CN105315813A - Water-based automobile metal base coat and preparing method thereof - Google Patents
Water-based automobile metal base coat and preparing method thereof Download PDFInfo
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- CN105315813A CN105315813A CN201510383508.9A CN201510383508A CN105315813A CN 105315813 A CN105315813 A CN 105315813A CN 201510383508 A CN201510383508 A CN 201510383508A CN 105315813 A CN105315813 A CN 105315813A
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Abstract
The invention relates to a water-based automobile metal base coat and a preparing method thereof. The base coat is prepared from, by weight, 30-40 parts of water-based acrylic emulsion, 5-10 parts of water-based aluminum paste, 0.3-1 part of dispersing agent, 3-6 parts of cosolvent, 0.3-1 part of antifoaming agent, 0.4-1 part of flatting agent, 7-12 parts of thickening agent, 1.5-3.5 parts of anti-settling agent, 0.02-0.05 part of pH regulator, and 35-45 parts of deionized water. The water-based automobile metal base coat is basically odorless after being exposed from a container, is diluted with clean tap water during construction, is a non-dangerous chemical article, and does not contain toxic and harmful substances including benzene, heavy metal and high-content VOC. Therefore, the base coat is more targeted and higher in directivity compared with oily products, and has broader market prospects.
Description
Technical field
The present invention relates to technical field of environmental protection paint, be specifically related to aqueous automobile metal bottom colored paint and preparation method thereof.
Background technology
According to the statistic data display that State Statistics Bureau announces, within 2014, Chinese coating ultimate production reaches 1648.188 ten thousand tons, increases by 7.87% on a year-on-year basis after adjustment.1303.349 ten thousand tons that compare coating ultimate production in 2013, within 2014,344.839 ten thousand tons are newly increased.Record high again.Wherein, the annual coating output in Guangdong Province is 333.99 ten thousand tons, increases by 6.92% on a year-on-year basis, and the annual coating output 187.09 ten thousand tons in Shanghai City, increases by 10.54% on a year-on-year basis, and the annual coating output 182.15 ten thousand tons in Jiangsu Province, increases by 5.43% on a year-on-year basis.Calculate with 2013 annual production, if use oil-base paint, annual air VOC total emission volumn is 1145 tons, and after using water-miscible paint, annual VOC total emission volumn is only 19 tons, the range of decrease up to 98%, as seen its to protection of the environment, to fall haze effect huge; Secondly, be coated with efficiency and significantly promote, oil-base paint is coated with efficiency only 35% ~ 40% before, and water-miscible paint is coated with efficiency and rises to more than 79% now, has both effectively reduced cost and has additionally reduced environmental pollution; Along with popularizing of environmental protection concept, water-borne coatings obtains the accreditation of more and more human consumer as the product with environmental-protecting performance.On January 16th, 2015, National Ministry of Finance combines with the national taxation bureau and has issued " notice about imposing the excise to battery, coating ", and environment-friendly water-basedization of coating is irresistible, and market outlook are wide.
Summary of the invention
The object of the invention is the deficiency for solving the problems of the technologies described above, a kind of aqueous automobile metal bottom colored paint and preparation method thereof is provided, this automobile metal base coat is nontoxic, do not fire, not containing benzene homologues, environmentally safe, healthy harmless to workmen, safe and convenient to use.
The present invention is the deficiency solved the problems of the technologies described above, the technical scheme adopted is: a kind of aqueous automobile metal bottom colored paint, is made up of the raw material of following portions by weight: aqueous acrylic emulsion 30 ~ 40 parts, water aluminum-silver slurry 5-10 part, dispersion agent 0.3 ~ 1 part, solubility promoter 3-6 part, defoamer 0.3 ~ 1 part, flow agent 0.4 ~ 1 part, thickening material 7 ~ 12 parts, anti-settling agent 1.5 ~ 3.5 parts, pH adjusting agent 0.02 ~ 0.05 part and deionized water 35 ~ 45 parts.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned aqueous acrylic emulsion is one in water-borne acrylic resin and Aqueous acrylic urethane's dispersion or arbitrarily than mixture.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned water aluminum-silver slurry is non-floating type aluminium-silver slurry, the aluminium silver powder particle diameter of aluminium-silver slurry is 5-80 micron, and the shape of aluminium-silver slurry is rice krispies flower pattern or silver dollar type.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned dispersion agent is that one or more in modified polyacrylate superpolymer, modified polyacrylate and ethylenic copolymer, the alkanolamine salt of high molecular weight carboxylic, fatty acid modified polyester are arbitrarily than mixture.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned defoamer is arbitrarily than mixture containing one or more in organic-silicon-modified water-based emulsion shape defoamer, organically-modified polydimethylsiloxane, ethylenic copolymer, vinyl polymer.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned solubility promoter is one or more any mixture in ethylene glycol fourth mystery, propylene glycol monomethyl ether, PMA, DBE, ethanol, butanols, Virahol, butanone, acetone.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned flow agent is that one or more in organic silicon modified by polyether polymkeric substance, organic silicon modified by polyether, modified polyorganosiloxane emulsion, the polyacrylic hydrosol of fluorine-carbon modified pre-neutralization, vinylformic acid-Organosiliconcopolymere are arbitrarily than mixture.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned thickening material is association type polyurethane thickener, the swelling acroleic acid polyurethane of alkali or cellulose thickener.
