CN107760492A - A kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method - Google Patents
A kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method Download PDFInfo
- Publication number
- CN107760492A CN107760492A CN201610692347.6A CN201610692347A CN107760492A CN 107760492 A CN107760492 A CN 107760492A CN 201610692347 A CN201610692347 A CN 201610692347A CN 107760492 A CN107760492 A CN 107760492A
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- Prior art keywords
- soap
- lemongrass
- pearl
- oil
- alkali
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
Soap preparation method is ground the present invention relates to the pearl lemongrass of a kind of collapsible pore, antibacterial whitening is cold, is comprised the steps of：(1) take lemongrass appropriate, add water, decoct, obtain lemongrass extract；It is standby that pearl Ultramicro-powder is made again；(2) alkali lye is prepared：Pearl Ultramicro-powder and pure water are dissolved, alkali thing mixing mixed with water is until alkali is completely dissolved；(3) grease is prepared；(4) alkali oil mixing：Grease and alkali lye are mixed；(5) pour mask；(6) it is stripped；(7) pressing mold：Soap base is ground to scattered, lemongrass extract addition soap base, it is well mixed, pressing mold, cut soap.The present invention has the beneficial effect that：The pearl powder of citronella oil and modern ultramicro grinding by the extraction of traditional Chinese medicine extraction technology, it can effectively suppress lipofuscin and remove free radical, anti-bacterial, anti-itching, promote skin microcirculation, strengthen skin elasticity and tender degree；With reference to the effective ingredient such as olive oil, grape-kernel oil, coconut oil in soap, collapsible pore, antiphlogistic antibacterial, toxin-expelling and face nourishing, make skin soft and smooth thin white.
Description
Technical field
It is combined the present invention relates to traditional Chinese medicine extraction technology with cold soap technology by hand, more particularly to it is a kind of collapsible pore, anti-
The pearl lemongrass of bacterium whitening is cold to grind soap preparation method.
Background technology
Soaps product can be divided into hot soap and cold soap from technique, and hot soap is to isolate the soap obtained after glycerine with industry refining
Raw material based on base, add the compositions such as various additives, pigment, glycerine and be sufficiently mixed dissolving or be directly compressed into soap, have outer
The advantages that shape is attractive in appearance, neat, with short production cycle, and cost is low, yield is big；Cold soap is after being mixed with grease and alkali under low-temperature condition
Natural saponification is formed saponified for a period of time, and the main distinction of itself and hot soap is exactly cold soap because its natural saponification is without chemistry point
From and contain a large amount of natural glycerins in making, can nourishes rough skin (or curing quilt washing articles), but because its production cycle is long and outer
The reasons such as shape is unmanageable, yield is low to its in soap market always known to most of audients.
Current commercially available soap is there is many deficiencies in terms of raw material, and first, cold soap is mostly small handicraft workshop production, its
Grease is hand-to-mouth buying mostly, uncontrollable to oil quality；Secondly, commercially available soap additive is mostly chemical synthesis additive or will
Into powder, grain or addition to boil water, its additive effective ingredient fails to discharge and transform into completely to be easy to human body for additive preliminary working
The state of absorption.
It is important to note that the cold soap series of lemongrass, lemongrass is because there is citris aromas, therefore the lemon grass (Cymbopogon citratus) that is otherwise known as, and controls for this case
It is rather good to treat rheumatism effect, treats antimigraine, it is anti-infective, improve digestive function, deodorization, expelling parasite；It is anti-infective, Cress, conditioning
Greasy unclean skin, it can also be used to work as aromatic in interior.
At present, commercially available cold soap is mostly small handicraft workshop production, and its additive is mostly chemical synthesis additive or will
Additive preliminary working fails to discharge completely and is not easy to be absorbed by the body into powder, grain or addition to boil water, its additive effective ingredient.Solution
Certainly the technical scheme of above mentioned problem is on condition that using the traditional Chinese medicine extraction workshop modernized, and Chinese medical extract can obtain at any time, and it adds
Add thing strictly by Chinese Pharmacopoeia Traditional Chinese medicine extraction method extract, extract effective component of chinese medicine can be used for it is medicinal or edible, make an addition to
In soap, its active ingredient passes through Transdermal absorption, it is easier to which absorption of human body, this is also that non-drug manufacturing enterprise can not obtain, institute
There is pharmaceutical producing enterprise also not allow the enterprise to beyond this enterprise to provide Chinese medical extract.
Therefore, according to problem above, it is necessary to effectively be innovated to prior art.
