CN105342888A - Environment-friendly nail polish and preparation method thereof - Google Patents
Environment-friendly nail polish and preparation method thereof Download PDFInfo
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- CN105342888A CN105342888A CN201510834452.4A CN201510834452A CN105342888A CN 105342888 A CN105342888 A CN 105342888A CN 201510834452 A CN201510834452 A CN 201510834452A CN 105342888 A CN105342888 A CN 105342888A
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- Prior art keywords
- environmental
- nail enamel
- pigment
- friendnail nail
- friendnail
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
Abstract
The invention discloses environment-friendly nail polish and a preparation method thereof. The environment-friendly nail polish comprises 5-10% of nitrocellulose, 5-10% of alkyd resin, 5-10% of acetyl tributyl citrate, 30-40% of bisphenol A epoxy resin, 10-18% of essential oil, 5-10% of ethyl alcohol, 3-9% of solvents, 2-6% of pigment and the balance purified water. The environment-friendly nail polish solves the problem that traditional environment-friendly nail polish is always added with a great quantity of acetone and bisphenol A epoxy resin and can release a great quantity of pungent smell during application as well as the problem that current environment-friendly nail polish is scratched and sheds easily.
Description
Technical field
The present invention relates to cosmetic field, particularly a kind of Environmental-friendnail nail enamel and preparation method thereof.
Background technology
Nial polish is more and more subject to liking to be beautiful the welcome of personage, in General nail oil, in order to reach the object making nial polish parch fast, adds a large amount of acetone, bisphenol A type epoxy resin composition,
As Chinese invention patent CN102846523A discloses a kind of long-acting nial polish, it is characterized in that: be made up of the raw material of following parts by weight: acetone 10-30 part, ethyl acetate 8-20 part, amino resins 7-15 part, ethyl acetate 5-15 part, rose essence 5-8 part, NC Nitroncellulose 9-17 part, vitamin A 7-12 part, cod-liver oil 5-8 part, Radix Ginseng extractive solution 3-5 part, pearl essence 2-6 part, the inside is just containing this type of harm composition a large amount of.
As Chinese invention patent CN101829029B discloses a kind of nial polish, its component comprises Phthalide type leuco dye, acetone, developer, pearl essence and diluent.Preparation method first adds in acetone by Phthalide type leuco dye, stirs, and after dissolving completely, adds diluent, then add developer, stirs and make it to dissolve completely, finally add pearl essence, stirs 30-60min, just containing this type of harm composition in obtained product.
The feature of these two kinds of compositions is highly volatiles, so nial polish can be killed very soon.But acetone, bisphenol A type epoxy resin belong to hazardous chemical, they are inflammable and explosive, the penetrating odor of giddy is produced when volatilizing, room air is produced and stains (after volatilization, their volume is by expansion 1,000 times), when long-term suction, may harm be produced to nervous system, also have strong and stimulating to mucosa.If have baby in family, contact this constituents just more dangerous.These organic solvents also have a harm, are exactly at repeatedly Reusability, can make fingernail variable color, become fragile, turn white after fingernail, cause " manicure does not become counter and ruins first ", and current nial polish is also easy to scrape and damages and drop.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of Environmental-friendnail nail enamel and preparation method thereof, solve in traditional Environmental-friendnail nail enamel and often add a large amount of acetone, bisphenol A type epoxy resin, can discharge a large amount of penetrating odor when smearing, current Environmental-friendnail nail enamel is also easy to scrape the problem of damaging and dropping simultaneously.
For achieving the above object, the invention provides following technical scheme: a kind of Environmental-friendnail nail enamel, wherein, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 5-10%, alkyd resins 5-10%, Fructus Citri Limoniae join acetyl tributyl 5-10%, bisphenol A type epoxy resin 30-40%, calcium carbonate 2-5%, quintessence oil 10-18%, ethanol 5-10%, solvent 3-9%, pigment 2-6%, surplus pure water.
Preferably, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 6-8%, alkyd resins 5-7%, Fructus Citri Limoniae join acetyl tributyl 7-9%, bisphenol A type epoxy resin 32-38%, calcium carbonate 3-4%, quintessence oil 5-7%, ethanol 6-8%, solvent 5-7%, pigment 4-5%, surplus pure water.
Preferably, described solvent is the mixed solution of isomery dodecane and citric acid.
