CN106039266A - Ginger tea electuary and preparation method thereof - Google Patents

Ginger tea electuary and preparation method thereof Download PDF

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Publication number
CN106039266A
CN106039266A CN201610559082.2A CN201610559082A CN106039266A CN 106039266 A CN106039266 A CN 106039266A CN 201610559082 A CN201610559082 A CN 201610559082A CN 106039266 A CN106039266 A CN 106039266A
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Prior art keywords
ginger tea
weight portion
filtering residue
filtrate
rhizoma atractylodis
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Inventor
缪剑华
周小雷
王硕
莫单丹
唐炳兰
龚小妹
候小莉
欧春丽
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Guangxi Botanical Garden of Medicinal Plants
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Guangxi Botanical Garden of Medicinal Plants
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    • A—HUMAN NECESSITIES
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    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/906—Zingiberaceae (Ginger family)
    • A61K36/9068—Zingiber, e.g. garden ginger
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    • A61K36/185—Magnoliopsida (dicotyledons)
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    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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    • A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
    • A61K9/1605—Excipients; Inactive ingredients
    • A61K9/1617—Organic compounds, e.g. phospholipids, fats
    • A61K9/1623—Sugars or sugar alcohols, e.g. lactose; Derivatives thereof; Homeopathic globules
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Abstract

The invention discloses ginger tea electuary and a preparation method thereof. The ginger tea electuary is prepared from the following raw materials: zingiber mioga (Thunb.) rosc., rhizoma atractylodis macrocephalae preparata, rhizoma atractylodis, radix saposhnikoviae, pericarpium citri reticulatae, radix glycyrrhizae, bulbus allii fistulosi, fructus lycii, plumula nelumbinis, grape seeds, rhizoma dioscoreae, chrysanthemum morifolium ramat, herba menthae, fructus jujubae, an inclusion agent, brown sugar, nigecose, dextrin, a plasticizer and an adsorbent. pungent and hot zingiber mioga (Thunb.) rosc. is used as monarch drug of the ginger tea electuary, rhizoma atractylodis macrocephalae which has effects of strengthening the spleen and drying damp is used as ministerial drug, rhizoma atractylodis and radix saposhnikoviae which have effects of expelling wind and removing dampness are used as adjuvant drug, pericarpium citri reticulatae which has effect of eliminating dampness by warm and can invigorate the spleen and promoting circulation of qi is also used as adjuvant drug, radix glycyrrhizae, bulbus allii fistulosi, fructus lycii, plumula nelumbinis, grape seeds, rhizoma dioscoreae, chrysanthemum morifolium ramat, herba menthae, fructus jujubae and the like are used as auxiliary materials, in a preparation method, combined action of a supercritical CO2 extraction method and ethanol extraction is implemented, and effective ingredients of main materials and the auxiliary materials are fully utilized to carry out comprehensive regulation. The ginger tea electuary has effects of benefiting vital qi and blood, strengthening the spleen to dry, and expelling pathogenic wind and relieving pain to treat emesis and singultus, abdominal pain and gastric abscess, loose stool and greasy fur, and limb joint pain which are caused by attack of pathogenic cold, eating and drinking without temperance and weakness of the spleen and stomach.

Description

Ginger tea granules and preparation method thereof
Technical field
The present invention relates to a kind of ginger tea granules and preparation method thereof.It is more particularly related to one comprises compound recipe Ginger tea granules of volatile oil and preparation method thereof.
Background technology
Integrate in nutrition, seasoning, the Rhizoma Zingiberis Recens that keeps healthy containing pungent and fragrant composition, possibly together with protein, starch, many Sugar, vitamin and various trace elements, wherein, piquancy component includes pungency component gingerol, oily pungency component zingiberene, crystallization Property pungency component (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, gingerol has a stimulation to oral cavity stomach function regulating mucosa, can the secretion of facilitating digestion liquid, appetite stimulator, can Make intestinal tension force, the rhythm and pace of moving things and wriggling increase, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone to breathing and vasomotor center has excitation, can blood circulation promoting, Promoting that adipose cell increases, adipose cell can suck the dextrose components in blood and then alleviate blood glucose rising；Fragrance ingredient master Will be from volatile oil, it includes zingiberol, zingiberene, camphene, Herba Limnophilae rugosae alkene, Borneolum Syntheticum, citral and press olein etc., have induce sweat scattered Cold, warming middle-JIAO to arrest vomiting, preventing phlegm from forming and stopping coughing, effect of removing toxic substances.Therefore Rhizoma Zingiberis Recens is extensive by everybody as the interpolation of flavoring agent and Traditional Chinese medicinal prescription Generally acknowledge.Fiery Rhizoma Zingiberis Recens in Rhizoma Zingiberis Recens contains strong volatile oil and gingerol because of it, and is suitable for and is fabricated to roasting Rhizoma Zingiberis Recens to remain fresh ginger former Taste, it is easy to preservation and transport and be widely used.
Traditional ginger tea granules such as Fructus Jujubae ginger decoction, brown sugar ginger decoction, green tea ginger decoction etc. be take shredded ginger raw material mix adjuvant punching Bubble or decoct prepared, not only operation inconvenience and also contained volatile oil can not be embodied in Rhizoma Zingiberis Recens completely, gingerol, the work of (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone etc. By, the unicity of adjuvant, can not omnibearing comprehensively regulating, therefore take preparation and be dried the ginger tea mouthfeel difference or effect prepared The poorest, and the medicinal effects of Rhizoma Zingiberis Recens can not be played very well.
