CN105254419A - Liquid fermentation type fertilizer for pear trees and preparation method of fertilizer - Google Patents
Liquid fermentation type fertilizer for pear trees and preparation method of fertilizer Download PDFInfo
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- CN105254419A CN105254419A CN201510667566.4A CN201510667566A CN105254419A CN 105254419 A CN105254419 A CN 105254419A CN 201510667566 A CN201510667566 A CN 201510667566A CN 105254419 A CN105254419 A CN 105254419A
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Abstract
The invention discloses a liquid fermentation type fertilizer for pear trees and a preparation method of the fertilizer. The fertilizer is prepared from raw materials in parts by weight as follows: industrial starch, soybean meal, a compound microbial agent, bran, earthworm soil, withered leaves, humic acid, saturated lime water, monopotassium phosphate, ammonium bicarbonate, boric acid, quartz sand, a coagulant and a proper amount of water. With the adoption of the liquid fermentation manner, the fertilizer is fermented more completely, various ingredients beneficial to crops are dissolved in water and then are coagulated through the special coagulant and spin-dried. The preparation method is used for processing of the fertilizer.
Description
Technical field
The invention belongs to the Technology field of fertilizer, pear tree fertilizer being specifically related to a kind of liquid state fermentation and preparation method thereof.
Background technology
Excrement of animals and the resistates of various organic domestic waste after fermentation are the organic colloids that a kind of size distribution is very wide, and the thorough separation difficulty of its solid-liquid is very large, and this makes fermented liquid be restricted to commercial fertilizer transformation by traditional Land use systems.To the organic waste water of different sources, there is different treatment processs, as the flocculation agent such as Tai-Ace S 150 and active silica, chitin and chitosan, polyacrylamide or flocculation agent are reported a lot to the treatment effect of suspension system, but be the theoretical investigation in laboratory mostly.
Residue after disposed waste in agricultural crop straw, biology and the manure fermentation of livestock is mainly divided into nutritive substance, mineral substance and active substance, nutritive substance is wherein divided into again crude protein, crude fat, humic acid, crude fibre, nitrogen-free extract, mineral substance is divided into again trace element and major element, and activeconstituents is amino acid, plant hormone, vitamin B group, lytic enzyme and microbiotic substantially.Containing abundant nutritive element and organic matter.
Summary of the invention
Be fully utilized to make each composition in fermented ingredient, the present invention uses flocculation agent to be adsorbed by each for fermented ingredient kind of plant beneficiating ingredient, then the fertilizer of different-effect and type is prepared for fertilizer additive, be satisfied with the demand of various Different Crop, not only self provide abundant nutritive ingredient, and can promote that crop is to the absorption of NPK, concrete grammar is as follows:
A kind of pear tree fertilizer of liquid state fermentation, it is characterized in that, be made up of the raw material of following weight part: industrial starch 30 ~ 35, soyabean expeller 25 ~ 35, complex micro organism fungicide 3 ~ 5, wheat bran 45 ~ 60, earthworm soil 15 ~ 20, withered leaf 10 ~ 15, humic acid 6 ~ 8, saturated limewater 12 ~ 18, potassium primary phosphate 10 ~ 16, bicarbonate of ammonia 20 ~ 25, boric acid 8 ~ 12, quartz sand 4 ~ 6, flocculation agent 7 ~ 10 and appropriate water;
Described flocculation agent is made up of the raw material of following weight part: terra alba 15 ~ 20,10% ferrum sulfuricum oxydatum solutum 10 ~ 14,10% acetic acid solution 4 ~ 6, primary isoamyl alcohol 0.6 ~ 1.2, methyl acrylate 6 ~ 8, tween 80 1 ~ 2, peanut oil 3 ~ 5, ethanol 4 ~ 8 and water 60; The mixing of second alcohol and water is poured in reactor by preparation method, then methyl acrylate is added, be heated to 60 ~ 70 DEG C of stirring and dissolving, then add 10% ferrum sulfuricum oxydatum solutum, 10% acetic acid solution, primary isoamyl alcohol and terra alba, keep temperature of reaction kettle, adjustment rotating speed 100 ~ 120r/min stirs 20 ~ 30min, finally add tween 80 and peanut oil simultaneously, insulated and stirred 30min is emulsion uniformly, obtains pulvis by funnel suction filtration, namely obtains pulvis flocculation agent after oven dry.
