CN105985190A - Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof - Google Patents
Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof Download PDFInfo
- Publication number
- CN105985190A CN105985190A CN201610097837.1A CN201610097837A CN105985190A CN 105985190 A CN105985190 A CN 105985190A CN 201610097837 A CN201610097837 A CN 201610097837A CN 105985190 A CN105985190 A CN 105985190A
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- China
- Prior art keywords
- herbal medicine
- chinese herbal
- fertilizer
- water
- bentonite
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4806—Sorbents characterised by the starting material used for their preparation the starting material being of inorganic character
Abstract
The invention discloses a fertilizer capable of efficiently utilizing a Chinese herbal medicine extracting solution for adsorption and a preparation method thereof. The fertilizer is prepared from the following raw materials in parts by weight: sodium bentonite, carbon powder, starch, an aldol resin, cement, gypsum powder, ethanol, Raphanus sativus seed, cottonseed hull, edible fungus dregs, folium artemisiae argyi, Chrysanthemum cinerariaefolium, mulberry leaves, Herba Patriniae, Melia azedarach fruit, sweet potato vine, urea and a proper amount of water. The common Chinese herbal medicine effective fertilizer can only display the effects instantaneously since the effective components extracted from plants can be easily decomposed and lose functions in the natural world environment. After the bentonite is modified, the structure is enhanced on the original basis, so that the bentonite has better adsorption effects and can easily adsorb and retain water, and is always in a moist state, thereby prolonging the effective time of the plant extracting solution. Thus, the multi-miniature-tube bentonite particles can be pulverized and cracked more easily in the soil, and can improve the soil quality.
Description
Technical field
The invention belongs to the Technology field of fertilizer, be specifically related to one and efficiently utilize extracts of Chinese herbal medicine adsorption fertilizer and preparation method thereof.
Background technology
Bentonite is the clay mineral with montmorillonite as main component.Montmorillonite has the structure of simple Oblique Crystal, it is a kind of aqueous dioctahedron or trioctahedral layer aluminosilicate mineral, two-layer silicon-oxy tetrahedron is had in the outside of single cell, middle one layer of hydrogen-oxygen aluminum of folder is octahedra, and in tetrahedron and octahedron, the silicon ion of high price and aluminium ion can be by its cation replacements at a low price, make montmorillonite structure cell electronegative, become a big anion, so that it has the ability of Liquidity limit, but to Anion-adsorption less effective.
Flaky graphite has preferable electric conductivity, but its layer structure is allowed to be not suitable for being individually used in conducting resinl, to be generally used in mixed way with white carbon black.Spherical carbon black particle is filled between the graphite of stratiform, applies certain pressure to graphite linings so that it is can preferably contact.The great advantage of graphite conductive adhesive is that Performance comparision is stable, has certain acid and alkali-resistance ability, and cheap, relative density is little, and dispersive property is good, but resistivity is higher, is typically only used for middle resistance slurry.
Summary of the invention
In order to preferably play modified alta-mud absorption property in fertilizer, the present invention utilizes inorganic pore creating material to manufacture countless interconnective microporous pipeline in spray profit soil, thus has higher adsorption effect, and concrete grammar is as follows:
One efficiently utilizes extracts of Chinese herbal medicine adsorption fertilizer, it is characterized in that, be made up of the raw material of following weight portion: sodium bentonite 20 ~ 30, carbon dust 6 ~ 8, starch 1 ~ 2, aldol resin 0.5 ~ 1, cement 2 ~ 3, Gypsum Fibrosum powder 0.2 ~ 0.5, ethanol 7 ~ 10, Semen Raphani 5 ~ 9, cotton seed hulls 20 ~ 30, edible fungi residue 45 ~ 60, Folium Artemisiae Argyi 6 ~ 10, pyrethrum flowers 5 ~ 8, mulberry leaves 6 ~ 9, Herba Patriniae 2 ~ 5, neem fruit 3 ~ 6, Rhizoma Dioscoreae rattan 10 ~ 15, carbamide 5 ~ 10 and appropriate water；
A kind of preparation method efficiently utilizing extracts of Chinese herbal medicine adsorption fertilizer, it is characterised in that include following step:
(1) being mixed by the water of aldol resin and 4 ~ 5 times of its weight portions, stir to being completely dissolved after being heated to 70 ~ 80 DEG C, be subsequently poured into the starch and carbon dust of mixing, stirring and evenly mixing becomes viscosity to be homogenized；