The present invention also provides a kind of preparation method of Environmental-friendnail nail enamel, and described method comprises:
(1) nitrocellulose, alkyd resins, Fructus Citri Limoniae are joined acetyl tributyl, bisphenol A type epoxy resin, quintessence oil Homogeneous phase mixing 5-10min at 20-30 DEG C, at 20-30 DEG C, put 10-12min afterwards, form mixed liquor M;
(2) the mixed liquor M in step (1) is heated to 30-35 DEG C, and adds ethanol, calcium carbonate and solvent and stir, after stirring 10-12min, add pigment and pure water continues to stir 5-10min, tinning after cooling.
Preferably, described pigment comprises one or more in sunset yellow, carmine pigment and erythrosine color.
Preferably, described mixed liquor M needs before heating after filtration to remove insoluble matter wherein.
Preferably, the method for described filtration is sucking filtration, and being specially described sucking filtration is vacuum filtration or decompress filter.
Beneficial effect: the invention provides a kind of Environmental-friendnail nail enamel and preparation method thereof, not containing volatile material such as acetone in the raw material of Environmental-friendnail nail enamel of the present invention, can not penetrating odor be distributed when smearing, Health cost is caused to human body, use bisphenol A type epoxy resin, environment friendly and pollution-free, quick volatilization, makes the molding of Environmental-friendnail nail enamel rapid solidification, is dissolved in pure water, be convenient to pure washing, conveniently unload Environmental-friendnail nail enamel; Containing quintessence oil and calcium carbonate, fingernail is nursed, supplement calcium composition, nail surface is made to have more gloss, nitrocellulose is added with in the present invention simultaneously, greatly can improve the stickup performance of Environmental-friendnail nail enamel, make the Environmental-friendnail nail enamel after smearing have good wearability, make it be not easy scrape damage and come off.The method of manufacture Environmental-friendnail nail enamel provided by the invention, not only step is simple, and raw material is easy to get, and can provide the production efficiency of Environmental-friendnail nail enamel.
Detailed description of the invention
The following detailed description of the preferred embodiment of the present invention.
Embodiment 1
A preparation method for Environmental-friendnail nail enamel, described method comprises: nitrocellulose, alkyd resins, Fructus Citri Limoniae are joined acetyl tributyl, bisphenol A type epoxy resin, quintessence oil Homogeneous phase mixing 10min at 20 DEG C, puts 10min afterwards at 20 DEG C, forms mixed liquor M; Mixed liquor M is heated to 30 DEG C, and adds ethanol, calcium carbonate and solvent and stir, after stirring 10min, add pigment and pure water continues to stir 10min, tinning after cooling.
Wherein, solvent is the mixed solution of isomery dodecane and citric acid, and pigment is carmine pigment.
Wherein, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 8%, alkyd resins 5%, Fructus Citri Limoniae join acetyl tributyl 7%, bisphenol A type epoxy resin 32%, quintessence oil 12%, ethanol 6%, solvent 5%, pigment 4%, calcium carbonate 5%, surplus pure water.
Embodiment 2
A preparation method for Environmental-friendnail nail enamel, described method comprises: nitrocellulose, alkyd resins, Fructus Citri Limoniae are joined acetyl tributyl, bisphenol A type epoxy resin, quintessence oil Homogeneous phase mixing 15min at 30 DEG C, puts 12min afterwards at 30 DEG C, forms mixed liquor M; Mixed liquor M is heated to 35 DEG C, and adds ethanol, calcium carbonate and solvent and stir, after stirring 12min, add pigment and pure water continues to stir 15min, tinning after cooling.
Wherein, solvent is the mixed solution of isomery dodecane and citric acid, and pigment is erythrosine color.
Wherein, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 6%, alkyd resins 7%, Fructus Citri Limoniae join acetyl tributyl 9%, bisphenol A type epoxy resin 38%, quintessence oil 14%, ethanol 8%, solvent 7%, pigment 5%, calcium carbonate 2% surplus pure water.
Embodiment 3
A preparation method for Environmental-friendnail nail enamel, described method comprises: nitrocellulose, alkyd resins, Fructus Citri Limoniae are joined acetyl tributyl, bisphenol A type epoxy resin, quintessence oil Homogeneous phase mixing 12min at 25 DEG C, puts 11min afterwards at 25 DEG C, forms mixed liquor M; Mixed liquor M is heated to 32 DEG C, and adds ethanol, calcium carbonate and solvent and stir, after stirring 11min, add pigment and pure water continues to stir 13min, tinning after cooling.
Wherein, solvent is the mixed solution of isomery dodecane and citric acid, and pigment is sunset yellow.
Wherein, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 6%, alkyd resins 8%, Fructus Citri Limoniae join acetyl tributyl 8%, bisphenol A type epoxy resin 36%, quintessence oil 13%, ethanol 7%, solvent 6%, pigment 4.5%, calcium carbonate 4%, surplus pure water.
