CN105232372B - A kind of Angelica sinensis rhodiola root smoothing toner and preparation method thereof - Google Patents
A kind of Angelica sinensis rhodiola root smoothing toner and preparation method thereof Download PDFInfo
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- CN105232372B CN105232372B CN201510675132.9A CN201510675132A CN105232372B CN 105232372 B CN105232372 B CN 105232372B CN 201510675132 A CN201510675132 A CN 201510675132A CN 105232372 B CN105232372 B CN 105232372B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/61—Surface treated
- A61K2800/62—Coated
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Abstract
The invention discloses a kind of Angelica sinensis rhodiola root smoothing toner and preparation method thereof, it is related to toner field, in parts by mass, in every 100 parts of smoothing toners, contains following component:1~10 part of glycerine, 0.1~2 part of angelica extract, 0.1~2 part of vitamin E, 0.1~2 part of hydrolyzing lactoalbumin/oat amino acids, 0.1~3 part of beet root extract, 0.1~3 part of extract solution from aloe, 0.1~5 part of rhodiola extract, 0.2~10 part of tomato extracting solution, 0.01~0.5 part of EDTA 2NA, 0.1~1 part of allantoin, surplus are pure water or mineral water.The present invention can prevent that rhodioside from being aoxidized, the skin effect after the corkage of effective guarantee skin care item.
Description
Technical field
The present invention relates to toner field, and in particular to a kind of Angelica sinensis rhodiola root smoothing toner and preparation method thereof
Background technology
Rhodiola root be it is a kind of be grown in rare wild plant of the height above sea level for 1800~2500 meters of severe cold areas, due to its growth
Oxygen content is than relatively low in environment, and is low temperature drying condition, and ultraviolet is stronger, and day and night temperature is larger, and therefore, rhodiola root has
Very strong vitality and special adaptability, containing rhodioside, tyrosol etc., have the multi-efficiencies such as anti anoxia, uvioresistant,
Be respectively provided with and be widely applied in pharmacy and skin care industry, since the growth of rhodiola root is slower, but the demand of people compared with
Greatly, rhodiola root price continuous rise is caused.
When rhodiola root is added in skin care item, usually it is mainly using water as solvent extraction rhodiola extract, active ingredient
Rhodioside, after rhodioside is added to skin care item, main is combined into micro-soluble material with water, after corkage in air is subject to oxygen
Under being acted on illumination, rotten, active ingredient loss, skin effect variation are oxidized easily.
The content of the invention
For defect existing in the prior art, it is an object of the invention to provide a kind of Angelica sinensis rhodiola root smoothing toner and its
Preparation method, can prevent that rhodioside from being aoxidized, the skin effect after the corkage of effective guarantee skin care item.
To achieve the above objectives, the present invention adopts the technical scheme that:A kind of Angelica sinensis rhodiola root smoothing toner, by mass parts
Count, in every 100 parts of smoothing toners, contain following component:
Based on the above technical solutions, the smoothing toner further includes 0.1~4 part of honeysuckle extracting solution.
Based on the above technical solutions, the tomato extracting solution is coated in microcapsules, and the cyst wall of the microcapsules is adopted
It is made of chitosan or pearl powder, which is slow-release type microcapsule.
Based on the above technical solutions, the mass ratio of the rhodiola extract and tomato extracting solution is 1:2.
Based on the above technical solutions, the smoothing toner further includes 0.1~0.5 portion of preservative.
Compared with prior art, the advantage of the invention is that:
(1) the Angelica sinensis rhodiola root smoothing toner in the present invention, including tomato extracting solution, rhodiola extract and Angelica sinensis extraction
Liquid, containing components such as vitamin C, carrotene, vitamin B, glutathione in tomato extracting solution, vitamin C has preferable anti-
Oxidation, can effectively avoid the oxidation deterioration of rhodioside, the skin effect after the corkage of effective guarantee skin care item.Angelica sinensis energy
Facial blood circulation is enough nursed one's health, promotes absorption of the skin to active ingredients such as rhodioside, vitamin Cs, improves the profit of smoothing toner
Use efficiency.
(2) the Angelica sinensis rhodiola root smoothing toner in the present invention, including honeysuckle extracting solution, contains reseda in honeysuckle extracting solution
The components such as the double galactosides of element, honeysuckle element, isochlorogenic acid, caffeic acid, cyanidenon -7-O-, wherein, cyanidenon is in smoothing toner
In content be more than 0.001%, can effectively suppress the content of bacterium in smoothing toner, avoid in smoothing toner caused by bacterial multiplication
Active ingredient is decomposed, meanwhile, Luteolin can also clear up the bacterium of skin surface, alleviate scytitis.
