CN106221445A - A kind of wicker plaiting article base paint special - Google Patents

A kind of wicker plaiting article base paint special Download PDF

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Publication number
CN106221445A
CN106221445A CN201610601869.0A CN201610601869A CN106221445A CN 106221445 A CN106221445 A CN 106221445A CN 201610601869 A CN201610601869 A CN 201610601869A CN 106221445 A CN106221445 A CN 106221445A
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China
Prior art keywords
mixture
plaiting article
mass ratio
wicker plaiting
base paint
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Pending
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CN201610601869.0A
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Chinese (zh)
Inventor
朱春辉
朱洪阳
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Funan County Dong'ao Handicraft Ltd Co
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Funan County Dong'ao Handicraft Ltd Co
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Priority to CN201610601869.0A priority Critical patent/CN106221445A/en
Publication of CN106221445A publication Critical patent/CN106221445A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08—Anti-corrosive paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of wicker plaiting article base paint special, it is made up of following components: acrylic resin, deionized water, alkyd resin, modified silicasol, calcium stearate, glyceryl tristearate, modified rubber powder, dodecyl sodium sulfate, preservative, Polyethylene Glycol, celluloid, Colophonium, coalescents, Sucus Cocois, pigment, a kind of wicker plaiting article base paint special cost of material that the present invention provides is low, in priming paint and use be free from the volatile material such as benzene, user health will not be had side effects, paint film good toughness is difficult to split, adhesive force is strong, antiseptic property is excellent, it is resistant to 612 DEG C of high temperature and does not bursts apart, the solvent resistant of resistance to crude oil is effective, and can preferably combine finish paint, can preserve wicker products more than 6 years will not depainting.

