CN105769730B - A kind of agalloch eaglewood pearl amino acid soap and preparation method thereof - Google Patents
A kind of agalloch eaglewood pearl amino acid soap and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The present invention relates to field of commodity production, provide a kind of agalloch eaglewood pearl amino acid soap and preparation method thereof, by weight, raw material is：100 parts of cocounut oil acyl glutamic acid, 30~45 parts of glycerine, 15~25 parts of propylene glycol, 30~50 parts of water, 68~72 parts of triethanolamine, 5.0~6.0 parts of ethyl alcohol, 1.0~3.0 parts of Lignum Aquilariae Resinatum extract, 1.0~3.0 parts of Margarita extract.Cocounut oil acyl glutamic acid is dissolved to obtain solution I by preparation method；Glycerine, propylene glycol, water, triethanolamine and ethyl alcohol are sequentially added into solution I, obtains solution II；Lignum Aquilariae Resinatum extract, Margarita extract are sequentially added into solution II, obtains solution III；Solution III is stood, is cooled down, obtains molding agalloch eaglewood pearl amino acid soap.Agalloch eaglewood pearl amino acid soap of the present invention can improve user's skin quality, prevent from having dry skin；Preparation method of the present invention can guarantee the effect of agalloch eaglewood pearl amino acid soap improves skin quality.
Description
Technical field
The present invention relates to field of commodity production, in particular to a kind of agalloch eaglewood pearl amino acid soap and its preparation side
Method.
Background technology
It is higher and higher with requirement of the people to quality of the life with advances in technology, for articles for washing demand also increasingly
Diversification.The function of articles for washing has been not limited only to washing and has lost no time, and needs to adapt to the various demands of people's life.Common
Commercially available perfumed soap materials are common, the considerations of in production cost, often add in some oil recovery, adjusted with common essence and flavoring agent
Fragrance, covering smell are undoubtedly no benefit to human body commonly using such perfumed soap.
Agalloch eaglewood, alias are honey perfume, lignum aquilariae resinatum, are dicotyledonous medicine Thymelaeceae magaphanerophytes, also refer to suspension culture of Aquilaria sinensis contains resin
Timber.There are many effect of agalloch eaglewood, not only have obvious curative effects to abdominal distension, stomach cold, kidney deficiency, asthma, moreover it can be used to treat angina pectoris
With bad odor carbuncle.In addition, also there is the extract of agalloch eaglewood sleeping to resist strongly fragrant, stable mood, the work(such as nervous, help qi-blood circulating of releiving
Effect.In the fields such as healthcare products and daily necessities, agalloch eaglewood is also widely used, such as：It agalloch eaglewood dish, Agilawood toothpaste, perfumed soap and washes
Hair agent, the anti-pharynx frost of agalloch eaglewood freshener, agalloch eaglewood, agalloch eaglewood safety are burnt incense, agilawood essential oil atomized liquid, fragrant product etc..
Application publication number is that the application for a patent for invention document of CN103054778A discloses a kind of Agilawood toothpaste and its making
Method, raw material contain the medicine material composition of following weight：20~50 parts of agilawood essential oil, 10~40 parts of Radix Notoginseng essential oil,
5~30 parts of 20~60 parts of Radix zanthoxyli essential oil and Mint Essence；By the agilawood essential oil of the parts by weight, Radix Notoginseng essential oil, Radix zanthoxyli essence
Oil and Mint Essence are proportionally uniformly mixed, then the essential oil of above-mentioned mixing and water are proportionally added into toothpaste matrix, and mixing is equal
It is even.The Agilawood toothpaste is easy to use, good effect, without any toxicity and side effects, can auxiliary treatment toothache, tooth haemorrhagia, apicitis,
Periodontitis, canker sore, abscess of throat, treatment odontopathy, toothache, cough and phlegm and pharyngitis.
Application publication number be CN103054777A application for a patent for invention document disclose a kind of agalloch eaglewood Chinese medicine shampoo and
Its preparation method, the Chinese medicine shampoo contain Surfactant SDS or lauryl alcohol sulfuric acid ethanolamine salt, stabilizer, suitable
Lubrication prescription and agilawood essential oil, agilawood essential oil content are the 1.5~8% of total weight.The Chinese medicine shampoo can reach hair care effect,
And significant effect.