(3) the Angelica sinensis rhodiola root smoothing toner in the present invention, tomato extract are coated in microcapsules, the cyst wall of the microcapsules
It is made of chitosan or pearl powder, which is slow-release type microcapsule, in use, microcapsules gradually release kind
Eggplant extracting solution, can avoid vitamin C from quickly being aoxidized, and can have the function that sustainable protection rhodioside, can effectively prolong
The shelf-life of long rhodioside.
Embodiment
The present invention is described in further detail with reference to embodiments.
The embodiment of the present invention provides a kind of Angelica sinensis rhodiola root smoothing toner, in parts by mass, in every 100 parts of smoothing toners, contains
Following component:
Containing in the embodiment of the present invention, in Angelica sinensis rhodiola root smoothing toner includes 0.1~4 part of honeysuckle extracting solution;And rhodiola root carries
The mass ratio for taking liquid and tomato extracting solution is 1:2.
Contain cyanidenon, honeysuckle element, isochlorogenic acid, caffeic acid, the double galactolipins of cyanidenon -7-O- in honeysuckle extracting solution
The components such as glucoside, wherein, content of the cyanidenon in smoothing toner is more than 0.001%, can effectively suppress bacterium in smoothing toner
Content, avoids in smoothing toner that active ingredient is decomposed caused by bacterial multiplication, meanwhile, Luteolin can also clear up skin surface
Bacterium, alleviate scytitis.
Containing the component such as vitamin C, carrotene, vitamin B, glutathione in tomato extracting solution, vitamin C have compared with
Good antioxidation, can effectively avoid the oxidation deterioration of rhodioside, and glutathione can effectively suppress black in skin
The generation of element, there is preferable whitening function.And the tomato extract is coated in microcapsules, the cyst wall of the microcapsules uses shell
Glycan or pearl powder are made, which is slow-release type microcapsule, and in use, microcapsules gradually discharge tomato extraction
Liquid, can avoid vitamin C from quickly being aoxidized, and can have the function that sustainable protection rhodioside, can effectively extend red scape
The shelf-life of its glycosides.
Angelica sinensis can nurse one's health facial blood circulation, promote absorption of the skin to active ingredients such as rhodioside, vitamin Cs,
Improve the utilization ratio of smoothing toner.
The present invention also provides a kind of preparation method of Angelica sinensis rhodiola root smoothing toner, it is characterised in that comprises the following steps:
S1:Pure water is added in reaction kettle, then successively by 0.01~0.5 part of EDTA-2NA, 1~10 part of glycerine and 0.1
~2 parts of angelica extracts add reaction kettles, under conditions of low whipping speed is 800~1000 turns/min, by speed for 3~5 DEG C/
The speed of min is warming up to 70~75 DEG C, and 55~63 DEG C are cooled to after 10~20min of insulated and stirred, and reaction kettle is evacuated to very
Reciprocal of duty cycle is -0.04~-0.06Mpa, in confined conditions, 0.1~2 part of vitamin E and 0.1~2 part of water is pumped into reaction kettle
Solve lactalbumin/oat amino acids.
S2:Temperature of reaction kettle is decreased below 45 DEG C, in confined conditions, 0.1~3 portion of beet is pumped into reaction kettle
Root extract, 0.1~3 part of extract solution from aloe, 0.1~5 part of rhodiola extract, 0.2~10 part of tomato extracting solution, 0.1~4 part
Honeysuckle extracting solution, under conditions of reaction kettle vacuum is -0.06~-0.08Mpa, after 20~40min of insulated and stirred, is filtered
To rhodiola root smoothing toner.
In the following, by 5 embodiments, the present invention is described in detail.
Embodiment 1
Pure water is added in reaction kettle, then successively by 0.01 part of EDTA-2NA, 1 part of glycerine and 0.1 part of angelica extract
Reaction kettle is added, under conditions of low whipping speed is 1000 turns/min, 75 DEG C is warming up to by the speed that speed is 5 DEG C/min, protects
55 DEG C are cooled to after temperature stirring 20min, it is -0.04Mpa that reaction kettle is evacuated to vacuum, in confined conditions, to reaction
2 parts of vitamin Es and 2 parts of hydrolyzing lactoalbumins/oat amino acids are pumped into kettle.
