CN109824396A - A kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material - Google Patents

A kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material Download PDF

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Publication number
CN109824396A
CN109824396A CN201910247194.8A CN201910247194A CN109824396A CN 109824396 A CN109824396 A CN 109824396A CN 201910247194 A CN201910247194 A CN 201910247194A CN 109824396 A CN109824396 A CN 109824396A
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poultry
livestock
feces
preparation
organic
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张树明
武庆树
张宝民
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Tianjin Shiyide Fertilizer Co Ltd
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Tianjin Shiyide Fertilizer Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

The present invention provides a kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, comprising the following steps: the preparation of raw material;The removal of feces of livestock and poultry heavy metal;The preparation of wormcast;The removal of feces of livestock and poultry antibiotic;Fermentation, is made innoxious organic fertilizer raw material;Using granulating method compound fertilizer producing equipment, first time granulation is carried out;Enter drying machine after carrying out secondary granulation;Material enters cooler;Screening;Qualified product enters coating machine, packaging.The present invention solves the problems, such as antibiotic pollution environment and endangers human health, the secondary fermentation process of use, have the characteristics that ferment effect is good and high-efficient, the fertilizer makes crop yield, improves the effect of crop quality, but also is avoided that pollution and the harm to the mankind brought by heavy metal and antibiotic noxious material, the present invention improves material granulating rate using secondary granulation technology, reduction system drying load, it is energy-saving, solve the problems, such as that organic fertilizer granulating is difficult.

Description

A kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material
Technical field
The present invention relates to a kind of organic and inorganic fertilizer special for vegetable material technical field more particularly to a kind of environmental protection of organic and inorganic The preparation method of environmental pollution free vegetable special fertilizer material.
Background technique
Currently, China's organic-inorganic complex fertilizer majority makees organic matter material using feces of livestock and poultry, using fermentation process into Row processing, this processing mode has obvious effects on the germs such as living body roundworm egg and Escherichia coli, but to heavy metal cadmium, lead, The noxious materials such as arsenic, chromium and antibiotic treatment effect are limited, more than the 800 tons of quinolone drugs that China produces every year, only this Class antibiotic just has half to be used for aquaculture, and the organic-inorganic complex fertilizer produced with such feces of livestock and poultry is by a huge sum of money Belong to the serious pollution with antibiotic, and the influence can have an effect to advanced bio by food chain, to destroy entire raw The balance of state system, poses a threat to human health, and the poultry abuse of antibiotic causes zoonosis to increase, in addition, production Process is to guarantee material granulating effect, needs to be added a large amount of clay as adhesive, be added a large amount of steam and water as at Amount of liquid phase needed for grain, so that the organic matter and nitrogen of fertilizer, phosphorus, potassium nutrition ratio can be only sustained at lower degree, product moisture contains Amount is high, and the easy dusting of resting period long grain influences mechanical application.
Summary of the invention
Present invention seek to address that the deficiencies in the prior art, and a kind of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable is provided The preparation method of material, the secondary fermentation process of use have the characteristics that ferment effect is good and high-efficient, which can not only provide Organic matter and inorganic elements are also rich in middle microelement, reach improvement soil, improve fertilizer efficiency, make crop yield, and article is made in raising The effect of matter, but also it is avoided that pollution and the harm to the mankind brought by heavy metal and antibiotic noxious material.
It is another object of the present invention to improve material granulating rate using secondary granulation technology, system drying load, section are reduced It can lower consumption, solve the problems, such as that organic fertilizer granulating is difficult, not need that the clay for promoting granulating is separately added and supplements a large amount of liquid phases to steam There is nutrient content height, Shui to divide Han Liang≤2.5%, be far below moisture content for vapour or water, prevented from caking and dusting, manufactured product ≤ 12% national standard, the advantage that granule strength is good, at low cost, long time stored particle will not occur and become mildewed and dusting Problem is suitable for mechanical application.