A preparation method for the pear tree fertilizer of liquid state fermentation, is characterized in that, comprises following step:
(1) mixed industrial starch, soyabean expeller, wheat bran, withered leaf and humic acid, add the water of 4 ~ 5 times of its weight parts, ball milling 30 ~ 45min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) complex microorganism bacterial classification is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH5.5 ~ 7, temperature 24 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 5 ~ 7 days;
(3) after (2) complete, pour out fermented liquid and add flocculation agent, spraying saturated limewater after stirring 8 ~ 10min in fermented liquid surface, leave standstill 30 ~ 40min and carry out precipitation adsorption process voluntarily, dry in drier after completing;
(4) by the mixing of the precipitation material described in (3) earthworm soil, potassium primary phosphate, bicarbonate of ammonia, boric acid, quartz sand and other remaining component, pasty state is modulated into, by spray granulating.
Study Tai-Ace S 150, ferric sulfate, iron(ic) chloride, ferrous sulfate by experiment under the effect of saturated limewater to the cohesion of fermented liquid, first stage is mixed with the fermented liquid of excrement of animals a kind of elder generation of four kinds of flocculation agent above, then add saturated limewater and carry out precipitation adsorption, then all the components is transferred in filter bag, with the centrifugal 3 ~ 5min of drier, by for subsequent use for air-dry for gained material rear pulverizing, be the fermented ingredient after cohesion;
Above-mentioned fermented ingredient is added in the ternary compound fertilizer of urea-primary ammonium phosphate-Repone K of 10-10-10 ratio as the additive of Chemical Mixed Fertilizer, for planting common agricultural, agrochemical analytical procedure detects the available nutrient of soil routinely simultaneously, wherein N is 72.4mg/kg, P is 3.4mg/kg, K be 156mg/kg, K is 421mg/kg, organic matter is 18.2g/kg, pH is 5.5.
Compared with un-added chemical fertilizer, Chemical Mixed Fertilizer volume increase 9.5 ~ 11.6% of the present invention, and the mixed organic manure volume increase 14.5% ~ 16.4% of 80% amount of nutrients, can also make the Vc of agricultural-food improve.
In separation test, by being in the test of main component to flocculation agent in 4, prove to adopt ferric sulfate to be the main component of flocculation agent, the flocculating result reached is best, then 10% acetic acid is adopted to have certain promoter action as the separating effect of cohesion medium to inorganic flocculant, but the reaction of acetic acid and fermented liquid is comparatively slow, period, some fermented liquid was overflowed with the bubble of densification, so add primary isoamyl alcohol when preparing flocculation agent as defoamer, adding the minimum terra alba of particle diameter is stablizer, make each composition of ferric sulfate and cohesion promoter action under the cohesive action of methyl acrylate, be adsorbed on the surface of landplaster particle, after all the components has adsorbed, finally adding a certain amount of vegetables oil can effectively prevent flocculation agent particle to be mutually sticked together, become agglomerate, influence effect, particle aggregation agent after completing just can with an overall form storage, transport and use, successful.
Beneficial effect of the present invention: the present invention adopts liquid fermenting formula to ferment, what ferment is more thorough, in the water of the various component dissolves useful to farm crop, recycling special flocculation agent condenses in together, then dries the processing being used for fertilizer, and test proves the absorption that effectively can promote chemical fertilizer NPK, simultaneously through liquid state fermentation, be fermentation speed, efficiency or result is all better than solid state fermentation, the various wastes in life are utilized, realize merchandized handling.
Embodiment
Embodiment 1:
A kind of pear tree fertilizer of liquid state fermentation, it is characterized in that, be made up of the raw material of following weight part (Kg): industrial starch 30, soyabean expeller 35, complex micro organism fungicide 5, wheat bran 45, earthworm soil 20, withered leaf 15, humic acid 6, saturated limewater 18, potassium primary phosphate 12, bicarbonate of ammonia 22, boric acid 8, quartz sand 6, flocculation agent 8 and appropriate water;
Described flocculation agent is made up of the raw material of following weight part: terra alba 15,10% ferrum sulfuricum oxydatum solutum 10,10% acetic acid solution 4, primary isoamyl alcohol 1, methyl acrylate 8, tween 80 1, peanut oil 3, ethanol 6 and water 60; The mixing of second alcohol and water is poured in reactor by preparation method, then methyl acrylate is added, be heated to 60 ~ 70 DEG C of stirring and dissolving, then add 10% ferrum sulfuricum oxydatum solutum, 10% acetic acid solution, primary isoamyl alcohol and terra alba, keep temperature of reaction kettle, adjustment rotating speed 100 ~ 120r/min stirs 20 ~ 30min, finally add tween 80 and peanut oil simultaneously, insulated and stirred 30min is emulsion uniformly, obtains pulvis by funnel suction filtration, namely obtains pulvis flocculation agent after oven dry.