The content of the invention
For disadvantages described above, the present invention provides a kind of collapsible pore for being beneficial to health, the pearl of antibacterial whitening
Lemongrass is cold to grind soap preparation method.
To achieve the above object, the present invention uses following technical scheme：
A kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method, comprises the steps of：
(1) take lemongrass appropriate, put and chosen on sorting table except moldy metamorphism part, after being cleaned up with the running water of flowing, put
Enter in multi-function extractor, add the water equivalent to 8 times of lemongrass weight, decoct 5 hours, extract volatile oil, obtain lemongrass extraction
Thing is standby；Take pearl appropriate again, after being cleaned up with the running water of flowing, dry, ultramicro grinding, it is standby to obtain pearl Ultramicro-powder
With；
(2) alkali lye is prepared：Pearl Ultramicro-powder and pure water are dissolved into obtain water-phase extract, alkali and water-phase extract by 1: 3~
5 ratio mixing controls temperature during mixing below 40 DEG C until alkali is completely dissolved；
(3) grease is prepared, the weight percentage ranges of grease formula are：
(4) alkali oil mixing：The grease that step (3) prepares is mixed with the alkali lye that step (2) prepares, and at the uniform velocity
Quick stirring clockwise, switchs to stirring at low speed, to be mixed to pasty state soap lye, alkali lye is with grease when mixing after stirring
The temperature difference is controlled within 5 DEG C；
(5) pour mask：The soap lye that step (4) is uniformly mixing to obtain slowly is poured into soap-film by several times and avoids bubble from producing
Raw, standing treats its solidification；
(6) it is stripped：A week is stood, soap is taken out from mould, the soap after the demoulding is stood, and natural saponification 60 days, is stored
Environment shading, room temperature are maintained at 20 DEG C ± 5 DEG C, and humidity is maintained at 45%~70%, obtains basis soap；
(7) pressing mold：The basis soap of maturation is ground scattered, standby lemongrass extract is weighed by the 1%~2% of grease gross weight
And add in basis soap, it is well mixed, pressing mold, soap is cut after drying shaping.
After the demoulding, during detection, 2g is taken, the 100ml that adds diethyl ether dissolvings, filtering is used as need testing solution, separately takes thymol pair
According to product, carvacrol reference substance, add diethyl ether and solution of every 1ml containing 1mg is respectively prepared, as reference substance solution；According to thin-layer chromatography
Method is tested, and draws above-mentioned each 5 μ l of three kinds of solution, is put on same silica gel g thin-layer plate, using toluene as solvent, is deployed, exhibition respectively
Away from more than 15cm, take out, dry, spray with 5% vanillin-sulfuric acid solution, it is clear to be heated to spot development at 105 DEG C, test sample color
In spectrum, on position corresponding with reference substance chromatogram, show the spot of same color.
Collapsible pore of the present invention, the pearl lemongrass of antibacterial whitening is cold grinds having the beneficial effect that for soap preparation method：
(1) in terms of raw material, this method uses Chinese medical extract, alkali and food-grade and above rank natural oil, passes through
It is pure to carry, wherein effective ingredient it will be extracted, be concentrated, and turn into the material being easily absorbed by the human body；The day extracted using plant as raw material
Containing various to human body beneficial in right grease；Used additive is that strictly can be used for by Traditional Chinese medicine extraction method extraction
The extract that medicinal, directly edible or skin absorbs, makes an addition in soap, it is easier to absorption of human body；
(2) in process aspect, it is used for using Chinese medicine extractor, in strict accordance with extracting technique of Chinese medicine concentration extraction additive
Soap, while production process and storage process are strictly controlled by constant-temperature constant-humidity environment, allows grease and the saponification of alkali nature, maturation, maximum
Degree keeps the effective ingredient in grease and extract；
(3) in terms of practicality, the pearl powder of citronella oil and modern ultramicro grinding by the extraction of traditional Chinese medicine extraction technology, make
For skin surface, the pore thoroughly cleaned, it can effectively suppress lipofuscin and remove free radical, anti-bacterial, anti-itching, promote skin micro-
Circulation, strengthen skin elasticity and tender degree；With reference to olive oil, grape-kernel oil, coconut oil, missible oil wood fruit fat etc. in soap effectively into
Part, collapsible pore, antiphlogistic antibacterial, toxin-expelling and face nourishing, make skin soft and smooth thin white.
Brief description of the drawings
The present invention is described in further detail below according to accompanying drawing.
Fig. 1 is collapsible pore described in the embodiment of the present invention, the cold work for grinding soap preparation method of the pearl lemongrass of antibacterial whitening
Skill schematic flow sheet.
