CN105523861A - Suspension-type vinasse fermented liquid fertilizer and preparation method thereof - Google Patents
Suspension-type vinasse fermented liquid fertilizer and preparation method thereof Download PDFInfo
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- CN105523861A CN105523861A CN201610105625.3A CN201610105625A CN105523861A CN 105523861 A CN105523861 A CN 105523861A CN 201610105625 A CN201610105625 A CN 201610105625A CN 105523861 A CN105523861 A CN 105523861A
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- Prior art keywords
- vinasse
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
- C05F5/008—Waste from biochemical processing of material, e.g. fermentation, breweries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Environmental & Geological Engineering (AREA)
- Fertilizers (AREA)
Abstract
The invention relates to suspension-type vinasse fermented liquid fertilizer and a preparation method thereof. The suspension-type vinasse fermented liquid comprises, by weight, 85-90 parts of mother liquor treated by vinasse fermentation liquor, 1-2 parts of suspension stabilizers, 3-5 parts of urea, 1-3 parts of diammonium phosphate and 2-6 parts of potassium sulphate. The preparation method includes the steps of vinasse pretreatment, anaerobic fermentation, solid-liquid separation, grinding, vibrating-screen separation, product compounding, product packaging and the like. The suspension-type vinasse fermented liquid fertilizer and the preparation method thereof have the advantages that the high-efficiency liquid fertilizer with high economic added value is produced, so that crop yield can be increased, fruit quality and soil fertility can be improved, and crop pests can be prevented and reduced.
Description
Technical field
The invention belongs to fertilizer field, be specifically related to a kind of suspension-type vinasse fermentation liquid fertilizer and preparation method thereof.
Background technology
In White wine brewing process, the residue steamed in cereal after alcohol or alcoholic beverage is called vinasse.Vinasse organic content is high, and rich in proteins, Mierocrystalline cellulose, starch etc., be rich in nitrogen, phosphorus, potassium, calcium and various trace element, simultaneously also perishable, rotten, smelly, grows mosquitos and flies.Vinasse anaerobic fermentation technology has the outstanding advantages such as resource conversion efficiency is high, adaptability to raw materials is wide, but the bulk fermentation raffinate that current large-scale vinasse anaerobically fermenting engineering is formed is because transporting the reason such as inconvenience, processing cost, cause major part directly to enter environment, cause the nitrate in environment water eutrophication, underground water to increase and regional soil eutrophication etc.For the purpose of environment protection in conventional biochemical-materialization governance process not only consume fermentation raffinate in organic matter and nutritive element after qualified discharge; although protect environment; but high cost; the consumption energy wastes the nutritive substance in raffinate simultaneously; so far do not find one can obtain certain economic benefit yet, the desirable technique of the fermentation minimizing of raffinate, resource utilization and harmless treatment can be reached again.
Vinasse anaerobic fermented liquid is for supplementary plant-growth desired nutritional element, stimulating plant physiologically active, suppress pathogenic micro-organism growth etc. to have comparatively significantly to act on, there is the slow fertilizer efficiency feature had both of speed, there is the double effects of bio-feritlizer and biological pesticide, but vinasse anaerobic fermented liquid xylogen and content of cellulose high, liquid thickness uses inconvenience, local usage quantity conference causes soil surface crust to be unfavorable for plant-growth, these factors seriously govern vinasse anaerobic fermented liquid recycling, the enthusiasm that peasant utilizes is not high, limit the feasibility that agricultural is dissolved to a certain extent.Vinasse anaerobic fermented liquid dissolve difficult also directly limit vinasse biological flue gas engineering popularization and long-term efficient stable run.
Summary of the invention
The object of the present invention is to provide a kind of suspension-type vinasse fermentation liquid fertilizer and preparation method thereof, produce the liquid fertilizer product of efficient high economic value added, can crop yield be increased, improve fruit quality, increase soil fertility, prevention and minimizing crop pest.
The object of the invention is to be achieved through the following technical solutions:
A kind of suspension-type vinasse fermentation liquid fertilizer, comprises the raw material of following parts by weight: mother liquor 85-90 part, suspension stabilizer 1-2 part, urea 3-5 part, diammonium phosphate 1-3 part and potassium sulfate 2-6 part after the process of vinasse fermentation liquid.
The preparation method of described suspension-type vinasse fermentation liquid fertilizer, comprises the following steps:
1) vinasse add natural pond liquid and inoculate and add the nitrogen that a small amount of urea supplements microorganism growth needs, carry out pre-treatment;
2) anaerobically fermenting that anaerobic fermentation tank carries out 35-45 days is added after vinasse pre-treatment;
3) bulk fermentation raffinate can be produced after producing biogas, its water ratio is usually more than 90%, solid content is 8%-9%, segregative solid matter and natural pond slag is isolated through spiral solid-liquid separating machine, water content is 75%, the brownish black thick liquid separated and natural pond liquid, water content is 93%-95%.