A preparation method for the pear tree fertilizer of liquid state fermentation, is characterized in that, comprises following step:
(1) mixed industrial starch, soyabean expeller, wheat bran, withered leaf and humic acid, add the water of 4 ~ 5 times of its weight parts, ball milling 30 ~ 45min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) complex microorganism bacterial classification is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH5.5 ~ 7, temperature 24 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 5 ~ 7 days;
(3) after (2) complete, pour out fermented liquid and add flocculation agent, spraying saturated limewater after stirring 8 ~ 10min in fermented liquid surface, leave standstill 30 ~ 40min and carry out precipitation adsorption process voluntarily, dry in drier after completing;
(4) by the mixing of the precipitation material described in (3) earthworm soil, potassium primary phosphate, bicarbonate of ammonia, boric acid, quartz sand and other remaining component, pasty state is modulated into, by spray granulating.
The pear tree fertilizer of a kind of liquid state fermentation of the present invention is used for the fertilizer of planting pear tree; select 5 mu of pear tree fields as experimental group, use fertilizer of the present invention to be main fertilizer, 5 mu of pear trees of control group use common fertilizer; the control of other curing conditions and disease and pest is all identical; result shows the pear tree of experimental group, can greatly reduce chemical fertilizer usage quantity, available protecting Soil structure; environmental protection; raw material sources are various, and cost is lower, year economy raising 24.6%.
Claims (2)
1. the pear tree fertilizer of a liquid state fermentation, it is characterized in that, be made up of the raw material of following weight part: industrial starch 30 ~ 35, soyabean expeller 25 ~ 35, complex micro organism fungicide 3 ~ 5, wheat bran 45 ~ 60, earthworm soil 15 ~ 20, withered leaf 10 ~ 15, humic acid 6 ~ 8, saturated limewater 12 ~ 18, potassium primary phosphate 10 ~ 16, bicarbonate of ammonia 20 ~ 25, boric acid 8 ~ 12, quartz sand 4 ~ 6, flocculation agent 7 ~ 10 and appropriate water;
Described flocculation agent is made up of the raw material of following weight part: terra alba 15 ~ 20,10% ferrum sulfuricum oxydatum solutum 10 ~ 14,10% acetic acid solution 4 ~ 6, primary isoamyl alcohol 0.6 ~ 1.2, methyl acrylate 6 ~ 8, tween 80 1 ~ 2, peanut oil 3 ~ 5, ethanol 4 ~ 8 and water 60; The mixing of second alcohol and water is poured in reactor by preparation method, then methyl acrylate is added, be heated to 60 ~ 70 DEG C of stirring and dissolving, then add 10% ferrum sulfuricum oxydatum solutum, 10% acetic acid solution, primary isoamyl alcohol and terra alba, keep temperature of reaction kettle, adjustment rotating speed 100 ~ 120r/min stirs 20 ~ 30min, finally add tween 80 and peanut oil simultaneously, insulated and stirred 30min is emulsion uniformly, obtains pulvis by funnel suction filtration, namely obtains pulvis flocculation agent after oven dry.
2. the preparation method of the pear tree fertilizer of a kind of liquid state fermentation according to claim 1, is characterized in that, comprises following step:
(1) mixed industrial starch, soyabean expeller, wheat bran, withered leaf and humic acid, add the water of 4 ~ 5 times of its weight parts, ball milling 30 ~ 45min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) complex microorganism bacterial classification is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH5.5 ~ 7, temperature 24 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 5 ~ 7 days;
(3) after (2) complete, pour out fermented liquid and add flocculation agent, spraying saturated limewater after stirring 8 ~ 10min in fermented liquid surface, leave standstill 30 ~ 40min and carry out precipitation adsorption process voluntarily, dry in drier after completing;
(4) by the mixing of the precipitation material described in (3) earthworm soil, potassium primary phosphate, bicarbonate of ammonia, boric acid, quartz sand and other remaining component, pasty state is modulated into, by spray granulating.