Further improvement as a kind of aqueous automobile of the present invention metal bottom colored paint: above-mentioned anti-settling agent polyamide wax ammonium salt or organobentonite; PH adjusting agent is dimethylethanolamine, ammoniacal liquor or triethylamine.
The preparation method of above-mentioned aqueous automobile metal bottom colored paint: comprise the following steps:
(1), aqueous ACRYLIC EMULSION 30 ~ 40 parts, water aluminum-silver slurry 5-10 part, dispersion agent 0.3 ~ 1 part, solubility promoter 3-6 part, defoamer 0.3 ~ 1 part, flow agent 0.4 ~ 1 part, thickening material 7 ~ 12 parts, anti-settling agent 1.5 ~ 3.5 parts, pH adjusting agent 0.02 ~ 0.05 part and deionized water 35 ~ 45 parts by weight, for subsequent use;
(2), by dispersion agent, solubility promoter, water aluminum-silver slurry and 5 parts of deionized water mixing and stirring, soak 15-20 minute, obtain component A for subsequent use;
(3), by aqueous acrylic emulsion, defoamer, flow agent, thickening material, anti-settling agent and residue deionized water mix, stir at low shear, obtain component B, for subsequent use;
(4), component B under stirring at low speed (stirring velocity is no more than 100r/min), stir while add component A, stir, obtain component C, for subsequent use;
(5), pH value is adjusted to 7.5-8.5 by component C pH adjusting agent, namely obtains environmental protection aluminium powder paint.
The using method of aqueous automobile metal bottom colored paint of the present invention is: first stirred by aluminium powder paint during construction, and with deionized water or the drinking public water supply latting drown of 5-15%, then according to construction requirement, even application is on workpiece to be coated.
Beneficial effect
Aqueous automobile metal bottom color paint coating of the present invention, compared with oil paint, has the following advantages:
(1) coating of the present invention adopts water-dispersible acrylic's emulsion, can give the ornamental of paint film excellence and film-forming properties;
(2) coating of the present invention possesses good snappiness, can prevent paint film cracking, come off;
(3) coating of the present invention has outstanding moisture resistance, directly can apply construction in wet structure and wet environment;
(4) coating of the present invention has good application property, fire hazard when eliminating construction;
(5) coating of the present invention is with water as solvent, saves ample resources, and can reduce topsoil;
(6) coating of the present invention only adopts a small amount of hypotoxicity alcohol ether organic solvent, improves operating environmental condition;
(7) paint spraying instrument of the present invention can wash by water, and greatly reduces the consumption of cleaning solvent.
Aqueous automobile metal bottom color paint coating of the present invention is all basic hear the taste that holds one's breath after can opening, is with clean water-reducible from the beginning, belongs to benign chemical during construction, and environmental protection index is not containing the hazardous and noxious substances such as VOC of benzene, heavy metal and high-content.Therefore, the present invention has more specific aim, clear and definite compared to oiliness series products directive property, has demand and the prospect in more wide market.
Embodiment
Following examples are used for further illustrating but are not limited to the present invention.
Embodiment 1
A kind of aqueous automobile metal bottom colored paint, be made up of the raw material of following portions by weight: aqueous acrylic emulsion 30 parts (E-125 of DSM N. V.), water aluminum-silver slurry 8 parts (SBCAQJ6811B5B of Xing Bolian company), dispersion agent 0.5 part (AFCONA6226), solubility promoter 4 parts (Virahol), defoamer 0.6 part (containing organosilyl water-based emulsion shape defoamer AFCONA2501), flow agent 0.6 part (vinylformic acid-Organosiliconcopolymere AQ-7130), thickening material 9 parts (HV-30 of BASF AG), anti-settling agent 2 parts (polyamide wax salt AQ607), pH adjusting agent 0.05 part (dimethylethanolamine) and deionized water 35 ~ 45 parts.
