CN105367339A - Long-acting shellfish-algae soil conditioner and preparation method therefor - Google Patents
Long-acting shellfish-algae soil conditioner and preparation method therefor Download PDFInfo
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- CN105367339A CN105367339A CN201510851890.1A CN201510851890A CN105367339A CN 105367339 A CN105367339 A CN 105367339A CN 201510851890 A CN201510851890 A CN 201510851890A CN 105367339 A CN105367339 A CN 105367339A
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Abstract
The invention provides a long-acting shellfish-algae soil conditioner. The soil conditioner contains the following ingredients: scallop shell powder, oyster shell powder, perilla frutescens oil, clove oil, pericarpium zanthoxyli powder, cortex albiziae, calcium alginate, crab shells, pulverized coal ash, ammonium sulfate, monosodium glutamate residue, ferrous sulfate, raddle powder, ground phosphorite and calcium carbonate. The soil conditioner provided by the invention has a good impervious soil amendment effect; after amendment, soil has the total porosity of 55-60%, the soil retention of 17.5-18.1%, the average grain size of 2.1-2.6mm, the pH of 6.9-7.1 and the volume weight of 1.40-1.45g/cm<3>; and the effect holding time reaches 3 years.
Description
Technical field
The invention provides a kind of soil conditioner, be specifically related to a kind of long-acting shellfish algae soil conditioner and preparation method thereof, belong to agricultural technology field.
Background technology
Soil conditioner can administer soil compaction, desertification, salinization phenomenon, improve soil permeability, increase the preserve moisture and fertility ability of soil, reduce soil water evaporation, increase the cation exchange capacity (CEC) of soil, promote that trace element is better absorbed by root system of plant, be conducive to the chelating of plant to iron, magnesium, zinc, copper, reduce the Na+ etc. in salinity absorption soil.
In recent years, soil excessive use, a large amount of chemical fertilizer, agricultural chemicals cause Soil structure to be destroyed, and cause soil water-retaining, fertilizer-preserving ability and permeability to reduce, cause soil compaction.
The soil conditioner of prior art has following defect: the effect improving soil is bad, and after using, this season is effective, and effect duration is too short.
Summary of the invention
The present invention is the deficiency solving prior art existence, provides a kind of long-acting shellfish algae soil conditioner and preparation method thereof, to realize following goal of the invention:
(1) improve the soil that hardens, improve soil porosity, improve water capacity; Make soil porosity be 55-60%, water capacity is 17.5-18.1%;
(2) soil weight is reduced;
(3) time that after extending improvement, soil property maintains;
For solving the problems of the technologies described above, by the following technical solutions:
A kind of long-acting shellfish algae soil conditioner, described soil conditioner comprises following component: scallop shell powder, oyster shell powder, perilla oil, Syzygium aromaticum stem oil, zanthoxylum powder, Silktree Albizzia Bark, alginate calcium, crab shell, flyash, ammonium sulfate, residue of monosodium glutamate, ferrous sulfate, reddle powder, floats, calcium carbonate.
The weight part of each component of described soil conditioner is: scallop shell powder 12-23 part, oyster shell powder 29-35 part, perilla oil 2.2-3.4 part, Syzygium aromaticum stem oil 1.8-2.4 part, zanthoxylum powder 5-8 part, Silktree Albizzia Bark 10-15 part, alginate calcium 3-4.5 part, crab shell 7-10 part, flyash 6-9 part, ammonium sulfate 11-14 part, residue of monosodium glutamate 9-13 part, ferrous sulfate 6-11 part, reddle powder 3-7 part, floats 8-14 part, calcium carbonate 8-14 part.
The weight part of each component of described soil conditioner is: 18 parts, scallop shell powder, oyster shell powder 30 parts, perilla oil 3.0 parts, Syzygium aromaticum stem oil 2.2 parts, zanthoxylum powder 6 parts, Silktree Albizzia Bark 13 parts, alginate calcium 4 parts, 9 parts, crab shell, 8 parts, flyash, 12 parts, ammonium sulfate, residue of monosodium glutamate 10 parts, 8 parts, ferrous sulfate, 5 parts, reddle powder, floats 11 parts, 10 parts, calcium carbonate.
Described perilla oil: containing perillaldehyde 63-68%, specific optical rotation is-10 °-+100 °, and specific refractory power is 1.4680-1.4998.
Described Syzygium aromaticum stem oil: containing Eugenol 54-60%, the refractive index at 20 DEG C is 1.5200-15360, and the relative density at 20 DEG C is 1.001-1.060.
Described residue of monosodium glutamate: crude ash content is 2.35%, crude fat content is 3.46%, and calcium contents is 0.12%; Albumen total content is 70%.
A preparation method for long-acting shellfish algae soil conditioner, described preparation method comprises perilla oil extraction step; Described perilla oil extracts: yield is 45-48%.
