CN105534791A - Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof - Google Patents
Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The invention relates to medicinal toothpaste containing nutgall ethyl acetate extract and a production method thereof. The medicinal toothpaste provided by the invention contains the nutgall ethyl acetate extract, an abrasive, a foaming agent, a humectant, a thickening agent, a sweetening agent, a preservative, a corrosion inhibitor, essence and refined water. The production method of the medicinal toothpaste containing the nutgall ethyl acetate extract comprises the following steps: firstly, preparing nutgall ethyl acetate extract; secondly, taking the abrasive, foaming agent, humectant, thickening agent, preservative, corrosion inhibitor and sweetening agent for later use; and thirdly, preparing toothpaste by adopting a two-step process. The medicinal toothpaste provided by the invention has the advantages that nutgall active ingredient is added during production of the toothpaste, guarantee period of a product is prolonged and number of times of the product is increased, the toothpaste can have antibacterial and anti-inflammation effects, and besides cleaning teeth, the toothpaste also can be used for treating limp teeth, chewing disability, gingival bleeding, mouth and tongue sores, swelling and pain in throat, halitosis and the like which are caused by periodontal disease.
Description
Technical field
The present invention relates to a kind of Chinese herbal toothpaste and production method thereof, especially a kind of medicated toothpaste and production method thereof containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract.
Background technology
Periodontitis is a kind of common oral disease, and its prevalence is up to more than 80% in China adult, and main manifestations symptom is gingival hemorrhage, red swelling of gingiva, halitosis, and this disease is many to be caused because oral cavity bacterium is unbalance.
The solid gum liquid of Xi Payi is the classics recipe of Uygur medicine oral cavity health, being prepared from by Galla Turcica (Galla Helepensis) single medicinal material, is that " Drug Standard of Ministry of Public Health of the Peoples Republic of China-Uigurs medicine fascicle " (hereinafter referred " dimension medicine fascicle ") version in 1999 records kind.The complete preparation method of dimension medicine fascicle record is: " get Galla Turcica (Galla Helepensis) 20g, be ground into coarse powder, after soaking 1 hour; decoct 3 times; each 0.5 hour, collecting decoction, filter; add cyclamate 20g successively in filtrate; Mint Essence 1mL and sodium benzoate 0.5g, is stirred to dissolve, adds water and be adjusted to 1000mL; subpackage, to obtain final product." said preparation has effect of the solid gum of strong tooth, the pain relieving that purifies the blood, antibacterial preventing decayed tooth.
In Galla Turcica (Galla Helepensis), the content of tannin is 60%-80%, and has effect that is antibacterial, antiinflammatory.In order to better play tannin effect, tannin extracts by the method that applicant is extracted with ethyl acetate, and adds as effective ingredient.But, there is in gallotannin structure a large amount of ortho positions phenolic hydroxyl group, easily oxidized, the solid gum liquid of part Xi Payi there will be macroscopic precipitation during the shelf-life at the bottom of bottle, and the stability improving gallotannin is also that Xi Payi bursts one of difficulty that knot peace research worker faces.
Summary of the invention
The first object of the present invention is to provide a kind of medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract;
The present invention, its feature is: (material of getting is weight portion).
The present invention contains: containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract: 0.5 ~ 10 part, thickening agent: 0.5 ~ 2.5 part, wetting agent: 10 ~ 20 parts, foaming agent: 2 ~ 5 parts, antiseptic: 0.2 ~ 0.6 part, corrosion inhibiter: 0.3 ~ 0.6 part, essence: 1 ~ 1.4 part, sweeting agent: 0.3 ~ 0.6 part, abrasivus: 10 ~ 30 parts, Purified Water: be added to 5 ~ 30 parts.
Above-mentioned wetting agent is: sorbitol: 10 ~ 20 parts, glycerol: 10 ~ 20 parts, butanediol: 10 ~ 15 parts, Polyethylene Glycol: 10 ~ 15 parts, at least one in adding four kinds.
Above-mentioned abrasivus is: calcium carbonate: 10 ~ 15 parts, silicon dioxide: 20 ~ 30 parts, calcium bicarbonate: 10 ~ 15, at least one in adding three kinds.
Above-mentioned foaming agent is: sodium lauryl sulphate: 2 ~ 5 parts, sodium bicarbonate 2 ~ 3 parts, ammonium bicarbonate 2 ~ 3 parts, at least one in adding three kinds.
Above-mentioned thickening agent is: sodium carboxymethyl cellulose: 0.8 ~ 1.8 part, methylcellulose: 0.5 ~ 1.2 part, guar gum: 0.5 ~ 2 part, at least one in adding three kinds.
