CN105796427B - A kind of preparation method of ice plant extract - Google Patents
A kind of preparation method of ice plant extract Download PDFInfo
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- CN105796427B CN105796427B CN201610225468.XA CN201610225468A CN105796427B CN 105796427 B CN105796427 B CN 105796427B CN 201610225468 A CN201610225468 A CN 201610225468A CN 105796427 B CN105796427 B CN 105796427B
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- 235000009071 Mesembryanthemum crystallinum Nutrition 0.000 title claims abstract description 14
- 239000000419 plant extract Substances 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 240000006236 Martynia annua Species 0.000 title abstract 2
- 238000001914 filtration Methods 0.000 claims abstract description 20
- 238000005360 mashing Methods 0.000 claims abstract description 11
- 238000012545 processing Methods 0.000 claims abstract description 11
- 230000008014 freezing Effects 0.000 claims abstract description 7
- 238000007710 freezing Methods 0.000 claims abstract description 7
- 238000004140 cleaning Methods 0.000 claims abstract description 6
- 239000000706 filtrate Substances 0.000 claims description 39
- 239000000463 material Substances 0.000 claims description 14
- 241000196324 Embryophyta Species 0.000 claims description 13
- 244000025254 Cannabis sativa Species 0.000 claims description 12
- 244000021685 Mesembryanthemum crystallinum Species 0.000 claims description 12
- 239000006260 foam Substances 0.000 claims description 10
- 239000012535 impurity Substances 0.000 claims description 10
- 238000011085 pressure filtration Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 229930002875 chlorophyll Natural products 0.000 claims description 5
- 235000019804 chlorophyll Nutrition 0.000 claims description 5
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 claims description 5
- 239000000084 colloidal system Substances 0.000 claims description 5
- 239000003792 electrolyte Substances 0.000 claims description 5
- 238000005562 fading Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- YAVVGPBYBUYPSR-UHFFFAOYSA-N benzene;oxygen Chemical compound [O].C1=CC=CC=C1 YAVVGPBYBUYPSR-UHFFFAOYSA-N 0.000 claims description 4
- 235000019441 ethanol Nutrition 0.000 claims 1
- 239000002537 cosmetic Substances 0.000 abstract description 9
- 238000000034 method Methods 0.000 abstract description 7
- 150000001413 amino acids Chemical class 0.000 abstract description 5
- 230000009286 beneficial effect Effects 0.000 abstract description 4
- 239000011148 porous material Substances 0.000 abstract description 4
- 230000008569 process Effects 0.000 abstract description 4
- 239000000516 sunscreening agent Substances 0.000 abstract description 4
- 239000011782 vitamin Substances 0.000 abstract description 4
- 229940088594 vitamin Drugs 0.000 abstract description 4
- 229930003231 vitamin Natural products 0.000 abstract description 4
- 235000013343 vitamin Nutrition 0.000 abstract description 4
- 150000003722 vitamin derivatives Chemical class 0.000 abstract description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 3
- 239000011707 mineral Substances 0.000 abstract description 3
- 230000003020 moisturizing effect Effects 0.000 abstract description 3
- 238000007670 refining Methods 0.000 abstract description 3
- 230000001835 salubrious effect Effects 0.000 abstract description 3
- 239000004910 After sun product Substances 0.000 abstract description 2
- 238000000605 extraction Methods 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 230000000475 sunscreen effect Effects 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 11
- 230000036541 health Effects 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 239000000243 solution Substances 0.000 description 6
- 241000283977 Oryctolagus Species 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000284 extract Substances 0.000 description 4
- 239000002366 mineral element Substances 0.000 description 4
- 239000004744 fabric Substances 0.000 description 3
- 206010015946 Eye irritation Diseases 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 231100000490 OECD 405 Acute Eye Irritation/Corrosion Toxicity 0.000 description 2
- 206010040880 Skin irritation Diseases 0.000 description 2
- 230000001154 acute effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 231100000013 eye irritation Toxicity 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 231100000475 skin irritation Toxicity 0.000 description 2
- 230000036556 skin irritation Effects 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 1
- 241000219479 Aizoaceae Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 210000000744 eyelid Anatomy 0.000 description 1
- GNBHRKFJIUUOQI-UHFFFAOYSA-N fluorescein Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC=C(O)C=C1OC1=CC(O)=CC=C21 GNBHRKFJIUUOQI-UHFFFAOYSA-N 0.000 description 1
- 229940020947 fluorescein sodium Drugs 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000000622 irritating effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of preparation methods of ice plant extract, include the following steps：S1, picking；S2, cleaning equipment；S3, mashing processing；S4, centrifugal treating；S5, primary filtering；S6, secondary filter；S7, it filters three times；S8, four filterings；S9, it weighs.The advantage of the invention is that：It is simple for process, whole process does not use solvent, extraction process uses cryogenic freezing and normal-temperature operation, have the characteristics that working substance can be made completely to retain, wherein it has been rich in the nutriments such as a large amount of minerals, amino acid, vitamin, the extracting solution of the present invention can be used for the various sunscreen products of cosmetics, after-sun product, releive, calm skin class product, sensibility skin reparation product, salubrious moisturizing product, pore refining product, create considerable beneficial value.