Described perilla oil extracts: purple perilla is put into still kettle, adds the normal hexane of purple perilla 2 times of quality, and 120rpm stirs, heating, and control temperature is 55 DEG C; Cooling, refluxes 1 hour.
Described preparation method also comprises Syzygium aromaticum stem oil and extracts, weighs, pulverizes Silktree Albizzia Bark and crab shell, mixing, granulation.
Described Syzygium aromaticum stem oil extracts: Flos Caryophylli puts into still kettle, adds 95% ethanol of Flos Caryophylli 10 times of quality, is heated to micro-boiling, and continues 60min, cooling for reflux; In phegma 5% sodium hydroxide solution, be 9-10 to pH value; Heating, steams ethanol; Extracted with diethyl ether 3 times; Dry; Yield is 28-33%;
Described pulverizing Silktree Albizzia Bark and crab shell: Silktree Albizzia Bark and crab shell being pulverized respectively is 80 object fine powders;
Described granulation: the particle produced is spherical, particle diameter is 2-3.5cm.
Compared with prior art, the invention has the beneficial effects as follows:
(1) the soil conditioner of the present invention improvement soil that hardens is effective, and after improvement, soil porosity is 55-60%, and water capacity is 17.5-18.1%, and soil median size is 2.1-2.6mm, pH is 6.9-7.1, and unit weight is 1.40-1.45g/cm
3;
(2) after soil conditioner of the present invention is used, effect is held time and is reached 3 years, and in 3 years, soil occurs without the phenomenon that hardens;
(3) soil conditioner of the present invention improvement soil is adopted, long-term cropping quality better.
Embodiment
The long-acting shellfish algae soil conditioner of embodiment 1 one kinds
The weight part of each component of soil conditioner is:
Described perilla oil: faint yellow clarified liq, has amber aroma, containing perillaldehyde 63-68%, specific optical rotation is-10 °-+100 °, and specific refractory power is 1.4680-1.4998;
Described Syzygium aromaticum stem oil: containing Eugenol 54-60%, the refractive index at 20 DEG C is 1.5200-15360, and the relative density at 20 DEG C is 1.001-1.060;
Described zanthoxylum powder: fineness is 80 orders;
Described residue of monosodium glutamate: crude ash content is 2.35%, crude fat content is 3.46%, and calcium contents is 0.12%; Albumen total content is 70%, and wherein aspartic acid content is 7.33%, and threonine content is 3.88%, and serine content is 2.43%, and histidine content is 1.19%, and content of glutamic acid is 21.98%;
Above-mentioned percentage ratio is mass percent.
The long-acting shellfish algae soil conditioner of embodiment 2 one kinds
The weight part of each component of soil conditioner is:
Described perilla oil: faint yellow clarified liq, has amber aroma, containing perillaldehyde 63-68%, specific optical rotation is-10 °-+100 °, and specific refractory power is 1.4680-1.4998;
Described Syzygium aromaticum stem oil: containing Eugenol 54-60%, the refractive index at 20 DEG C is 1.5200-15360, and the relative density at 20 DEG C is 1.001-1.060;
Described zanthoxylum powder: fineness is 80 orders;
Described residue of monosodium glutamate: crude ash content is 2.35%, crude fat content is 3.46%, and calcium contents is 0.12%; Albumen total content is 70%, and wherein aspartic acid content is 7.33%, and threonine content is 3.88%, and serine content is 2.43%, and histidine content is 1.19%, and content of glutamic acid is 21.98%;
Above-mentioned percentage ratio is mass percent.
The long-acting shellfish algae soil conditioner of embodiment 3 one kinds
The weight part of each component of soil conditioner is:
Described perilla oil: faint yellow clarified liq, has amber aroma, containing perillaldehyde 63-68%, specific optical rotation is-10 °-+100 °, and specific refractory power is 1.4680-1.4998;
Described Syzygium aromaticum stem oil: containing Eugenol 54-60%, the refractive index at 20 DEG C is 1.5200-15360, and the relative density at 20 DEG C is 1.001-1.060;
Described zanthoxylum powder: fineness is 80 orders;
Described residue of monosodium glutamate: crude ash content is 2.35%, crude fat content is 3.46%, and calcium contents is 0.12%; Albumen total content is 70%, and wherein aspartic acid content is 7.33%, and threonine content is 3.88%, and serine content is 2.43%, and histidine content is 1.19%, and content of glutamic acid is 21.98%;
Above-mentioned percentage ratio is mass percent.
The preparation method of the long-acting shellfish algae soil conditioner of embodiment 4 one kinds
Concrete steps are as follows:
1, perilla oil extracts
(1) raw material prepares
Fresh perilla stem and leaves is cleaned, dried, chopping, for subsequent use.