Summary of the invention
It is an object of the invention to solve at least the above, and the advantage that at least will be described later is provided.
It is a still further object of the present invention to provide a kind of ginger tea granules and preparation method thereof, it is with hot fire Rhizoma Zingiberis Recens as monarch, Rhizoma Atractylodis Macrocephalae the spleen strengthening and damp drying is ministerial drug, and Rhizoma Atractylodis, Radix Saposhnikoviae expelling wind and removing dampness are adjuvant drug, and Pericarpium Citri Reticulatae warm-dryness syndrome is wet and energy spleen invigorating circulation of qi promoting be adjuvant drug, and joins With adjuvants such as Radix Glycyrrhizae, Bulbus Allii Fistulosi, Fructus Lycii, Plumula Nelumbinis, Semen Vitis viniferae, Rhizoma Dioscoreae, Flos Chrysanthemi, Herba Menthae, Fructus Jujubaes, preparation process uses supercritical CO2Extraction acts on jointly with ethanol extraction, sufficiently make use of the effective ingredient of described major ingredient and adjuvant to carry out comprehensively regulating, Having benefiting vital QI and blood, the spleen strengthening and damp drying wind-expelling pain-stopping is with treatment because experiencing cold-evil, and eating and drinking without temperance, the vomiting that weakness of the spleen and stomach causes is oh Inverse, stomachache gastric abscess, loose stool greasy fur, extremities joint pain.
In order to realize according to object of the present invention and further advantage, it is provided that a kind of ginger tea granules, including following heavy The raw material of amount part: fire Rhizoma Zingiberis Recens 100-130 part, Rhizoma Atractylodis Macrocephalae (parched) 40-50 part, Rhizoma Atractylodis 30-35 part, Radix Saposhnikoviae 30-35 part, Pericarpium Citri Reticulatae 25-30 part, sweet Grass 15-20 part, Bulbus Allii Fistulosi 30-35 part, Fructus Lycii 10-15 part, Plumula Nelumbinis 35-40 part, Semen Vitis viniferae 40-45 part, Rhizoma Dioscoreae 15-25 part, Hangzhoupro Flos Chrysanthemi 20-25 part, Herba Menthae 5-10 part, Fructus Jujubae 60-70 part, inclusion agents 25-30 part, brown sugar 40-45 part, nigecose 40-45 part, dextrin 20-30 part, plasticizer 10-15 part and adsorbent 5-10 part.
Preferably, described inclusion agents is second group-beta-cyclodextrin.
Preferably, described plasticizer be mass ratio be the arabic gum of 10:3:1:1:1, locust bean gum, sucrose, Fructus Vitis viniferae Calciofon and potassium chloride.
Preferably, described adsorbent is Magnesiumaluminumsilicate.
Present invention also offers the preparation method of a kind of ginger tea granules, comprise the following steps:
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 100-130 part, Rhizoma Atractylodis Macrocephalae (parched) 40-50 part, Rhizoma Atractylodis 30-35 part, Radix Saposhnikoviae 30-35 Part and the mixing of Pericarpium Citri Reticulatae 25-30 part are sent into after pulverizer is pulverized and are joined in extractor, when temperature reaches 55-60 DEG C, open Dynamic high-pressure pump, when pressure reaches 25-30MPa, discharges pressure and carries out dynamic extraction, dynamic extraction work after static extracting 30-40min Skill parameter is: when temperature is heated to 40-50 DEG C, pressurize system, after pressure reaches 30-35MPa, regulates CO2Flow For 3-6L/h, after keeping constant temperature and pressure to be circulated extraction 3-4h, 40-60 mesh double-layer nylon sock filtration, prepare compound recipe volatilization Oil and the first filtering residue；
Component meter the most by weight, by Radix Glycyrrhizae 15-20 part, Bulbus Allii Fistulosi 30-35 part, Fructus Lycii 10-15 part, Plumula Nelumbinis 35-40 part, Semen Vitis viniferae 40-45 part, Rhizoma Dioscoreae 15-25 part, Flos Chrysanthemi 20-25 part, Herba Menthae 5-10 part and the mixing of Fructus Jujubae 60-70 part, obtain first Mixture, after being pulverized by the first mixture feeding pulverizer, adds the 65%-75% ethanol of the first mixture 7-9 times amount It is sealed in container with lid immersion 8-12h after stirring 5-8min, filters, obtain the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the second filtering residue quality summation 7-9 times amount are added 65%-75% ethanol extraction 2-2.5h, filters, obtains the second filtrate and the 3rd filtering residue, will add its 7-9 times amount in the 3rd filtering residue 65%-75% ethanol extraction 1-1.5h, filters, takes the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate are mixed, The clear paste that relative density is 1.30-1.33 it is concentrated at 50-60 DEG C；
S4. 25-30 weight portion second group-beta-cyclodextrin is weighed, while adding water and be stirred continuously and make it dissolve prepared second Group-beta-cyclodextrin saturated solution, after compound volatile oil is dissolved in ethanol solution by 2-4:1, is added dropwise to described ethyl-β-ring In dextrin saturated solution and be stirred continuously, regulating pH value at 20-25 DEG C is 5-6, after ultrasonic agitation 2-3h, after cold preservation 18-24h Precipitation filters, and takes solid particle, 35-45 DEG C of hot-air seasoning, obtains volatile oil clathrate compound；
S5. 40-45 weight portion brown sugar, 40-45 weight portion nigecose and 20-30 weight portion dextrin heating for dissolving are processed After mixed crystal be milled to powder, the mass ratio adding 10-15 weight portion is the arabic gum of 10:3:1:1:1, locust bean gum The clear paste that glue, sucrose, calcium gluconate, potassium chloride, 5-10 weight portion Magnesiumaluminumsilicate, and S3 obtain is placed in granulation machine mixed Even and after making granule, and subpackage after the volatile oil clathrate compound mix homogeneously that obtains of S4, obtain ginger tea granules.