Description
Technical field
The present invention relates to Cosmetic Manufacture technical field, specially a kind of preparation method of ice plant extract.
Background technology
Ice plant is commonly called as ice leaf grass.Belong to Aizoaceae (Aizoaseae), cat-chop class plant is annual or 2 years
Raw herbaceous plant is a kind of plant grown in the nano-cloth Namib deserts in South Africa, and it is most ancient that nano-cloth desert is referred to as the whole world
Always, one of most arid desert.Nano-cloth Namib deserts daylight is strong, and ice plant passes through the strong photograph of ultraviolet light
After penetrating, a kind of ice crystal of similar salt grain of rhizome Surface Creation, the fresh and tender succulence of leaf can be eaten raw, often be made in France arranges
With there is salt capsule on blade face, and entrance has saline taste, and is then mostly used for ornamental plantation in China.
At present, there is no the ice leaf grass extracting solutions of complete effective ingredient in the market.
Invention content
The purpose of the present invention is to provide a kind of preparation method of ice plant extract, to solve above-mentioned background technology
The problem of middle proposition.
To achieve the above object, the present invention provides following technical solution：A kind of preparation method of ice plant extract,
Include the following steps：
S1, picking：Fresh ice leaf grass is picked, impurity is removed, is placed in insulating foam case so that insulating foam the temperature inside the box
At 25 degrees Celsius hereinafter, and being sent in 24 hours to processing factory；
S2, cleaning equipment：All devices are cleaned, are sterilized, it is dry；
S3, mashing processing：Colloid mill mashing is crossed after ice leaf grass is weighed, 1.0~5.0%K350 is added, stirs evenly；
S4, centrifugal treating：Remove filter residue with centrifuge, then stand 24~72 hours, obtain material body；
S5, primary filtering：The material body that step S4 is obtained with 100~500 mesh filter plants is filtered, collects filtrate,
Then coarse filtration liquid is irradiated 24~72 hours with light irradiation device, until it is light yellow that chlorophyll is made, which to decompose colour fading,；
S6, secondary filter：The filtrate that step S5 is obtained, freezing thermostat is at 2~10 degrees Celsius, holding 2~8 hours, so
It is filtered afterwards with 400~1000 mesh filter plants, collects filtrate；
S7, it filters three times：The filtrate Medium speed filter paper that step S6 is obtained, and with frame plate filter pressure filtration, receive
Take filtrate；
S8, four filterings：By 0.15~0.35 micron of miillpore filter of the filtrate that step S7 is obtained, and with deckle board formula mistake
Filter pressure filtration removes micron order impurity and partial electrolyte, collects filtrate；
S9, it weighs：The obtained filtrates of step S8 are weighed, calculates yield, is sealed.