4) natural pond liquid grinds emulsification through colloidal mill, and most of suspended particulate is ground to below 200 orders;
5) the natural pond liquid after colloidal mill grinding, by 300 order vibratory screening apparatuss, obtains the mother liquor of natural pond liquid as formula for a product of the suspended particle of below 300 orders;
6) add suspension stabilizer, urea, diammonium phosphate and potassium sulfate by proportioning raw materials of the present invention, fully stir all dissolvings and mix;
7) product is filling.
Wherein,
Vinasse fermentation liquid second-stage treatment liquid, the trace elements such as iron, zinc, copper are provided, and amino acid, small molecular organic acid, growth hormone, multiple natural Broad spectrum antibiotics, lignocellulolytic enzymes class etc. are organic and part nutrient content, with a small amount of nitrogen, phosphorus, potassium, micronutrient element needed for plant-growth can be supplemented, stimulating plant physiologically active, suppresses pathogenic micro-organism growth.
Suspension stabilizer, its composition has carboxymethyl cellulose etc., increases vinasse fermentation liquid suspended particle stability.
Urea, diammonium phosphate and potassium sulfate, provide macroelement nitrogen, phosphorus, potassium, meets the nutrient demand that crop grows fast.
Beneficial effect of the present invention is:
Containing abundant nutritive element and organic substance in vinasse fermentation liquid, but the liquid-solid amount of vinasse fermentation is high, comparatively thickness, the demixing phenomenon of easy generation solid-liquid separation, lower floor's sticky precipitate is difficult to flowing, can cause pumping difficulties as directly used the equipment such as water pump, burn the consequences such as motor, fermented liquid thickness instability is difficult to transport and preserves on the one hand, peasant uses inconvenience on the other hand, and topical application too much can cause sealing of soil, is difficult to extensively use on land for growing field crops and industrialized agriculture.After colloidal mill grinding in the present invention and vibratory screening apparatus sorting, the suspended particle particle diameter of vinasse fermentation liquid greatly reduces and comparatively even, good fluidity, after fine processing technology and fertilizer commercial treatment, organotrophy particle is carried out grinding and classifying and carries out maximization and collect, facilitate peasant and large-scale agricultural planting base to use.
Compare other water-soluble fertilizer, vinasse fermentation liquid fertilizer contains the material such as the various nutrient elements such as nitrogen, phosphorus, potassium and each amino acid, VITAMIN, protein, Plant hormones regulators,gibberellins, growth hormone, carbohydrate, nucleic acid and microbiotic, very important regulating and controlling effect is had to growth and development of plants, improve the nutrition content such as VITAMIN, sugar of crop and fruit, greatly promote mouthfeel and the quality of fruit.About impelling crop maturity to shift to an earlier date 1-2 week, and later stage early ageing can be prevented, extend the crop harvesting phase.There is the slow fertilizer efficiency feature had both of speed, there is the double effects of bio-feritlizer and biological pesticide, there is the characteristic of green, efficient, environmental protection.Containing antibiotic and improve stress resistance of plant class material etc., there is unique control plant pest effect, such as anti-ly to eliminate aphis, prevent and treat fruit tree red spider mite, prevent and treat wheat scab, watermelon blight etc., improve stress resistance of plant.
Manure trial result shows: on summer squash, use product of the present invention and simple applications of farmyard manure is tested, the ripe summer squash fruit type of results statistics, weight parameter comparison diagram represent: after products applied, fruit is thick, fruit is long and weight all promotes to some extent than contrast, reduced form Vc increases, illustrate that product is compared common farm manure medium trace element and amino acid etc. and promoted that the substances content of Vc synthesis is high, compare farm manure nutrition more comprehensively; After products applied, the nitrate nitrogen content of summer squash fruit significantly declines, and illustrates that rate of fertilizer application is lower, under the relatively less condition of fertilising, but improve crop yield and quality, illustrates product to fruit and vegetable absorption and the fertilizer efficiency of growing remarkable.
Accompanying drawing explanation
Fig. 1 is the process flow sheet of suspension-type vinasse fermentation liquid fertilizer preparation method of the present invention.
Embodiment
Below by embodiment, the present invention is described in further detail, is intended to non-limiting the present invention for illustration of the present invention.
Embodiment 1
Suspension-type vinasse fermentation liquid fertilizer described in the present embodiment, comprises the raw material of following proportioning: 89.2 parts, mother liquor after the process of vinasse fermentation liquid, suspension stabilizer 1 part, 3 parts, urea, diammonium phosphate 1.2 parts, potassium sulfate 5.6 parts.
