CN105400617B - A kind of preparation method of cold handmade soap processed - Google Patents
A kind of preparation method of cold handmade soap processed Download PDFInfo
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- CN105400617B CN105400617B CN201510962610.4A CN201510962610A CN105400617B CN 105400617 B CN105400617 B CN 105400617B CN 201510962610 A CN201510962610 A CN 201510962610A CN 105400617 B CN105400617 B CN 105400617B
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- sodium hydroxide
- handmade soap
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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Abstract
The present invention relates to a kind of preparation methods of cold handmade soap processed, this method processing step is simple, traditional sodium hydrate aqueous solution is replaced with the dispersion liquid of sodium hydroxide or itself and glycerine, since sodium hydroxide can not be dissolved completely in glycerine, simply disperse in glycerine, the problem of reaction speed is too fast after sodium hydroxide solution is mixed with grease is avoided, initial stage saponification speed is reduced, saponification speed is made to be effectively controlled；With the progress of saponification, glycerine can be continuously increased as reaction product, so as to help sodium hydroxide more fully scattered, sodium hydroxide is promoted to accelerate reaction speed with remaining grease, since the present invention is anhydrous formulations, soap lye is into being not required water evaporation process after soap so that fabrication cycle significantly shortens；Nutriment is added in solidapowder form, is effectively prevented not alkaline-resisting nutriment and is reacted with sodium hydroxide molecule contacts, the active ingredient of nutriment is remained in soap body, has given full play to the skin care effect of nutriment.
Description
Technical field
The present invention relates to the preparing technical fields of handmade soap, refer specifically to a kind of preparation method of cold handmade soap processed.
Background technology
In the prior art, the manufacture craft of handmade soap is generally divided into following a few classes：
1) preparation method again is melted, i.e., by, with additives mixed, another rise injects mold, simple fast after industrial soap base heating and melting
The soap of various moulding is made fastly；Handmade soap washing effect made of this technique and the basic indifference of commercially available perfumed soap, do not dash forward
Go out advantage；
2) soapmaking method is regenerated, i.e., is heated the Manufactured perfumed soap addition suitable quantity of water after silk that is cut into small pieces or dig, again
Enter to be molded as the soap of given shape；For this technique at present using less, handmade soap shaping is bad, and washing effect can under
Drop；
3) liquid soap is made by saponification raw material and grease reaction of potassium hydroxide in liquid soap method；Since people are more accustomed to
With solid soap, thus this technique is not universal；
4) cold preparation method, this is the most ancient soap manufacturing process of the mankind, it is that sodium hydroxide solution is added to oil at room temperature
Saponification generation sodium soap and glycerine occur in fat, foam exquisiteness is made and enriches, there is superpower clean power and moisturizing effect
Cold congealed fat soap processed, cold handmade soap processed can completely decompose by natural environment, will not cause burden and the pollution of soil environment；Together
When, since reaction temperature is low, the nutritional ingredient of grease and various natural additives is remained to greatest extent；But this work
Skill is more demanding to reaction controlling, and saponification excessive velocities be easy to cause soap lye and solidified before mould is entered；And due to needing foot
The enough time allows grease fully to be reacted with remaining sodium hydroxide, and general fabrication cycle is longer, no less than January；
5) hot preparation method, this method is the raising saponification temperature on the basis of cold preparation method, although fabrication cycle can be shortened,
The fine and smooth degree of soap body can be influenced, and be easy to cause nutrient loss in raw material.
For above-mentioned handmade soap manufacture craft of the prior art, cold preparation method prepare handmade soap be technical difficulty most
Greatly while it is also the highest handmade soap of added value.In recent years, more have been disclosed in the prior art on cold handmade soap system processed
The patent report of standby technique, such as：
Application publication number is the Chinese invention patent application of CN104130888A《A kind of special formula of cold process handmade soap and its
Preparation method and application》(application number：201410385926.7) a kind of method is disclosed, basic grease is first heated to 50 DEG C
More than, then 40 DEG C or so of sodium hydroxide saturated solution added in grease, and sequentially add preservative in whipping process, plant
Object additive, essential oil, dispensing oil and extract prepare handmade soap.Although not using chemical synthesis ingredient, it is prepared this method
The concentration of alkali and temperature are all higher in the process, are easy to cause reaction and are difficult to control, and additive etc. can be caused to be readily destroyed by base.