The K350 is the mixture of Phenoxyethanol and Sensiva SC50.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention have it is simple for process, whole process without using solvent,
Extraction process uses cryogenic freezing and normal-temperature operation, has the characteristics that working substance can be made completely to retain, wherein being rich in a large amount of
The nutriments such as minerals, amino acid, vitamin.The a variety of natural activity mineral elements being rich in have ultraviolet light irradiation strong
Strong protective action, being used cooperatively with sun-screening agent has apparent synergy preventing ultraviolet effect.Contain various amino acid and Wei Sheng
Element has repair to impaired skin.Patch skin has unique slight cool feeling, with reference to its active mineral element, to pore refining
It is of miraculous efficacy, creates smooth careful skin.The extracting solution of the present invention can be used for the various sunscreen products of cosmetics, solarization
Product is repaired afterwards, is releived, calm skin class product, sensibility skin reparation product, salubrious moisturizing product, pore refining product,
Create considerable beneficial value.
Specific embodiment
Below in conjunction with embodiment, the technical solution in the embodiment of the present invention is clearly and completely described, it is clear that
Described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based on the implementation in the present invention
Example, those of ordinary skill in the art's all other embodiments obtained without making creative work, belongs to
The scope of protection of the invention.
【Embodiment 1】
A kind of preparation method of ice plant extract, includes the following steps：
S1, picking：The fresh ice leaf grass of 50 kilograms of picking, removes impurity, is placed in insulating foam case so that insulating foam case
Interior temperature is at 25 degrees Celsius hereinafter, and being sent in 24 hours to processing factory；
S2, cleaning equipment：All devices are cleaned, are sterilized, it is dry；
S3, mashing processing：Colloid mill mashing is crossed after ice leaf grass is weighed, adds 1.0%K350, the K350 is benzene oxygen second
The mixture of alcohol and Sensiva SC50, stirs evenly；
S4, centrifugal treating：Remove filter residue with centrifuge, then stand 24 hours, obtain material body；
S5, primary filtering：The material body that step S4 is obtained with 100 mesh filter plants is filtered, collects filtrate, Ran Houyong
Light irradiation device irradiation coarse filtration liquid 24 hours, until it is light yellow that chlorophyll is made, which to decompose colour fading,；
S6, secondary filter：The filtrate that step S5 is obtained, freezing thermostat are kept for 2 hours, at 2 degrees Celsius then with 400
Filter plant is filtered, and collects filtrate；
S7, it filters three times：The filtrate Medium speed filter paper that step S6 is obtained, and with frame plate filter pressure filtration, receive
Take filtrate；
S8, four filterings：By 0.15 micron of miillpore filter of the filtrate that step S7 is obtained, and added with frame plate filter
Press filtration removes micron order impurity and partial electrolyte, collects filtrate；
S9, it weighs：The obtained filtrates of step S8 are weighed, calculates yield, is sealed.The yield of the present embodiment is
89%.
【Embodiment 2】
A kind of preparation method of ice plant extract, includes the following steps：
S1, picking：Fresh ice leaf grass is picked, impurity is removed, is placed in insulating foam case so that insulating foam the temperature inside the box
At 25 degrees Celsius hereinafter, and being sent in 24 hours to processing factory；
S2, cleaning equipment：All devices are cleaned, are sterilized, it is dry；
S3, mashing processing：Colloid mill mashing is crossed after ice leaf grass is weighed, adds 3.0%K350, the K350 is benzene oxygen second
The mixture of alcohol and Sensiva SC50, stirs evenly；
S4, centrifugal treating：Remove filter residue with centrifuge, then stand 48 hours, obtain material body；
S5, primary filtering：The material body that step S4 is obtained with 300 mesh filter plants is filtered, collects filtrate, Ran Houyong
Light irradiation device irradiation coarse filtration liquid 48 hours, until it is light yellow that chlorophyll is made, which to decompose colour fading,；
S6, secondary filter：The filtrate that step S5 is obtained, freezing thermostat are kept for 5 hours, at 6 degrees Celsius then with 700
Mesh filter plant is filtered, and collects filtrate；
S7, it filters three times：The filtrate Medium speed filter paper that step S6 is obtained, and with frame plate filter pressure filtration, receive
Take filtrate；
S8, four filterings：By 0.25 micron of miillpore filter of the filtrate that step S7 is obtained, and added with frame plate filter
Press filtration removes micron order impurity and partial electrolyte, collects filtrate；
S9, it weighs：The obtained filtrates of step S8 are weighed, calculates yield, is sealed.The yield of the present embodiment is
91%.