Embodiment 4
Preparation method is identical with embodiment 1, unlike, the formula of described Environmental-friendnail nail enamel is: nitrocellulose 10%, alkyd resins 10%, Fructus Citri Limoniae join acetyl tributyl 5%, bisphenol A type epoxy resin, 30%, quintessence oil 10%, ethanol 5%, solvent 3%, pigment 2%, calcium carbonate 4% surplus pure water.
Embodiment 5
Preparation method is identical with embodiment 3, unlike, nitrocellulose 5%, alkyd resins 5%, Fructus Citri Limoniae join acetyl tributyl 5%, bisphenol A type epoxy resin 40%, quintessence oil 16%, ethanol 8%, solvent 6%, pigment 6%, calcium carbonate 5%, surplus pure water.
Comparative example 1
Preparation method is identical with embodiment 3, unlike, nitrocellulose 5%, alkyd resins 5%, Fructus Citri Limoniae join acetyl tributyl 2%, bisphenol A type epoxy resin 15%, quintessence oil 5%, ethanol 2%, solvent 1%, pigment 1%, surplus pure water.
Comparative example 2
Preparation method is identical with embodiment 3, unlike, nitrocellulose 20%, alkyd resins 20%, Fructus Citri Limoniae join acetyl tributyl 15%, bisphenol A type epoxy resin 30%, quintessence oil 25%, ethanol 15%, solvent 15%, pigment 10%, surplus pure water.
Table 1
| Embodiment is numbered | Expulsion rate (%) | Harmful substance release rate (%) |
| Embodiment 1 | 4 | 4 |
| Embodiment 2 | 5 | 7 |
| Embodiment 3 | 2 | 5 |
| Embodiment 4 | 7 | 11 |
| Embodiment 5 | 8 | 9 |
| Comparative example 1 | 15 | 33 |
| Comparative example 2 | 24 | 31 |
Can be found out by table 1, the expulsion rate of Environmental-friendnail nail enamel obtained within the scope of the present invention and harmful substance release rate all will lower than the Environmental-friendnail nail enamel obtained outward in the scope of the invention, and simultaneously obtained in the preferred scope of the present invention Environmental-friendnail nail enamel performance is more excellent.
The invention provides a kind of Environmental-friendnail nail enamel and preparation method thereof, the raw material of described Environmental-friendnail nail enamel comprises nitrocellulose 5-10%, alkyd resins 5-10%, Fructus Citri Limoniae joins acetyl tributyl 5-10%, bisphenol A type epoxy resin 30-40%, quintessence oil 10-18%, ethanol 5-10%, solvent 3-9%, pigment 2-6%, surplus pure water, present invention also offers a kind of preparation method of Environmental-friendnail nail enamel, the method comprises nitrocellulose, alkyd resins, Fructus Citri Limoniae joins acetyl tributyl, bisphenol A type epoxy resin, quintessence oil is Homogeneous phase mixing 5-10min at 20-30 DEG C, 10-12min is put afterwards at 20-30 DEG C, form mixed liquor M, mixed liquor M is heated to 30-35 DEG C, and adds ethanol, calcium carbonate and solvent and stir, after stirring 10-12min, add pigment and pure water continues to stir 5-10min, tinning after cooling.Not containing volatile material such as acetone in the raw material of Environmental-friendnail nail enamel of the present invention, penetrating odor can not be distributed when smearing, Health cost is caused to human body, nitrocellulose is added with in the present invention simultaneously, greatly can improve the stickup performance of Environmental-friendnail nail enamel, make the Environmental-friendnail nail enamel after smearing have good wearability, make it be not easy scrape damage and come off.The method of manufacture Environmental-friendnail nail enamel provided by the invention, not only step is simple, and raw material is easy to get, and can provide the production efficiency of Environmental-friendnail nail enamel.
Above-described is only the preferred embodiment of the present invention, it should be pointed out that for the person of ordinary skill of the art, and without departing from the concept of the premise of the invention, can also make some distortion and improvement, these all belong to protection scope of the present invention.
Claims (8)
1. an Environmental-friendnail nail enamel, it is characterized in that, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 5-10%, alkyd resins 5-10%, Fructus Citri Limoniae join acetyl tributyl 5-10%, bisphenol A type epoxy resin 30-40%, quintessence oil 10-18%, calcium carbonate 2-5%, ethanol 5-10%, solvent 3-9%, pigment 2-6%, surplus pure water.
