CN1055380C - Wet bead grinding pollen-breaking technique - Google Patents
Wet bead grinding pollen-breaking technique Download PDFInfo
- Publication number
- CN1055380C CN1055380C CN95110207A CN95110207A CN1055380C CN 1055380 C CN1055380 C CN 1055380C CN 95110207 A CN95110207 A CN 95110207A CN 95110207 A CN95110207 A CN 95110207A CN 1055380 C CN1055380 C CN 1055380C
- Authority
- CN
- China
- Prior art keywords
- pollen
- suspension
- water
- wet bead
- grinding
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims abstract description 18
- 238000000227 grinding Methods 0.000 title claims abstract description 16
- 239000011324 bead Substances 0.000 title claims abstract description 7
- 239000000725 suspension Substances 0.000 claims description 13
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 235000016709 nutrition Nutrition 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 230000035764 nutrition Effects 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 235000013361 beverage Nutrition 0.000 claims description 3
- 239000000498 cooling water Substances 0.000 claims description 3
- 239000005331 crown glasses (windows) Substances 0.000 claims description 3
- 239000003814 drug Substances 0.000 claims description 3
- 235000012907 honey Nutrition 0.000 claims description 3
- 239000006004 Quartz sand Substances 0.000 claims description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- 239000008367 deionised water Substances 0.000 claims description 2
- 229910021641 deionized water Inorganic materials 0.000 claims description 2
- 239000012153 distilled water Substances 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 230000001954 sterilising effect Effects 0.000 claims description 2
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- 239000013543 active substance Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 238000005336 cracking Methods 0.000 abstract 2
- 238000012962 cracking technique Methods 0.000 abstract 1
- 238000009775 high-speed stirring Methods 0.000 abstract 1
- 239000002304 perfume Substances 0.000 abstract 1
- 239000012530 fluid Substances 0.000 description 3
- 238000013467 fragmentation Methods 0.000 description 3
- 238000006062 fragmentation reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 239000012190 activator Substances 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 1
- AEMOLEFTQBMNLQ-BKBMJHBISA-N alpha-D-galacturonic acid Chemical compound O[C@H]1O[C@H](C(O)=O)[C@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-BKBMJHBISA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000001079 digestive effect Effects 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 229940099909 multivitamin and iron Drugs 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 229940100688 oral solution Drugs 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Landscapes
- Jellies, Jams, And Syrups (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a pollen wall cracking technique which is characterized in that a high-speed stirring type bead grinder is used for grinding pollen walls to obtain homogenate. By adopting the technique, the wall cracking ratio of pollen reaches 100%. Simultaneously, the present invention can effectively keep the physiological active substances and the original color, perfume and taste of the pollen. In the wall cracking process, no chemical substance is added. The present invention has the advantages of low cost and simple process.
Description
The present invention relates to a kind of pollen wall breaking technology, particularly utilize the natural spp. pollen wall that ball mill will contain abundant nutrition composition and physiological activator to grind.
The melissa powder is a kind of nutritious bee product, it contains twenties kinds of free amino acids (comprising eight kinds of essential amino acids), several physiological active substances, as enzyme, protein, nucleic acid, flavones etc., 15 kinds of trace elements such as multivitamin and iron, zinc, iodine, selenium, therefore bee product is described as " the natural nutrition storehouse that concentrates " by people, is widely used in aspects such as food, nourishing healthy, daily cosmetics and medicine.The Chinese people foodstuff for the people has long history with the melissa powder, and just on the books in Shennong's Herbal, the Tang Dynasty, the Qing Dynasty are more popular.Countries such as Sweden, the U.S., Japan, France, Russia have carried out a large amount of research and development aspect the commercialization of pollen, make a series of pollen products, as pollen oral solution, pollen essence, pollen honey, trehalose, pollen liquor, pollen tea, pollen cake, pollen beverage, various pollen cosmetics, compound pollen capsule or the like.China is pollen big producing country, and a lot of countries are from China's import pollen raw material, but China the pollen consumption figure is very low per capita, therefore, be badly in need of exploitation pollen and utilize technology.
The active ingredient of pollen is wrapped up by two-layer tough and tensile wall, and pollen wall is made up of sporopollenin, cellulose, pectic substance etc.Wherein sporopollenin all has very strong resistance to acid, alkali and digestive ferment, behind the human edible pollen, can only absorb a part of nutriment by the germinal aperature on the outer wall, and the pollen utilization rate is low.Therefore pollen broken wall is the key that makes full use of pollen resource.Aspect pollen broken wall, carried out big quantity research both at home and abroad, develop many methods, as colloid milling (CN 2082197U, CN 1049595A), high pressure draught comminuting method (CN 85102850), temperature differential method (Japanese Patent Publication 54-31067, CN 85109099A), enzyme process (CN1039708A, CN 1069632A) etc.But these methods all exist sporoderm-broken rate low in various degree, and the processing time is long, complex operation, and energy consumption is big, the cost height, active material loses problems such as many.Ball mill has been applied to the aspects such as homogenate of microbial cell fragmentation, dyestuff and pigment, yet there are no the open report or the patent application that are used for pollen broken wall.