Application publication number is the Chinese invention patent application of CN 103834505A《One kind smears tea handmade soap》(application number：
201410113357.0) a kind of method is disclosed, first add in stearic acid in lye and is warming up to 65 DEG C, is then added in all kinds of
Oil and matcha powder carry out soapmaking.This method is to generate odium stearate (most common soap base) using stearic acid and alkali reaction, so as to
The basicity of handmade soap is reduced to a certain extent, but simultaneously, the quality of soap can also be inferior to the cold system modulated completely with grease with alkali
Handmade soap, and the nutritional ingredient that higher reaction temperature will also result in oil is destroyed.
Application publication number is the Chinese invention patent application of CN 104277941A《A kind of production method of aloe handmade soap》
(application number：201410514581.0) a kind of method is disclosed, first oil is added in lye and is reacted, adds fresh aloe system
Soap.In said program, greatly speeded up since grease is added to after saponification reaction in lye, easily cause to react uncontrollable and soap
The saponification degree for changing liquid is uneven.
Application publication number is the Chinese invention patent application of CN 104327983A《A kind of production technology of handmade soap》(Shen
Please number：201410651028.1) a kind of method is disclosed, first mixes oily alkali, enters mould after high rotating speed stirring a few hours, enters mould
It is dried again with vacuum drier afterwards, such method is to accelerate the speed of moisture evaporation, to grease in soap body and remaining lye
Saponification there is no apparent acceleration effect.
Therefore, cold handmade soap processed of the prior art has the following problems：
1) saponification speed is difficult to control.The concentration and temperature of lye, reaction rotating speed, the proportioning of alkali and oil can all influence
The speed of saponification, reaction speed can influence very much soap lye and enter mould soon, and handmade soap necessarily requires soap lye to enter mould, if before entering mould
Solidification then causes to prepare failure；
2) fabrication cycle is long.Soap lye enters after mould, it is necessary to which the time of one month or more is so that alkaline reaction is complete, while makes soap
Moisture evaporation in liquid is gone out, this is resulted in, and the fabrication cycle of cold handmade soap processed is too long, and cost of manufacture greatly increases；
3) beneficiating ingredient of nutriment is difficult to save from damage.In Hydroxyapatite Coatings in Alkaline Solution, water can quickly dissolve water-soluble additive,
The nutriments such as not alkaline-resisting milk, fruit syrup, hydrosol, chlorophyll and alkali reaction cause its beneficiating ingredient to fail.For this
Problem, Authorization Notice No. are the Chinese invention patent of CN103224848B《A kind of craft cold process soap and preparation method thereof》(application
Number：201310157112.3) a kind of method is proposed, is first wrapped up not alkaline-resisting substance with high molecular material, then in soap
Change the addition of reaction later stage, this method reduces destruction of the lye to not alkaline-resisting nutriment to a certain extent, still,
Its dispersion effect can be declined after nutriment is wrapped, and some natural polymers such as carbohydrate, protein, lipid
Material can also react in itself with alkali, cause this package action that can gradually weaken in maturing process, still there are nutriments
With the possibility of alkaline reaction failure.
The content of the invention
The technical problem to be solved by the invention for the present situation of prior art is to provide a kind of process is simple, energy
Effectively control saponification speed, the preparation method for the cold handmade soap processed for shortening fabrication cycle and nutritional ingredient being enable to save from damage.
Technical solution is used by the present invention solves above-mentioned technical problem：A kind of preparation method of cold handmade soap processed,
It is characterized in that comprising the following steps：
(1) by weight, 7~14 parts of sodium hydroxides are added in 0.1~20 part of glycerine, with 1000~5000rpm's
Rotating speed cutting emulsifies 0.5~2 minute, and sodium hydroxide glycerine dispersion liquid is made；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 parts of greases, at 20~40 DEG C with
The rotating speed cutting of 1000~5000rpm emulsifies 0.5~2 minute；
(3) emulsification pretreatment machine is closed, additive is added in into mixed liquor obtained by step (2), and is turned with 100~300rpm
Speed stirring 0.5~2 minute, is made saponification liquor；
(4) saponification liquor for obtaining step (3) injects mold, and moulding after 1~3 day was using maturation in 5~10 days
It can.