Application publication number be CN103060126A application for a patent for invention document disclose a kind of Agilawood essential oil soap and its
Production method, the composition and mass percentage content of the Agilawood essential oil soap are grease：Water：NaOH：Agilawood essential oil=48：13：
5：1；Wherein, agilawood essential oil is refined by precious agalloch eaglewood.The perfumed soap agilawood essential oil is instead of the perfume (or spice) in conventional toilet soaps
Material and essence, not only smell fragrant, moreover it is possible to which benefit is brought to health.
Although the Related product about Lignum Aquilariae Resinatum extract, agilawood essential oil is a lot of, played the role of also different；And
In daily necessities field, the document that Lignum Aquilariae Resinatum extract is fully applied in perfumed soap also has been reported that, but the said goods are for improving
The problems such as having dry skin, is dark yellow need to be improved.
In view of this, it is special to propose the present invention.
Invention content
The first object of the present invention is to provide a kind of agalloch eaglewood pearl amino acid soap, the agalloch eaglewood pearl amino acid soap energy
Enough improve user's skin quality, prevent dry skin, it is dark yellow.
The second object of the present invention is to provide a kind of preparation method of agalloch eaglewood pearl amino acid soap, this method operation letter
List, agalloch eaglewood pearl amino acid soap skin effect obtained are good.
In order to realize the above-mentioned purpose of the present invention, spy uses following technical scheme：A kind of agalloch eaglewood pearl amino acid soap, by weight
Part meter is measured, is mainly made of following raw material：100 parts of cocounut oil acyl glutamic acid, 30~45 parts of glycerine, 15~25 parts of propylene glycol, water 30
~50 parts, 68~72 parts of triethanolamine, 5.0~6.0 parts of ethyl alcohol, 1.0~3.0 parts of Lignum Aquilariae Resinatum extract, Margarita extract 1.0~
3.0 part.
The designer of the present invention passes through long-term exploration and trial and multiple experiment and effort, continuous reform wound
Newly, it is special to determine Lignum Aquilariae Resinatum extract, Margarita extract and cocounut oil acyl glutamic acid as important source material, have devised the agalloch eaglewood pearl ammonia
Base acid soap, takes full advantage of the intrinsic penetration power of Lignum Aquilariae Resinatum extract, and with glycerine, triethanolamine and ethanol composition, improve it
Penetration makes Lignum Aquilariae Resinatum extract directly reach skin corium, keeps the skin wet, prevent dry skin, it is dark yellow.
In above-mentioned agalloch eaglewood pearl amino acid soap, water and ethyl alcohol are used as solvent, and propylene glycol, glycerine rise as moisturizer
To the effect of moisturizing skin, triethanolamine plays the role of pH adjustings, and Lignum Aquilariae Resinatum extract and Margarita extract are as skin tune
Agent is managed, plays the role of conditioning skin skin quality.
The present invention also provides the preparation methods of this agalloch eaglewood pearl amino acid soap, include the following steps：
(1) it after the slow heating dissolving of cocounut oil acyl glutamic acid, will stir to be slowly heated with the heating rate of 1-5 DEG C/min and rise
Temperature obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and ethyl alcohol are sequentially added into solution I, and continues to stir and heat up, until
Raw material is completely dissolved, and obtains solution II；
(3) Lignum Aquilariae Resinatum extract, Margarita extract are sequentially added into solution II, after stirring evenly, obtains solution III；
(4) solution III is stood, cooled down, obtain molding agalloch eaglewood pearl amino acid soap.
Stirring needs at the uniform velocity, and its mixing speed is unsuitable too fast, otherwise easily cause excessive thermal losses and water loss and
Reduce the dissolution rate of raw material；Preferably, in step (1), the speed of stirring is 20~30r/min.
Compared with prior art, beneficial effects of the present invention are：
(1) agalloch eaglewood pearl amino acid soap of the present invention using cocounut oil acyl glutamic acid, Lignum Aquilariae Resinatum extract, Margarita extract as raw material into
Row is prepared, and not only fragrance is fresh, simple and elegant, but also can improve user's skin quality, and desalination melanin, skin whitening, through skin are true
Cortex keeps the skin wet for skin, solves the problems, such as the skin such as skin dimness.
