CN105714557A - 一种吸湿排汗型整理剂及其制备方法 - Google Patents

一种吸湿排汗型整理剂及其制备方法 Download PDF

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CN105714557A
CN105714557A CN201610111003.1A CN201610111003A CN105714557A CN 105714557 A CN105714557 A CN 105714557A CN 201610111003 A CN201610111003 A CN 201610111003A CN 105714557 A CN105714557 A CN 105714557A
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钱华
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SUZHOU FANGYOU NEW MATERIAL Co Ltd
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Abstract

本发明公开了一种吸湿排汗型整理剂，包括如下重量份数的成分：4,4ˊ二硝基二苯甲醇1320份，双巯基乙酸乙二醇酯2025份，壬基酚聚氧乙烯醚1525份，2羟基5氯二苯甲酮812份，硅油1015份，4羟基苯乙胺38份，甘油磷酸酯716份，柠檬酸钠26份，磷酸二氢钾16份，去离子水3050份。纺织衣物利用本发明的整理剂后吸湿、排汗性能得到显著提高，能够及时有效的将人体汗液排出，避免产生闷热感。

Description

一种吸湿排汗型整理剂及其制备方法
技术领域
本发明属于整理剂领域，具体涉及一种吸湿排汗型整理剂及其制备方法。
背景技术
人们在炎热的夏天常常会大量排汗，如果排出的汗水不能及时散发，皮肤与衣物之间的湿度就会上升，而这种持续上升的湿度会让使人体感到非常闷热，进而导致身体进一步排汗来散发多余的热量，如此时间过长会导致人们干渴、缺水、心情烦躁等不良状况。现有的大部分纺织衣物中排汗、吸湿性能都不显著，无法有效将汗液及时透过衣物散发出去。
发明内容
针对现有技术中存在的以上技术问题，本发明提供一种吸湿排汗型整理剂及其制备方法，利用该整理剂处理衣物，提高衣物的吸湿、排汗性能，及时的帮助人们将汗液排出体外，保持愉快的心境。
技术方案：一种吸湿排汗型整理剂，包括如下重量份数的成分：4,4'-二硝基二苯甲醇13-20份，双巯基乙酸乙二醇酯20-25份，壬基酚聚氧乙烯醚15-25份，2-羟基-5-氯二苯甲酮8-12份，硅油10-15份，4-羟基苯乙胺3-8份，甘油磷酸酯7-16份，柠檬酸钠2-6份，磷酸二氢钾1-6份，去离子水30-50份。
优选的，所述4,4'-二硝基二苯甲醇15-18份，双巯基乙酸乙二醇酯22-25份，壬基酚聚氧乙烯醚18-23份，2-羟基-5-氯二苯甲酮9-11份，硅油12-14份，4-羟基苯乙胺4-7份，甘油磷酸酯10-13份，柠檬酸钠3-5份，磷酸二氢钾2-5份，去离子水35-45份。
优选的，所述4,4'-二硝基二苯甲醇17份，双巯基乙酸乙二醇酯24份，壬基酚聚氧乙烯醚20份，2-羟基-5-氯二苯甲酮10份，硅油13份，4-羟基苯乙胺5份，甘油磷酸酯12份，柠檬酸钠4份，磷酸二氢钾4份，去离子水40份。
一种吸湿排汗型整理剂的制备方法，具体包含如下步骤：
S1：将4,4'-二硝基二苯甲醇13-20份、双巯基乙酸乙二醇酯20-25份、2-羟基-5-氯二苯甲酮8-12份和硅油10-15份加入反应器中磁力搅拌20-30min，随后升高温度至40-50℃，继续加入柠檬酸钠2-6份和磷酸二氢钾1-6份，边滴加边反应1-2h；
S2：将壬基酚聚氧乙烯醚15-25份、4-羟基苯乙胺3-8份、甘油磷酸酯7-16份和去离子水30-50份在温度30-40℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应10-15min；
S3：继续升温至100-110℃，回流反应2-3h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
优选的，步骤S1中所述磁力搅拌的时间为25min，温度为48℃，边滴加边反应1.5h。
优选的，步骤S2中所述温度为35℃，不搅拌反应13min。
优选的，步骤S3中所述温度为106℃，回流反应2.5h。
有益效果：本发明所述一种吸湿排汗型整理剂的制备方法，以4,4'-二硝基二苯甲醇、双巯基乙酸乙二醇酯、壬基酚聚氧乙烯醚等物质为原料，经磁力搅拌、加热反应等步骤制备得到吸湿排汗型整理剂；本制备工艺简单、过程较短；纺织衣物利用本发明的整理剂后吸湿、排汗性能得到显著提高，能够及时有效的将人体汗液排出，避免产生闷热感。
具体实施方式
实施例1
S1：将4,4'-二硝基二苯甲醇13份、双巯基乙酸乙二醇酯20份、2-羟基-5-氯二苯甲酮8份和硅油10份加入反应器中磁力搅拌20min，随后升高温度至40℃，继续加入柠檬酸钠2份和磷酸二氢钾1份，边滴加边反应1h；
S2：将壬基酚聚氧乙烯醚15份、4-羟基苯乙胺3份、甘油磷酸酯7份和去离子水30份在温度30℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应10min；
S3：继续升温至100℃，回流反应2h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
对比例1
S1：将2-羟基-5-氯二苯甲酮8份和硅油10份加入反应器中磁力搅拌20min，随后升高温度至40℃，继续加入柠檬酸钠2份和磷酸二氢钾1份，边滴加边反应1h；
S2：将4-羟基苯乙胺3份、甘油磷酸酯7份和去离子水30份在温度30℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应10min；
S3：继续升温至100℃，回流反应2h，待反应液冷却后即可得到整理剂。
实施例2
S1：将4,4'-二硝基二苯甲醇20份、双巯基乙酸乙二醇酯25份、2-羟基-5-氯二苯甲酮12份和硅油15份加入反应器中磁力搅拌30min，随后升高温度至50℃，继续加入柠檬酸钠6份和磷酸二氢钾6份，边滴加边反应2h；
S2：将壬基酚聚氧乙烯醚25份、4-羟基苯乙胺8份、甘油磷酸酯16份和去离子水50份在温度40℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应15min；
S3：继续升温至110℃，回流反应3h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
对比例2
S1：将2-羟基-5-氯二苯甲酮12份和硅油15份加入反应器中磁力搅拌30min，随后升高温度至50℃，继续加入柠檬酸钠6份和磷酸二氢钾6份，边滴加边反应2h；
S2：将4-羟基苯乙胺8份、甘油磷酸酯16份和去离子水50份在温度40℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应15min；
S3：继续升温至110℃，回流反应3h，待反应液冷却后即可得到整理剂。
实施例3
S1：将4,4'-二硝基二苯甲醇15份、双巯基乙酸乙二醇酯22份、2-羟基-5-氯二苯甲酮9份和硅油12份加入反应器中磁力搅拌20min，随后升高温度至40℃，继续加入柠檬酸钠3份和磷酸二氢钾2份，边滴加边反应1h；
S2：将壬基酚聚氧乙烯醚18份、4-羟基苯乙胺4份、甘油磷酸酯10份和去离子水35份在温度30℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应10min；
S3：继续升温至100℃，回流反应2h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
实施例4
S1：将4,4'-二硝基二苯甲醇18份、双巯基乙酸乙二醇酯25份、2-羟基-5-氯二苯甲酮11份和硅油14份加入反应器中磁力搅拌30min，随后升高温度至50℃，继续加入柠檬酸钠5份和磷酸二氢钾5份，边滴加边反应2h；
S2：将壬基酚聚氧乙烯醚23份、4-羟基苯乙胺7份、甘油磷酸酯13份和去离子水45份在温度40℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应15min；
S3：继续升温至110℃，回流反应3h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
实施例5
S1：将4,4'-二硝基二苯甲醇17份、双巯基乙酸乙二醇酯24份、2-羟基-5-氯二苯甲酮10份和硅油13份加入反应器中磁力搅拌25min，随后升高温度至48℃，继续加入柠檬酸钠4份和磷酸二氢钾4份，边滴加边反应1.5h；
S2：将壬基酚聚氧乙烯醚20份、4-羟基苯乙胺5份、甘油磷酸酯12份和去离子水40份在温度35℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应13min；
S3：继续升温至106℃，回流反应2.5h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
将各个实施例和对比例所得到的整理剂，应用于纺织衣物中，测试经处理纺织衣物的透湿量，结果如下：