The preparation method of above-mentioned aqueous automobile metal bottom colored paint is as follows:
(1), aqueous ACRYLIC EMULSION 30 parts (E-125 of DSM N. V.) by weight, water aluminum-silver slurry 8 parts (SBCAQJ6811B5B of Xing Bolian company), dispersion agent 0.5 part (AFCONA6226), solubility promoter 4 parts (Virahol), defoamer 0.6 part (containing organosilyl water-based emulsion shape defoamer AFCONA2501), flow agent 0.6 part (vinylformic acid-Organosiliconcopolymere AQ-7130), thickening material 9 parts (HV-30 of BASF AG), anti-settling agent 2 parts (polyamide wax salt AQ607), pH adjusting agent 0.05 part (dimethylethanolamine) and deionized water 35 parts, for subsequent use,
(2), by dispersion agent, solubility promoter, water aluminum-silver slurry and 5 parts of deionized water mixing and stirring, soak 15-20 minute, obtain component A for subsequent use;
(3), by aqueous acrylic emulsion, defoamer, flow agent, thickening material, anti-settling agent and residue deionized water mix, after stirring, obtain component B, for subsequent use;
(4), component B under stirring at low speed (100r/min), stir while add component A, stir, obtain component C, for subsequent use;
(5), pH value is adjusted to 7.5 by component C pH adjusting agent, namely obtains aqueous automobile metal bottom colored paint.
Embodiment 2
A kind of aqueous automobile metal bottom colored paint, be made up of the raw material of following portions by weight: aqueous acrylic emulsion (Aqueous acrylic urethane's dispersion) 30 parts, water aluminum-silver slurry 10 parts, dispersion agent (alkanolamine salt of high molecular weight carboxylic) 0.3 part, solubility promoter (propylene glycol monomethyl ether) 6 parts, defoamer (water-based emulsion shape defoamer) 0.3 part, flow agent (modified polyorganosiloxane emulsion) 01 part, thickening material (the swelling acroleic acid polyurethane of alkali) 7 parts, anti-settling agent (organobentonite) 3.5 parts, pH adjusting agent (ammoniacal liquor) 0.02 part and deionized water 45 parts.
The preparation method of above-mentioned aqueous automobile metal bottom colored paint is as follows:
(1), aqueous ACRYLIC EMULSION 30 parts, water aluminum-silver slurry 10 parts, dispersion agent 0.3 part, solubility promoter 6 parts, defoamer 0.3 part, flow agent 01 part, thickening material 7 parts, anti-settling agent 3.5 parts, pH adjusting agent 0.02 part and deionized water 45 parts by weight, for subsequent use;
(2), by dispersion agent, solubility promoter, water aluminum-silver slurry and 5 parts of deionized water mixing and stirring, soak 15-20 minute, obtain component A for subsequent use;
(3), by aqueous acrylic emulsion, defoamer, flow agent, thickening material, anti-settling agent and residue deionized water mix, after stirring, obtain component B, for subsequent use;
(4), component B under stirring at low speed (80r/min), stir while add component A, stir, obtain component C, for subsequent use;
(5), pH value is adjusted to 8.5 by component C pH adjusting agent, namely obtains aqueous automobile metal bottom colored paint.
Embodiment 3
A kind of aqueous automobile metal bottom colored paint, is made up of the raw material of following portions by weight: aqueous acrylic emulsion (water-borne acrylic resin) 40 parts, water aluminum-silver slurry 5 parts, dispersion agent (fatty acid modified polyester) 1 part, solubility promoter (DBE) 3 parts, defoamer (ethylenic copolymer) 1 part, flow agent (vinylformic acid-Organosiliconcopolymere) 0.4 part, thickening material (cellulose thickener) 12 parts, anti-settling agent (polyamide wax ammonium salt) 1.5 parts, pH adjusting agent 0.05 part and deionized water 40 parts.
The preparation method of above-mentioned aqueous automobile metal bottom colored paint is as follows:
(1), a kind of aqueous automobile metal bottom colored paint is got by weight, be made up of the raw material of following portions by weight: aqueous acrylic emulsion (water-borne acrylic resin) 40 parts, water aluminum-silver slurry 5 parts, dispersion agent (fatty acid modified polyester) 1 part, solubility promoter (DBE) 3 parts, defoamer (ethylenic copolymer) 1 part, flow agent (vinylformic acid-Organosiliconcopolymere) 0.4 part, thickening material (cellulose thickener) 12 parts, anti-settling agent (polyamide wax ammonium salt) 1.5 parts, pH adjusting agent 0.05 part and deionized water 40 parts, for subsequent use;
(2), by dispersion agent, solubility promoter, water aluminum-silver slurry and 5 parts of deionized water mixing and stirring, soak 15-20 minute, obtain component A for subsequent use;
(3), by aqueous acrylic emulsion, defoamer, flow agent, thickening material, anti-settling agent and residue deionized water mix, after stirring, obtain component B, for subsequent use;
(4), component B under stirring at low speed (90/min), stir while add component A, stir, obtain component C, for subsequent use;
(5), pH value is adjusted to 8 by component C pH adjusting agent, namely obtains aqueous automobile metal bottom colored paint.