(2) agalloch eaglewood pearl amino acid soap of the present invention takes full advantage of the superpower penetration power and penetration of agalloch eaglewood, can dredge
Blood vessel；During DOMS, using agalloch eaglewood pearl amino acid soap of the present invention, DOMS can be alleviated.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person, the condition suggested according to normal condition or manufacturer carry out.Reagents or instruments used without specified manufacturer is
The conventional products that can be obtained by commercially available purchase.
Lignum Aquilariae Resinatum extract and Margarita extract can directly buy acquisition, can also process preparation.One kind is provided below
The preparation method of Lignum Aquilariae Resinatum extract and a kind of preparation method of Margarita extract.
Wherein, the preparation method of Lignum Aquilariae Resinatum extract is：(1) agalloch eaglewood of Edgeworthia chrysantha is taken, after being cut into small pieces, is crushed to 15 mesh
Agalloch eaglewood powder；(2) water is added in into agalloch eaglewood powder, is heated to 100 DEG C, and keep temperature 12h, then carried out refrigerated separation, obtain
Obtain Lignum Aquilariae Resinatum extract (or being linaloe oil).Above-mentioned Lignum Aquilariae Resinatum extract includes chromone, triterpene, calacone and furans acid.
Volume agalloch eaglewood pearl amino acid soap of the present invention, by weight, is mainly made of following raw material：Cocounut oil acyl glutamic acid
100 parts, 30~45 parts of glycerine, 15~25 parts of propylene glycol, 30~50 parts of water, 68~72 parts of triethanolamine, 5.0~6.0 parts of ethyl alcohol,
1.0~3.0 parts of Lignum Aquilariae Resinatum extract, 1.0~3.0 parts of Margarita extract.
Experiment proves that rational amounts of components can preferably improve user's skin quality, prevents dry skin, dark yellow, clearly
New smell, preferably, by weight, being mainly made of following raw material：100 parts of cocounut oil acyl glutamic acid, 33~43 parts of glycerine,
16~23 parts of propylene glycol, 33~45 parts of water, 68~70 parts of triethanolamine, 5.5~5.8 parts of ethyl alcohol, Lignum Aquilariae Resinatum extract 1.3~2.9
Part, 1.3~2.9 parts of Margarita extract.
It is further preferred that it by weight, is mainly made of following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, third
22.5 parts of glycol, 45 parts of water, 70 parts of triethanolamine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
The preparation method of the agalloch eaglewood pearl amino acid soap of the present invention, includes the following steps：
(1) it after the slow heating dissolving of cocounut oil acyl glutamic acid, will stir to be slowly heated with the heating rate of 1-5 DEG C/min and rise
Temperature obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and ethyl alcohol are sequentially added into solution I, and continues to stir and heat up, until
Raw material is completely dissolved, and obtains solution II；
(3) Lignum Aquilariae Resinatum extract, Margarita extract are sequentially added into solution II, after stirring evenly, obtains solution III；
(4) solution III is stood, cooled down, obtain molding agalloch eaglewood pearl amino acid soap.
In step (1), stirring needs at the uniform velocity, and its mixing speed is unsuitable too fast, otherwise easily cause excessive thermal losses and
Water is lost and reduces the dissolution rate of raw material；Preferably, in step (1), the speed of stirring is 20~30r/min.
In step (1), the speed of control heating is needed, it is necessary to which slowly heating, too fast to prevent heating, hot-spot causes
There is metachromatism in manufactured soap.Preferably, the speed of heating is 1~3 DEG C/min.
Equally, in step (2), mixing speed is also unsuitable too fast, preferably, the speed of stirring is 25~30r/min.
Preferably, in step (2), 80~85 DEG C are warming up to, observation is expected whether body is uniform and is completely dissolved, and stirs to molten
Xie Hou adds follow-up raw material.
Preferably, in step (3), the time of stirring is 5~15 minutes.
Preferably, in step (3), the time of standing is 4~5 hours.