【Embodiment 3】
A kind of preparation method of ice plant extract, includes the following steps：
S1, picking：Fresh ice leaf grass is picked, impurity is removed, is placed in insulating foam case so that insulating foam the temperature inside the box
At 25 degrees Celsius hereinafter, and being sent in 24 hours to processing factory；
S2, cleaning equipment：All devices are cleaned, are sterilized, it is dry；
S3, mashing processing：Colloid mill mashing is crossed after ice leaf grass is weighed, adds 5.0%K350, the K350 is benzene oxygen second
The mixture of alcohol and Sensiva SC50, stirs evenly；
S4, centrifugal treating：Remove filter residue with centrifuge, then stand 72 hours, obtain material body；
S5, primary filtering：The material body that step S4 is obtained with 500 mesh filter plants is filtered, collects filtrate, Ran Houyong
Light irradiation device irradiation coarse filtration liquid 72 hours, until it is light yellow that chlorophyll is made, which to decompose colour fading,；
S6, secondary filter：The filtrate that step S5 is obtained, freezing thermostat are kept for 8 hours, Ran Houyong at 10 degrees Celsius
1000 mesh filter plants are filtered, and collect filtrate；
S7, it filters three times：The filtrate Medium speed filter paper that step S6 is obtained, and with frame plate filter pressure filtration, receive
Take filtrate；
S8, four filterings：By 0.35 micron of miillpore filter of the filtrate that step S7 is obtained, and added with frame plate filter
Press filtration removes micron order impurity and partial electrolyte, collects filtrate；
S9, it weighs：The obtained filtrates of step S8 are weighed, calculates yield, is sealed.The yield of the present embodiment is
89.5%.
This method is extracted to the sample of ice plant extract, composition detection is carried out, wherein each ingredient is：Albumen
Matter：0.21g/100g, potassium：46.60mg/100g sodium：44.48mg/100g calcium：0.06mg/100g, zinc：9.8mg/kg, iron：
0.49mg/100g, 1.54mg/100g.
It is made whether to can apply to the verification of cosmetics：
First, detection project：Multiple skin irritation test
2nd, foundation is detected：Ministry of Health of the People's Republic of China《Cosmetics health specification》Version skin irritation/corruption in 2007
Corrosion test method
3rd, testing result：Within the observation period tested new zealand rabbit skin be occur erythema and oedema skin irritatin it is anti-
Should, every animal integrated value is 0 to sample sets daily.
4th, evaluation of result：According to Ministry of Health of the People's Republic of China《Cosmetics health specification》Version skin irritatin in 2007
Property/corrosion test criterion, the multiple skin irritatin intensity of frost flower extract of inspection is nonirritant.
In addition, this method is extract obtained also to have carried out acute eye irritation/corrosion test：
First, detection project：Acute eye irritation/corrosion test
2nd, foundation is detected：Ministry of Health of the People's Republic of China《Cosmetics health specification》The acute eye irritation of version in 2007/
Corrosion test method
3rd, testing result：0.1ml tested materials are directly painted on the right side of new zealand rabbit in the conjunctival sac of eyes, make upper and lower eye
Eyelid, which is passively closed 1s, prevents tested material from flowing out, and left side eyes, which are not handled, does own control, is not rinsed within 24 hours after being painted into tested material
Eyes instill 2% fluorescein sodium dilution after observation in 24 hours, clean up after 30s, after tested material is painted into 1h, for 24 hours,
48h and 72h checks new zealand rabbit eyes, is irritative response occur.
4th, evaluation of result：According to Ministry of Health of the People's Republic of China《Cosmetics health specification》Version acute ocular thorn in 2007
Swash property/corrosion test criterion, the frost flower extract of inspection is nonirritant to new zealand rabbit eye irritation intensity.