A kind of preparation method of cold handmade soap processed, it is characterised in that comprise the following steps：
(1) by weight, 7~14 parts of sodium hydroxides are mixed with 100 parts of greases, at 20~40 DEG C with 1000~
The rotating speed cutting of 5000rpm emulsifies 0.5~2 minute；
(2) emulsification pretreatment machine is closed, additive is added in into mixed liquor obtained by step (1), and is turned with 100~300rpm
Speed stirring 0.5~2 minute, is made saponification liquor；
(3) saponification liquor for obtaining step (2) injects mold, and moulding after 1~3 day was using maturation in 5~10 days
It can.
In the above embodiments, the additive described in step (3) is nutriment and/or natural essential oil and/or natural
Preservative.
Preferably, the additive includes 0.1~5 part of nutriment, 0.1~1 part of natural essential oil and 0.1~1 part
Natural antiseptic agent.
As an improvement, the nutriment adds in powder form, which is selected from dried milk, fruit
Juice, hydrosol, herb powder, bamboo charcoal, red bean, smear tea at chlorophyll, can be one kind therein, or two or more of
Mixture.Nutriment is added in powder form, can effectively avoid not alkaline-resisting nutriment and sodium hydroxide molecule contacts
Reaction so as to which the active ingredient of nutriment is remained in soap body, gives full play to the skin care effect of nutriment.
Preferably, the natural essential oil is selected from Lavender, lemon, tea tree ethereal oil, Rosa Damascana, chamomile
Essential oil, sweet orange oil, bamboo charcoal essential oil can be one kind therein, or two or more of mixtures.
Preferably, the natural antiseptic agent is selected from vitamin E, honey, propolis, essential oil, tea polyphenols, allicin, can
Think one kind therein, or two or more of mixtures.
Preferably, the grease is selected from coconut oil, olive oil, palm oil, canola oil, sesame oil, cocoa butter, soybean
Oil, Sweet Almond Oil, vegetalitas white oil, shea butter, Groomwell root oil, castor oil, Camellia oil, SIMMONDSIA CHINENSIS SEED OIL, rice bran oil, walnut oil,
Sunflower oil, Avocado Oil, wheat-germ oil, rose hip oil, peanut oil, linseed oil, macadamia nut oil, evening primrose oil, grape seed oil,
Hazelnut oil can be one kind therein, or two or more of mixtures.
Compared with prior art, the advantage of the invention is that：Present invention process method is simple, with sodium hydroxide in itself or its
Traditional sodium hydrate aqueous solution is replaced with the dispersion liquid of glycerine, using whole non-aqueous technique, since sodium hydroxide can not be complete
Fully dissolved is simply disperseed in glycerine in glycerine, avoids reaction speed after sodium hydroxide solution is mixed with grease
The problem of too fast, reduces the speed of initial stage saponification, so that saponification speed is effectively controlled；As saponification is anti-
The progress answered, glycerine can be continuously increased as reaction product, i.e., the amounts of glycerol in entire reaction system as dispersion is gradual
Increase, so as to help sodium hydroxide more fully scattered, sodium hydroxide is promoted to accelerate reaction speed with remaining grease, made entire
Saponification progress faster, better than traditional handicraft, also, since the present invention is anhydrous formulations, soap lye is into being not required moisture after soap
Evaporation process so that fabrication cycle significantly shortens；Meanwhile the nutriment in the present invention is added in solidapowder form, and it is whole
Anhydrous participation in a preparation process, sodium hydroxide glycerine dispersion liquid can not dissolved solid pulverulence nutriment, this is very
It avoids not alkaline-resisting nutriment in big degree to react with sodium hydroxide molecule contacts, so as to by the active ingredient of nutriment
It remaines in soap body, gives full play to the effective efficiency of nutriment.
Description of the drawings
Fig. 1 is the structure diagram of preparation method of the embodiment of the present invention.
Specific embodiment
The present invention is described in further detail below in conjunction with attached drawing embodiment.