The preparation process of above-mentioned agalloch eaglewood pearl amino acid soap can improve cocounut oil acyl glutamic acid, Lignum Aquilariae Resinatum extract, pearl and carry
The dissolubility of object is taken, active ingredient in the agalloch eaglewood prepared pearl amino acid soap is made to be more easy to be absorbed by user.
Embodiment 1
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Embodiment 2
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 30 parts of glycerine, 15 parts of propylene glycol, 30 parts of water, triethanolamine 68
Part, 5.0 parts of ethyl alcohol, 1.0 parts of Lignum Aquilariae Resinatum extract, 1.0 parts of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Embodiment 3
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 45 parts of glycerine, 25 parts of propylene glycol, 50 parts of water, triethanolamine 72
Part, 6.0 parts of ethyl alcohol, 3.0 parts of Lignum Aquilariae Resinatum extract, 3.0 parts of Margarita extract.
It is operated according to following steps：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Embodiment 4
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 33 parts of glycerine, 16 parts of propylene glycol, 33 parts of water, triethanolamine 68
Part, 5.5 parts of ethyl alcohol, 1.3 parts of Lignum Aquilariae Resinatum extract, 1.3 parts of Margarita extract.
It is operated according to following steps：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Embodiment 5
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 43 parts of glycerine, 23 parts of propylene glycol, 45 parts of water, triethanolamine 70
Part, 5.8 parts of ethyl alcohol, 2.9 parts of Lignum Aquilariae Resinatum extract, 2.9 parts of Margarita extract.
It is operated according to following steps：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Embodiment 6
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
30r/min is persistently stirred, and is constantly heated up with 3 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Embodiment 7
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
30r/min is persistently stirred, and is constantly heated up with 3 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
30r/min is persistently stirred, and is warming up to 85 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Comparative example 1
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Margarita extract of above-mentioned usage ratio is added in into solution II, is stirred 10 minutes, after solution is uniform, is obtained
Solution III；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding amino acid soap.
(5) by the demoulding of molding amino acid soap, taking-up, packaging and storage.
Comparative example 2
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract of above-mentioned usage ratio is added in into solution II, is stirred 10 minutes, after solution is uniform, is obtained
Solution III；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding amino acid soap.
(5) by the demoulding of molding amino acid soap, taking-up, packaging and storage.
Comparative example 3
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 0.5 part of Lignum Aquilariae Resinatum extract, 0.5 part of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Comparative example 4
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 3.5 parts of Lignum Aquilariae Resinatum extract, 4.0 parts of Margarita extract.
Follow the steps below preparation：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
25r/min is persistently stirred, and is constantly heated up with 1 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Comparative example 5
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
It is operated according to following steps：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
35r/min is persistently stirred, and is constantly heated up with 5 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
25r/min is persistently stirred, and is warming up to 80 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Comparative example 6
Take following raw material：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, three ethyl alcohol
70 parts of amine, 5.6 parts of ethyl alcohol, 1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
It is operated according to following steps：
(1) first cocounut oil acyl glutamic acid is added in the emulsification pot cleaned up, slow heating, dissolving after, start with
35r/min is persistently stirred, and is constantly heated up with 5 DEG C/min, obtains solution I；
(2) glycerine, propylene glycol, water, triethanolamine and the ethyl alcohol of above-mentioned usage ratio are sequentially added into solution I, and with
35r/min is persistently stirred, and is warming up to 85 DEG C, until raw material is completely dissolved, obtains solution II；
(3) Lignum Aquilariae Resinatum extract, the Margarita extract of above-mentioned usage ratio are sequentially added into solution II, is stirred 10 minutes,
After solution is uniform, solution III is obtained；
(4) solution III is stood into 5h, after being cooled to room temperature, obtains molding agalloch eaglewood pearl amino acid soap.
(5) by the demoulding of molding agalloch eaglewood pearl amino acid soap, taking-up, packaging and storage.
Experimental example
Examples 1 to 7 and comparative example 1~6 are repeated, agalloch eaglewood pearl amino acid soap or amino acid soap is made, according to QB/T
2485-2008《Perfumed soap》Requirement, above-mentioned agalloch eaglewood pearl amino acid soap or amino acid soap are subjected to safety examination, testing result
As shown in table 1：
1. inspection result of table
Through examining, soap body appearance, smell, moisture and volatile matter, total substance content, chloride (in terms of NaCl) are total to swim
From alkali (in terms of NaOH), dissociate caustic alkali (in terms of NaOH), and the content of total phosphorus pentoxide meets the requirements.