(2) distill
Ready purple perilla is put into still kettle, adds the normal hexane of purple perilla 2 times of quality, open and stir, rotating speed is 120rpm, and heating, control temperature is 55 DEG C.
(3) cooling for reflux
Cool with the water that temperature is 10-18 DEG C, reflux 1 hour.
(4) obtained perilla oil
Reflux the liquid mixture that obtains after filtration, distillation, collect distillate, obtain perilla oil; Yield is 45-48%.
2, Syzygium aromaticum stem oil extracts
(1) distill
Get Flos Caryophylli, join in still kettle, add the ethanol of Flos Caryophylli 10 times of quality, ethanol mass content is 95%;
Be heated to micro-boiling, continue 60min, cooling for reflux, collect phegma.
(2) be separated
In phegma, add the sodium hydroxide solution that mass content is 5%, stir while adding, simultaneously the pH value of test mixing liquid, to pH value is 9-10;
Heating, steams ethanol;
By extracted with diethyl ether 3 times, collect and merge organic phase extraction liquid, aqueous phase discarded.
(3) purify
With anhydrous sodium sulfate drying, steam ether, obtain Syzygium aromaticum stem oil, yield is 28-33%.
3, weigh
By the formula of soil conditioner, take scallop shell powder, oyster shell powder, perilla oil, Syzygium aromaticum stem oil, zanthoxylum powder, Silktree Albizzia Bark, alginate calcium, crab shell, flyash, ammonium sulfate, residue of monosodium glutamate, ferrous sulfate, reddle powder, floats, calcium carbonate respectively, for subsequent use.
4, Silktree Albizzia Bark and crab shell is pulverized
Silktree Albizzia Bark and crab shell being pulverized respectively is 80 object fine powders.
5, mix
By oyster shell powder, reddle powder, floats, calcium carbonate mixing, stir, levigate, cross 80 mesh sieves, obtain blended solid powders A;
By zanthoxylum powder, Silktree Albizzia Bark powder, alginate calcium, the mixing of crab shell powder, instillation perilla oil, stirs, obtains solid mixture B;
By scallop shell powder, flyash, ammonium sulfate, residue of monosodium glutamate, ferrous sulfate mixing, instillation Syzygium aromaticum stem oil, stirs, obtains solid mixture C.
6, granulation
Blended solid powders A, solid mixture B, solid mixture C are merged, after stirring, adds tablets press;
Through granulator granulation, during granulation, the distilled water of spray trace, after making particle, then dries, sieves, and removing moisture, obtain finished product soil conditioner, spherical, particle diameter is 2-3.5cm.
Result detects:
(1) Indexs measure is carried out to soil conditioner of the present invention, the results are shown in Table 1;
The Indexs measure result of table 1 soil conditioner
From table 1, the granulating rate of soil conditioner of the present invention is 95.6-98.7%, and anti-crushing power is 17-20N.
(2) adopt the soil conditioner of embodiment 1-3 to process the soil that hardens, mu amount of application 200-250kg, after process, soil property detected result is in table 2;
Table 2 Soil Quality Indexes detected result
From table 3, after using soil conditioner process soil of the present invention, soil porosity is 55-60%, and soil median size is 2.1-2.6mm, and water capacity is 17.5-18.1%, pH is 6.9-7.1, and unit weight is 1.40-1.45g/cm
3;
Through test, after soil conditioner of the present invention is used, Effect of improving soil is obvious, and effect is held time and reached 3 years, and in 3 years, soil occurs without the phenomenon that hardens.
(3) after adopting the soil conditioner of embodiment 1-3 to process the soil that hardens, plantation cucumber, plantation the results are shown in Table 3;
Table 3 green cucumber result
From table 3, adopt soil conditioner process of the present invention to harden after soil, plantation cucumber, cucumber quality is good, and output is high; Cucumber yield is 1600-1800kg/ mu, and single cucumber weight in average is 270-290g, and the protein content of cucumber is 64-66g/100g, and the vitamin contents of cucumber is 11.2-12.1g/100g.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.The above is the citing of best mode for carrying out the invention, and the part wherein do not addressed in detail is the common practise of those of ordinary skill in the art; Protection scope of the present invention is as the criterion with the content of claim, and any equivalent transformation carried out based on technology enlightenment of the present invention, also within protection scope of the present invention.
Claims (10)
1. a long-acting shellfish algae soil conditioner, is characterized in that: described soil conditioner comprises following component: scallop shell powder, oyster shell powder, perilla oil, Syzygium aromaticum stem oil, zanthoxylum powder, Silktree Albizzia Bark, alginate calcium, crab shell, flyash, ammonium sulfate, residue of monosodium glutamate, ferrous sulfate, reddle powder, floats, calcium carbonate.