Description

A kind of wicker plaiting article base paint special
Technical field
The present invention relates to paint field, particularly relate to a kind of wicker plaiting article base paint special.
Background technology
Wicker products is the artifacts of China's widespread among the people, " compile basket, compile basket, every household has ".This is because this The raw material sources planting technique are quite varied.The primary raw material of basket is compiled in the north for compiling basket Ramulus Salicis Babylonicae, Ramulus et Folium Tamaricis branch, mulberry shoot, Vitex chinensis Mill., purple Fringe Rumalus sophorae etc. are multiple, produce in salt-soda soil and marshland.A variety of wicker productses are all the article of people's close contact, It is thus desirable to use nontoxic coating or paint to process, prevent toxic residue.
Priming paint is the ground floor of paint system, for improving the adhesive force of finish paint, increasing the richness of finish paint, offer alkali resistant Property, anti-corrosion function etc. is provided, can ensure that the uniform pickup of finish paint simultaneously, be that paint system plays optimum efficiency.Traditional willow Volume priming paint is usually solvent bottom paint, and containing substantial amounts of organic solvent, human body not only when construction, is caused one by these solvents Fixed injury, and it is after construction, can slowly evaporate in air, thus contactee is caused certain injury, and attached Put forth effort, alkali resistance, anti-corrosion function general, the richness of follow-up increase finish paint is general.
Summary of the invention
In order to overcome above-mentioned deficiency, the invention provides a kind of wicker plaiting article base paint special.
The present invention is achieved through the following technical solutions:
A kind of wicker plaiting article base paint special, is made up of following components: acrylic resin 46, deionized water 32, alkyd tree by weight Fat 20, modified silicasol 12, calcium stearate 3, glyceryl tristearate 4, modified rubber powder 6, dodecyl sodium sulfate 1, anticorrosion Agent 1, Polyethylene Glycol 3, celluloid 2, Colophonium 3, coalescents 1, Sucus Cocois 15, pigment 0.5；
Described Sucus Cocois preparation method is:
1. taking new fresh cocoanut juice, put into cold preservation 2-3 days in cold room, refrigerated storage temperature is 1-3 DEG C；
2. the Sucus Cocois after cold preservation is taken out, be heated to 26-28 DEG C, then add the sodium carbonate of its quality 3% and sulfur for sulfur Acid sodium mixture, stirs to thoroughly dissolving；Wherein sodium carbonate and sodium thiosulfate are mixed by 4.75:1 mass ratio；
3. using anode and negative electrode is all ferrum, carries out being electrolysed 1-2min to 2. middle Sucus Cocois；
4. the Sucus Cocois through electrolysis after centrifugal treating 40 minutes, is respectively charged into 500mL circle under 850-900r/min rotating speed In cylindrical container, after sealing and standing 3-4 hour, the Sucus Cocois of extracting container 250mL, as priming paint raw material.
Further, the preparation method of described modified silicasol is:
1. nano aluminium oxide is evenly spread in Ludox by 1:50 mass ratio, form mixture 1；
2. being distributed in mixture 1 by 1:100 mass ratio by initiator, form mixture 2, described initiator is acyl phosphonic acid Sodium；
3. the zinc powder that granularity is 700-800 mesh is evenly spread in mixture 2 by 1:85 mass ratio, after stirring, shape Resulting mixture 3, then by 1:110 mass ratio, silane coupler KH-560 is evenly spread in mixture 3, form mixture 4；
4. with 550r/min rotary speed stirring mixture 4, and constant temperature is at 78-82 DEG C, reacts 3-4 hour, obtains modified silicasol.
Further, the preparation method of described modified rubber powder is: by 1:100 mass ratio by nano zine oxide and rubber Powder is the most admixed together, then adds the silane coupler KH-560 of mixture quality 0.5%, after stirring, carries out ball milling 30-40min,；The granularity of rubber powder is 650-700 mesh.
Further, described preservative uses extract solution of bamboo leaves, and its preparation method is: takes fresh Folium Bambusae, first uses clear water After cleaning up, then pulverize, be then added in the ethanol solution that mass concentration is 72.5%, enter with 200r/min rotating speed Row stirring, and use ultrasonic assistant to extract 30-35min, finally, filter, obtain extracting solution, then concentrate,.
Further, one or more combinations during described pigment is titanium dioxide, lead chromate yellow, red, phthalocyanine blue.
Further, described coalescents is that diethylene glycol, Oleum Terebinthinae are mixed by 1:4 mass ratio.
The present invention is through substantial amounts of experimentation, by being modified Ludox such that it is able to be greatly improved inorganic material The compatibility between material silicon dioxide and organic resin, and improve hardness and the adhesive force of coating, and simple process, controlled Property strong, there is high value of practical, the present invention uses modified silicasol to be main film forming substance, solves tradition priming paint storage steady Qualitative, film property is the best and the problem such as easy gel unstability, and, Sucus Cocois prepared by the present invention, modified rubber powder, Colophonium with change Property Ludox when preparing priming paint, Ludox micelle is had bondage effect, assists Ludox film forming to reduce its rigidity, coordinate other The synergism of auxiliary agent, has given play to the excellent characteristics after Ludox film forming, the wicker plaiting article priming paint of preparation have hardness height, drying speed, The initial stage crushing resistance that had, resistance to water is excellent, adhesive force good, grinability is good.