Recruit volunteer, choose that skin quality dries up, coarse and dim volunteer is tested, with above-mentioned Examples 1 to 7 and
Agalloch eaglewood pearl amino acid soap made from comparative example 1~6 or amino acid soap are sample, using conventional toilet soaps as control, experimenter are allowed (to try
The person of testing is divided into 14 groups, every group of 30 people, totally 420 people) bathing is carried out using sample or control daily, each bathing is primary sooner or later, 15 days
For a test period, observation improves situation using rear experimenter's skin quality, and record skin quality improves and the number of skin lubrication, as a result
Such as table 2：
2. experimenter's skin quality of table improves situation survey graft.
As shown in the above results, can most effectively it be improved using the agalloch eaglewood pearl amino acid soap of the preparation of embodiment 1 tested
Person's skin quality, makes skin more lubricate；Agalloch eaglewood pearl amino acid soap prepared by embodiment 2~5 omits in amounts of components with embodiment 1
Different, effect is slightly worse than embodiment 1, but still can effectively improve subject's skin quality, and skin is made more to lubricate.
Embodiment 6~7 is matched using raw material components same as Example 1, but condition and embodiment 1 in preparation process
Difference, finally, effect are slightly worse than embodiment；The preparation process for illustrating agalloch eaglewood pearl amino acid soap of the present invention can influence to sink
The effect of fragrant pearl amino acid soap, it should stringent control.
Lack pearl mud extract in the amino acid soap prepared in comparative example 1, although the skin of part subject can be improved
Matter, still, for most subjects, to no effect.
Lack Lignum Aquilariae Resinatum extract in the amino acid soap prepared in comparative example 2, it is apparent that effect compares from result
Ratio 1 is worse, illustrates that Lignum Aquilariae Resinatum extract as improvement of the component of agalloch eaglewood pearl amino acid soap of the present invention to subject's skin quality, is prevented
It only has dry skin, is dark yellow, playing the role of very important.
In the amino acid soap prepared in comparative example 3~4, because the dosage of raw material components is not reasonable, hence it is evident that reduce tested
The successful number that person's skin quality improves；Comparative example 5~6, although employing raw material components same as Example 1 and dosage, because
It is had differences for preparation process, also resulting in the successful number of subject's skin quality improvement reduces.In conventional toilet soaps control group, subject
Skin quality and skin lubrication degree do not improve.
Although illustrate and describing the present invention with specific embodiment, it will be appreciated that without departing substantially from the present invention's
Many other change and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (10)
1. a kind of agalloch eaglewood pearl amino acid soap, which is characterized in that by weight, be mainly made of following raw material：Cocounut oil acyl paddy
100 parts of propylhomoserin, 30~45 parts of glycerine, 15~25 parts of propylene glycol, 30~50 parts of water, 68~72 parts of triethanolamine, ethyl alcohol 5.0~
6.0 parts, 1.0~3.0 parts of Lignum Aquilariae Resinatum extract, 1.0~3.0 parts of Margarita extract；
The agalloch eaglewood pearl amino acid soap preparation method, includes the following steps：
(1) it by after the slow heating dissolving of cocounut oil acyl glutamic acid, stirs and heating is slowly heated with the heating rate of 1-3 DEG C/min,
Obtain solution I；
(2) glycerine, propylene glycol, water, triethanolamine and ethyl alcohol are sequentially added into solution I, and continue to stir and it is warming up to 80~
85 DEG C, until raw material is completely dissolved, obtain solution II；
(3) Lignum Aquilariae Resinatum extract, Margarita extract are sequentially added into solution II, after stirring evenly, obtains solution III；
(4) solution III is stood, cooled down, obtain molding agalloch eaglewood pearl amino acid soap.
2. agalloch eaglewood pearl amino acid soap as described in claim 1, which is characterized in that by weight, mainly by following raw material
It is made：100 parts of cocounut oil acyl glutamic acid, 33~43 parts of glycerine, 16~23 parts of propylene glycol, 33~45 parts of water, triethanolamine 68~70
Part, 5.5~5.8 parts of ethyl alcohol, 1.3~2.9 parts of Lignum Aquilariae Resinatum extract, 1.3~2.9 parts of Margarita extract.