The present invention to achieve the above object, using following technical scheme:
A kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, which is characterized in that including following step It is rapid:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 is soluble in water by oxalic acid, and the mass ratio of oxalic acid and water is 1:3, is sprayed in feces of livestock and poultry, mixes after mixing It is mixed even, stacking 3-5 days, the heavy metal ion in feces of livestock and poultry using oxalic acid soak extraction and is chelated using chemical extraction method;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 45-55%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.08-0.09kg, obtains wormcast, real The harmless treatment of existing heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
Calcium hydroxide is added in the feces of livestock and poultry of step (2) processing and blends uniformly, reaches the pH value of mixed material Between 8.0-9.0, potassium bichromate is added and blends uniformly, pilling up time 5-7 days, the mass ratio of feces of livestock and poultry and potassium bichromate is 100:1.5;
4.2 biological method
Microbial bacterial agent is added in the feces of livestock and poultry handled by step 4.1 and blends uniformly feces of livestock and poultry and micro- life The mass ratio of object microbial inoculum is 1000:3;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and humic acid is uniformly mixed, and obtains the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature scope control is in 70-80 DEG C, outlet temperature scope control is completed to ferment for the first time at 50-60 DEG C, fermentation time 2-3h;
5.3 will complete the material heap wedgewise heap body of fermentation for the first time;
5.4 compost fermentation times were 6-9 days, and every turning in 3 days is primary, completed second and fermented, innoxious organic fertilizer is made Raw material;
(6) granulating method compound fertilizer producing equipment is utilized, by urea, potassium dihydrogen phosphate, potassium sulfate, middle microelement and is passed through The innoxious organic fertilizer raw material of above-mentioned steps preparation is added rotary drum granulator through computer metering and carries out first time granulation, utilizes steam Material granulation process is completed as amount of liquid phase, temperature of charge scope control is at 65-75 DEG C in rotary drum granulator, granulation time 7- 9min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature scope control is at 115-125 DEG C, drying time 40-45min;
(9) material after drying enters cooler, cooling time 35-40min;
(10) material after cooling is sieved through dusting cover and scalping respectively, and dusting cover sieve diameter is between 2.0-2.5mm, scalping Sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover returns to rotary drum granulator after crushing, qualified Product enter coating machine, pack after anti-caking is handled.
Preferably, the mass ratio of the feces of livestock and poultry and calcium hydroxide is 5:1.
Preferably, microbial bacterial agent is the combination of one or both of actinomyces or saccharomycete in the step (4).
Preferably, in the preparation method of the organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material compost fermentation heap Body is the wedge-shaped heap body of width 4m, high 2m, long 16m.
Preferably, the middle microelement is one of calcium, magnesium, sulphur, zinc, iron, boron needed for vegetable growth or several Kind combination.
The beneficial effects of the present invention are: the present invention provides a kind of system of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material Preparation Method using antibiotic in the method for chemistry and biology removal feces of livestock and poultry, solves antibiotic dirt compared with prior art Dye environment and the problem of endangering human health, the secondary fermentation process of use, have the characteristics that ferment effect is good and high-efficient, should Fertilizer can not only provide organic matter and inorganic elements, also be rich in middle microelement, reach improvement soil, improve fertilizer efficiency, make crop Volume increase, improves the effect of crop quality, but also is avoided that brought by heavy metal and antibiotic noxious material and pollutes and to people The harm of class, the present invention improve material granulating rate using secondary granulation technology, reduce system drying load, energy-saving, solve The problem of organic fertilizer granulating difficulty does not need that the clay for promoting granulating and a large amount of liquid phase steam of supplement or water is separately added, is not easy Agglomeration and dusting, there is manufactured product nutrient content height, Shui to divide Han Liang≤2.5%, far below the state that Shui divides Han Liang≤12% Family standard, the advantage that granule strength is good, at low cost, long time stored particle will not occur and become mildewed and the problem of dusting, be applicable in It is applied in machinery, it is low to solve organic and inorganic fertilizer special for vegetable material product nitrogen, phosphorus, potassium nutrition content made from traditional granulating method, Product moisture is high, and Source Organic Matter contains heavy metal cadmium, lead, arsenic, chromium and antibiotic harmful substance, causes environmental pollution and harm The problem of public hazards of human health.