(2) sodium bentonite is removed sand, it is subsequently adding the viscosity homogenate described in (1), cement and Gypsum Fibrosum powder, stir to becoming uniform slurry while add waterside, then it is placed in the energising field that voltage is 300 ~ 350V, is slowly stirred 10 ~ 15min and makes carbon dust linear array, dry, then being put under the hot conditions of 500 ~ 550 DEG C calcining 30 ~ 40min and become the solid block of porous, crushing and screening is crossed 20 ~ 30 mesh sieves and is obtained granule；
(3) mixing Semen Raphani, pyrethrum flowers, neem fruit and other following residual components being not directed to, add water in right amount and be milled to homogenate, be subsequently adding ethanol, stand 2 ~ 3h, obtain filtrate and filtering residue by sucking filtration after stirring；
(4) being added to (3) gained filtrate by the granule described in (2), unification is put in ultrasonic washing unit, power 600 ~ 750W, and effect 20 ~ 25min makes to be full of in micropore filtrate；
(5) mixing cotton seed hulls, edible fungi residue and carbamide, add the water of its weight portion of equivalent, and ball milling becomes paste, is subsequently adding the granule described in (3) gained filtering residue, (4) and residual filtrate, stirred after by slurry-spraying pelletizing and dry.
Bentonite is prepared the method for adsorbent and is substantially: the high-quality sodium bentonite selecting nonmetallic ore is raw material, 4g200 mesh inflammable micropowder carbon dust and 2g starch is mixed at dry 100g bentonite after removing sand, add appropriate water and stir evenly the granule being squeezed into a diameter of 3mm, dry, high temperature sintering again, owing to losing of water of crystallization and inflammable micropowder combustion generate CO2Releasing, define substantial amounts of micropore.
The final purpose of the present invention is for the mineral element of sorption chemical element, the most tiny by the micropore stayed after carbon dust high-temp combustion, the inorganic elements of fertilizer first must be dissolved, it is reinfiltrated in tiny hole, but there is Railway Project here: 1, the surface tension of water is very big, penetrate in trickle hole the most slowly and more difficulty；2, the inorganic chemistry element after dissolving is through dilution, even if permeating completely, amount is the least；3, the micropore manufacture being made up of carbon dust microgranule is micropore, is present in inside bentonite, and the most burned rear micropore formed belongs to air-tight state, it is impossible to reserve, let alone absorption.
nullSeveral measures of the present invention just solve problem above，First carbon dust is processed modification，Using a kind of viscosity, epoxy resin that is stronger and that have electric conductivity joins in carbon dust after diluting as binding agent for we，Stirred postadhesion is on carbon dust surface，Become the carbon dust microgranule of a kind of sticky particle，Then carbon dust is added in spray profit soil，Freely it is energized under the electric field action of conduction，Carbon dust freely connects in the case of conduction，Form toner chain，And the effect of epoxy resin be that make chain there is a period of time (epoxy resin becomes advanced technology already as the binding agent of electric conductivity，Effect is obvious)，Then according to step，High temperature sintering，So form micro-tube，Rather than micropore，Ul-trasonic irradiation is carried out the when of being then placed in the chemical element dissolved，The surface tension of the least water，Finally dry，Carry out second adsorption simultaneously，So chemicals quality of residual will be greatly improved，In order to improve the water absorbing properties of spray profit soil particle and rapid functions/drying，It is especially added with a certain amount of cement，Add strong absorptive and maintain spray to moisten the stability that soil particle is certain.
Beneficial effects of the present invention: common Chinese herbal medicine effect fertilizer is only possible to moment performance effect, because the effective ingredient extracted in plant is easy to decomposition in nature environment and loses function, the present invention is to after bentonite modified, strengthening it on the original basis can not structure, adsorption effect is more preferable, it is easy to water suction and stays water, remain self a kind of state containing profit, thus can extend the efficacy window of plant extraction liquid, the bentonite clay particle of many micro-tubes the most easily pulverizes cracking in soil, improves soil property.