Preferably, regulating the solvent of pH in step S4 is one or both in sodium bicarbonate, citric acid and malic acid.
Preferably, it is by 40-45 weight portion brown sugar that step S5 produces the method for described mixed crystal, is heated to 120- 130 DEG C and after being stirred continuously and making it be dissolved into liquid, increase temperature to 140-150 DEG C, the most persistently after 15-18 minute Add 40-45 weight portion nigecose, 20-30 weight portion dextrin continues stirring to becoming thick rear crystallisation by cooling.
The present invention at least includes following beneficial effect:
The first, the ginger tea granules of the present invention is with hot fire Rhizoma Zingiberis Recens as monarch, and Rhizoma Atractylodis Macrocephalae the spleen strengthening and damp drying is ministerial drug, and Rhizoma Atractylodis, Radix Saposhnikoviae are dispelled Wind dehumidifying is for adjuvant drug, and Pericarpium Citri Reticulatae warm-dryness syndrome is wet and can spleen invigorating circulation of qi promoting be adjuvant drug, and be equipped with Radix Glycyrrhizae, Bulbus Allii Fistulosi, Fructus Lycii, Plumula Nelumbinis, Semen Vitis viniferae, The adjuvants such as Rhizoma Dioscoreae, Flos Chrysanthemi, Herba Menthae, Fructus Jujubae, have benefiting vital QI and blood, and the spleen strengthening and damp drying wind-expelling pain-stopping, is drunk because experiencing cold-evil with treatment Food does not saves, and the vomiting singultus that weakness of the spleen and stomach causes, suffer from abdominal pain gastric abscess, extremities joint pain, retention of dampness in middle-JIAO, gastral cavity abdominal distention are vexed, loose stool Greasy fur.
The second, on the one hand the preparation method of the ginger tea granules of the present invention uses supercritical CO2Extraction is white to fire Rhizoma Zingiberis Recens, stir-fry The derived essential oil of art, Rhizoma Atractylodis, Radix Saposhnikoviae and Pericarpium Citri Reticulatae extracts, and by inclusion technique, prepared compound volatile oil is carried out inclusion Compound volatile oil clathrate, on the other hand by ethanol extraction fire Rhizoma Zingiberis Recens, Rhizoma Atractylodis Macrocephalae (parched), Rhizoma Atractylodis, Radix Saposhnikoviae, Pericarpium Citri Reticulatae, Radix Glycyrrhizae, Bulbus Allii Fistulosi, Active ingredient in Fructus Lycii, Plumula Nelumbinis, Semen Vitis viniferae, Rhizoma Dioscoreae, Flos Chrysanthemi, Herba Menthae, Fructus Jujubae, with above-mentioned compound volatile oil bag after granulation Pack after compound mix homogeneously, embody contained volatile oil in fire Rhizoma Zingiberis Recens completely, gingerol, the effect of (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone etc., sufficiently profit Comprehensively regulating is carried out with the effective ingredient of described major ingredient and adjuvant.
3rd, plasticizer described in the ginger tea granules of the present invention be mass ratio be the arabic gum of 10:3:1:1:1, Robinia pseudoacacia L. Locust beam gum, sucrose, calcium gluconate and potassium chloride, described arabic gum has stronger adhesion strength and soft elasticity, passes through Adding locust bean gum, make the more high resilience of described arabic gum and toughness, the interpolation of sucrose adds the saturating of described arabic gum The interpolation of lightness, calcium gluconate and potassium chloride promotes it to shrink while increasing described arabic gum intensity and tends to crisp Property, by rational proportioning so that clear paste more easy-formation during pelletizing, and there is certain transparency.
4th, described in the ginger tea granules of the present invention, adsorbent is Magnesiumaluminumsilicate, and it adsorbs in ginger tea granules effectively Moisture, while extending the ginger tea granules shelf-life, it is possible to makes ginger tea granules product obtain optimal color and luster, tissue exquisiteness.
5th, described in the ginger tea granules of the present invention, inclusion agents is second group-beta-cyclodextrin, and second group-beta-cyclodextrin is β-ring The derivant that in dextrin molecule, the H of hydroxyl is replaced by ethyl, replaces degree the highest, and slow-releasing is the most obvious, and it has surface and lives Property, more stable.
Part is embodied by further advantage part, target and the feature of the present invention by description below, and part also will be by right Research and the practice of the present invention and be understood by the person skilled in the art.