Testing data
With reference to the countries concerned or industry standard, Performance Detection is carried out to above specific embodiment:
The proportioning of embodiment 1-3 aluminium powder paint with deionized water or drinking public water supply 100:10 is mixed, be sprayed on tinplate, place in thermostatic constant wet chamber's (23 ± 2 DEG C, 50 ± 5%) and dry and select corresponding regulating time by technical indicator, record all technical and see the following form:
Claims (10)
1. aqueous automobile metal bottom colored paint, is characterized in that: be made up of the raw material of following parts by weight: aqueous acrylic emulsion 30 ~ 40 parts, water aluminum-silver slurry 5-10 part, dispersion agent 0.3 ~ 1 part, solubility promoter 3-6 part, defoamer 0.3 ~ 1 part, flow agent 0.4 ~ 1 part, thickening material 7 ~ 12 parts, anti-settling agent 1.5 ~ 3.5 parts, pH adjusting agent 0.02 ~ 0.05 part and deionized water 35 ~ 45 parts.
2. aqueous automobile metal bottom colored paint as claimed in claim 1, is characterized in that: described aqueous acrylic emulsion is one in water-borne acrylic resin and Aqueous acrylic urethane's dispersion or arbitrarily than mixture.
3. aqueous automobile metal bottom colored paint as claimed in claim 1, it is characterized in that: described water aluminum-silver slurry is non-floating type aluminium-silver slurry, the aluminium silver powder particle diameter of aluminium-silver slurry is 5-80 micron, and the shape of aluminium-silver slurry is rice krispies flower pattern or silver dollar type.
4. aqueous automobile metal bottom colored paint as claimed in claim 1, is characterized in that: described dispersion agent is that one or more in modified polyacrylate superpolymer, modified polyacrylate and ethylenic copolymer, the alkanolamine salt of high molecular weight carboxylic, fatty acid modified polyester are arbitrarily than mixture.
5. aqueous automobile metal bottom colored paint as claimed in claim 1, is characterized in that: described defoamer is arbitrarily than mixture containing one or more in organic-silicon-modified water-based emulsion shape defoamer, organically-modified polydimethylsiloxane, ethylenic copolymer, vinyl polymer.
6. aqueous automobile metal bottom colored paint as claimed in claim 1, is characterized in that: described flow agent is that one or more in organic silicon modified by polyether polymkeric substance, organic silicon modified by polyether, modified polyorganosiloxane emulsion, the polyacrylic hydrosol of fluorine-carbon modified pre-neutralization, vinylformic acid-Organosiliconcopolymere are arbitrarily than mixture.
7. aqueous automobile metal bottom colored paint as claimed in claim 1, is characterized in that: described thickening material is association type polyurethane thickener, the swelling acroleic acid polyurethane of alkali or cellulose thickener.
8. aqueous automobile metal bottom colored paint as claimed in claim 1, is characterized in that: described anti-settling agent polyamide wax ammonium salt or organobentonite; PH adjusting agent is dimethylethanolamine, ammoniacal liquor or triethylamine.
9. the preparation method of aqueous automobile metal bottom colored paint as described in claim as arbitrary in claim 1-8, is characterized in that: comprise the following steps:
(1), aqueous ACRYLIC EMULSION 30 ~ 40 parts, water aluminum-silver slurry 5-10 part, dispersion agent 0.3 ~ 1 part, solubility promoter 3-6 part, defoamer 0.3 ~ 1 part, flow agent 0.4 ~ 1 part, thickening material 7 ~ 12 parts, anti-settling agent 1.5 ~ 3.5 parts, pH adjusting agent 0.02 ~ 0.05 part and deionized water 35 ~ 45 parts by weight, for subsequent use;
(2), by dispersion agent, solubility promoter, water aluminum-silver slurry and 5 parts of deionized water mixing and stirring, soak 15-20 minute, obtain component A for subsequent use;
(3), by aqueous acrylic emulsion, defoamer, flow agent, thickening material, anti-settling agent and residue deionized water mix, after stirring, obtain component B, for subsequent use;
(4), component B under stirring at low speed, stir while add component A, stir, obtain component C, for subsequent use;
(5), pH value is adjusted to 7.5-8.5 by component C pH adjusting agent, namely obtains aqueous automobile metal bottom colored paint.
10. the preparation method of aqueous automobile metal bottom colored paint as claimed in claim 9, is characterized in that: the stirring velocity of the stirring at low speed in described step (4) is no more than 100r/min.
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Application publication date: 20160210 |