Detailed description of the invention
Fig. 1 is the flow chart of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material of the present invention preparation;
It is described in detail below with reference to the embodiment of the present invention referring to attached drawing.
Specific embodiment
Below with reference to embodiment, the invention will be further described:
A kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, which is characterized in that including following step It is rapid:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 is soluble in water by oxalic acid, and the mass ratio of oxalic acid and water is 1:3, is sprayed in feces of livestock and poultry, mixes after mixing It is mixed even, stacking 3-5 days, the heavy metal ion in feces of livestock and poultry using oxalic acid soak extraction and is chelated using chemical extraction method;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 45-55%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.08-0.09kg, obtains wormcast, real The harmless treatment of existing heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
Calcium hydroxide is added in the feces of livestock and poultry of step (2) processing and blends uniformly, reaches the pH value of mixed material Between 8.0-9.0, potassium bichromate is added and blends uniformly, pilling up time 5-7 days, the mass ratio of feces of livestock and poultry and potassium bichromate is 100:1.5;
4.2 biological method
Microbial bacterial agent is added in the feces of livestock and poultry handled by step 4.1 and blends uniformly feces of livestock and poultry and micro- life The mass ratio of object microbial inoculum is 1000:3;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and humic acid is uniformly mixed, and obtains the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature scope control is in 70-80 DEG C, outlet temperature scope control is completed to ferment for the first time at 50-60 DEG C, fermentation time 2-3h;
5.3 will complete the material heap wedgewise heap body of fermentation for the first time;
5.4 compost fermentation times were 6-9 days, and every turning in 3 days is primary, completed second and fermented, innoxious organic fertilizer is made Raw material;
(6) granulating method compound fertilizer producing equipment is utilized, by urea, potassium dihydrogen phosphate, potassium sulfate, middle microelement and is passed through The innoxious organic fertilizer raw material of above-mentioned steps preparation is added rotary drum granulator through computer metering and carries out first time granulation, utilizes steam Material granulation process is completed as amount of liquid phase, temperature of charge scope control is at 65-75 DEG C in rotary drum granulator, granulation time 7- 9min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature scope control is at 115-125 DEG C, drying time 40-45min;
(9) material after drying enters cooler, cooling time 35-40min;
(10) material after cooling is sieved through dusting cover and scalping respectively, and dusting cover sieve diameter is between 2.0-2.5mm, scalping Sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover returns to rotary drum granulator after crushing, qualified Product enter coating machine, pack after anti-caking is handled.
Preferably, the mass ratio of the feces of livestock and poultry and calcium hydroxide is 5:1.
Preferably, microbial bacterial agent is the combination of one or both of actinomyces or saccharomycete in the step (4).
Preferably, in the preparation method of the organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material compost fermentation heap Body is the wedge-shaped heap body of width 4m, high 2m, long 16m.
Preferably, the middle microelement is one of calcium, magnesium, sulphur, zinc, iron, boron needed for vegetable growth or several Kind combination.