Detailed description of the invention
The invention discloses a kind of ginger tea granules and preparation method thereof, those skilled in the art can use for reference present disclosure, It is suitably modified technological parameter to realize.Special needs to be pointed out is, those skilled in the art are come by all similar replacements and change Saying and be apparent from, they are considered as being included in the present invention.Preferred embodiment has been passed through in method and the application of the present invention Being described, method described herein substantially can be carried out in without departing from present invention, spirit and scope by related personnel Change or suitably change realizes with combination and applies the technology of the present invention.
The invention provides a kind of ginger tea granules, including the raw material of following weight portion: fire Rhizoma Zingiberis Recens 100-130 part, Rhizoma Atractylodis Macrocephalae (parched) 40- 50 parts, Rhizoma Atractylodis 30-35 part, Radix Saposhnikoviae 30-35 part, Pericarpium Citri Reticulatae 25-30 part, Radix Glycyrrhizae 15-20 part, Bulbus Allii Fistulosi 30-35 part, Fructus Lycii 10-15 part, Plumula Nelumbinis 35-40 part, Semen Vitis viniferae 40-45 part, Rhizoma Dioscoreae 15-25 part, Flos Chrysanthemi 20-25 part, Herba Menthae 5-10 part, Fructus Jujubae 60-70 part, Inclusion agents 25-30 part, brown sugar 40-45 part, nigecose 40-45 part, dextrin 20-30 part, plasticizer 10-15 part and adsorbent 5- 10 parts.
Wherein, the source of described raw material is not particularly limited by the present invention, for commercially available.
In some embodiments of the invention, described inclusion agents is second group-beta-cyclodextrin.Second group-beta-cyclodextrin is β-ring The derivant that in dextrin molecule, the H of hydroxyl is replaced by ethyl, replaces degree the highest, and slow-releasing is the most obvious, and it has surface and lives Property, more stable.
In some embodiments of the invention, described plasticizer be mass ratio be the arabic gum of 10:3:1:1:1, Robinia pseudoacacia L. Locust beam gum, sucrose, calcium gluconate and potassium chloride.Arabic gum has stronger adhesion strength and soft elasticity, by adding Locust bean gum, makes the more high resilience of described arabic gum and toughness, and the interpolation of sucrose adds the transparency of described arabic gum, The interpolation of calcium gluconate and potassium chloride promotes it to shrink while increasing described arabic gum intensity and tends to fragility, logical Cross rational proportioning so that clear paste is more easy-formation during pelletizing, and has certain transparency.
In some embodiments of the invention, described adsorbent is Magnesiumaluminumsilicate.Magnesiumaluminumsilicate can adsorb Rhizoma Zingiberis Recens effectively Moisture in tea electuary, while extending the ginger tea granules shelf-life, it is possible to making ginger tea granules product obtain optimal color and luster, tissue is thin Greasy
Present invention also offers the preparation method of a kind of ginger tea granules, comprise the following steps:
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 100-130 part, Rhizoma Atractylodis Macrocephalae (parched) 40-50 part, Rhizoma Atractylodis 30-35 part, Radix Saposhnikoviae 30-35 Part and the mixing of Pericarpium Citri Reticulatae 25-30 part are sent into after pulverizer is pulverized and are joined in extractor, when temperature reaches 55-60 DEG C, open Dynamic high-pressure pump, when pressure reaches 25-30MPa, discharges pressure and carries out dynamic extraction, dynamic extraction work after static extracting 30-40min Skill parameter is: when temperature is heated to 40-50 DEG C, pressurize system, after pressure reaches 30-35MPa, regulates CO2Flow For 3-6L/h, after keeping constant temperature and pressure to be circulated extraction 3-4h, 40-60 mesh double-layer nylon sock filtration, prepare compound recipe volatilization Oil and the first filtering residue；
Component meter the most by weight, by Radix Glycyrrhizae 15-20 part, Bulbus Allii Fistulosi 30-35 part, Fructus Lycii 10-15 part, Plumula Nelumbinis 35-40 part, Semen Vitis viniferae 40-45 part, Rhizoma Dioscoreae 15-25 part, Flos Chrysanthemi 20-25 part, Herba Menthae 5-10 part and the mixing of Fructus Jujubae 60-70 part, obtain first Mixture, after being pulverized by the first mixture feeding pulverizer, adds the 65%-75% ethanol of the first mixture 7-9 times amount It is sealed in container with lid immersion 8-12h after stirring 5-8min, filters, obtain the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the second filtering residue quality summation 7-9 times amount are added 65%-75% ethanol extraction 2-2.5h, filters, obtains the second filtrate and the 3rd filtering residue, will add its 7-9 times amount in the 3rd filtering residue 65%-75% ethanol extraction 1-1.5h, filters, takes the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate are mixed, The clear paste that relative density is 1.30-1.33 it is concentrated at 50-60 DEG C；
S4. 25-30 weight portion second group-beta-cyclodextrin is weighed, while adding water and be stirred continuously and make it dissolve prepared second Group-beta-cyclodextrin saturated solution, after compound volatile oil is dissolved in ethanol solution by 2-4:1, is added dropwise to described ethyl-β-ring In dextrin saturated solution and be stirred continuously, one or both added at 20-25 DEG C in sodium bicarbonate, citric acid and malic acid are adjusted Joint pH value is 5-6, and after ultrasonic agitation 2-3h, cold preservation 18-24h postprecipitation filters, and takes solid particle, 35-45 DEG C of hot-air seasoning, i.e. Obtain volatile oil clathrate compound；
S5., by 40-45 weight portion brown sugar, after being heated to 120-130 DEG C and being stirred continuously and make it be dissolved into liquid, temperature is increased Degree is to 140-150 DEG C, and the most persistently after 15-18 minute, addition 40-45 weight portion nigecose, 20-30 weight portion dextrin continue Continuous stirring is to becoming thick rear crystallisation by cooling obtain mixed crystal and be milled to powder, and the mass ratio adding 10-15 weight portion is The arabic gum of 10:3:1:1:1, locust bean gum, sucrose, calcium gluconate, potassium chloride, 5-10 weight portion Magnesiumaluminumsilicate, and The clear paste that S3 obtains is placed in granulation machine after mixing and making granule, and after the volatile oil clathrate compound mix homogeneously that obtains of S4 point Dress, obtains ginger tea granules.