Embodiment 1：
As shown in Figure 1, the preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 7 parts of sodium hydroxides are added in 10 parts of glycerine, 0.5 is emulsified with the rotating speed cutting of 1000rpm
Minute, sodium hydroxide glycerine dispersion liquid is made；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 portions of coconut oil, at 20 DEG C with
The rotating speed cutting of 1000rpm emulsifies 0.5 minute；
(3) emulsification pretreatment machine is closed, 0.1 part of milk powder, 0.1 part of lavender essence are added in into mixed liquor obtained by step (2)
Oil and 0.1 part of vitamin E, and stirred 0.5 minute with the rotating speed of 100rpm, saponification liquor is made；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 1 day, using maturation in 10 days.
Embodiment 2：
The preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 14 parts of sodium hydroxides are added in 20 parts of glycerine, 2 points is emulsified with the rotating speed cutting of 5000rpm
Sodium hydroxide glycerine dispersion liquid is made in clock；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 parts of Sweet Almond Oils, at 40 DEG C with
The rotating speed cutting of 5000rpm emulsifies 2 minutes；
(3) emulsification pretreatment machine is closed, 5 parts of herb powders, 1 part of Rosa Damascana and 1 are added in into mixed liquor obtained by step (2)
Part propolis, and stirred 2 minutes with the rotating speed of 300rpm, saponification liquor is made；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 3 days, using maturation in 10 days.
Embodiment 3：
The preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 10 parts of sodium hydroxides are added in 15 parts of glycerine, 1 point is emulsified with the rotating speed cutting of 3000rpm
Sodium hydroxide glycerine dispersion liquid is made in clock；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 parts of rose hip oils, at 30 DEG C with
The rotating speed cutting of 2000rpm emulsifies 0.5~2 minute；
(3) close emulsification pretreatment machine, added in the mixed liquor obtained by the step (2) 2 parts of matcha powders, 0.5 part of tea tree ethereal oil and
0.5 part of honey, and stirred 1 minute with the rotating speed of 200rpm, saponification liquor is made；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 2 days, using maturation in 7 days.
Embodiment 4：
The preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 8 parts of sodium hydroxides are added in 8 parts of glycerine, 0.5 point is emulsified with the rotating speed cutting of 4000rpm
Sodium hydroxide glycerine dispersion liquid is made in clock；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 parts of grape seed oils, at 35 DEG C with
The rotating speed cutting of 1000rpm emulsifies 2 minutes；
(3) emulsification pretreatment machine is closed, 3 parts of bamboo charcoal powders, 0.5 part of sweet orange oil are added in into mixed liquor obtained by step (2), and
It is stirred 0.5 minute with the rotating speed of 150rpm, saponification liquor is made；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 2 days, using maturation in 6 days.
Embodiment 5：
The preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 12 parts of sodium hydroxides are added in 0.1 part of glycerine, 2 is emulsified with the rotating speed cutting of 5000rpm
Minute, sodium hydroxide glycerine dispersion liquid is made；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 parts of macadamia nut oils, at 40 DEG C with
The rotating speed cutting of 3000rpm emulsifies 1 minute；
(3) emulsification pretreatment machine is closed, 4 parts of roses are added in into mixed liquor obtained by step (2), and are turned with 300rpm
Speed stirring 2 minutes, is made saponification liquor；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 1 day, using maturation in 5 days.
Embodiment 6：
The preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 14 parts of sodium hydroxides are added in 20 parts of glycerine, 2 points is emulsified with the rotating speed cutting of 5000rpm
Sodium hydroxide glycerine dispersion liquid is made in clock；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 40 parts of Sweet Almond Oils, 60 parts of hazelnut oils,
It is emulsified 2 minutes with the rotating speed cutting of 5000rpm at 40 DEG C；
(3) emulsification pretreatment machine is closed, 5 parts of herb powders, 1 part of Rosa Damascana and 1 are added in into mixed liquor obtained by step (2)
Part propolis, and stirred 2 minutes with the rotating speed of 300rpm, saponification liquor is made；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 3 days, using maturation in 10 days.