The present invention is intended to address the above problem, and is with pollen 100% broken wall, and simple to operate, with low cost with ball mill under the prerequisite that keeps fovilla matter physiologically active, is fit to large-scale production.Do not add any chemical composition in the pollen broken wall process, product meets national food hygienic standard.
Design of the present invention is to adopt the ball mill pollen-breaking.The mechanism of bead mill is that grinding agent (diameter 0.1-1 millimeter) (rotating speed is at 2000-5000 rev/min) under the ball mill agitator drives fully mixes with pollen suspension, pollen is broken in the shearing force acting in conjunction that produces of colliding mutually between the grinding agent, rub and move, thereby discharges fovilla.Grinding agent can be crown glass pearl, stainless steel ball, quartz sand etc., and the volume ratio of grinding agent and pollen suspension is 0.5～1.5: 1, and the diameter of grinding agent and consumption directly influence the shell-broken effect of pollen.Generally speaking, the less pollen of size is suitable for the grinding agent of selecting diameter less, and vice versa; The grinding agent consumption very little, rate of breaking pollen wall is low; Consumption is too many, the corresponding minimizing of pollen treating capacity, and also the heat that shattering process produces increases total energy consumption raising.In order to get rid of by grinding agent collision, fricative heat, to safeguard the activity of physiological activator, the crushing chamber of ball mill has cooling jacket, can limit broken limit cooling.The temperature of recirculated cooling water generally is lower than 10 ℃, can guarantee that the temperature of the exit pollen homogenate of ball mill is no more than 40 ℃.But but also continued operation of ball mill intermittently operated, the broken time is 1～3 minute during intermittently operated, and the flow of pollen suspension is 5～15 liters/hour during continued operation, and the concentration of suspension is 5%～30% (weight ratio).
Technical scheme of the present invention is as follows:
The alcohol of 1 usefulness 75% is with the pollen sterilization;
2 usefulness distilled water, sterilized water or rinsed with deionized water removal of impurities, precipitation are removed silt particle, make the pollen suspension of finite concentration (5～30% (percentage by weight)) simultaneously; In suspension, also can add honey, alcohol, Powdered Chinese medicine or other auxiliary material;
3 under certain flow rate (5～15 liters/hour), and pollen suspension is pumped into the fragmentation of ball mill crushing chamber, and outlet promptly obtains the pollen treatment fluid of broken wall;
4 is centrifugal or filter water soluble ingredient and water insoluble active ingredient (comprising the pollen wall fragment) are separated, and perhaps the treatment fluid spray-drying got dry powder.Clear liquid centrifugal or that filtration obtains can be used for the making of beverage, and the water-insoluble nutritional labeling that correspondingly obtains can further be processed into the oil-soluble product.
The kind of the present invention and pollen and character are irrelevant, and applicable to the broken wall of any kind of pollen, sporoderm-broken rate reaches 100%, and effective ingredient is discharged fully, can keep the physiologically active and the original color of pollen of fovilla simultaneously effectively.
The embodiment of ball mill pollen-breaking is as follows:
Adopt the continued operation mode, 2500 rev/mins of rotating speeds, crown glass pearl diameter is the 0.5-0.75 millimeter, the volume ratio of pearl and suspension is 1: 1, and pollen concentration is 20% (weight ratio), and flow velocity is 10 liters/hour, the recirculated cooling water temperature is 6 ℃, and the treatment fluid outlet temperature is lower than 30 ℃.With the pollen of present technique fragmentation, microscopically (amplifying 1000 times) observe to show, the pollen wall attenuation, becomes broken, and inclusion discharges fully, rate of breaking pollen wall 100%.The homogenate temperature is lower than 30 ℃, so the physiologically active composition is not damaged.Handle 1 kilogram of pollen power consumption, 1.8 degree, per hour handle 2 kilograms of pollen.