Embodiment 1
Organic to one kind provided in this embodiment for preparing 1 ton of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material- Inorganic environment-friendly environmental pollution free vegetable special fertilizer material to prepare specific production procedure as follows:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 are dissolved in 20 kilograms of oxalic acid in 60 kg of water, are sprayed in 200 kilograms of feces of livestock and poultry after mixing, blending Uniformly, it stacks 3 days, the heavy metal ion in feces of livestock and poultry using oxalic acid soak extraction and is chelated using chemical extraction method;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 45%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.08kg, obtain 40 kilograms of wormcasts, Realize the harmless treatment of heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
40 kilograms of calcium hydroxides are added in the feces of livestock and poultry of step (2) processing and blend uniformly, make the pH of mixed material Value reaches 8.0, and 3 kilograms of potassium bichromates are added and blend uniformly, pilling up time 5 days;
4.2 biological method
0.6 kilogram of actinomyces is added in the feces of livestock and poultry handled by step 4.1 and blends uniform;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and 100 kilograms of humic acids are uniformly mixed, and obtain the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature is 70 DEG C, outlet temperature It is 50 DEG C, fermentation time 2h, completes to ferment for the first time;
The material for completing fermentation for the first time is piled wide 4m, the wedge-shaped heap body of high 2m, long 16m by 5.3;
5.4 compost fermentation times were 6 days, and every turning in 3 days is primary, completed second and fermented, it is former that innoxious organic fertilizer is made Material;
(6) granulating method compound fertilizer producing equipment is utilized, by 280 kilograms of urea, 240 kg of phosphoric acid potassium dihydrogens, 60 kilograms of sulphur Sour potassium, 20 kilograms of calcics, magnesium, the middle microelement of sulphur and the innoxious organic fertilizer raw material for preparing through the above steps are through microcomputer meter Amount is added rotary drum granulator and carries out first time granulation, uses steam as amount of liquid phase and completes material granulation process, rotary drum granulator Interior temperature of charge is 65 DEG C, granulation time 9min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature is 115 DEG C, drying time 45min;
(9) material after drying enters cooler, cooling time 35min;
(10) material after cooling is sieved through dusting cover and scalping respectively, dusting cover sieve diameter 2.0mm, scalping sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover return to rotary drum granulator after crushing, and qualified product enters packet Film machine is packed after anti-caking is handled.
Embodiment 2
Organic to one kind provided in this embodiment for preparing 1 ton of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material- Inorganic environment-friendly environmental pollution free vegetable special fertilizer material to prepare specific production procedure as follows:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 are dissolved in 20 kilograms of oxalic acid in 60 kg of water, are sprayed in 250 kilograms of feces of livestock and poultry after mixing, blending Uniformly, it stacks 5 days, the heavy metal ion in feces of livestock and poultry using oxalic acid soak extraction and is chelated using chemical extraction method;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 55%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.09kg, obtain 50 kilograms of wormcasts, Realize the harmless treatment of heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
50 kilograms of calcium hydroxides are added in the feces of livestock and poultry of step (2) processing and blend uniformly, make the pH of mixed material Value reaches 9.0, and 3.75 kilograms of potassium bichromates are added and blend uniformly, pilling up time 7 days;
4.2 biological method
0.75 kilogram of saccharomycete is added in the feces of livestock and poultry handled by step 4.1 and blends uniform;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and 130 kilograms of humic acids are uniformly mixed, and obtain the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature is 80 DEG C, outlet temperature It is 60 DEG C, fermentation time 2h, completes to ferment for the first time;
The material for completing fermentation for the first time is piled wide 4m, the wedge-shaped heap body of high 2m, long 16m by 5.3;
5.4 compost fermentation times were 9 days, and every turning in 3 days is primary, completed second and fermented, it is former that innoxious organic fertilizer is made Material;
(6) granulating method compound fertilizer producing equipment is utilized, by 200 kilograms of urea, 190 kg of phosphoric acid potassium dihydrogens, 90 kilograms of sulphur Sour potassium, 20 kilograms containing zinc, iron, the middle microelement of boron and through the above steps the innoxious organic fertilizer raw material for preparing through microcomputer meter Amount is added rotary drum granulator and carries out first time granulation, uses steam as amount of liquid phase and completes material granulation process, rotary drum granulator Interior temperature of charge is 75 DEG C, granulation time 7min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature is 125 DEG C, drying time 40min;
(9) material after drying enters cooler, cooling time 40min;
(10) material after cooling is sieved through dusting cover and scalping respectively, dusting cover sieve diameter 2.5mm, scalping sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover return to rotary drum granulator after crushing, and qualified product enters packet Film machine is packed after anti-caking is handled.