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Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105523859A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Water-holding fertilizer for dry-land corn planting and preparation method of water-holding fertilizer |
CN105523858A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Peach tree fertilizer capable of supplying nitrogen for long time and preparation method of peach tree fertilizer |
CN105523856A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Organic base fertilizer with long effect for vegetable planting and preparation method thereof |
CN105523860A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Porous bentonite particle adsorptive microbial fertilizer and preparation method thereof |
CN105523857A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Bentonite-particle-adsorbing fertilizer and preparation method thereof |
CN105967818A (en) * | 2016-02-24 | 2016-09-28 | 叶集试验区华农种植专业合作社 | Fertilizer for pear trees in germination stage in spring and manufacturing method of fertilizer |
CN105985094A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Liquid-fermentation organic matter adsorption fertilizer and preparation method thereof |
CN105985189A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Silicate-complexed organic root system fertilizer and preparation method thereof |
CN105985197A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Selenium-rich type slow-release watermelon planting fertilizer and preparation method thereof |
CN105985190A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof |
CN105985191A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Modified-bentonite-adsorption minor element fertilizer and preparation method thereof |
CN107177357A (en) * | 2016-03-12 | 2017-09-19 | 厦门市鲁巴卡生物科技有限公司 | Arenaceous qualitative soil conditioner that a kind of gypsum is made and preparation method thereof |
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EP1077252A1 (en) * | 1998-05-06 | 2001-02-21 | Keijiro Nakamura | Microbial culture liquors containing microorganisms differing in characteristics and living in symbiosis and metabolites thereof, carriers and adsorbents containing the active components of the culture liquors and utilization of the same |
CN103333841A (en) * | 2013-07-11 | 2013-10-02 | 内蒙古永业生物技术有限责任公司 | Highly-active humic acid microbial inoculant and preparation method thereof |
CN103553828A (en) * | 2013-11-12 | 2014-02-05 | 天津北洋百川生物技术有限公司 | Liquid compound biological fertilizer with long shelf life as well as preparation method and application thereof |
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Patent Citations (4)
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EP1077252A1 (en) * | 1998-05-06 | 2001-02-21 | Keijiro Nakamura | Microbial culture liquors containing microorganisms differing in characteristics and living in symbiosis and metabolites thereof, carriers and adsorbents containing the active components of the culture liquors and utilization of the same |
CN103333841A (en) * | 2013-07-11 | 2013-10-02 | 内蒙古永业生物技术有限责任公司 | Highly-active humic acid microbial inoculant and preparation method thereof |
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Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105523859A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Water-holding fertilizer for dry-land corn planting and preparation method of water-holding fertilizer |
CN105523858A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Peach tree fertilizer capable of supplying nitrogen for long time and preparation method of peach tree fertilizer |
CN105523856A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Organic base fertilizer with long effect for vegetable planting and preparation method thereof |
CN105523860A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Porous bentonite particle adsorptive microbial fertilizer and preparation method thereof |
CN105523857A (en) * | 2016-02-23 | 2016-04-27 | 安徽凤阳德诚科技有限公司 | Bentonite-particle-adsorbing fertilizer and preparation method thereof |
CN105985094A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Liquid-fermentation organic matter adsorption fertilizer and preparation method thereof |
CN105985189A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Silicate-complexed organic root system fertilizer and preparation method thereof |
CN105985197A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Selenium-rich type slow-release watermelon planting fertilizer and preparation method thereof |
CN105985190A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Fertilizer capable of efficiently utilizing Chinese herbal medicine extracting solution for adsorption and preparation method thereof |
CN105985191A (en) * | 2016-02-23 | 2016-10-05 | 安徽凤阳德诚科技有限公司 | Modified-bentonite-adsorption minor element fertilizer and preparation method thereof |
CN105967818A (en) * | 2016-02-24 | 2016-09-28 | 叶集试验区华农种植专业合作社 | Fertilizer for pear trees in germination stage in spring and manufacturing method of fertilizer |
CN107177357A (en) * | 2016-03-12 | 2017-09-19 | 厦门市鲁巴卡生物科技有限公司 | Arenaceous qualitative soil conditioner that a kind of gypsum is made and preparation method thereof |
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