Above-mentioned sweeting agent is: saccharin sodium: 0.3 ~ 0.6 part, sucrose: 0.3 ~ 0.6 part, at least one in adding two kinds.
Above-mentioned essence is: Mentholum: 1 ~ 1.4 part, fragrant citrus essence: 1 ~ 1.4 part, Green tea essence: 1 ~ 1.4 part, at least one in adding three kinds.
Above-mentioned corrosion inhibiter is Chile saltpeter: 0.3 ~ 0.6 part, sodium nitrite: 0.3 ~ 0.6 part, at least one in adding two kinds.
Above-mentioned antiseptic is sodium benzoate: 0.2 ~ 0.6 part, hydroxybenzoate 0.2 ~ 0.6 part, at least one in adding two kinds.
The second object of the present invention provides a kind of production method of the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract.
The second object of the present invention is achieved through the following technical solutions:
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract;
Second step: get abrasivus, foaming agent, wetting agent, thickening agent, sweeting agent are for subsequent use;
3rd step: cream processed, is first dispersed in wetting agent by thickening agent, separately sweeting agent, antiseptic is dissolved in the water, and under agitation makes it expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then abrasivus, foaming agent are added in glue successively and be fully uniformly mixed, then through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Abrasivus of getting described in above-mentioned second step is: silicon dioxide, calcium carbonate, calcium bicarbonate, at least one in adding three kinds; Described foaming agent is: sodium lauryl sulphate, sodium bicarbonate, ammonium bicarbonate, at least one in adding three kinds; Described wetting agent is: glycerol, sorbitol, butanediol, Polyethylene Glycol, at least one in adding four kinds; Described thickening agent is: sodium carboxymethyl cellulose, methylcellulose, guar gum, at least one in adding three kinds; Described sweeting agent is: saccharin sodium, sucrose add at least one in two kinds; Described essence is: Mentholum, fragrant citrus essence, Green tea essence, at least one in adding three kinds; Described corrosion inhibiter is Chile saltpeter, sodium nitrite, at least one in adding two kinds; Described antiseptic is sodium benzoate, hydroxybenzoate, at least one in adding two kinds.
The present invention compared with prior art, by the production of the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract, its effective ingredient is by parcels such as abrasivus, wetting agent, foaming agent, decrease the chance that effective ingredient contacts in oxygen, improve the stability of Galla Turcica (Galla Helepensis) effective ingredient, add product service life and number of times.The present invention passes through the interpolation of Galla Turcica (Galla Helepensis) effective ingredient in toothpaste is produced, impart that Galla Turcica (Galla Helepensis) toothpaste tool is antibacterial, effect of antiinflammatory, except cleaning one's teeth, also can be used for that the tooth that periodontal causes is aching and limp, masticatory atonia, gingival hemorrhage and aphtha of the mouth and tongue, laryngopharynx swelling and pain, halitosis etc.
Detailed description of the invention
Above Materials Examples has been operated by the following method:
Embodiment 1
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract.
Second step: get silica 10 part, calcium carbonate 25 parts, sodium lauryl sulphate 2 parts, glycerol 15 parts, sorbitol 15 parts, sodium carboxymethyl cellulose 1.5, saccharin sodium 0.6 part, 1.4 parts, essence are for subsequent use.
3rd step: cream processed, first by sodium carboxymethyl cellulose 1.5 parts, is dispersed in glycerol 15 parts, sorbitol 15 parts, another by saccharin sodium 0.6 part, Chile saltpeter 0.4 part, be dissolved in Purified Water 15 parts, under agitation make it expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then by Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract 3 parts, silica 10 part, calcium carbonate 25 parts, sodium lauryl sulphate 2 parts and 1.4 parts, essence, add successively in the glue after ageing and be fully uniformly mixed, again through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Embodiment 2
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract.
Second step: get silicon dioxide 30 parts, sodium lauryl sulphate 2.2 parts, glycerol 10 parts, sorbitol 20 parts, sodium carboxymethyl cellulose 0.5 part, saccharin sodium 0.3 part, 1.2 parts, essence are for subsequent use.
3rd step: cream processed, first by sodium carboxymethyl cellulose 0.5 part, be dispersed in glycerol 10 parts, sorbitol 20 parts, separately saccharin sodium 0.3 part, Chile saltpeter 0.3 part be dissolved in Purified Water 15 parts, under agitation it is made to expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract 2.4 parts, silicon dioxide 30 parts, sodium lauryl sulphate 2.2 parts and 1.2 parts, essence are added in the glue after ageing successively and be fully uniformly mixed, again through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Embodiment 3
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract.