The invention has the beneficial effects as follows: a kind of wicker plaiting article base paint special cost of material that the present invention provides is low, in priming paint and make With being free from the volatile material such as benzene, will not have side effects user health, paint film good toughness is difficult to split, and adhesive force is strong, Antiseptic property is excellent, be resistant to 612 DEG C of high temperature and do not burst apart, and the solvent resistant of resistance to crude oil is effective, and can preferably combine finish paint, Can preserve wicker products more than 6 years will not depainting, can be in conjunction with multiple finish paint.
Detailed description of the invention
A kind of wicker plaiting article base paint special, is made up of following components: acrylic resin 46, deionized water 32, alcohol by weight Acid resin 20, modified silicasol 12, calcium stearate 3, glyceryl tristearate 4, modified rubber powder 6, dodecyl sodium sulfate 1, Preservative 1, Polyethylene Glycol 3, celluloid 2, Colophonium 3, coalescents 1, Sucus Cocois 15, pigment 0.5；
Described Sucus Cocois preparation method is:
1. taking new fresh cocoanut juice, put into cold preservation 2-3 days in cold room, refrigerated storage temperature is 1-3 DEG C；
2. the Sucus Cocois after cold preservation is taken out, be heated to 26-28 DEG C, then add the sodium carbonate of its quality 3% and sulfur for sulfur Acid sodium mixture, stirs to thoroughly dissolving；Wherein sodium carbonate and sodium thiosulfate are mixed by 4.75:1 mass ratio；
3. using anode and negative electrode is all ferrum, carries out being electrolysed 1-2min to 2. middle Sucus Cocois；
4. the Sucus Cocois through electrolysis after centrifugal treating 40 minutes, is respectively charged into 500mL circle under 850-900r/min rotating speed In cylindrical container, after sealing and standing 3-4 hour, the Sucus Cocois of extracting container 250mL, as priming paint raw material.
Further, the preparation method of described modified rubber powder is: by 1:100 mass ratio by nano zine oxide and rubber Powder is the most admixed together, then adds the silane coupler KH-560 of mixture quality 0.5%, after stirring, carries out ball milling 30-40min,；The granularity of rubber powder is 650-700 mesh.
Further, the preparation method of described modified silicasol is:
1. nano aluminium oxide is evenly spread in Ludox by 1:50 mass ratio, form mixture 1；
2. being distributed in mixture 1 by 1:100 mass ratio by initiator, form mixture 2, described initiator is acyl phosphonic acid Sodium；
3. the zinc powder that granularity is 700-800 mesh is evenly spread in mixture 2 by 1:85 mass ratio, after stirring, shape Resulting mixture 3, then by 1:110 mass ratio, silane coupler KH-560 is evenly spread in mixture 3, form mixture 4；
4. with 550r/min rotary speed stirring mixture 4, and constant temperature is at 78-82 DEG C, reacts 3-4 hour, obtains modified silicasol.
Further, described preservative uses extract solution of bamboo leaves, and its preparation method is: takes fresh Folium Bambusae, first uses clear water After cleaning up, then pulverize, be then added in the ethanol solution that mass concentration is 72.5%, enter with 200r/min rotating speed Row stirring, and use ultrasonic assistant to extract 30-35min, finally, filter, obtain extracting solution, then concentrate,.
Further, one or more combinations during described pigment is titanium dioxide, lead chromate yellow, red, phthalocyanine blue.
Further, described coalescents is that diethylene glycol, Oleum Terebinthinae are mixed by 1:4 mass ratio.
Two batches of identical wicker plaiting articles are selected to be respectively adopted wicker plaiting article priming paint of the present invention and common wicker plaiting article priming paint, the effect after statistics use Really.
Whether containing volatile material such as benzene Levelability Drying time at 30 DEG C Normal use occurs falling the paint time for the first time There is the paint time at the wicker plaiting article product frequently used and often deform
The present invention No Good 20min 7th year A year and a half
Common priming paint It is Typically 2h 2.5th year Two months
Table 1
Wicker plaiting article primer performance the most of the present invention is more excellent.
Performance detects:
The present invention Comparative example 1 Comparative example 2
Gloss (60 °) 40 42 48
Impact resistance, cm 52 48 40
Adhesive force, level 1 2 3
Pencil hardness 3H 2H H
At salt fog resistance (3% saline) 240h(line, single-point expands erosion less than 1.5mm) Qualified Qualified Defective
Resistance to water (1h of resistance to boiling water boiling, each performance is constant) Qualified Defective Defective
Table 2
Wherein, comparative example 1 is the Sucus Cocois prepared without the present invention, and other composition is identical with the present invention, the priming paint of preparation；
Comparative example 2 is, uses the Ludox modified without the present invention, and other composition is identical with the present invention, the priming paint of preparation.
As can be seen from Table 2, the Sucus Cocois prepared without the present invention, priming paint various aspects of performance has declined, and adopts With the Ludox modified without the present invention, priming paint various aspects of performance significantly declines.