Below in conjunction with example, the present invention is described in further detail, to make those skilled in the art with reference to description literary composition Word can be implemented according to this.
<embodiment 1>
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 100 parts, Rhizoma Atractylodis Macrocephalae (parched) 40 parts, Rhizoma Atractylodis 30 parts, Radix Saposhnikoviae 30 parts and Pericarpium Citri Reticulatae 25 parts Mixing is sent into after pulverizer is pulverized and is joined in extractor, when temperature reaches 55 DEG C, starts high-pressure pump, and pressure reaches During 25MPa, discharging pressure and carry out dynamic extraction after static extracting 30min, dynamic extraction technological parameter is: when temperature is heated to 40 DEG C time, system is pressurizeed, after pressure reaches 30MPa, regulate CO2Flow is 3L/h, keeps constant temperature and pressure to be circulated extraction After taking 3h, 40 mesh double-layer nylon sock filtration, prepare compound volatile oil and the first filtering residue；
Component meter the most by weight, by 15 parts of Radix Glycyrrhizae, Bulbus Allii Fistulosi 30 parts, Fructus Lycii 10 parts, Plumula Nelumbinis 35 parts, Semen Vitis viniferae 40 parts, mountain Medicine 15 parts, Flos Chrysanthemi 20 parts, Herba Menthae 5 parts and Fructus Jujubae 60 parts mixing, obtain the first mixture, is sent into by the first mixture and pulverizes After machine is pulverized, after adding 65% ethanol stirring 5min of the first mixture 9 times amount, it is sealed in container with lid immersion 8- 12h, filters, obtains the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the second filtering residue quality summation 9 times amount are added 65% ethanol extraction 2h, filters, obtains the second filtrate and the 3rd filtering residue, 65% ethanol adding its 9 times amount carried in the 3rd filtering residue Take 1h, filter, take the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate being mixed, at 50-60 DEG C, be concentrated into phase It is the clear paste of 1.30 to density；
S4. second group-beta-cyclodextrin 25 parts is weighed, while adding water and be stirred continuously and make it dissolve prepared ethyl-β-ring Dextrin saturated solution, after compound volatile oil is dissolved in ethanol solution by 2:1, is added dropwise to described second group-beta-cyclodextrin saturated In solution and be stirred continuously, one or both regulation pH value added at 20 DEG C in sodium bicarbonate, citric acid and malic acid are 5, After ultrasonic agitation 2h, cold preservation 18h postprecipitation filters, and takes solid particle, and 35 DEG C of hot-air seasonings obtain volatile oil clathrate compound；
S5., by 40 parts of brown sugar, after being heated to 120 DEG C and being stirred continuously and make it be dissolved into liquid, temperature is increased to 140 DEG C, Add nigecose 40 parts after continuing 15 minutes at such a temperature, 20 parts of dextrin continues stirring to becoming thick rear crystallisation by cooling to mix Crystal is also milled to powder, and the mass ratio adding 10 parts is the arabic gum of 10:3:1:1:1, locust bean gum, sucrose, Fructus Vitis viniferae The clear paste that Calciofon, potassium chloride, Magnesiumaluminumsilicate 5 parts, and S3 obtain is placed in granulation machine after mixing and making granule, and S4 Subpackage after the volatile oil clathrate compound mix homogeneously obtained, obtains ginger tea granules.