Embodiment 3
Organic to one kind provided in this embodiment for preparing 1 ton of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material- Inorganic environment-friendly environmental pollution free vegetable special fertilizer material to prepare specific production procedure as follows:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 are dissolved in 30 kilograms of oxalic acid in 90 kg of water, are sprayed in 225 kilograms of feces of livestock and poultry after mixing, blending Uniformly, it stacks 4 days, the heavy metal ion in feces of livestock and poultry using oxalic acid soak extraction and is chelated using chemical extraction method;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 50%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.085kg, obtain 70 kilograms of wormcasts, Realize the harmless treatment of heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
45 kilograms of calcium hydroxides are added in the feces of livestock and poultry of step (2) processing and blend uniformly, make the pH of mixed material Value reaches 8.5, and 3.375 kilograms of potassium bichromates are added and blend uniformly, pilling up time 6 days;
4.2 biological method
0.675 kilogram of actinomyces is added in the feces of livestock and poultry handled by step 4.1 and blends uniform;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and 110 kilograms of humic acids are uniformly mixed, and obtain the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature is 75 DEG C, outlet temperature It is 55 DEG C, fermentation time 2.5h, completes to ferment for the first time;
The material for completing fermentation for the first time is piled wide 4m, the wedge-shaped heap body of high 2m, long 16m by 5.3;
5.4 compost fermentation times were 9 days, and every turning in 3 days is primary, completed second and fermented, it is former that innoxious organic fertilizer is made Material;
(6) granulating method compound fertilizer producing equipment is utilized, by 200 kilograms of urea, 220 kg of phosphoric acid potassium dihydrogens, 60 kilograms of sulphur Sour potassium, 40 kilograms containing magnesium, sulphur, the middle microelement of zinc and through the above steps the innoxious organic fertilizer raw material for preparing through microcomputer meter Amount is added rotary drum granulator and carries out first time granulation, uses steam as amount of liquid phase and completes material granulation process, rotary drum granulator Interior temperature of charge is 70 DEG C, granulation time 8min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature is 120 DEG C, drying time 43min;
(9) material after drying enters cooler, cooling time 38min;
(10) material after cooling is sieved through dusting cover and scalping respectively, dusting cover sieve diameter 2.2mm, scalping sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover return to rotary drum granulator after crushing, and qualified product enters packet Film machine is packed after anti-caking is handled.
Embodiment 4
Organic to one kind provided in this embodiment for preparing 1 ton of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material- Inorganic environment-friendly environmental pollution free vegetable special fertilizer material to prepare specific production procedure as follows:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 are dissolved in 20 kilograms of oxalic acid in 60 kg of water, are sprayed at 200 kilograms of feces of livestock and poultry after mixing (containing organic Matter mass percent be 40%) in, blending uniformly, is stacked 3 days, using chemical extraction method using oxalic acid soak extraction and chelating poultry Heavy metal ion in poultry manure;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 45%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.08kg, obtain 40 kilograms of wormcasts (mass percent containing organic matter is 35%), realizes the harmless treatment of heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
40 kilograms of calcium hydroxides are added in the feces of livestock and poultry of step (2) processing and blend uniformly, make the pH of mixed material Value reaches 8.0, and 3 kilograms of potassium bichromates are added and blend uniformly, pilling up time 5 days;
4.2 biological method
0.4 kilogram of actinomyces and 0.2 kilogram of saccharomycete are added in the feces of livestock and poultry handled by step 4.1 and blends equal It is even;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and 100 kilograms of humic acids are uniformly mixed, and obtain the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature is 75 DEG C, outlet temperature It is 55 DEG C, fermentation time 2.5h, completes to ferment for the first time;
The material for completing fermentation for the first time is piled wide 4m, the wedge-shaped heap body of high 2m, long 16m by 5.3;
5.4 compost fermentation times were 6 days, and every turning in 3 days is primary, completed second and fermented, it is former that innoxious organic fertilizer is made Material;