Embodiment 2
Suspension-type vinasse fermentation liquid fertilizer described in the present embodiment, comprises the raw material of following proportioning: 89.5 parts, mother liquor after the process of vinasse fermentation liquid, suspension stabilizer 1 part, 4.5 parts, urea, diammonium phosphate 2.5 parts, potassium sulfate 2.5 parts.
Embodiment 3
Suspension-type vinasse fermentation liquid fertilizer described in the present embodiment, comprises the raw material of following proportioning: 90 parts, mother liquor after the process of vinasse fermentation liquid, suspension stabilizer 1 part, 3 parts, urea, diammonium phosphate 3 parts, potassium sulfate 3 parts.
Embodiment 4
Suspension-type vinasse fermentation liquid fertilizer described in the present embodiment, comprises the raw material of following proportioning: 85 parts, mother liquor after the process of vinasse fermentation liquid, suspension stabilizer 2 parts, 5 parts, urea, diammonium phosphate 1 part, potassium sulfate 4 parts.
Embodiment 5
Suspension-type vinasse fermentation liquid fertilizer described in the present embodiment, comprises the raw material of following proportioning: 87 parts, mother liquor after the process of vinasse fermentation liquid, suspension stabilizer 1.5 parts, 3 parts, urea, diammonium phosphate 2 parts, potassium sulfate 6 parts.
The preparation method of the suspension-type vinasse fermentation liquid fertilizer described in above-described embodiment, comprises the following steps:
1) vinasse add natural pond liquid and inoculate and add the nitrogen that a small amount of urea supplements microorganism growth needs, carry out pre-treatment;
2) anaerobically fermenting that anaerobic fermentation tank carries out 35-45 days is added after vinasse pre-treatment;
3) bulk fermentation raffinate can be produced after producing biogas, its water ratio is usually more than 90%, solid content is 8%-9%, segregative solid matter and natural pond slag is isolated through spiral solid-liquid separating machine, water content is 75%, the brownish black thick liquid separated and natural pond liquid, water content is 93%-95%.
4) natural pond liquid grinds emulsification through colloidal mill, and most of suspended particulate is ground to below 200 orders;
5) the natural pond liquid after colloidal mill grinding, by 300 order vibratory screening apparatuss, obtains the mother liquor of natural pond liquid as formula for a product of the suspended particle of below 300 orders;
6) add suspension stabilizer, urea, diammonium phosphate and potassium sulfate by the proportioning raw materials described in above embodiment, fully stir all dissolvings and mix;
7) product is filling.
Manure trial result shows: on summer squash, use product of the present invention and simple applications of farmyard manure is tested, the ripe summer squash fruit type of results statistics, weight parameter comparison diagram represent: after products applied, fruit is thick, fruit is long and weight all promotes to some extent than contrast, reduced form Vc increases, illustrate that product is compared common farm manure medium trace element and amino acid etc. and promoted that the substances content of Vc synthesis is high, compare farm manure nutrition more comprehensively; After products applied, the nitrate nitrogen content of summer squash fruit significantly declines, and illustrates that rate of fertilizer application is lower, under the relatively less condition of fertilising, but improve crop yield and quality, illustrates product to fruit and vegetable absorption and the fertilizer efficiency of growing remarkable.
Above-mentionedly only several specific embodiments in the present invention to be illustrated, but can not protection scope of the present invention to be defined as, every according to the change of the equivalence done by design spirit in the present invention or modify, all should think and fall into protection scope of the present invention.
Claims (2)
1. a suspension-type vinasse fermentation liquid fertilizer, is characterized in that, comprises the raw material of following parts by weight: mother liquor 85-90 part, suspension stabilizer 1-2 part, urea 3-5 part, diammonium phosphate 1-3 part and potassium sulfate 2-6 part after the process of vinasse fermentation liquid.
2. the preparation method of suspension-type vinasse fermentation liquid fertilizer according to claim 1, is characterized in that, comprise the following steps:
1) vinasse add natural pond liquid and inoculate and add the nitrogen that a small amount of urea supplements microorganism growth needs, carry out pre-treatment;
2) anaerobically fermenting that anaerobic fermentation tank carries out 35-45 days is added after vinasse pre-treatment;
3) bulk fermentation raffinate can be produced after producing biogas, its water ratio is usually more than 90%, solid content is 8%-9%, segregative solid matter and natural pond slag is isolated through spiral solid-liquid separating machine, water content is 75%, the brownish black thick liquid separated and natural pond liquid, water content is 93%-95%.
4) natural pond liquid grinds emulsification through colloidal mill, and most of suspended particulate is ground to below 200 orders;
5) the natural pond liquid after colloidal mill grinding, by 300 order vibratory screening apparatuss, obtains the mother liquor of natural pond liquid as formula for a product of the suspended particle of below 300 orders;
6) add suspension stabilizer, urea, diammonium phosphate and potassium sulfate by proportioning raw materials according to claim 1, fully stir all dissolvings and mix;
7) product is filling.