Second step: get silicon dioxide 20 parts, calcium carbonate 10 parts, sodium lauryl sulphate 3 parts, glycerol 30 parts, sodium carboxymethyl cellulose 1.2 parts, saccharin sodium 0.5 part, 1.2 parts, essence are for subsequent use.
3rd step: cream processed, first will, as sodium carboxymethyl cellulose 1.2 parts, be dispersed in glycerol 30 parts, separately saccharin sodium 0.5 part, Chile saltpeter 0.3 part will be dissolved in Purified Water 25 parts, under agitation it is made to expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract 3.5 parts, silicon dioxide 20 parts, calcium carbonate 10 parts, sodium lauryl sulphate 3 parts and 1.2 parts, essence are added in the glue after ageing successively and be fully uniformly mixed, again through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Embodiment 4
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract.
Second step: get silica 15 parts, calcium carbonate 15 parts, sodium lauryl sulphate 2.5 parts, glycerol 20 parts, sorbitol 10 parts, sodium carboxymethyl cellulose 2.5 parts, saccharin sodium 0.4 part, 1.2 parts, essence are for subsequent use.
3rd step: cream processed, first sodium carboxymethyl cellulose 2.5 parts etc. is dispersed in glycerol 20 parts, sorbitol 10 parts, separately saccharin sodium 0.4 part, Chile saltpeter 0.5 part are dissolved in Purified Water 10 parts, under agitation make it expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract 0.5 part, silica 15 parts, calcium carbonate 15 parts, sodium lauryl sulphate 2.5 parts and 1.2 parts, essence are added in the glue after ageing successively and be fully uniformly mixed, again through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Embodiment 5
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract.
Second step: get calcium carbonate 30 parts, sodium lauryl sulphate 1.8 parts, sorbitol 30 parts, sodium carboxymethyl cellulose 1.8 parts, saccharin sodium 0.6 part, 1 part, essence are for subsequent use.
3rd step: cream processed, first by sodium carboxymethyl cellulose 1.8 parts, is dispersed in sorbitol 30 parts, another by saccharin sodium 0.6 part, Chile saltpeter 0.6 part, additive is dissolved in Purified Water 30 parts, under agitation makes it expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract 10 parts, calcium carbonate 30 parts, sodium lauryl sulphate 1.8 parts and 1 part, essence are added in the glue after ageing successively and be fully uniformly mixed, again through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Embodiment 6
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract.
Second step: get silicon dioxide 25 parts, calcium carbonate 15 parts, sodium lauryl sulphate, glycerol 25 parts, sorbitol 15 parts, sodium carboxymethyl cellulose 1 part, saccharin sodium 0.5 part, 1.3 parts, essence are for subsequent use.
3rd step: cream processed, first by sodium carboxymethyl cellulose 1 part, be dispersed in glycerol 25 parts, sorbitol 15 parts, separately by saccharin sodium 0.5 part, Chile saltpeter 0.5 part, be dissolved in Purified Water 20 parts, under agitation it is made to expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract 8 parts, silicon dioxide 25 parts, calcium carbonate 15 parts, sodium lauryl sulphate 4.5 parts and 1.3 parts, essence are added in the glue after ageing successively and be fully uniformly mixed, again through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
Claims (11)
1. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract, it is characterized in that: containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract: 0.5 ~ 10 part, thickening agent: 0.5 ~ 2.5 part, wetting agent: 10 ~ 30 parts, foaming agent: 2 ~ 5 parts, antiseptic: 0.2 ~ 0.6 part, corrosion inhibiter: 0.3 ~ 0.6 part, essence: 1 ~ 1.4 part, sweeting agent: 0.3 ~ 0.6 part, abrasivus: 10 ~ 30 parts, Purified Water: 5 ~ 30 parts, (material of getting is weight portion).
2. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, it is characterized in that: described wetting agent is: sorbitol: 10 ~ 30 parts, glycerol: 10 ~ 30 parts, butanediol: 10 ~ 15 parts, Polyethylene Glycol: 10 ~ 15 parts, at least one in adding four kinds.
3. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, it is characterized in that: described abrasivus is: calcium carbonate: 10 ~ 15 parts, silicon dioxide: 20 ~ 30 parts, calcium bicarbonate: 10 ~ 15 parts, at least one in adding three kinds.
4. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, it is characterized in that: described foaming agent is: sodium lauryl sulphate: 2 ~ 5 parts, sodium bicarbonate: 2 ~ 3 parts, ammonium bicarbonate: 2 ~ 3 parts, at least one in adding three kinds.
5. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, it is characterized in that: described thickening agent is: sodium carboxymethyl cellulose: 0.8 ~ 1.8 part, methylcellulose: 0.5 ~ 1.2 part, guar gum: 0.5 ~ 2 part, at least one in adding three kinds.
6. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, is characterized in that: described sweeting agent is: saccharin sodium: 0.3 ~ 0.6 part, sucrose: 0.3 ~ 0.6 part, at least one in adding two kinds.
7. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, it is characterized in that: described essence is: Mentholum: 1 ~ 1.4 part, fragrant citrus essence: 1 ~ 1.4 part, Green tea essence: 1 ~ 1.4 part, at least one in adding three kinds.
8. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, is characterized in that: described corrosion inhibiter is Chile saltpeter: 0.3 ~ 0.6 part, sodium nitrite: 0.3 ~ 0.6 part, at least one in adding two kinds.
9. the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 1, is characterized in that: described antiseptic is sodium benzoate: 0.2 ~ 0.6 part, hydroxybenzoate 0.2 ~ 0.6 part, at least one in adding two kinds.
10. the production method of the medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claims 1 to 9, carry out according to the following steps (material of getting is weight portion):
The first step: percolation after Galla Turcica (Galla Helepensis) soaks with petroleum ether, reclaims residue, volatilizes the petroleum ether in residue, then use deionized water reflux, extract, with extraction into ethyl acetate isopyknic with concentrated solution after extracting solution is concentrated, collect the supernatant, evaporate to dryness, obtains acetic acid ethyl ester extract;
Second step: get abrasivus, foaming agent, wetting agent, thickening agent, sweeting agent are for subsequent use.
3rd step: cream processed.First thickening agent etc. is dispersed in wetting agent, separately other a small amount of additives such as sweeting agent, antiseptic is dissolved in the water, under agitation make it expand into uniform colloid, also referred to as glue two kinds of solution mixing; And within 8 ~ 12 hours, carry out suitable ageing by standing for glue, then abrasivus, foaming agent and other powder additives and essence are added in glue successively and be fully uniformly mixed, then through grinding homogenizing, vacuum outgas becomes lotion of toothpaste.
The production method of 11. medicated toothpaste containing Galla Turcica (Galla Helepensis) acetic acid ethyl ester extract according to claim 10, the abrasivus of getting described in second step is: silicon dioxide, calcium carbonate, calcium bicarbonate, at least one in adding three kinds; Described foaming agent is: sodium lauryl sulphate, sodium bicarbonate, ammonium bicarbonate, at least one in adding three kinds; Described wetting agent is: glycerol, sorbitol, butanediol, Polyethylene Glycol, at least one in adding four kinds; Described thickening agent is: sodium carboxymethyl cellulose, methylcellulose, guar gum, at least one in adding three kinds; Described sweeting agent is: saccharin sodium, sucrose, at least one in adding two kinds; Described essence is: Mentholum, fragrant citrus essence, Green tea essence, at least one in adding three kinds; Described antiseptic is sodium benzoate, hydroxybenzoate, at least one in adding two kinds; Described corrosion inhibiter is: Chile saltpeter, sodium nitrite, at least one in adding two kinds.
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| CN201511008011.5A CN105534791A (en) | 2015-12-23 | 2015-12-23 | Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof |
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| CN201511008011.5A CN105534791A (en) | 2015-12-23 | 2015-12-23 | Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107789368A (en) * | 2017-09-30 | 2018-03-13 | 石河子大学 | Galla halepensis extract prepares method of hollow micro capsule and application thereof |
| CN109260130A (en) * | 2018-10-26 | 2019-01-25 | 纳诺神蜂（福建）个人护理用品有限公司 | A kind of children's mothproof toothpaste and preparation method thereof |
| CN113576961A (en) * | 2021-07-20 | 2021-11-02 | 海南林鹏茶业有限公司 | Agilawood toothpaste and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107789368A (en) * | 2017-09-30 | 2018-03-13 | 石河子大学 | Galla halepensis extract prepares method of hollow micro capsule and application thereof |
| CN109260130A (en) * | 2018-10-26 | 2019-01-25 | 纳诺神蜂（福建）个人护理用品有限公司 | A kind of children's mothproof toothpaste and preparation method thereof |
| CN113576961A (en) * | 2021-07-20 | 2021-11-02 | 海南林鹏茶业有限公司 | Agilawood toothpaste and preparation method thereof |
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Application publication date: 20160504 |