Embodiment
As shown in figure 1, the pearl lemongrass of the collapsible pore, antibacterial whitening described in the embodiment of the present invention is cold to grind soap preparation side
Method, for ease of the understanding this programme become apparent from, links are stated in detail by the way of chapter merogenesis is divided below：
1st, the preparation of aqueous phase (extract)；
1.1 extracting method：
1.1.1 take lemongrass appropriate, put and choose moldy metamorphism part on sorting table, after being cleaned up with the running water of flowing,
It is put into multi-function extractor, adds 8 times of water, decoct 5 hours, extracts volatile oil, it is standby；
1.1.2 take pearl appropriate, after being cleaned up with the running water of flowing, dry, ultramicro grinding is standby；
1..2 quality standard：
1.2.1 lemongrass must not be less than 0.60% (ml/g) containing volatile oil；
1.2.2 lemongrass is calculated by dry product, containing thymol (C10H14O) with carvacrol (C10H14O total amount) must not be lacked
In 0.16%；
1.2.3 pearl powder powder 2g is taken, is put in the crucible of ignition to constant weight, blazing to complete ashing, adds people's watery hydrochloric acid about
20ml, determined according to acid-insoluble ash determination method, 4.0% must not be crossed；
2 aqueous phase Alkali liquid compoundings；
The metering of 2.1 alkali：
Institute's alkali needed is calculated according to the saponification number corresponding to grease amount and its；
Base amount=∑ (every kind of grease weighs weight × correspondence saponification number)；
2.2 weigh alkali by gained alkali number is calculated, and standby pearl Ultramicro-powder, which is dissolved in purified water, turns into aqueous phase, by 1:
3~5 ratio is mixed with water until alkali is completely dissolved by alkali, should be noted that during mixing control temperature below 40 DEG C.
3 aqueous phase oil phases mix：The grease mixed is mixed with alkali lye, and at the uniform velocity clockwise direction quickly stirs, and stirs
After switch to stirring at low speed, to be mixed to pasty state, the temperature difference when mixing should control within 5 DEG C alkali lye with grease.
4 pour masks：By the soap lye to stir by several times slowly pour into soap-film (generation that attention avoids bubble), after the completion of it is quiet
Put and treat its solidification.
5 demouldings：One week or so is stood, soap is taken out from mould.
The control requirement of 6 natural saponification process：Soap after the demoulding should be stood, and give free rein to saponification 60 days, and storing environment should
Shading, room temperature are maintained at 20 DEG C ± 5 DEG C, and humidity is maintained at 45%~70%.
7 pressing molds：The basis soap of maturation is ground scattered, weigh lemongrass extract in 0.5% ratio of grease total amount and add soap base
In, it is well mixed, pressing mold, soap is cut after one day.
The detection control of 8 finished product soaps requires；
8.1 total working substance >=70%, chloride≤1.0, glycerol content >=30%, moisture and volatile matter≤25%, dissociate
Alkali≤0.1%, pH value≤7.8；
8.2 take this product 2g, and the 100ml that adds diethyl ether dissolvings, filtering is used as need testing solution, separately takes thymol reference substance, perfume (or spice)
Schizonepeta phenol reference substance, add diethyl ether and solution of every 1ml containing 1mg is respectively prepared, as reference substance solution；Tested according to thin-layered chromatography,
Above-mentioned each 5 μ l of three kinds of solution are drawn, puts on same silica gel g thin-layer plate, using toluene as solvent, expansion, opens up away from 15cm respectively
More than, take out, dry, spray with 5% vanillin-sulfuric acid solution, it is clear to be heated to spot development at 105 DEG C；In test sample chromatogram,
On position corresponding with reference substance chromatogram, show the spot of same color.
9th, pack.
Pearl lemongrass described in the above embodiment of the present invention is cold to grind, and application method is：
1. moistening soap body with warm water, rub out the fine and smooth foam rich in pearl powder and lemongrass concentration elite and (coordinated and indulged in serfing the Net
It is better)；
2. foam is applied to skin surface and softly massaged, about 1 minute or so use warm water cleaning, can whole body make
With；
3. use towel.
Above example is one kind of the present invention more preferably embodiment, and those skilled in the art are in the technical program
In the range of the usual variations and alternatives that carry out should include it is within the scope of the present invention.