Detailed description of the invention
Embodiment 1:
One efficiently utilizes extracts of Chinese herbal medicine adsorption fertilizer, it is characterized in that, be made up of the raw material of following weight portion (Kg): sodium bentonite 24, carbon dust 7, starch 1, aldol resin 0.5, cement 2, Gypsum Fibrosum powder 0.2, ethanol 8, Semen Raphani 6, cotton seed hulls 30, edible fungi residue 55, Folium Artemisiae Argyi 7, pyrethrum flowers 6, mulberry leaves 7, Herba Patriniae 3, neem fruit 5, Rhizoma Dioscoreae rattan 12, carbamide 7 and appropriate water；
A kind of preparation method efficiently utilizing extracts of Chinese herbal medicine adsorption fertilizer, it is characterised in that include following step:
(1) being mixed by the water of aldol resin and 4 ~ 5 times of its weight portions, stir to being completely dissolved after being heated to 70 ~ 80 DEG C, be subsequently poured into the starch and carbon dust of mixing, stirring and evenly mixing becomes viscosity to be homogenized；
(2) sodium bentonite is removed sand, it is subsequently adding the viscosity homogenate described in (1), cement and Gypsum Fibrosum powder, stir to becoming uniform slurry while add waterside, then it is placed in the energising field that voltage is 300 ~ 350V, is slowly stirred 10 ~ 15min and makes carbon dust linear array, dry, then being put under the hot conditions of 500 ~ 550 DEG C calcining 30 ~ 40min and become the solid block of porous, crushing and screening is crossed 20 ~ 30 mesh sieves and is obtained granule；
(3) mixing Semen Raphani, pyrethrum flowers, neem fruit and other following residual components being not directed to, add water in right amount and be milled to homogenate, be subsequently adding ethanol, stand 2 ~ 3h, obtain filtrate and filtering residue by sucking filtration after stirring；
(4) being added to (3) gained filtrate by the granule described in (2), unification is put in ultrasonic washing unit, power 600 ~ 750W, and effect 20 ~ 25min makes to be full of in micropore filtrate；
(5) mixing cotton seed hulls, edible fungi residue and carbamide, add the water of its weight portion of equivalent, and ball milling becomes paste, is subsequently adding the granule described in (3) gained filtering residue, (4) and residual filtrate, stirred after by slurry-spraying pelletizing and dry.
The a kind of of the present invention is used efficiently to utilize extracts of Chinese herbal medicine adsorption fertilizer for the planting experiment of Semen sojae atricolor, select 5 mu of Soybean Fields as experimental group, planting site Semen sojae atricolor mixes as the ratio of base manure with subsoil 1:4,5 mu of Soybean Fields of matched group implantation methods routinely carries out plantation, other water and fertilizer management and the prevention and control of plant diseases, pest control are implemented according to the practical situation of its growing way later, result: the Semen sojae atricolor growing way of experimental group is more preferable, moisture is sufficient, the ability of resistance and disease and insect resistance is strengthened, and saves financial expenditure 7.9%.
Claims (2)
1. one kind efficiently utilizes extracts of Chinese herbal medicine adsorption fertilizer, it is characterized in that, be made up of the raw material of following weight portion: sodium bentonite 20 ~ 30, carbon dust 6 ~ 8, starch 1 ~ 2, aldol resin 0.5 ~ 1, cement 2 ~ 3, Gypsum Fibrosum powder 0.2 ~ 0.5, ethanol 7 ~ 10, Semen Raphani 5 ~ 9, cotton seed hulls 20 ~ 30, edible fungi residue 45 ~ 60, Folium Artemisiae Argyi 6 ~ 10, pyrethrum flowers 5 ~ 8, mulberry leaves 6 ~ 9, Herba Patriniae 2 ~ 5, neem fruit 3 ~ 6, Rhizoma Dioscoreae rattan 10 ~ 15, carbamide 5 ~ 10 and appropriate water.