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| CN201610105625.3A CN105523861A (en) | 2016-02-25 | 2016-02-25 | Suspension-type vinasse fermented liquid fertilizer and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106431581A (en) * | 2016-08-31 | 2017-02-22 | 中国农业科学院农业资源与农业区划研究所 | Organic liquid fertilizer based on concentrated biogas slurry as well as preparation and application methods thereof |
| CN107056383A (en) * | 2017-04-25 | 2017-08-18 | 中国地质大学（北京） | A kind of high solid phase stability concentrates the preparation method of biogas slurry |
| CN107188658A (en) * | 2017-04-25 | 2017-09-22 | 中国地质大学（北京） | A kind of biogas slurry rheology modifier and its application in high solid phase concentrates biogas slurry preparation |
| CN107986875A (en) * | 2017-12-20 | 2018-05-04 | 四川国科中农生物科技有限公司 | A kind of humic acid Water soluble fertilizer and its preparation process using yellow water as carrier |
| CN108314536A (en) * | 2018-03-27 | 2018-07-24 | 贵州茅台酒厂（集团）绿生有机肥有限责任公司 | A method of producing Liquid Fertilizer using biogas slurry |
| CN108546177A (en) * | 2018-03-21 | 2018-09-18 | 东莞翔液体肥料有限公司 | A kind of efficient biogas slurry organic suspension liquid fertilizer and preparation method thereof |
| CN108558489A (en) * | 2018-02-06 | 2018-09-21 | 金华市飞凌生物科技有限公司 | A kind of preparation method of slow-release compound fertilizer |
| CN108834754A (en) * | 2018-08-09 | 2018-11-20 | 合肥福泉现代农业科技有限公司 | A kind of method of fruit fermentation culture material cultured mushroom |
| CN108863657A (en) * | 2018-07-25 | 2018-11-23 | 娄作富 | It is a kind of to utilize vinasse and spent wash production bio-organic liquid fertilizer and its method |
| CN111533626A (en) * | 2020-05-19 | 2020-08-14 | 郑州正赢石化有限公司 | Liquid fertilizer using vinasse, pond residue leachate or waste vegetable oil as substrate and preparation method thereof |
| CN113527001A (en) * | 2020-04-13 | 2021-10-22 | 石小和 | Lees treatment method, foliar fertilizer, organic fertilizer and preparation method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106431581A (en) * | 2016-08-31 | 2017-02-22 | 中国农业科学院农业资源与农业区划研究所 | Organic liquid fertilizer based on concentrated biogas slurry as well as preparation and application methods thereof |
| CN107056383A (en) * | 2017-04-25 | 2017-08-18 | 中国地质大学（北京） | A kind of high solid phase stability concentrates the preparation method of biogas slurry |
| CN107188658A (en) * | 2017-04-25 | 2017-09-22 | 中国地质大学（北京） | A kind of biogas slurry rheology modifier and its application in high solid phase concentrates biogas slurry preparation |
| CN107188658B (en) * | 2017-04-25 | 2020-11-17 | 中国地质大学（北京） | Biogas slurry rheological property regulator and application thereof in preparation of high-solid-phase concentrated biogas slurry |
| CN107986875A (en) * | 2017-12-20 | 2018-05-04 | 四川国科中农生物科技有限公司 | A kind of humic acid Water soluble fertilizer and its preparation process using yellow water as carrier |
| CN108558489A (en) * | 2018-02-06 | 2018-09-21 | 金华市飞凌生物科技有限公司 | A kind of preparation method of slow-release compound fertilizer |
| CN108546177A (en) * | 2018-03-21 | 2018-09-18 | 东莞翔液体肥料有限公司 | A kind of efficient biogas slurry organic suspension liquid fertilizer and preparation method thereof |
| CN108314536A (en) * | 2018-03-27 | 2018-07-24 | 贵州茅台酒厂（集团）绿生有机肥有限责任公司 | A method of producing Liquid Fertilizer using biogas slurry |
| CN108863657A (en) * | 2018-07-25 | 2018-11-23 | 娄作富 | It is a kind of to utilize vinasse and spent wash production bio-organic liquid fertilizer and its method |
| CN108834754A (en) * | 2018-08-09 | 2018-11-20 | 合肥福泉现代农业科技有限公司 | A kind of method of fruit fermentation culture material cultured mushroom |
| CN113527001A (en) * | 2020-04-13 | 2021-10-22 | 石小和 | Lees treatment method, foliar fertilizer, organic fertilizer and preparation method thereof |
| CN111533626A (en) * | 2020-05-19 | 2020-08-14 | 郑州正赢石化有限公司 | Liquid fertilizer using vinasse, pond residue leachate or waste vegetable oil as substrate and preparation method thereof |
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Application publication date: 20160427 |