Claims (7)

1.一种吸湿排汗型整理剂，其特征在于，包括如下重量份数的成分：4,4'-二硝基二苯甲醇13-20份，双巯基乙酸乙二醇酯20-25份，壬基酚聚氧乙烯醚15-25份，2-羟基-5-氯二苯甲酮8-12份，硅油10-15份，4-羟基苯乙胺3-8份，甘油磷酸酯7-16份，柠檬酸钠2-6份，磷酸二氢钾1-6份，去离子水30-50份。
2.根据权利要求1所述的一种吸湿排汗型整理剂，其特征在于，所述4,4'-二硝基二苯甲醇15-18份，双巯基乙酸乙二醇酯22-25份，壬基酚聚氧乙烯醚18-23份，2-羟基-5-氯二苯甲酮9-11份，硅油12-14份，4-羟基苯乙胺4-7份，甘油磷酸酯10-13份，柠檬酸钠3-5份，磷酸二氢钾2-5份，去离子水35-45份。
3.根据权利要求2所述的一种吸湿排汗型整理剂，其特征在于，所述4,4'-二硝基二苯甲醇17份，双巯基乙酸乙二醇酯24份，壬基酚聚氧乙烯醚20份，2-羟基-5-氯二苯甲酮10份，硅油13份，4-羟基苯乙胺5份，甘油磷酸酯12份，柠檬酸钠4份，磷酸二氢钾4份，去离子水40份。
4.一种吸湿排汗型整理剂的制备方法，其特征在于，具体包含如下步骤：
S1：将4,4'-二硝基二苯甲醇13-20份、双巯基乙酸乙二醇酯20-25份、2-羟基-5-氯二苯甲酮8-12份和硅油10-15份加入反应器中磁力搅拌20-30min，随后升高温度至40-50℃，继续加入柠檬酸钠2-6份和磷酸二氢钾1-6份，边滴加边反应1-2h；
S2：将壬基酚聚氧乙烯醚15-25份、4-羟基苯乙胺3-8份、甘油磷酸酯7-16份和去离子水30-50份在温度30-40℃下充分搅拌混合，随后步骤S1所得到的反应液，不搅拌反应10-15min；
S3：继续升温至100-110℃，回流反应2-3h，待反应液冷却后即可得到所述吸湿排汗型整理剂。
5.根据权利要求4所述的一种吸湿排汗型整理剂的制备方法，其特征在于，步骤S1中所述磁力搅拌的时间为25min，温度为48℃，边滴加边反应1.5h。
6.根据权利要求4所述的一种吸湿排汗型整理剂的制备方法，其特征在于，步骤S2中所述温度为35℃，不搅拌反应13min。
7.根据权利要求4所述的一种吸湿排汗型整理剂的制备方法，其特征在于，步骤S3中所述温度为106℃，回流反应2.5h。
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