3. agalloch eaglewood pearl amino acid soap as described in claim 1, which is characterized in that by weight, mainly by following raw material
It is made：100 parts of cocounut oil acyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, 70 parts of triethanolamine, 5.6 parts of ethyl alcohol,
1.4 parts of Lignum Aquilariae Resinatum extract, 1.4 parts of Margarita extract.
4. a kind of preparation method of agalloch eaglewood pearl amino acid soap, which is characterized in that include the following steps：
(1) it by after the slow heating dissolving of cocounut oil acyl glutamic acid, stirs and heating is slowly heated with the heating rate of 1-5 DEG C/min,
Obtain solution I；
(2) glycerine, propylene glycol, water, triethanolamine and ethyl alcohol are sequentially added into solution I, and continue to stir and it is warming up to 80~
85 DEG C, until raw material is completely dissolved, obtain solution II；
(3) Lignum Aquilariae Resinatum extract, Margarita extract are sequentially added into solution II, after stirring evenly, obtains solution III；
(4) solution III is stood, cooled down, obtain molding agalloch eaglewood pearl amino acid soap；
By weight, 100 parts of cocounut oil acyl glutamic acid, 30~45 parts of glycerine, 15~25 parts of propylene glycol, 30~50 parts of water, three second
68~72 parts of hydramine, 5.0~6.0 parts of ethyl alcohol, 1.0~3.0 parts of Lignum Aquilariae Resinatum extract, 1.0~3.0 parts of Margarita extract.
5. preparation method as claimed in claim 4, which is characterized in that in step (1), the speed of the stirring is 20~30r/
min。
6. preparation method as claimed in claim 4, which is characterized in that in step (2), the speed of the stirring is 25~30r/
min。
7. preparation method as claimed in claim 4, which is characterized in that in step (3), the time of the stirring is 5~15 points
Clock.
8. preparation method as claimed in claim 4, which is characterized in that in step (4), the time of the standing is small for 4~5
When.
9. preparation method as claimed in claim 4, which is characterized in that by weight, be mainly made of following raw material：Cocounut oil
100 parts of acyl glutamic acid, 33~43 parts of glycerine, 16~23 parts of propylene glycol, 33~45 parts of water, 68~70 parts of triethanolamine, ethyl alcohol 5.5
~5.8 parts, 1.3~2.9 parts of Lignum Aquilariae Resinatum extract, 1.3~2.9 parts of Margarita extract.
10. preparation method as claimed in claim 4, which is characterized in that by weight, be mainly made of following raw material：Coconut palm
100 parts of oleoyl glutamic acid, 42.0 parts of glycerine, 22.5 parts of propylene glycol, 45 parts of water, 70 parts of triethanolamine, 5.6 parts of ethyl alcohol, agalloch eaglewood carries
Take 1.4 parts of object, 1.4 parts of Margarita extract.
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| CN107868737A (en) * | 2016-09-23 | 2018-04-03 | 金凯 | A kind of preparation method of new amino acid Aloe care skin soap |
| CN106701375A (en) * | 2016-12-28 | 2017-05-24 | 广东国方医药科技有限公司 | Amino acid facial soap containing Dendrobium officinale and preparation method thereof |
| CN107384597B (en) * | 2017-07-25 | 2020-07-14 | 北京斯利安药业有限公司 | Amino acid soap and preparation method thereof |
| CN107699406A (en) * | 2017-09-12 | 2018-02-16 | 北京品瑞珠宝有限责任公司 | A kind of amino acid amber soap |
| CN109370785B (en) * | 2018-09-30 | 2021-02-05 | 江门职业技术学院 | Amino acid soap containing dried orange peel extract and preparation method thereof |
| CN109609300A (en) * | 2018-12-28 | 2019-04-12 | 佛山科学技术学院 | A kind of agilawood essential oil soap |
| CN110484376A (en) * | 2019-09-12 | 2019-11-22 | 贵州沐木皙颜生物科技有限公司 | A kind of white tea amino acid nanometer transparent soap and its processing method |
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