Claims (6)

1. a wicker plaiting article base paint special, it is characterised in that be made up of following components by weight: acrylic resin 46, go from Sub-water 32, alkyd resin 20, modified silicasol 12, calcium stearate 3, glyceryl tristearate 4, modified rubber powder 6, dodecyl Sodium sulfonate 1, preservative 1, Polyethylene Glycol 3, celluloid 2, Colophonium 3, coalescents 1, Sucus Cocois 15, pigment 0.5；
Described Sucus Cocois preparation method is:
1. taking new fresh cocoanut juice, put into cold preservation 2-3 days in cold room, refrigerated storage temperature is 1-3 DEG C；
2. the Sucus Cocois after cold preservation is taken out, be heated to 26-28 DEG C, then add the sodium carbonate of its quality 3% and sulfur for sulfur Acid sodium mixture, stirs to thoroughly dissolving；Wherein sodium carbonate and sodium thiosulfate are mixed by 4.75:1 mass ratio；
3. using anode and negative electrode is all ferrum, carries out being electrolysed 1-2min to 2. middle Sucus Cocois；
4. the Sucus Cocois through electrolysis after centrifugal treating 40 minutes, is respectively charged into 500mL circle under 850-900r/min rotating speed In cylindrical container, after sealing and standing 3-4 hour, the Sucus Cocois of extracting container 250mL, as priming paint raw material.
A kind of wicker plaiting article base paint special the most according to claim 1, it is characterised in that the preparation method of described modified silicasol For:
1. nano aluminium oxide is evenly spread in Ludox by 1:50 mass ratio, form mixture 1；
2. being distributed in mixture 1 by 1:100 mass ratio by initiator, form mixture 2, described initiator is acyl phosphonic acid Sodium；
3. the zinc powder that granularity is 700-800 mesh is evenly spread in mixture 2 by 1:85 mass ratio, after stirring, shape Resulting mixture 3, then by 1:110 mass ratio, silane coupler KH-560 is evenly spread in mixture 3, form mixture 4；
4. with 550r/min rotary speed stirring mixture 4, and constant temperature is at 78-82 DEG C, reacts 3-4 hour, obtains modified silicasol.
A kind of wicker plaiting article base paint special the most according to claim 1, it is characterised in that the preparation method of described modified rubber powder For: by 1:100 mass ratio, nano zine oxide is the most admixed together with rubber powder, then add the silicon of mixture quality 0.5% Alkane coupling agent KH-560, after stirring, carries out ball milling 30-40min,；The granularity of rubber powder is 650-700 mesh.
A kind of wicker plaiting article base paint special the most according to claim 1, it is characterised in that described preservative uses Folium Bambusae to extract Liquid, its preparation method is: take fresh Folium Bambusae, after first using clean water clean, then pulverizes, is then added to mass concentration It is in the ethanol solution of 72.5%, is stirred with 200r/min rotating speed, and use ultrasonic assistant extraction 30-35min, finally, Filter, obtain extracting solution, then concentrate,.
A kind of wicker plaiting article base paint special the most according to claim 1, it is characterised in that described pigment be titanium dioxide, lead chromate yellow, One or more combinations in red, phthalocyanine blue.
A kind of wicker plaiting article base paint special the most according to claim 1, it is characterised in that described coalescents is a contracting second two Alcohol, Oleum Terebinthinae are mixed by 1:4 mass ratio.
CN201610601869.0A 2016-07-28 2016-07-28 A kind of wicker plaiting article base paint special Pending CN106221445A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108707399A (en) * 2018-07-03 2018-10-26 阜南县大自然工艺品有限公司 A kind of willow-plaited process product anti-fouling paint
CN108912917A (en) * 2018-06-26 2018-11-30 阜南县永盛工艺品有限公司 A kind of wicker plaiting article high-quality finishing coat

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105331214A (en) * 2015-10-31 2016-02-17 阜南县黄岗镇工艺柳编厂 Anti-corrosion paint for wickerwork made of purple willow

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105331214A (en) * 2015-10-31 2016-02-17 阜南县黄岗镇工艺柳编厂 Anti-corrosion paint for wickerwork made of purple willow

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Title
张生贵: "《农产品储藏加工100个为什么》", 30 June 2010 *
张默闻: "《卖点是把锤》", 31 October 2015 *
徐勤福等: "《防腐涂料配方精选》", 31 July 2011 *
杨智勇: "《汽车涂装技术》", 30 September 2005 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108912917A (en) * 2018-06-26 2018-11-30 阜南县永盛工艺品有限公司 A kind of wicker plaiting article high-quality finishing coat
CN108707399A (en) * 2018-07-03 2018-10-26 阜南县大自然工艺品有限公司 A kind of willow-plaited process product anti-fouling paint

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