Temperature of reaction kettle is reduced to 40 DEG C, in confined conditions, 3 parts of beet root extracts, 0.1 are pumped into reaction kettle
Part extract solution from aloe, 5 parts of rhodiola extracts, 10 parts of tomato extracting solutions, 0.1 part of honeysuckle extracting solution, reaction kettle vacuum for-
Under conditions of 0.08Mpa, after insulated and stirred 30min, rhodiola root smoothing toner is obtained by filtration.
Embodiment 2
Pure water is added in reaction kettle, is then successively added 0.5 part of EDTA-2NA, 10 parts of glycerine and 2 parts of angelica extracts
Enter reaction kettle, under conditions of low whipping speed is 800 turns/min, be warming up to 70 DEG C by the speed that speed is 4 DEG C/min, insulation is stirred
60 DEG C are cooled to after mixing 15min, it is -0.06Mpa that reaction kettle is evacuated to vacuum, in confined conditions, into reaction kettle
It is pumped into 0.1 part of vitamin E and 0.1 part of hydrolyzing lactoalbumin/oat amino acids.
Temperature of reaction kettle is reduced to 38 DEG C, in confined conditions, 0.1 part of beet root extract, 3 are pumped into reaction kettle
Part extract solution from aloe, 0.1 part of rhodiola extract, 0.2 part of tomato extracting solution, 4 parts of honeysuckle extracting solutions, in reaction kettle vacuum
For under conditions of -0.06Mpa, after insulated and stirred 40min, rhodiola root smoothing toner is obtained by filtration.
Embodiment 3
Pure water is added in reaction kettle, is then successively added 0.01 part of EDTA-2NA, 3 parts of glycerine and 2 parts of angelica extracts
Enter reaction kettle, under conditions of low whipping speed is 900 turns/min, be warming up to 73 DEG C by the speed that speed is 3 DEG C/min, insulation is stirred
60 DEG C are cooled to after mixing 13min, it is -0.05Mpa that reaction kettle is evacuated to vacuum, in confined conditions, into reaction kettle
It is pumped into 1 part of vitamin E and 1 part of hydrolyzing lactoalbumin/oat amino acids.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, into reaction kettle be pumped into 1 part of beet root extract, 2 parts
Extract solution from aloe, 5 parts of rhodiola extracts, 10 parts of tomato extracting solutions, 3 parts of honeysuckle extracting solutions, reaction kettle vacuum for-
Under conditions of 0.07Mpa, after insulated and stirred 30min, rhodiola root smoothing toner is obtained by filtration.
The present embodiment is optimal proportion embodiment, and the smoothing toner obtained using this embodiment, pH value 6.3, after corkage, is pressed
According to uncapping twice daily, the frequency that the time is 2min of uncapping every time, measures the content, ascorbic of rhodioside in smoothing toner
Content and total plate count, obtain, 1 to July after uncapping through measurement, the content of rhodioside and ascorbic content in smoothing toner
It is held essentially constant, total plate count is not exceeded.
Embodiment 4
Pure water is added in reaction kettle, is then successively added 0.01 part of EDTA-2NA, 3 parts of glycerine and 2 parts of angelica extracts
Enter reaction kettle, under conditions of low whipping speed is 900 turns/min, be warming up to 73 DEG C by the speed that speed is 3 DEG C/min, insulation is stirred
60 DEG C are cooled to after mixing 13min, it is -0.05Mpa that reaction kettle is evacuated to vacuum, in confined conditions, into reaction kettle
It is pumped into 1 part of vitamin E and 1 part of hydrolyzing lactoalbumin/oat amino acids.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, into reaction kettle be pumped into 1 part of beet root extract, 2 parts
Extract solution from aloe, 5 parts of rhodiola extracts, 10 parts of tomato extracting solutions, under conditions of reaction kettle vacuum is -0.07Mpa, are protected
After temperature stirring 30min, rhodiola root smoothing toner is obtained by filtration.
In the present embodiment in addition to no addition honeysuckle extract, remaining is same as Example 3, after corkage, according to daily
Uncap twice, the frequency that the time is 2min of uncapping every time, measure the content of rhodioside in smoothing toner, ascorbic content and
Total plate count, obtains, 1 to March after uncapping through measurement, and the content of rhodioside and ascorbic content are below in smoothing toner
After embodiment 3,3 months, the total plate count in smoothing toner is exceeded, and the content of rhodioside and ascorbic content drastically drop
It is low.
According to said determination result:Addition honeysuckle extract can suppress the bacterium in smoothing toner, effectively extend soft
The shelf-life of skin water, prevents the rhodioside in smoothing toner and vitamin C to be lost in.