By a variety of detections it is found that extract of the ice plant as obtained by extracting the method for the present invention, contains
The nutriments such as a large amount of minerals, amino acid, vitamin, a variety of natural activity mineral elements being rich in irradiate ultraviolet light
With strong protective action, being used cooperatively with sun-screening agent has apparent synergy preventing ultraviolet effect.Contain various amino acid
And vitamin, there is repair to impaired skin.Patch skin has unique slight cool feeling, with reference to its active mineral element, to receiving
Contracting pore is of miraculous efficacy, and creates smooth careful skin.The extracting solution of the present invention can be used for the various sun-proof of cosmetics
Product after-sun product, releives, calm skin class product, sensibility skin reparation product, salubrious moisturizing product, shrinks hair
Hole product creates considerable beneficial value.
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art,
It still can modify to the technical solution recorded in foregoing embodiments or which part technical characteristic is carried out etc.
With replacing, all within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in this
Within the protection domain of invention.
Claims (1)
1. a kind of preparation method of ice plant extract, it is characterised in that：Include the following steps：
S1, picking：Fresh ice leaf grass is picked, impurity is removed, is placed in insulating foam case so that insulating foam the temperature inside the box is 25
Degree Celsius hereinafter, and being sent in 24 hours to processing factory；
S2, cleaning equipment：All devices are cleaned, are sterilized, it is dry；
S3, mashing processing：Colloid mill mashing is crossed after ice leaf grass is weighed, adds 1.0~5.0%K350, the K350 is benzene oxygen
The mixture of ethyl alcohol and Sensiva SC50, stirs evenly；
S4, centrifugal treating：Remove filter residue with centrifuge, then stand 24~72 hours, obtain material body；
S5, primary filtering：The material body that step S4 is obtained with 100~500 mesh filter plants is filtered, collects filtrate, then
Coarse filtration liquid is irradiated with light irradiation device 24~72 hours, until it is light yellow that chlorophyll is made, which to decompose colour fading,；
S6, secondary filter：The filtrate that step S5 is obtained, freezing thermostat are kept for 2~8 hours, Ran Houyong at 2~10 degrees Celsius
400~1000 mesh filter plants are filtered, and collect filtrate；
S7, it filters three times：The filtrate Medium speed filter paper that step S6 is obtained, and with frame plate filter pressure filtration, collect filter
Liquid；
S8, four filterings：By 0.15~0.35 micron of miillpore filter of the filtrate that step S7 is obtained, and with frame plate filter
Pressure filtration removes micron order impurity and partial electrolyte, collects filtrate；
S9, it weighs：The obtained filtrates of step S8 are weighed, calculates yield, is sealed.
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| CN201610225468.XA CN105796427B (en) | 2016-04-13 | 2016-04-13 | A kind of preparation method of ice plant extract |
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| CN201610225468.XA CN105796427B (en) | 2016-04-13 | 2016-04-13 | A kind of preparation method of ice plant extract |
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| CN105796427A CN105796427A (en) | 2016-07-27 |
| CN105796427B true CN105796427B (en) | 2018-07-03 |
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| CN108096086A (en) * | 2016-11-25 | 2018-06-01 | 深圳市弘创农业科技有限公司 | A kind of method that the ice plant extract without preservative is prepared using ice plant freeze-dried powder |
Citations (2)
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|---|---|---|---|---|
| CN102302427A (en) * | 2011-09-23 | 2012-01-04 | 常德炎帝生物技术有限公司 | Production and extraction method of nostoc nourishing and moisturizing material |
| FR2949682B1 (en) * | 2009-09-07 | 2012-09-28 | Rocher Yves Biolog Vegetale | USE OF A GLACIAL FICOID EXTRACT AS A COSMETIC ACTIVE INGREDIENT |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2949682B1 (en) * | 2009-09-07 | 2012-09-28 | Rocher Yves Biolog Vegetale | USE OF A GLACIAL FICOID EXTRACT AS A COSMETIC ACTIVE INGREDIENT |
| CN102302427A (en) * | 2011-09-23 | 2012-01-04 | 常德炎帝生物技术有限公司 | Production and extraction method of nostoc nourishing and moisturizing material |
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