CN105659072B - 监测聚合反应控制参数的方法和实施所述方法的相关装置 - Google Patents

监测聚合反应控制参数的方法和实施所述方法的相关装置 Download PDF

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CN105659072B
CN105659072B CN201480055493.7A CN201480055493A CN105659072B CN 105659072 B CN105659072 B CN 105659072B CN 201480055493 A CN201480055493 A CN 201480055493A CN 105659072 B CN105659072 B CN 105659072B
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polymerization
polymerization reaction
mixture
control parameter
nir
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CN105659072A (zh
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F·博纳奇尼
E·曼托瓦尼
A·费兰多
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Versalis SpA
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/27—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration
    • G01N21/272—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration for following a reaction, e.g. for determining photometrically a reaction rate (photometric cinetic analysis)
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F112/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F112/02—Monomers containing only one unsaturated aliphatic radical
    • C08F112/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F112/06—Hydrocarbons
    • C08F112/08—Styrene
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3577—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/359—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N21/85—Investigating moving fluids or granular solids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N21/85—Investigating moving fluids or granular solids
    • G01N21/8507—Probe photometers, i.e. with optical measuring part dipped into fluid sample
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00—Features of devices classified in G01N21/00
    • G01N2201/06—Illumination; Optics
    • G01N2201/061—Sources
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00—Features of devices classified in G01N21/00
    • G01N2201/08—Optical fibres; light guides
    • G01N2201/0826—Fibre array at source, distributing
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00—Features of devices classified in G01N21/00
    • G01N2201/12—Circuits of general importance; Signal processing
    • G01N2201/13—Standards, constitution

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Theoretical Computer Science (AREA)
  • Mathematical Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Polymerisation Methods In General (AREA)
  • Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
CN201480055493.7A 2013-11-19 2014-11-18 监测聚合反应控制参数的方法和实施所述方法的相关装置 Active CN105659072B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IT001916A ITMI20131916A1 (it) 2013-11-19 2013-11-19 Metodo per monitorare un parametro di controllo di una reazione di polimerizzazione e relativo apparato per attuare detto metodo
ITMI2013A001916 2013-11-19
PCT/IB2014/066129 WO2015075629A1 (en) 2013-11-19 2014-11-18 Method for monitoring a control parameter of a polymerization reaction and relative apparatus for implementing said method

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CN105659072A CN105659072A (zh) 2016-06-08
CN105659072B true CN105659072B (zh) 2020-02-14

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US (1) US9714899B2 (https=)
EP (1) EP3071954B1 (https=)
JP (1) JP6619736B2 (https=)
KR (1) KR102209231B1 (https=)
CN (1) CN105659072B (https=)
BR (1) BR112016007745B1 (https=)
ES (1) ES2804087T3 (https=)
HU (1) HUE051229T2 (https=)
IT (1) ITMI20131916A1 (https=)
MX (1) MX368418B (https=)
MY (1) MY185715A (https=)
PL (1) PL3071954T3 (https=)
PT (1) PT3071954T (https=)
RU (1) RU2662039C1 (https=)
SA (1) SA516371040B1 (https=)
SI (1) SI3071954T1 (https=)
WO (1) WO2015075629A1 (https=)

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GB201704447D0 (en) * 2017-03-21 2017-05-03 Asterope Ltd Wire coating determination
CN112236667B (zh) * 2018-06-07 2024-11-01 横河电机株式会社 光学分析系统及光学分析方法
CN108872144B (zh) * 2018-09-13 2021-02-12 中国农业大学 一种用于厌氧消化过程的在线监测装置
EP3711852A1 (de) * 2019-03-21 2020-09-23 Covestro Deutschland AG Verfahren und vorrichtung zur quantitativen überwachung der zusammensetzung einer oligomer-/monomermischung
JPWO2022080367A1 (https=) * 2020-10-13 2022-04-21
JP7603629B2 (ja) * 2022-03-14 2024-12-20 Dic株式会社 樹脂物性値予測装置及び樹脂物性値の予測方法
CN117309793B (zh) * 2023-10-25 2024-05-07 连云港石化有限公司 一种苯乙烯装置聚合物测定方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0764843A2 (fr) * 1995-09-25 1997-03-26 SOLVAY (Société Anonyme) Procédé et dispositif de contrôle de la qualité de latex de polyméres vinyliques halogénés
EP1223186A1 (en) * 2000-12-22 2002-07-17 Mitsubishi Gas Chemical Company, Inc. Process for production of polyamide
CN1914254A (zh) * 2003-12-09 2007-02-14 菲纳科技股份有限公司 生产聚合物的方法

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US5604132A (en) * 1995-01-23 1997-02-18 Olin Corporation Process flow injection analyzer and method
DE19805612A1 (de) * 1998-02-12 1999-08-19 Bayer Ag Verfahren zur kontrollierten Herstellung oder Modifizierung von polymeren Produkten mittels IR-ATR-Spektroskopie
JP2000159897A (ja) * 1998-11-27 2000-06-13 Mitsui Chemicals Inc 高分子化合物の不良品分離方法
JP5255833B2 (ja) * 2004-03-24 2013-08-07 エクソンモービル・ケミカル・パテンツ・インク エチレン・インターポリマーの製造方法、該方法により製造されたインターポリマー、組成物、および該インターポリマーを含む電気デバイス
CA2470887C (en) * 2004-06-14 2014-10-21 Nova Chemicals Corporation Detection of gels in a solution polymerization
US8362178B2 (en) 2006-03-13 2013-01-29 Lg Chem, Ltd. 1-alkene-acrylate based copolymer
US8843324B2 (en) * 2011-02-03 2014-09-23 Nova Chemicals (International) S.A. Double derivative NIR process control
CN102288575B (zh) * 2011-07-25 2013-03-06 哈尔滨工业大学 在线监测甲氨基阿维菌素反应的装置

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0764843A2 (fr) * 1995-09-25 1997-03-26 SOLVAY (Société Anonyme) Procédé et dispositif de contrôle de la qualité de latex de polyméres vinyliques halogénés
US5898056A (en) * 1995-09-25 1999-04-27 Solvay (Societe Anonyme) Process and device for monitoring the quality of latices of halogen-containing vinyl polymers
EP1223186A1 (en) * 2000-12-22 2002-07-17 Mitsubishi Gas Chemical Company, Inc. Process for production of polyamide
CN1914254A (zh) * 2003-12-09 2007-02-14 菲纳科技股份有限公司 生产聚合物的方法

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KR102209231B1 (ko) 2021-01-29
JP6619736B2 (ja) 2019-12-11
RU2016116157A (ru) 2017-12-25
SI3071954T1 (sl) 2020-08-31
MX368418B (es) 2019-10-02
ES2804087T3 (es) 2021-02-03
HUE051229T2 (hu) 2021-03-01
EP3071954A1 (en) 2016-09-28
MX2016005767A (es) 2016-07-18
US9714899B2 (en) 2017-07-25
JP2016538536A (ja) 2016-12-08
PT3071954T (pt) 2020-07-09
CN105659072A (zh) 2016-06-08
KR20160088304A (ko) 2016-07-25
BR112016007745B1 (pt) 2020-11-24
PL3071954T3 (pl) 2020-10-05
ITMI20131916A1 (it) 2015-05-20
SA516371040B1 (ar) 2017-12-03
MY185715A (en) 2021-05-31
US20160231230A1 (en) 2016-08-11
EP3071954B1 (en) 2020-04-08
RU2662039C1 (ru) 2018-07-23
WO2015075629A1 (en) 2015-05-28

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