<embodiment 2>
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 120 parts, Rhizoma Atractylodis Macrocephalae (parched) 45 parts, Rhizoma Atractylodis 35 parts, Radix Saposhnikoviae 35 parts and Pericarpium Citri Reticulatae 30 parts Mixing is sent into after pulverizer is pulverized and is joined in extractor, when temperature reaches 56 DEG C, starts high-pressure pump, and pressure reaches During 28MPa, discharging pressure and carry out dynamic extraction after static extracting 35min, dynamic extraction technological parameter is: when temperature is heated to 45 DEG C time, system is pressurizeed, after pressure reaches 32MPa, regulate CO2Flow is 4L/h, keeps constant temperature and pressure to be circulated extraction After taking 3.5h, 50 mesh double-layer nylon sock filtration, prepare compound volatile oil and the first filtering residue；
Component meter the most by weight, by 17 parts of Radix Glycyrrhizae, Bulbus Allii Fistulosi 32 parts, Fructus Lycii 12 parts, Plumula Nelumbinis 37 parts, Semen Vitis viniferae 42 parts, mountain Medicine 17 parts, Flos Chrysanthemi 22 parts, Herba Menthae 6 parts and Fructus Jujubae 65 parts mixing, obtain the first mixture, is sent into by the first mixture and pulverizes After machine is pulverized, after adding 75% ethanol stirring 8min of the first mixture 7 times amount, it is sealed in container with lid immersion 12h, Filter, obtain the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the second filtering residue quality summation 7 times amount are added 75% ethanol extraction 2.5h, filters, obtains the second filtrate and the 3rd filtering residue, will add 75% ethanol of its 7 times amount in the 3rd filtering residue Extract 1.5h, filter, take the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate being mixed, at 60 DEG C, be concentrated into phase It is the clear paste of 1.32 to density；
S4. weigh 27 weight portion second group-beta-cyclodextrins, while adding water and be stirred continuously make its dissolve prepared ethyl- Beta-schardinger dextrin-saturated solution, after compound volatile oil is dissolved in ethanol solution by 2.5:1, is added dropwise to described ethyl-β-ring and sticks with paste In essence saturated solution and be stirred continuously, at 25 DEG C, add one or both regulations pH in sodium bicarbonate, citric acid and malic acid Value is 6, and after ultrasonic agitation 3h, cold preservation 24h postprecipitation filters, and takes solid particle, and 45 DEG C of hot-air seasonings obtain inclusion essential oil Thing；
S5., by 45 weight portion brown sugar, after being heated to 130 DEG C and being stirred continuously and make it be dissolved into liquid, temperature is increased to 150 DEG C, the most persistently add 45 weight portion nigecose, 30 weight portion dextrin continuation stirrings after 18 minutes to becoming thick rear cold But crystallizing to obtain mixed crystal be milled to powder, the mass ratio adding 15 weight portions is the arabic gum of 10:3:1:1:1, thorn Locust bean gum, sucrose, calcium gluconate, potassium chloride, 10 weight portion Magnesiumaluminumsilicates, and the clear paste that S3 obtains are placed in granulation machine After mixing and making granule, and subpackage after the volatile oil clathrate compound mix homogeneously that obtains of S4, obtain ginger tea granules.
<embodiment 3>
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 130 parts, Rhizoma Atractylodis Macrocephalae (parched) 50 parts, Rhizoma Atractylodis 35 parts, Radix Saposhnikoviae 35 parts and Pericarpium Citri Reticulatae 30 parts Mixing is sent into after pulverizer is pulverized and is joined in extractor, when temperature reaches 60 DEG C, starts high-pressure pump, and pressure reaches During 30MPa, discharging pressure and carry out dynamic extraction after static extracting 40min, dynamic extraction technological parameter is: when temperature is heated to 50 DEG C time, system is pressurizeed, after pressure reaches 35MPa, regulate CO2Flow is 6L/h, keeps constant temperature and pressure to be circulated extraction After taking 4h, 60 mesh double-layer nylon sock filtration, prepare compound volatile oil and the first filtering residue；
Component meter the most by weight, by 20 parts of Radix Glycyrrhizae, Bulbus Allii Fistulosi 35 parts, Fructus Lycii 15 parts, Plumula Nelumbinis 40 parts, Semen Vitis viniferae 45 parts, mountain Medicine 25 parts, Flos Chrysanthemi 25 parts, Herba Menthae 10 parts and Fructus Jujubae 70 parts mixing, obtain the first mixture, is sent into by the first mixture and pulverizes After machine is pulverized, after adding 75% ethanol stirring 8min of the first mixture 9 times amount, it is sealed in container with lid immersion 12h, Filter, obtain the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the second filtering residue quality summation 9 times amount are added 75% ethanol extraction 2.5h, filters, obtains the second filtrate and the 3rd filtering residue, will add 65% ethanol of its 7 times amount in the 3rd filtering residue Extract 1.5h, filter, take the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate being mixed, at 60 DEG C, be concentrated into phase It is the clear paste of 1.33 to density；
S4. weigh 30 weight portion second group-beta-cyclodextrins, while adding water and be stirred continuously make its dissolve prepared ethyl- Beta-schardinger dextrin-saturated solution, after compound volatile oil is dissolved in ethanol solution by 4:1, is added dropwise to described second group-beta-cyclodextrin In saturated solution and be stirred continuously, at 25 DEG C, add one or both regulation pH value in sodium bicarbonate, citric acid and malic acid Being 6, after ultrasonic agitation 3h, cold preservation 24h postprecipitation filters, and takes solid particle, and 45 DEG C of hot-air seasonings obtain volatile oil clathrate compound；
S5., by 45 weight portion brown sugar, after being heated to 130 DEG C and being stirred continuously and make it be dissolved into liquid, temperature is increased to 150 DEG C, the most persistently add 45 weight portion nigecose, 30 weight portion dextrin continuation stirrings after 18 minutes to becoming thick rear cold But crystallizing to obtain mixed crystal be milled to powder, the mass ratio adding 15 weight portions is the arabic gum of 10:3:1:1:1, thorn Locust bean gum, sucrose, calcium gluconate, potassium chloride, 10 weight portion Magnesiumaluminumsilicates, and the clear paste that S3 obtains are placed in granulation machine After mixing and making granule, and subpackage after the volatile oil clathrate compound mix homogeneously that obtains of S4, obtain ginger tea granules.