Embodiment 7：
As shown in Figure 1, the preparation method of the cold handmade soap processed of the present embodiment comprises the following steps：
(1) by weight, 10 parts of sodium hydroxides with 100 parts of hazelnut oils are mixed, is cut at 40 DEG C with the rotating speed of 4000rpm
Cut emulsification 2 minutes；
(2) emulsification pretreatment machine is closed, 5 parts of apple juice powders, 0.6 part of lemon are added in into mixed liquor obtained by step (1)
And 0.2 part of tea polyphenols, and stirred 1 minute with the rotating speed of 300rpm, saponification liquor is made；
(3) saponification liquor for obtaining step (2) injects mold, moulding after 2 days, using maturation in 7 days.
Claims (8)
1. a kind of preparation method of cold handmade soap processed, it is characterised in that comprise the following steps：
(1) by weight, 7~14 parts of sodium hydroxides are added in 0.1~20 part of glycerine, with the rotating speed of 1000~5000rpm
Sodium hydroxide glycerine dispersion liquid is made in emulsification pretreatment 0.5~2 minute；
(2) the sodium hydroxide glycerine dispersion liquid that step (1) obtains is mixed with 100 parts of greases, at 20~40 DEG C with 1000~
The rotating speed cutting of 5000rpm emulsifies 0.5~2 minute；
(3) emulsification pretreatment machine is closed, additive is added in into mixed liquor obtained by step (2), and is stirred with the rotating speed of 100~300rpm
It mixes 0.5~2 minute, saponification liquor is made；
(4) saponification liquor for obtaining step (3) injects mold, moulding after 1~3 day, using maturation in 5~10 days.
2. a kind of preparation method of cold handmade soap processed, it is characterised in that comprise the following steps：
(1) by weight, 7~14 parts of sodium hydroxides are mixed with 100 parts of greases, with 1000~5000rpm at 20~40 DEG C
Rotating speed cutting emulsify 0.5~2 minute；
(2) emulsification pretreatment machine is closed, additive is added in into mixed liquor obtained by step (1), and is stirred with the rotating speed of 100~300rpm
It mixes 0.5~2 minute, saponification liquor is made；
(3) saponification liquor for obtaining step (2) injects mold, moulding after 1~3 day, using maturation in 5~10 days.
3. the preparation method of cold handmade soap processed according to claim 1 or 2, it is characterised in that：The additive is battalion
Support substance and/or natural essential oil and/or natural antiseptic agent.
4. the preparation method of cold handmade soap processed according to claim 3, it is characterised in that：The additive includes 0.1
~5 parts of nutriments, 0.1~1 part of natural essential oil and 0.1~1 part of natural antiseptic agent.
5. the preparation method of cold handmade soap processed according to claim 4, it is characterised in that：The nutriment is with powder
Form is added, which is selected from dried milk, fruit syrup, hydrosol, chlorophyll, herb powder, bamboo charcoal, red bean, smears
Tea.
6. the preparation method of cold handmade soap processed according to claim 4, it is characterised in that：The natural essential oil is selected from and smokes
Clothing grass essential oil, lemon, tea tree ethereal oil, Rosa Damascana, chamomile essential oil, sweet orange oil, bamboo charcoal essential oil.
7. the preparation method of cold handmade soap processed according to claim 4, it is characterised in that：The natural antiseptic agent is selected from
Vitamin E, honey, propolis, essential oil, tea polyphenols, allicin.
8. the preparation method of cold handmade soap processed according to claim 1 or 2, it is characterised in that：The grease is selected from coconut palm
Seed oil, olive oil, palm oil, canola oil, sesame oil, cocoa butter, soybean oil, Sweet Almond Oil, vegetalitas white oil, shea butter,
Groomwell root oil, castor oil, Camellia oil, SIMMONDSIA CHINENSIS SEED OIL, rice bran oil, walnut oil, sunflower oil, Avocado Oil, wheat-germ oil, fructus rosae
Oil, peanut oil, linseed oil, macadamia nut oil, evening primrose oil, grape seed oil, hazelnut oil.
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|---|---|---|---|---|
| JPH01156400A (en) * | 1987-12-14 | 1989-06-19 | Tatsuya Kato | Production of soap from waste cow's milk as raw material |
| CN104130888A (en) * | 2014-08-07 | 2014-11-05 | 张萍 | Special formula of cold-process handmade soap as well as preparation method and application thereof |
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