2. Environmental-friendnail nail enamel according to claim 1, it is characterized in that, the formula of described Environmental-friendnail nail enamel comprises: nitrocellulose 6-8%, alkyd resins 5-7%, Fructus Citri Limoniae join acetyl tributyl 7-9%, bisphenol A type epoxy resin 32-38%, quintessence oil 5-7%, calcium carbonate 3-4%, ethanol 6-8%, solvent 5-7%, pigment 4-5%, surplus pure water.
3. Environmental-friendnail nail enamel according to claim 1 and 2, is characterized in that, described solvent is the mixed solution of isomery dodecane and citric acid.
4. utilize the formula described in claim 1 to prepare a method for Environmental-friendnail nail enamel, it is characterized in that, described method comprises:
(1) nitrocellulose, alkyd resins, Fructus Citri Limoniae are joined acetyl tributyl, bisphenol A type epoxy resin, quintessence oil Homogeneous phase mixing 5-10min at 20-30 DEG C, at 20-30 DEG C, put 10-12min afterwards, form mixed liquor M;
(2) the mixed liquor M in step (1) is heated to 30-35 DEG C, and adds ethanol, calcium carbonate and solvent and stir, after stirring 10-12min, add pigment and pure water continues to stir 5-10min, tinning after cooling.
5. the method preparing Environmental-friendnail nail enamel according to claim 4, is characterized in that, described pigment comprise in sunset yellow, carmine pigment and erythrosine color one or more.
6. the method preparing Environmental-friendnail nail enamel according to claim 4, is characterized in that, described mixed liquor M needs before heating after filtration to remove insoluble matter wherein.
7. the method preparing Environmental-friendnail nail enamel according to claim 6, is characterized in that, the method for described filtration is sucking filtration.
8. the method preparing Environmental-friendnail nail enamel according to claim 7, is characterized in that, described sucking filtration is vacuum filtration or decompress filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510834452.4A CN105342888A (en) | 2015-11-26 | 2015-11-26 | Environment-friendly nail polish and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510834452.4A CN105342888A (en) | 2015-11-26 | 2015-11-26 | Environment-friendly nail polish and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN105342888A true CN105342888A (en) | 2016-02-24 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510834452.4A Pending CN105342888A (en) | 2015-11-26 | 2015-11-26 | Environment-friendly nail polish and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101088487A (en) * | 2006-04-04 | 2007-12-19 | 莱雅公司 | Cosmetic or pharmaceutical composition comprising a condensation polymer, cosmetic treatment method employing said composition, said condensation polymer and preparation method |
| CN102090997A (en) * | 2009-12-11 | 2011-06-15 | 路雪 | Health-care nail polish |
| CN102228411A (en) * | 2011-06-23 | 2011-11-02 | 谭卓华 | Two-in-one water-soluble nail painting and protecting membrane solution |
| CN102475637A (en) * | 2010-11-23 | 2012-05-30 | 得昱国际股份有限公司 | Crack nail polish |
| CN103655277A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Light fragrance long-acting nail polish |
| CN103735427A (en) * | 2013-12-02 | 2014-04-23 | 林学荣 | Fluorescent color-changing nail polish |
-
2015
- 2015-11-26 CN CN201510834452.4A patent/CN105342888A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101088487A (en) * | 2006-04-04 | 2007-12-19 | 莱雅公司 | Cosmetic or pharmaceutical composition comprising a condensation polymer, cosmetic treatment method employing said composition, said condensation polymer and preparation method |
| CN102090997A (en) * | 2009-12-11 | 2011-06-15 | 路雪 | Health-care nail polish |
| CN102475637A (en) * | 2010-11-23 | 2012-05-30 | 得昱国际股份有限公司 | Crack nail polish |
| CN102228411A (en) * | 2011-06-23 | 2011-11-02 | 谭卓华 | Two-in-one water-soluble nail painting and protecting membrane solution |
| CN103655277A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Light fragrance long-acting nail polish |
| CN103735427A (en) * | 2013-12-02 | 2014-04-23 | 林学荣 | Fluorescent color-changing nail polish |
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Address after: Nansha District Fengze road Guangzhou city Guangdong province 510000 No. 106 X1301-B437 Applicant after: GUANGZHOU JUZHU PATENT RESEARCH AND DEVELOPMENT CO., LTD. Address before: 510370 Guangdong province Guangzhou City Creek Road in Panlong industrial zone of Liwan District dragon two friends of a 6 storey industrial building Applicant before: GUANGZHOU JUZHU PATENT RESEARCH AND DEVELOPMENT CO., LTD. |
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Application publication date: 20160224 |