2. one according to claim 1 long-acting shellfish algae soil conditioner, is characterized in that: the weight part of each component of described soil conditioner is: scallop shell powder 12-23 part, oyster shell powder 29-35 part, perilla oil 2.2-3.4 part, Syzygium aromaticum stem oil 1.8-2.4 part, zanthoxylum powder 5-8 part, Silktree Albizzia Bark 10-15 part, alginate calcium 3-4.5 part, crab shell 7-10 part, flyash 6-9 part, ammonium sulfate 11-14 part, residue of monosodium glutamate 9-13 part, ferrous sulfate 6-11 part, reddle powder 3-7 part, floats 8-14 part, calcium carbonate 8-14 part.
3. one according to claim 2 long-acting shellfish algae soil conditioner, is characterized in that: the weight part of each component of described soil conditioner is: 18 parts, scallop shell powder, oyster shell powder 30 parts, perilla oil 3.0 parts, Syzygium aromaticum stem oil 2.2 parts, zanthoxylum powder 6 parts, Silktree Albizzia Bark 13 parts, alginate calcium 4 parts, 9 parts, crab shell, 8 parts, flyash, 12 parts, ammonium sulfate, residue of monosodium glutamate 10 parts, 8 parts, ferrous sulfate, 5 parts, reddle powder, floats 11 parts, 10 parts, calcium carbonate.
4. one according to claim 1 long-acting shellfish algae soil conditioner, is characterized in that: described perilla oil: containing perillaldehyde 63-68%, and specific optical rotation is-10 °-+100 °, and specific refractory power is 1.4680-1.4998.
5. one according to claim 1 long-acting shellfish algae soil conditioner, it is characterized in that: described Syzygium aromaticum stem oil: containing Eugenol 54-60%, the refractive index at 20 DEG C is 1.5200-15360, the relative density at 20 DEG C is 1.001-1.060.
6. one according to claim 1 long-acting shellfish algae soil conditioner, is characterized in that: described residue of monosodium glutamate: crude ash content is 2.35%, and crude fat content is 3.46%, and calcium contents is 0.12%; Albumen total content is 70%.
7. a preparation method for long-acting shellfish algae soil conditioner, is characterized in that: described preparation method comprises perilla oil extraction step; Described perilla oil extracts: yield is 45-48%.
8. the preparation method of a kind of long-acting shellfish algae soil conditioner according to claim 7, is characterized in that: described perilla oil extracts: purple perilla is put into still kettle, adds the normal hexane of purple perilla 2 times of quality, and 120rpm stirs, heating, and control temperature is 55 DEG C; Cooling, refluxes 1 hour.
9. the preparation method of a kind of long-acting shellfish algae soil conditioner according to claim 7, is characterized in that: described preparation method also comprises Syzygium aromaticum stem oil and extracts, weighs, pulverizes Silktree Albizzia Bark and crab shell, mixing, granulation.
10. the preparation method of a kind of long-acting shellfish algae soil conditioner according to claim 9, it is characterized in that: described Syzygium aromaticum stem oil extracts: Flos Caryophylli puts into still kettle, adds 95% ethanol of Flos Caryophylli 10 times of quality, is heated to micro-boiling, continue 60min, cooling for reflux; In phegma 5% sodium hydroxide solution, be 9-10 to pH value; Heating, steams ethanol; Extracted with diethyl ether 3 times; Dry; Yield is 28-33%;
Described pulverizing Silktree Albizzia Bark and crab shell: Silktree Albizzia Bark and crab shell being pulverized respectively is 80 object fine powders;
Described granulation: the particle produced is spherical, particle diameter is 2-3.5cm.
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| CN104130085A (en) * | 2014-07-30 | 2014-11-05 | 烟台众德集团有限公司 | Soil conditioner produced from magnesium ore and shell and production method thereof |
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| CN105087016A (en) * | 2015-09-09 | 2015-11-25 | 南宁汉和生物科技有限公司 | Soil conditioner rich in marine substances |
-
2015
- 2015-11-30 CN CN201510851890.1A patent/CN105367339A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102321484A (en) * | 2011-06-09 | 2012-01-18 | 山东省农业科学院农业资源与环境研究所 | Organic environmentally-friendly soil conditioner for improving acidified or acid soil |
| CN103444390A (en) * | 2013-07-25 | 2013-12-18 | 王运海 | Method for planting radix aconiti agrestis |
| CN104130085A (en) * | 2014-07-30 | 2014-11-05 | 烟台众德集团有限公司 | Soil conditioner produced from magnesium ore and shell and production method thereof |
| CN104774087A (en) * | 2015-03-27 | 2015-07-15 | 深圳柏施泰环境科技有限公司 | Biological preparation, its preparation method, and its application in soil improvement and fertilizers |
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Application publication date: 20160302 |