A kind of preparation method efficiently utilizing extracts of Chinese herbal medicine adsorption fertilizer, it is characterised in that include following step:
(1) being mixed by the water of aldol resin and 4 ~ 5 times of its weight portions, stir to being completely dissolved after being heated to 70 ~ 80 DEG C, be subsequently poured into the starch and carbon dust of mixing, stirring and evenly mixing becomes viscosity to be homogenized；
(2) sodium bentonite is removed sand, it is subsequently adding the viscosity homogenate described in (1), cement and Gypsum Fibrosum powder, stir to becoming uniform slurry while add waterside, then it is placed in the energising field that voltage is 300 ~ 350V, is slowly stirred 10 ~ 15min and makes carbon dust linear array, dry, then being put under the hot conditions of 500 ~ 550 DEG C calcining 30 ~ 40min and become the solid block of porous, crushing and screening is crossed 20 ~ 30 mesh sieves and is obtained granule；
(3) mixing Semen Raphani, pyrethrum flowers, neem fruit and other following residual components being not directed to, add water in right amount and be milled to homogenate, be subsequently adding ethanol, stand 2 ~ 3h, obtain filtrate and filtering residue by sucking filtration after stirring；
(4) being added to (3) gained filtrate by the granule described in (2), unification is put in ultrasonic washing unit, power 600 ~ 750W, and effect 20 ~ 25min makes to be full of in micropore filtrate；
(5) mixing cotton seed hulls, edible fungi residue and carbamide, add the water of its weight portion of equivalent, and ball milling becomes paste, is subsequently adding the granule described in (3) gained filtering residue, (4) and residual filtrate, stirred after by slurry-spraying pelletizing and dry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610097837.1A CN105985190A (en) | 2016-02-23 | 2016-02-23 | Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610097837.1A CN105985190A (en) | 2016-02-23 | 2016-02-23 | Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN105985190A true CN105985190A (en) | 2016-10-05 |
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| CN201610097837.1A Pending CN105985190A (en) | 2016-02-23 | 2016-02-23 | Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof |
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| Country | Link |
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| CN (1) | CN105985190A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106673796A (en) * | 2016-11-30 | 2017-05-17 | 河池市金城江区科学技术情报研究所 | Special fertilizer for mulberry planting |
| CN106831044A (en) * | 2016-12-09 | 2017-06-13 | 河池市技术开发中心 | The preparation technology of fertilizer special for cotton |
| CN109315225A (en) * | 2018-10-24 | 2019-02-12 | 黎平青江农业开发有限公司 | A kind of gastrodin cultivation bacteria stick and preparation method thereof |
| CN112250519A (en) * | 2020-10-16 | 2021-01-22 | 广东石油化工学院 | Preparation method and application of biological modified bentonite |
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| CN102483970A (en) * | 2009-06-22 | 2012-05-30 | 孔达利恩股份有限公司 | Electrostatic Discharge Device And Method For Manufacturing The Same |
| CN105198632A (en) * | 2015-10-21 | 2015-12-30 | 滁州市施集茶场 | Antibacterial fertilizer special for health tea tree and preparation method of antibacterial fertilizer |
| CN105254419A (en) * | 2015-10-16 | 2016-01-20 | 阜南县阜合种养农民专业合作联合社 | Liquid fermentation type fertilizer for pear trees and preparation method of fertilizer |
| CN105272583A (en) * | 2015-10-21 | 2016-01-27 | 滁州市施集茶场 | Organic tea tree fertilizer with high water retention property and preparation method of organic tea tree fertilizer |
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2016
- 2016-02-23 CN CN201610097837.1A patent/CN105985190A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102483970A (en) * | 2009-06-22 | 2012-05-30 | 孔达利恩股份有限公司 | Electrostatic Discharge Device And Method For Manufacturing The Same |
| CN105254419A (en) * | 2015-10-16 | 2016-01-20 | 阜南县阜合种养农民专业合作联合社 | Liquid fermentation type fertilizer for pear trees and preparation method of fertilizer |
| CN105198632A (en) * | 2015-10-21 | 2015-12-30 | 滁州市施集茶场 | Antibacterial fertilizer special for health tea tree and preparation method of antibacterial fertilizer |
| CN105272583A (en) * | 2015-10-21 | 2016-01-27 | 滁州市施集茶场 | Organic tea tree fertilizer with high water retention property and preparation method of organic tea tree fertilizer |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106673796A (en) * | 2016-11-30 | 2017-05-17 | 河池市金城江区科学技术情报研究所 | Special fertilizer for mulberry planting |
| CN106831044A (en) * | 2016-12-09 | 2017-06-13 | 河池市技术开发中心 | The preparation technology of fertilizer special for cotton |
| CN109315225A (en) * | 2018-10-24 | 2019-02-12 | 黎平青江农业开发有限公司 | A kind of gastrodin cultivation bacteria stick and preparation method thereof |
| CN112250519A (en) * | 2020-10-16 | 2021-01-22 | 广东石油化工学院 | Preparation method and application of biological modified bentonite |
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