<embodiment 4>
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 125 parts, Rhizoma Atractylodis Macrocephalae (parched) 48 parts, Rhizoma Atractylodis 34 parts, Radix Saposhnikoviae 30 parts and Pericarpium Citri Reticulatae 25 parts Mixing is sent into after pulverizer is pulverized and is joined in extractor, when temperature reaches 58 DEG C, starts high-pressure pump, and pressure reaches During 28MPa, discharging pressure and carry out dynamic extraction after static extracting 38min, dynamic extraction technological parameter is: when temperature is heated to 44 DEG C time, system is pressurizeed, after pressure reaches 34MPa, regulate CO2Flow is 4L/h, keeps constant temperature and pressure to be circulated extraction After taking 4h, 60 mesh double-layer nylon sock filtration, prepare compound volatile oil and the first filtering residue；
Component meter the most by weight, by 20 parts of Radix Glycyrrhizae, Bulbus Allii Fistulosi 34 parts, Fructus Lycii 14 parts, Plumula Nelumbinis 38 parts, Semen Vitis viniferae 43 parts, mountain Medicine 23 parts, Flos Chrysanthemi 23 parts, Herba Menthae 8 parts and Fructus Jujubae 66 parts mixing, obtain the first mixture, is sent into by the first mixture and pulverizes After machine is pulverized, after adding 75% ethanol stirring 8min of the first mixture 8 times amount, it is sealed in container with lid immersion 12h, Filter, obtain the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the second filtering residue quality summation 8 times amount are added 75% ethanol extraction 2.4h, filters, obtains the second filtrate and the 3rd filtering residue, will add 75% ethanol of its 8 times amount in the 3rd filtering residue Extract 1.3h, filter, take the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate are mixed, concentrate at 50-60 DEG C It is the clear paste of 1.32 to relative density；
S4. weigh 27 weight portion second group-beta-cyclodextrins, while adding water and be stirred continuously make its dissolve prepared ethyl- Beta-schardinger dextrin-saturated solution, after compound volatile oil is dissolved in ethanol solution by 3.5:1, is added dropwise to described ethyl-β-ring and sticks with paste In essence saturated solution and be stirred continuously, at 25 DEG C, add one or both regulations pH in sodium bicarbonate, citric acid and malic acid Value is 6, and after ultrasonic agitation 3h, cold preservation 20h postprecipitation filters, and takes solid particle, and 40 DEG C of hot-air seasonings obtain inclusion essential oil Thing；
S5., by 43 weight portion brown sugar, after being heated to 125 DEG C and being stirred continuously and make it be dissolved into liquid, temperature is increased to 145 DEG C, the most persistently add 45 weight portion nigecose, 26 weight portion dextrin continuation stirrings after 18 minutes to becoming thick rear cold But crystallizing to obtain mixed crystal be milled to powder, the mass ratio adding 12 weight portions is the arabic gum of 10:3:1:1:1, thorn Locust bean gum, sucrose, calcium gluconate, potassium chloride, 7 weight portion Magnesiumaluminumsilicates, and the clear paste that S3 obtains are placed in granulation machine After mixing and making granule, and subpackage after the volatile oil clathrate compound mix homogeneously that obtains of S4, obtain ginger tea granules.
Although embodiment of the present invention are disclosed as above, but it is not restricted in description and embodiment listed Using, it can be applied to various applicable the field of the invention completely, for those skilled in the art, and can be easily Realizing other amendment, therefore, under the general concept limited without departing substantially from claim and equivalency range, the present invention does not limit In specific details with shown here as the embodiment with description.

Claims (7)

1. a ginger tea granules, it is characterised in that include the raw material of following weight portion: fire Rhizoma Zingiberis Recens 100-130 part, Rhizoma Atractylodis Macrocephalae (parched) 40-50 Part, Rhizoma Atractylodis 30-35 part, Radix Saposhnikoviae 30-35 part, Pericarpium Citri Reticulatae 25-30 part, Radix Glycyrrhizae 15-20 part, Bulbus Allii Fistulosi 30-35 part, Fructus Lycii 10-15 part, lotus Sub-heart 35-40 part, Semen Vitis viniferae 40-45 part, Rhizoma Dioscoreae 15-25 part, Flos Chrysanthemi 20-25 part, Herba Menthae 5-10 part, Fructus Jujubae 60-70 part, bag Mixture 25-30 part, brown sugar 40-45 part, nigecose 40-45 part, dextrin 20-30 part, plasticizer 10-15 part and adsorbent 5-10 Part.
Ginger tea granules the most according to claim 1, it is characterised in that described inclusion agents is second group-beta-cyclodextrin.
Ginger tea granules the most according to claim 1, it is characterised in that described plasticizer be mass ratio be 10:3:1:1:1's Arabic gum, locust bean gum, sucrose, calcium gluconate and potassium chloride.
Ginger tea granules the most according to claim 1, it is characterised in that described adsorbent is Magnesiumaluminumsilicate.