Claims (2)
1. a kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method, it is characterised in that by following steps group
Into：
(1) take lemongrass appropriate, put and chosen on sorting table except moldy metamorphism part, after being cleaned up with the running water of flowing, be put into more
In function extractor, the water equivalent to 8 times of lemongrass weight is added, is decocted 5 hours, volatile oil is extracted, it is standby to obtain lemongrass extract
With；Take pearl appropriate again, after being cleaned up with the running water of flowing, dry, ultramicro grinding, it is standby to obtain pearl Ultramicro-powder；
(2) alkali lye is prepared：Pearl Ultramicro-powder and pure water are dissolved into obtain water-phase extract, alkali is with water-phase extract by 1: 3~5
Ratio mixing controls temperature during mixing below 40 DEG C until alkali is completely dissolved；
(3) grease is prepared, the weight percentage ranges of grease formula are：
Coconut oil 25.00~30.00%；
Palm oil 15.00~20.00%；
Olive oil 10.00~20.00%；
Missible oil wood fruit fat 5.00~8.00%；
Cocoa butter 8.00~11.00%%；
Castor oil 5.00~10.00%；
Evening primrose oil 4.50~7.00%；
Grape-kernel oil 5.00~6.00%；
(4) alkali oil mixing：The grease that step (3) prepares is mixed with the alkali lye that step (2) prepares, and at the uniform velocity up time
Pin direction is quickly stirred, and stirring at low speed is switched to after stirring, to be mixed to pasty state soap lye, alkali lye temperature difference when mixing with grease
Control is within 5 DEG C；
(5) pour mask：The soap lye that step (4) is uniformly mixing to obtain slowly is poured into soap-film by several times and avoids bubble from producing, it is quiet
Put and treat its solidification；
(6) it is stripped：A week is stood, soap is taken out from mould, the soap after the demoulding is stood, and natural saponification 60 days, stores environment
Shading, room temperature are maintained at 20 DEG C ± 5 DEG C, and humidity is maintained at 45%~70%, obtains basis soap；
(7) pressing mold：The basis soap of maturation is ground scattered, weigh standby lemongrass extract by the 1%~2% of grease gross weight and add
Enter in basis soap, be well mixed, pressing mold, soap is cut after drying shaping.
2. collapsible pore according to claim 1, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method, its feature exists
In：After the demoulding, during detection, take 2g, the 100ml that adds diethyl ether dissolvings, filtering is used as need testing solution, separately take thymol reference substance,
Carvacrol reference substance, add diethyl ether and solution of every 1ml containing 1mg is respectively prepared, as reference substance solution；Tried according to thin-layered chromatography
Test, draw above-mentioned each 5 μ l of three kinds of solution, put respectively on same silica gel g thin-layer plate, using toluene as solvent, expansion, open up away from
More than 15cm, take out, dry, spray with 5% vanillin-sulfuric acid solution, it is clear to be heated to spot development at 105 DEG C, test sample chromatogram
In, on position corresponding with reference substance chromatogram, show the spot of same color.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610692347.6A CN107760492A (en) | 2016-08-18 | 2016-08-18 | A kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610692347.6A CN107760492A (en) | 2016-08-18 | 2016-08-18 | A kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method |
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| Publication Number | Publication Date |
|---|---|
| CN107760492A true CN107760492A (en) | 2018-03-06 |
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|---|---|---|---|
| CN201610692347.6A Pending CN107760492A (en) | 2016-08-18 | 2016-08-18 | A kind of collapsible pore, the pearl lemongrass of antibacterial whitening is cold grinds soap preparation method |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102002452A (en) * | 2010-11-23 | 2011-04-06 | 陈巍 | Method for preparing beautifying perfumed soap |
| CN103756817A (en) * | 2014-01-26 | 2014-04-30 | 夏程 | Preparation method for manually ground soap |
| CN104862130A (en) * | 2015-05-30 | 2015-08-26 | 防城港市防城区那梭香料厂 | Preparation method of cymbopogon citratus handmade soap |
| CN105400617A (en) * | 2015-12-17 | 2016-03-16 | 宁波工程学院 | Preparation method of cold-formed soap |
-
2016
- 2016-08-18 CN CN201610692347.6A patent/CN107760492A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102002452A (en) * | 2010-11-23 | 2011-04-06 | 陈巍 | Method for preparing beautifying perfumed soap |
| CN103756817A (en) * | 2014-01-26 | 2014-04-30 | 夏程 | Preparation method for manually ground soap |
| CN104862130A (en) * | 2015-05-30 | 2015-08-26 | 防城港市防城区那梭香料厂 | Preparation method of cymbopogon citratus handmade soap |
| CN105400617A (en) * | 2015-12-17 | 2016-03-16 | 宁波工程学院 | Preparation method of cold-formed soap |
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Application publication date: 20180306 |