(6) granulating method compound fertilizer producing equipment is utilized, by 217 kilograms of urea (mass percent containing N is 46.2%), 200 Kg of phosphoric acid potassium dihydrogen (contains P2O5Mass percent is 52%, K2O mass percent be 34%), 158 kilograms of potassium sulfates (contain K2O 52%) mass percent is, the middle microelement of 25 kilograms of sulfur-bearings, zinc, boron and prepares through the above steps innoxious organic Fertile raw material is added rotary drum granulator through computer metering and carries out first time granulation, uses steam as amount of liquid phase and completes material granulation mistake Journey, temperature of charge is 70 DEG C in rotary drum granulator, granulation time 8min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature scope control is at 120 DEG C, drying time 40min;
(9) material after drying enters cooler, cooling time 35min;
(10) material after cooling is sieved through dusting cover and scalping respectively, dusting cover sieve diameter 2.5mm, scalping sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover return to rotary drum granulator after crushing, and qualified product enters packet Film machine is packed after anti-caking is handled, and is detected, and total nutrient content 35.4% is made, wherein containing N-P2O5-K2O is 10.0%-10.4%-15.0%, the content of organic matter 15.9% contain middle microelement, moisture content 2.3%, 2.5mm granularity 97% Organic-inorganic fertilizer product.
Embodiment 5
Organic to one kind provided in this embodiment for preparing 1 ton of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material- Inorganic environment-friendly environmental pollution free vegetable special fertilizer material to prepare specific production procedure as follows:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 are dissolved in 25 kilograms of oxalic acid in 75 kg of water, are sprayed at 200 kilograms of feces of livestock and poultry after mixing (containing organic Matter mass percent be 40%) in, blending uniformly, is stacked 5 days, using chemical extraction method using oxalic acid soak extraction and chelating poultry Heavy metal ion in poultry manure;
2.2 treated feces of livestock and poultry is dehydrated by sludge dewatering equipment, remove the heavy metal that contains in feces of livestock and poultry from The waste water of son, obtains moisture content 55%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, be made be suitble to The earthworm base-material of earthworm growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.09kg, obtain 45 kilograms of wormcasts (quality of organic matter percentage is 35%), realizes the harmless treatment of heavy metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
40 kilograms of calcium hydroxides are added in the feces of livestock and poultry of step (2) processing and blend uniformly, make the pH of mixed material Value reaches 9.0, and 3 kilograms of potassium bichromates are added and blend uniformly, pilling up time 7 days;
4.2 biological method
0.3 kilogram of actinomyces and 0.3 kilogram of saccharomycete are added in the feces of livestock and poultry handled by step 4.1 and blends equal It is even;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) make Standby wormcast and 110 kilograms of humic acids are uniformly mixed, and obtain the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, and fermentation roller inlet temperature is 80 DEG C, outlet temperature It is 60 DEG C, fermentation time 2h, completes to ferment for the first time;
The material for completing fermentation for the first time is piled wide 4m, the wedge-shaped heap body of high 2m, long 16m by 5.3;
5.4 compost fermentation times were 9 days, and every turning in 3 days is primary, completed second and fermented, it is former that innoxious organic fertilizer is made Material;
(6) granulating method compound fertilizer producing equipment is utilized, by 260 kilograms of urea (mass percent containing N is 46.2%), 230 Kg of phosphoric acid potassium dihydrogen (contains P2O5Mass percent is 52%, K2O mass percent be 34%), 65 kilograms of potassium sulfates (contain K2O Mass percent be 52%), 25 kilograms containing magnesium, sulphur, the middle microelement of iron and through the above steps prepare it is innoxious organic Fertile raw material is added rotary drum granulator through computer metering and carries out first time granulation, uses steam as amount of liquid phase and completes material granulation mistake Journey, temperature of charge is 75 DEG C in rotary drum granulator, granulation time 8min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature scope control is at 125 DEG C, drying time 45min;
(9) material after drying enters cooler, cooling time 40min;
(10) material after cooling is sieved through dusting cover and scalping respectively, dusting cover sieve diameter 2.5mm, scalping sieve diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover return to rotary drum granulator after crushing, and qualified product enters packet Film machine is packed after anti-caking is handled, and is detected, and total nutrient content 35.2% is made, wherein containing N-P2O5-K2O is 12.0%-12.0%-11.2%, the content of organic matter 16.5% contain middle microelement, moisture content 2.0%, 4.5mm granularity 98% Organic-inorganic fertilizer product.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above, As long as using the various improvement that the inventive concept and technical scheme of the present invention carry out, or not improved directly apply to other fields It closes, it is within the scope of the present invention.