5. the preparation method of a ginger tea granules, it is characterised in that comprise the following steps:
Component meter the most by weight, by fire Rhizoma Zingiberis Recens 100-130 part, Rhizoma Atractylodis Macrocephalae (parched) 40-50 part, Rhizoma Atractylodis 30-35 part, Radix Saposhnikoviae 30-35 part, with And Pericarpium Citri Reticulatae 25-30 part mixing send into pulverizer pulverize after join in extractor, when temperature reaches 55-60 DEG C, start height Press pump, when pressure reaches 25-30MPa, discharges pressure and carries out dynamic extraction after static extracting 30-40min, dynamic extraction technique is joined Number is: when temperature is heated to 40-50 DEG C, pressurize system, after pressure reaches 30-35MPa, regulates CO2Flow is 3- 6L/h, keep constant temperature and pressure be circulated extraction 3-4h after, 40-60 mesh double-layer nylon sock filtration, prepare compound volatile oil and First filtering residue；
Component meter the most by weight, by Radix Glycyrrhizae 15-20 part, Bulbus Allii Fistulosi 30-35 part, Fructus Lycii 10-15 part, Plumula Nelumbinis 35-40 part, Fructus Vitis viniferae Seed 40-45 part, Rhizoma Dioscoreae 15-25 part, Flos Chrysanthemi 20-25 part, Herba Menthae 5-10 part and the mixing of Fructus Jujubae 60-70 part, obtain the first mixing Thing, after being pulverized by the first mixture feeding pulverizer, adds the 65%-75% ethanol stirring of the first mixture 7-9 times amount It is sealed in container with lid immersion 8-12h after 5-8min, filters, obtain the first filtrate and the second filtering residue；
S3. by the first filtering residue, after the second filtering residue mixing, the first filtering residue and the 65%-of the second filtering residue quality summation 7-9 times amount are added 75% ethanol extraction 2-2.5h, filters, obtains the second filtrate and the 3rd filtering residue, will add the 65%-of its 7-9 times amount in the 3rd filtering residue 75% ethanol extraction 1-1.5h, filters, takes the 3rd filtrate, after the first filtrate, the second filtrate and the 3rd filtrate being mixed, at 50- The clear paste that relative density is 1.30-1.33 it is concentrated at 60 DEG C；
S4. weigh 25-30 weight portion second group-beta-cyclodextrin, while adding water and be stirred continuously make its dissolve prepared ethyl-β- Cyclodextrin saturated solution, after compound volatile oil is dissolved in ethanol solution by 2-4:1, is added dropwise to described second group-beta-cyclodextrin In saturated solution and be stirred continuously, regulating pH value at 20-25 DEG C is 5-6, after ultrasonic agitation 2-3h, and cold preservation 18-24h postprecipitation Filter, take solid particle, 35-45 DEG C of hot-air seasoning, obtain volatile oil clathrate compound；
S5. after 40-45 weight portion brown sugar, 40-45 weight portion nigecose and 20-30 weight portion dextrin heating for dissolving being processed Mixed crystal is milled to powder, add the mass ratio of 10-15 weight portion be the arabic gum of 10:3:1:1:1, locust bean gum, The clear paste that sucrose, calcium gluconate, potassium chloride, 5-10 weight portion Magnesiumaluminumsilicate, and S3 obtain is placed in granulation machine mixing And after making granule, and subpackage after the volatile oil clathrate compound mix homogeneously that obtains of S4, obtain ginger tea granules.
The preparation method of ginger tea granules the most according to claim 5, it is characterised in that the solvent regulating pH in step S4 is One or both in sodium bicarbonate, citric acid and malic acid.
The preparation method of ginger tea granules the most according to claim 5, it is characterised in that step S5 produces described mixed crystal Method be by 40-45 weight portion brown sugar, after being heated to 120-130 DEG C and being stirred continuously and make it be dissolved into liquid, increase temperature To 140-150 DEG C, the most persistently after 15-18 minute, add 40-45 weight portion nigecose, the continuation of 20-30 weight portion dextrin Stirring is to becoming thick rear crystallisation by cooling.
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CN109221537A (en) * 2018-10-15 2019-01-18 沈捷 Formula and preparation method of ginger decoction tea cream
CN109645164A (en) * 2019-01-28 2019-04-19 蓝宇涛 A kind of Black Box Tracing ginger sugar health protection tea and preparation method thereof
CN113712106A (en) * 2021-09-02 2021-11-30 广东橘香斋大健康产业股份有限公司 Dried orange peel and ginger sugar dissolving block and packaging structure and preparation method thereof

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CN107019081A (en) * 2017-06-19 2017-08-08 安徽省天山茶业有限公司 A kind of grape pip brown sugar ginger tea drink
CN107114795A (en) * 2017-07-06 2017-09-01 胥永贵 A kind of weak base is replenished the calcium, soda alkalization ginger preparation and its preparation method and application
CN108048218A (en) * 2017-12-14 2018-05-18 柳州市象行教育科技有限责任公司 A kind of potato composite essential oil and preparation method thereof
CN109221537A (en) * 2018-10-15 2019-01-18 沈捷 Formula and preparation method of ginger decoction tea cream
CN109645164A (en) * 2019-01-28 2019-04-19 蓝宇涛 A kind of Black Box Tracing ginger sugar health protection tea and preparation method thereof
CN113712106A (en) * 2021-09-02 2021-11-30 广东橘香斋大健康产业股份有限公司 Dried orange peel and ginger sugar dissolving block and packaging structure and preparation method thereof
CN113712106B (en) * 2021-09-02 2024-01-30 广东橘香斋大健康产业股份有限公司 Dried orange peel ginger candy dissolved block and packaging structure and preparation method thereof

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Application publication date: 20161026