radix Astragali 20-30 part.
- nullSemen Tritici aestivi herbicides special the most according to claim 1,It is characterized in that,Include according to the raw material of weight portion: oxirane 6.5-7.5 part、Chlorimuron-ethyl 4.5-5.5 part、Metsulfuron-methyl 3.5-4.5 part、Tribenuron-methyl 2.5-3.5 part、Sodium polyacrylate 6.5-7.5 part、Diuron 7.5-8.5 part、Chlorpropham 6.5-7.5 part、Fluazifop 8.5-9.5 part、Fluorine worm cyanogen 4.5-5.5 part、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 3.5-4.5 part、Kaolin 5.5-6.5 part、Surfactant 1.5-2.5 part、Antibacterial 1.2-1.8 part、Herba Leonuri extracting solution 14-16 part、Rhizoma Pinelliae extracting solution 11-13 part、Rhizoma Atractylodis Macrocephalae lixiviating solution 6.5-7.5 part、Rhizoma Dioscoreae lixiviating solution 6.5-7.5 part、Radix Scrophulariae lixiviating solution 7-9 part、Licorice extract 5.5-6.5 part、Radix Saposhnikoviae lixiviating solution 11-13 part、Radix Astragali lixiviating solution 7-9 part、Radix Bupleuri lixiviating solution 8.5-9.5 part、Radix Salviae Miltiorrhizae lixiviating solution 9-11 part、RHIZOMA ANEMARRHENAE with peet lixiviating solution 9-11 part、Carbonate 25-35 part、Radix Tripterygii Wilfordii 25-35 part、Radix Stemonae 35-45 part、Fructus Quisqualis 12-18 part、Rhizoma Gastrodiae 12-18 part、Semen Cuscutae 18-22 part、Radix Sophorae Flavescentis 18-22 part、Radix Saposhnikoviae 9-11 part、Folium Artemisiae Argyi 15-25 part、Chinaberry seeds 15-25 part、Semen Pharbitidis 25-35 part、Bulbus Allii 18-22 part、Pericarpium Zanthoxyli 18-22 part、Rhizoma Osmundae 18-22 part、Radix Astragali 22-28 part.
- nullSemen Tritici aestivi herbicides special the most according to claim 1,It is characterized in that,Include according to the raw material of weight portion: 7 parts of oxirane、Chlorimuron-ethyl 5 parts、Metsulfuron-methyl 4 parts、Tribenuron-methyl 3 parts、Sodium polyacrylate 7 parts、Diuron 8 parts、Chlorpropham 7 parts、Fluazifop 9 parts、5 parts of fluorine worm cyanogen、N,N'-dimethyl-.gamma..gamma.'-dipyridylium 4 parts、Kaolin 6 parts、2 parts of surfactant、Antibacterial 1.5 parts、Herba Leonuri extracting solution 15 parts、Rhizoma Pinelliae extracting solution 12 parts、Rhizoma Atractylodis Macrocephalae lixiviating solution 7 parts、Rhizoma Dioscoreae lixiviating solution 7 parts、Radix Scrophulariae lixiviating solution 8 parts、Licorice extract 6 parts、Radix Saposhnikoviae lixiviating solution 12 parts、Radix Astragali lixiviating solution 8 parts、Radix Bupleuri lixiviating solution 9 parts、Radix Salviae Miltiorrhizae lixiviating solution 10 parts、RHIZOMA ANEMARRHENAE with peet lixiviating solution 10 parts、30 parts of carbonate、Radix Tripterygii Wilfordii 30 parts、The Radix Stemonae 40 parts、Fructus Quisqualis 15 parts、15 parts of Rhizoma Gastrodiae、Semen Cuscutae 20 parts、Radix Sophorae Flavescentis 20 parts、Radix Saposhnikoviae 10 parts、Folium Artemisiae Argyi 20 parts、Chinaberry seeds 20 parts、Semen Pharbitidis 30 parts、20 parts of Bulbus Allii、20 parts of Pericarpium Zanthoxyli、Rhizoma Osmundae 20 parts、The Radix Astragali 25 parts.
- 4. the preparation method of the Semen Tritici aestivi herbicides special as described in claim 1-3 is arbitrary, it is characterised in that specifically comprise the following steps that(1) each raw material is weighed according to weight portion;(2) by Radix Tripterygii Wilfordii, the Radix Stemonae, Fructus Quisqualis, Rhizoma Gastrodiae, Semen Cuscutae, Radix Sophorae Flavescentis, Radix Saposhnikoviae, Folium Artemisiae Argyi, chinaberry seeds, Semen Pharbitidis, Bulbus Allii, Pericarpium Zanthoxyli, Rhizoma Osmundae and Radix Astragali mix homogeneously, add the water of Chinese medicinal components gross weight 10-14 times, decoct 3-5h, filter, obtain filtrate;(3) filtrate is concentrated into the 0.5-0.7% of original volume, obtains concentration, and adding concentration in concentrated solution is the ethanol extract of 75-85%, reflux, extract, 20-40min;(4) oxirane, chlorimuron-ethyl, metsulfuron-methyl, tribenuron-methyl, diuron, chlorpropham, fluazifop, fluorine worm cyanogen and N,N'-dimethyl-.gamma..gamma.'-dipyridylium are mixed, add surfactant, mix homogeneously;(5) adding in agitator to the product of step (4) and the water of 15-25 part, control rotating speed is 200-400r/min, and mechanical agitation 30-50min adds sodium polyacrylate while stirring;(6) product Herba Leonuri extracting solution, Rhizoma Pinelliae extracting solution, Rhizoma Atractylodis Macrocephalae lixiviating solution, Rhizoma Dioscoreae lixiviating solution, Radix Scrophulariae lixiviating solution, licorice extract, Radix Saposhnikoviae lixiviating solution, Radix Astragali lixiviating solution, Radix Bupleuri lixiviating solution, Radix Salviae Miltiorrhizae lixiviating solution, RHIZOMA ANEMARRHENAE with peet lixiviating solution and step (3) obtained adds and all adds to agitator, adding Kaolin and antibacterial, stirring 20-30min obtains admixing medical solutions;(7) carbonate is carried out pulverizing, be sprinkled into uniformly in above-mentioned admixing medical solutions, after stirring, obtain finished product.
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