Claims (5)

1. a kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, which comprises the following steps:
(1) preparation of raw material
By mass percentage, raw material feed intake it is as follows:
(2) removal of feces of livestock and poultry heavy metal
2.1 is soluble in water by oxalic acid, and the mass ratio of oxalic acid and water is 1:3, is sprayed in feces of livestock and poultry after mixing, and blending is equal It is even, it stacks 3-5 days, the heavy metal ion in feces of livestock and poultry using oxalic acid soak extraction and is chelated using chemical extraction method;
2.2 are dehydrated treated feces of livestock and poultry by sludge dewatering equipment, remove the heavy metal ion contained in feces of livestock and poultry Waste water obtains moisture content 45-55%, removes the feces of livestock and poultry of removing heavy metals;
(3) preparation of wormcast
3.1 by the effluent containing heavy metal ions in step (2) be added to cow dung, soya-bean cake, vinasse mixture in, suitable earthworm is made The earthworm base-material of growth and breeding;
3.2 are put into earthworm in proportion in earthworm base-material, and injected volume is every cube of 0.08-0.09kg, obtain wormcast, realize weight The harmless treatment of metal ion;
(4) removal of feces of livestock and poultry antibiotic
4.1 chemical method
Calcium hydroxide is added in the feces of livestock and poultry of step (2) processing and blends uniformly, the pH value of mixed material is made to reach 8.0- Between 9.0, potassium bichromate is added and blends uniformly, pilling up time 5-7 days, the mass ratio of feces of livestock and poultry and potassium bichromate is 100: 1.5;
4.2 biological method
Microbial bacterial agent is added in the feces of livestock and poultry handled by step 4.1 and blends uniformly, feces of livestock and poultry and microbial bacteria The mass ratio of agent is 1000:3;
(5) it ferments
5.1 by the feces of livestock and poultry for removing removing heavy metals and antibiotic prepared through the above steps, through the above steps (3) preparation Wormcast and humic acid are uniformly mixed, and obtain the mixed material for fermentation;
5.2 are added to mixed material to be fermented in fermentation roller, fermentation roller inlet temperature scope control at 70-80 DEG C, Outlet temperature scope control is completed to ferment for the first time at 50-60 DEG C, fermentation time 2-3h;
5.3 will complete the material heap wedgewise heap body of fermentation for the first time;
5.4 compost fermentation times were 6-9 days, and every turning in 3 days is primary, completed second and fermented, innoxious organic fertilizer raw material is made;
(6) granulating method compound fertilizer producing equipment is utilized, by urea, potassium dihydrogen phosphate, potassium sulfate, middle microelement and is passed through above-mentioned The innoxious organic fertilizer raw material of step preparation is added rotary drum granulator through computer metering and carries out first time granulation, uses steam as Amount of liquid phase completes material granulation process, and temperature of charge scope control is at 65-75 DEG C in rotary drum granulator, granulation time 7-9min;
(7) material after being granulated for the first time enters after granulating disc carries out secondary granulation and enters drying machine;
(8) drying machine inlet temperature scope control is at 115-125 DEG C, drying time 40-45min;
(9) material after drying enters cooler, cooling time 35-40min;
(10) material after cooling is sieved through dusting cover and scalping respectively, and dusting cover sieve diameter is between 2.0-2.5mm, scalping sieve pore Diameter 4.5mm, the bulky grain after granular material and scalping screening after dusting cover return to rotary drum granulator after crushing, qualified product into Enter coating machine, is packed after anti-caking is handled.
