CN105612142B - 用于生产粗甲基丙烯酸甲酯的酯化单元、使用所述单元的酯化方法 - Google Patents

用于生产粗甲基丙烯酸甲酯的酯化单元、使用所述单元的酯化方法 Download PDF

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Publication number
CN105612142B
CN105612142B CN201480056810.7A CN201480056810A CN105612142B CN 105612142 B CN105612142 B CN 105612142B CN 201480056810 A CN201480056810 A CN 201480056810A CN 105612142 B CN105612142 B CN 105612142B
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reactor
outlet
phase
esterification
liquid
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Chinese (zh)
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CN105612142A (zh
Inventor
Y.贝尔纳丹
R.比永
X.马卡里安
F.瓦莱
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Trinseo Europe GmbH
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Arkema France SA
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/18—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group
    • C07C67/20—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group from amides or lactams
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2445—Stationary reactors without moving elements inside placed in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/245—Stationary reactors without moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002—Nozzle-type elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201480056810.7A 2013-10-18 2014-10-17 用于生产粗甲基丙烯酸甲酯的酯化单元、使用所述单元的酯化方法 Active CN105612142B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1360181A FR3012139B1 (fr) 2013-10-18 2013-10-18 Unite d'esterification pour la production de methacrylate de methyle brut, procede d'esterification utilisant ladite unite et installation comprenant ladite unite
FR1360181 2013-10-18
PCT/EP2014/072366 WO2015055842A1 (en) 2013-10-18 2014-10-17 Esterification unit for producing crude methyl methacrylate, esterification process using said unit and plant comprising sais unit

Publications (2)

Publication Number Publication Date
CN105612142A CN105612142A (zh) 2016-05-25
CN105612142B true CN105612142B (zh) 2021-09-07

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CN201480056810.7A Active CN105612142B (zh) 2013-10-18 2014-10-17 用于生产粗甲基丙烯酸甲酯的酯化单元、使用所述单元的酯化方法

Country Status (7)

Country Link
US (2) US10131614B2 (enExample)
EP (1) EP3057932B1 (enExample)
CN (1) CN105612142B (enExample)
BR (1) BR112016008635B1 (enExample)
FR (1) FR3012139B1 (enExample)
MX (1) MX2016004486A (enExample)
WO (1) WO2015055842A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106512879B (zh) * 2016-03-25 2019-04-12 中国石油集团东北炼化工程有限公司吉林设计院 在甲基丙烯酸甲酯的制备中防止酯化釜内结块的方法
CN107779482A (zh) * 2017-12-05 2018-03-09 山东宝莫生物化工股份有限公司 一种高浓度丙烯酰胺的生产工艺
CN110483271A (zh) * 2019-09-03 2019-11-22 陈国良 一种由反应酰胺盐制备甲基丙烯酸甲酯的方法
TWI732408B (zh) * 2019-12-31 2021-07-01 財團法人工業技術研究院 丙烯酸酯化合物連續式製備裝置及方法
CN113461522A (zh) * 2020-03-30 2021-10-01 中石油吉林化工工程有限公司 生产甲基丙烯酸甲酯的酯化方法
CN113461845B (zh) * 2020-03-30 2023-03-31 中石油吉林化工工程有限公司 一种pmma生产装置
CN115193344B (zh) * 2022-05-25 2023-08-18 安阳九天精细化工有限责任公司 一种高效节能甲胺合成系统及方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3006950A (en) * 1959-07-31 1961-10-31 Electro Chimie D Electrometall Process of making methyl methacrylate
EP0594008A1 (en) * 1992-10-22 1994-04-27 Sumitomo Chemical Company, Limited Process for producing methyl methacrylate
EP0945423A2 (en) * 1998-03-25 1999-09-29 Mitsubishi Gas Chemical Company, Inc. Process for preparing alpha-hydroxycarboxylate
WO2009156648A1 (fr) * 2008-05-30 2009-12-30 Arkema France Methacrylate de methyle derive de la biomasse, procede de fabrication, utilisations et polymeres correspondants

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL250852A (enExample) * 1959-04-24
US3996950A (en) 1975-04-30 1976-12-14 Randall Mier Obstacle detection device for use by the blind
GB8618888D0 (en) * 1986-08-01 1986-09-10 Davy Mckee Ltd Process
JP2588581B2 (ja) * 1988-05-06 1997-03-05 株式会社クラレ メタクリル酸エステルの製造法
ZA200303241B (en) * 2002-05-01 2003-11-04 Rohm & Haas Improved process for methacrylic acid and methcrylic acid ester production.
DE102006059513A1 (de) 2006-12-14 2008-06-19 Evonik Röhm Gmbh Verfahren zur Herstellung von Methacrylsäure alkylestern mittels azeotroper Destillation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3006950A (en) * 1959-07-31 1961-10-31 Electro Chimie D Electrometall Process of making methyl methacrylate
EP0594008A1 (en) * 1992-10-22 1994-04-27 Sumitomo Chemical Company, Limited Process for producing methyl methacrylate
EP0945423A2 (en) * 1998-03-25 1999-09-29 Mitsubishi Gas Chemical Company, Inc. Process for preparing alpha-hydroxycarboxylate
WO2009156648A1 (fr) * 2008-05-30 2009-12-30 Arkema France Methacrylate de methyle derive de la biomasse, procede de fabrication, utilisations et polymeres correspondants

Also Published As

Publication number Publication date
FR3012139B1 (fr) 2016-08-26
MX2016004486A (es) 2016-06-21
US11084774B2 (en) 2021-08-10
EP3057932B1 (en) 2022-06-22
US20200270195A1 (en) 2020-08-27
WO2015055842A1 (en) 2015-04-23
BR112016008635B1 (pt) 2022-04-12
FR3012139A1 (enExample) 2015-04-24
US20160257639A1 (en) 2016-09-08
CN105612142A (zh) 2016-05-25
US10131614B2 (en) 2018-11-20
BR112016008635A2 (enExample) 2017-08-01
EP3057932A1 (en) 2016-08-24

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Effective date of registration: 20220106

Address after: Horgen Switzerland

Patentee after: TRINSEO EUROPE GmbH

Address before: Cologne, France

Patentee before: ARKEMA FRANCE