Embodiment 5
Pure water is added in reaction kettle, is then successively added 0.01 part of EDTA-2NA, 3 parts of glycerine and 2 parts of angelica extracts
Enter reaction kettle, under conditions of low whipping speed is 900 turns/min, be warming up to 73 DEG C by the speed that speed is 3 DEG C/min, insulation is stirred
60 DEG C are cooled to after mixing 13min, it is -0.05Mpa that reaction kettle is evacuated to vacuum, in confined conditions, into reaction kettle
It is pumped into 1 part of vitamin E and 1 part of hydrolyzing lactoalbumin/oat amino acids.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, into reaction kettle be pumped into 1 part of beet root extract, 2 parts
Extract solution from aloe, 5 parts of rhodiola extracts, 5 parts of tomato extracting solutions, 3 parts of honeysuckle extracting solutions, reaction kettle vacuum for-
Under conditions of 0.07Mpa, after insulated and stirred 30min, rhodiola root smoothing toner is obtained by filtration.
For the present embodiment in addition to tomato extracting solution is different from embodiment 3, remaining is same as Example 3, the present embodiment it is soft
After the corkage of skin water, according to uncapping twice daily, the frequency that the time is 2min of uncapping every time, rhodioside contains in measure smoothing toner
Amount, ascorbic content and total plate count, obtain, 1 to July after uncapping through measurement, and ascorbic content is less than in embodiment 3
Ascorbic content, and the content of rhodioside illustrates that tomato extracting solution can effectively prevent rhodiola root also below embodiment 3
Glycosides is aoxidized.
Embodiment 6
Pure water is added in reaction kettle, is then successively added 0.01 part of EDTA-2NA, 3 parts of glycerine and 2 parts of angelica extracts
Enter reaction kettle, under conditions of low whipping speed is 900 turns/min, be warming up to 73 DEG C by the speed that speed is 3 DEG C/min, insulation is stirred
60 DEG C are cooled to after mixing 13min, it is -0.05Mpa that reaction kettle is evacuated to vacuum, in confined conditions, into reaction kettle
It is pumped into 1 part of vitamin E and 1 part of hydrolyzing lactoalbumin/oat amino acids.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, into reaction kettle be pumped into 1 part of beet root extract, 2 parts
Extract solution from aloe, 5 parts of rhodiola extracts, 1 part of vitamin C (suitable with ascorbic content in 10 parts of tomato extracting solutions), 3
Part honeysuckle extracting solution, under conditions of reaction kettle vacuum is -0.07Mpa, after insulated and stirred 30min, is obtained by filtration rhodiola root
Smoothing toner.
In addition to tomato extracting solution is replaced as vitamin C, remaining is same as Example 3 for this implementation, according to uncapping daily
Twice, uncap every time the time be 2min frequency, measure smoothing toner in rhodioside content, ascorbic content and bacterium colony
Sum, obtains, after uncapping 2 months, without vitamin C in smoothing toner, and the content of rhodioside is substantially reduced through measurement.Illustrate this hair
It is bright that tomato extracting solution is coated in microcapsules, it is sustained, the utilization rate of tomato extracting solution can be effectively improved.
The present invention is not limited to the above-described embodiments, for those skilled in the art, is not departing from
On the premise of the principle of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as the protection of the present invention
Within the scope of.The content not being described in detail in this specification belongs to the prior art known to professional and technical personnel in the field.
Claims (5)
- A kind of 1. Angelica sinensis rhodiola root smoothing toner, it is characterised in that:In parts by mass, in every 100 parts of smoothing toners, containing below into Point:Surplus is pure water or mineral water.
- A kind of 2. Angelica sinensis rhodiola root smoothing toner as claimed in claim 1, it is characterised in that:The smoothing toner further includes 0.1~4 Part honeysuckle extracting solution.
- A kind of 3. Angelica sinensis rhodiola root smoothing toner as claimed in claim 1, it is characterised in that:The tomato extracting solution is coated on micro- In capsule, the cyst wall of the microcapsules is made of chitosan or pearl powder, which is slow-release type microcapsule.
- A kind of 4. Angelica sinensis rhodiola root smoothing toner as claimed in claim 1, it is characterised in that:The rhodiola extract and tomato The mass ratio of extracting solution is 1:2.
- A kind of 5. Angelica sinensis rhodiola root smoothing toner as claimed in claim 1, it is characterised in that:The smoothing toner further includes 0.1~ 0.5 portion of preservative.
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