2. a kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, feature exist according to claim 1 In the mass ratio of the feces of livestock and poultry and calcium hydroxide is 5:1.
3. a kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, feature exist according to claim 1 In microbial bacterial agent is the combination of one or both of actinomyces or saccharomycete in the step (4).
4. a kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, feature exist according to claim 1 In, in the preparation method of the organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material heap body of compost fermentation be width 4m, high 2m, The wedge-shaped heap body of long 16m.
5. a kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material, feature exist according to claim 1 In the middle microelement is the combination of one or more of calcium, magnesium, sulphur, zinc, iron, boron needed for vegetable growth.
CN201910247194.8A 2019-03-29 2019-03-29 A kind of preparation method of organic and inorganic environmental protection and public nuisance free fertilizer special for vegetable material Pending CN109824396A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110833016A (en) * 2019-12-09 2020-02-25 和县农丰龙虾养殖专业合作社 Vegetable seed grading cultivation method
CN111217624A (en) * 2020-01-16 2020-06-02 福建省田伯生物肥有限公司 Preparation method of antibiotic-free high-quality organic fertilizer for livestock and poultry manure
CN111233583A (en) * 2020-03-23 2020-06-05 汤秋华 Composite organic granular fertilizer containing rich ionic nutrients and preparation method thereof
CN111517887A (en) * 2020-04-20 2020-08-11 张瑞霞 Efficient production method of granular organic fertilizer

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2125168A1 (en) * 1971-02-16 1972-09-29 Cidr Complete fertilizer - by continuous composting of waste organic matter with added complete mineral fertilizer
CN107459425A (en) * 2017-08-09 2017-12-12 天津益农赢丰生态科技有限公司 A kind of high-activity straw organic and inorganic fertilizer and preparation method
CN109206169A (en) * 2018-11-22 2019-01-15 天津市大环生物肥料有限公司 A kind of feces of livestock and poultry environment-protecting type organic fertilizer and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2125168A1 (en) * 1971-02-16 1972-09-29 Cidr Complete fertilizer - by continuous composting of waste organic matter with added complete mineral fertilizer
CN107459425A (en) * 2017-08-09 2017-12-12 天津益农赢丰生态科技有限公司 A kind of high-activity straw organic and inorganic fertilizer and preparation method
CN109206169A (en) * 2018-11-22 2019-01-15 天津市大环生物肥料有限公司 A kind of feces of livestock and poultry environment-protecting type organic fertilizer and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
印遇龙 等: "《改革开放40年中国猪业发展与进步 猪场废弃物处理和资源化利用》", 31 October 2018, 中国农业大学出版社 *
吴长航 等: "《环境保护概论》", 31 May 2017, 冶金工业出版社 *
张明露 等: "《饮用水微生物检验技术》", 31 August 2015, 中国环境出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110833016A (en) * 2019-12-09 2020-02-25 和县农丰龙虾养殖专业合作社 Vegetable seed grading cultivation method
CN111217624A (en) * 2020-01-16 2020-06-02 福建省田伯生物肥有限公司 Preparation method of antibiotic-free high-quality organic fertilizer for livestock and poultry manure
CN111233583A (en) * 2020-03-23 2020-06-05 汤秋华 Composite organic granular fertilizer containing rich ionic nutrients and preparation method thereof
CN111517887A (en) * 2020-04-20 2020-08-11 张瑞霞 Efficient production method of granular organic fertilizer

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Application publication date: 20190531