Claims (3)
1. wet bead grinding pollen-breaking method adopts the ball mill broken wall, its step be alcohol sterilization, removal of impurities, wet method pearl mill, centrifugal, filter or dry, feature of the present invention is can intermittently operated, also can continued operation; Grinding agent is that diameter is 0.1～1 millimeter crown glass pearl, stainless shot, a quartz sand; The volume ratio of grinding agent and pollen suspension is 0.5～1.5: 1, recirculated cooling water temperature≤10 ℃, the ball mill range of speeds is 2000～5000 rev/mins, the intermittently broken time is 1～3 minute, the flow of suspension is 5～15 liters/hour during continuous crushing, and the concentration of pollen suspension is 5～30% (weight ratios).
2. according to the described wet bead grinding pollen-breaking method of claim 1, it is characterized in that preparing pollen suspension, also can in suspension, add honey, alcohol or Powdered Chinese medicine with deionized water or distilled water.
3. according to the described wet bead grinding pollen-breaking method of claim 1, adopt centrifugal or filter method with water-soluble nutrition and pollen wall and water-insoluble nutrition separately, the latter can further be processed into the oil-soluble product, clear liquid centrifugal or that filtration obtains can be used for the making of beverage, the spray-dried dry powder that obtains of pollen homogenate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN95110207A CN1055380C (en) | 1995-04-24 | 1995-04-24 | Wet bead grinding pollen-breaking technique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN95110207A CN1055380C (en) | 1995-04-24 | 1995-04-24 | Wet bead grinding pollen-breaking technique |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1134241A CN1134241A (en) | 1996-10-30 |
| CN1055380C true CN1055380C (en) | 2000-08-16 |
Family
ID=5077617
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN95110207A Expired - Fee Related CN1055380C (en) | 1995-04-24 | 1995-04-24 | Wet bead grinding pollen-breaking technique |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1055380C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102793095A (en) * | 2012-08-21 | 2012-11-28 | 中国科学院西北高原生物研究所 | Rape bee pollen homogenizing wall-breaking method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86105550A (en) * | 1986-07-26 | 1987-02-11 | 广西亚热带作物研究所 | Method of breaking pollen cell wall with mechanical power |
| CN85106076A (en) * | 1985-08-09 | 1987-02-25 | 苏州医学院 | pollen wall breaking technology |
-
1995
- 1995-04-24 CN CN95110207A patent/CN1055380C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85106076A (en) * | 1985-08-09 | 1987-02-25 | 苏州医学院 | pollen wall breaking technology |
| CN86105550A (en) * | 1986-07-26 | 1987-02-11 | 广西亚热带作物研究所 | Method of breaking pollen cell wall with mechanical power |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1134241A (en) | 1996-10-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101347216B (en) | Method for preparing nutritional concentrated solution of red date | |
| CN101248890A (en) | Nutrition reinforced type high activity beche-de-mer products and method of preparing the same | |
| CN101690566A (en) | Method for making natural longan powder | |
| CN103238892A (en) | Production method of smallanthus sonchifolius normal juice and normal juice powder | |
| CN101161130A (en) | Agaric health beverage | |
| CN113717297A (en) | Rose polysaccharide and preparation method and application thereof | |
| CN101516380A (en) | Composition capable of reducing blood pressure and/or suppressing rise in blood temperature and drink containing same | |
| CN109662234A (en) | A kind of Astaxanthin In Haematococcus Pluvialis solid beverage adjusting women skin, anti-aging | |
| CN1055380C (en) | Wet bead grinding pollen-breaking technique | |
| CN1086721A (en) | Series beverage by Tricholoma matsutake (lto et lmai) Singer and fructus lycii extracted solution manufacturing | |
| CN105533326A (en) | Blueberry drink and preparation method thereof | |
| CN1225801A (en) | Compounded Mailusuo and preparation process thereof | |
| CN1051208C (en) | Process for producing instant nourishing lotus root starch | |
| CN107814854A (en) | A kind of method that polysaccharide is extracted from Gynura procumbens (Lour.) Merr | |
| CN1063803A (en) | From citrous fruit peels such as orange peel, obtain through refining the method for high-quality pectin | |
| CN1296774A (en) | Process for extracting nutrients from lotus and its products | |
| CN1086916C (en) | Process for preparing natural tea extract | |
| CN1027854C (en) | Technology of breaking pollen wall | |
| CN112156122A (en) | Micromolecular codonopsis pilosula instant powder and preparation method thereof | |
| CN1113698A (en) | Amorphophallus rivieri fine flour | |
| CN1102787A (en) | Preparation of nutrient oral liquid | |
| CN100490860C (en) | Preparation method of liver-benefiting face-beautifying oral liquid with micron pine pollen and pearl powder for women | |
| JP3779740B2 (en) | Agents for preventing and treating obesity from rice | |
| CN1190550A (en) | No-strinking spirulina nutrient health care series beverage and preparing method thereof | |
| CN1013549B (en) | Process for manufacturing olive drinking powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |