CN105232372A - Angelica sinensis and rhodiola rosea smoothing toner and preparation method thereof - Google Patents
Angelica sinensis and rhodiola rosea smoothing toner and preparation method thereof Download PDFInfo
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- CN105232372A CN105232372A CN201510675132.9A CN201510675132A CN105232372A CN 105232372 A CN105232372 A CN 105232372A CN 201510675132 A CN201510675132 A CN 201510675132A CN 105232372 A CN105232372 A CN 105232372A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 241000382455 Angelica sinensis Species 0.000 title abstract 4
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- 235000003713 Rhodiola rosea Nutrition 0.000 title abstract 4
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- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 18
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- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 9
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- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 4
- 239000011707 mineral Substances 0.000 claims abstract description 4
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- 101100381997 Danio rerio tbc1d32 gene Proteins 0.000 claims description 9
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- 101100381999 Mus musculus Tbc1d32 gene Proteins 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
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- 238000010792 warming Methods 0.000 claims description 9
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- 239000009188 angelicae sinensis extract Substances 0.000 claims description 4
- 208000031513 cyst Diseases 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 230000002421 anti-septic effect Effects 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 230000003647 oxidation Effects 0.000 abstract description 3
- 238000007254 oxidation reaction Methods 0.000 abstract description 3
- 235000007688 Lycopersicon esculentum Nutrition 0.000 abstract 1
- ILRCGYURZSFMEG-UHFFFAOYSA-N Salidroside Natural products OC1C(O)C(O)C(CO)OC1OCCC1=CC=C(O)C=C1 ILRCGYURZSFMEG-UHFFFAOYSA-N 0.000 abstract 1
- 240000003768 Solanum lycopersicum Species 0.000 abstract 1
- 108010046377 Whey Proteins Proteins 0.000 abstract 1
- 102000007544 Whey Proteins Human genes 0.000 abstract 1
- 239000006210 lotion Substances 0.000 abstract 1
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- ILRCGYURZSFMEG-RQICVUQASA-N salidroside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)OC1OCCC1=CC=C(O)C=C1 ILRCGYURZSFMEG-RQICVUQASA-N 0.000 abstract 1
- 235000021119 whey protein Nutrition 0.000 abstract 1
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 24
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 12
- 229930003268 Vitamin C Natural products 0.000 description 12
- 235000019154 vitamin C Nutrition 0.000 description 12
- 239000011718 vitamin C Substances 0.000 description 12
- 235000001014 amino acid Nutrition 0.000 description 8
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 6
- IQPNAANSBPBGFQ-UHFFFAOYSA-N luteolin Chemical compound C=1C(O)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(O)C(O)=C1 IQPNAANSBPBGFQ-UHFFFAOYSA-N 0.000 description 6
- LRDGATPGVJTWLJ-UHFFFAOYSA-N luteolin Natural products OC1=CC(O)=CC(C=2OC3=CC(O)=CC(O)=C3C(=O)C=2)=C1 LRDGATPGVJTWLJ-UHFFFAOYSA-N 0.000 description 6
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- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 5
- 230000003203 everyday effect Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- QAIPRVGONGVQAS-DUXPYHPUSA-N trans-caffeic acid Chemical compound OC(=O)\C=C\C1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-DUXPYHPUSA-N 0.000 description 4
- 235000001892 vitamin D2 Nutrition 0.000 description 4
- 230000002500 effect on skin Effects 0.000 description 3
- RWSXRVCMGQZWBV-WDSKDSINSA-N glutathione Chemical compound OC(=O)[C@@H](N)CCC(=O)N[C@@H](CS)C(=O)NCC(O)=O RWSXRVCMGQZWBV-WDSKDSINSA-N 0.000 description 3
- 235000003969 glutathione Nutrition 0.000 description 3
- 229960003180 glutathione Drugs 0.000 description 3
- CWVRJTMFETXNAD-BMNNCGMMSA-N (1s,3r,4s,5r)-3-[(e)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy-1,4,5-trihydroxycyclohexane-1-carboxylic acid Chemical compound O[C@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-BMNNCGMMSA-N 0.000 description 2
- ACEAELOMUCBPJP-UHFFFAOYSA-N (E)-3,4,5-trihydroxycinnamic acid Natural products OC(=O)C=CC1=CC(O)=C(O)C(O)=C1 ACEAELOMUCBPJP-UHFFFAOYSA-N 0.000 description 2
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 2
- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 229930003270 Vitamin B Natural products 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 230000017531 blood circulation Effects 0.000 description 2
- 229940074360 caffeic acid Drugs 0.000 description 2
- 235000004883 caffeic acid Nutrition 0.000 description 2
- 150000001746 carotenes Chemical class 0.000 description 2
- 235000005473 carotenes Nutrition 0.000 description 2
- QAIPRVGONGVQAS-UHFFFAOYSA-N cis-caffeic acid Natural products OC(=O)C=CC1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-UHFFFAOYSA-N 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 230000001815 facial effect Effects 0.000 description 2
- 150000008195 galaktosides Chemical class 0.000 description 2
- KRZBCHWVBQOTNZ-DLDRDHNVSA-N isochlorogenic acid Natural products O[C@@H]1[C@H](C[C@@](O)(C[C@H]1OC(=O)C=Cc2ccc(O)c(O)c2)C(=O)O)OC(=O)C=Cc3ccc(O)c(O)c3 KRZBCHWVBQOTNZ-DLDRDHNVSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- -1 rhodioside Substances 0.000 description 2
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 2
- 235000019156 vitamin B Nutrition 0.000 description 2
- 239000011720 vitamin B Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 206010021143 Hypoxia Diseases 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
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- 239000002195 soluble material Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/61—Surface treated
- A61K2800/62—Coated
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses angelica sinensis and rhodiola rosea smoothing toner and a preparation method thereof, relating to the field of lotions. Each 100 parts of the smoothing toner comprises the following components in parts by weight: 1-10 parts of glycerinum, 0.1-2 parts of angelica sinensis extract, 0.1-2 parts of Vitamin E, 0.1-2 parts of whey protein hydrolysate/oat amino acid, 0.1-3 parts of beet root extract, 0.1-3 parts of aloe extracting solution, 0.1-5 parts of rhodiola rosea extracting solution, 0.2-10 parts of tomato extracting solution, 0.01-0.5 part of EDTA-2NA, 0.1-1 part ofallantoin, and the balance of pure water or mineral water. According to the angelica sinensis and rhodiola rosea smoothing toner, salidroside is prevented from oxidation, and the skin care effect of the skin care product after bottle opening can be effectively guaranteed.
Description
Technical field
The present invention relates to astringent field, be specifically related to a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner and preparation method thereof
Background technology
Radix Rhodiolae is a kind of growth is the rare wild plant of 1800 ~ 2500 meters of severe cold areas at height above sea level, because in its growing environment, oxygen content is lower, and be cold drying condition, ultraviolet is stronger, day and night temperature is larger, therefore, Radix Rhodiolae has very strong vitality and special adaptability, containing rhodioside, butyl alcohol etc., there is the multi-efficiency such as anti-hypoxia, uvioresistant, all have a wide range of applications in pharmacy and skin care industry, because the growth fraction of Radix Rhodiolae is slower, but the demand of people is comparatively large, causes Radix Rhodiolae price continuous rise.
When adding Radix Rhodiolae in skin care item, usually using water as solvent extraction Radix Rhodiolae extracting solution, active component is mainly rhodioside, after rhodioside adds skin care item to, main is combined into micro-soluble material with water, being subject in air under oxygen and illumination effect after uncork, easy to be oxidized rotten, effective ingredient runs off, and skin effect is deteriorated.
Summary of the invention
For the defect existed in prior art, the object of the present invention is to provide a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner and preparation method thereof, rhodioside can be prevented oxidized, the skin effect after the uncork of effective guarantee skin care item.
For reaching above object, the technical scheme that the present invention takes is: a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner, by mass parts, in every 100 parts of toner/smoothing toners, containing following composition:
Surplus is pure water or mineral water.
On the basis of technique scheme, described toner/smoothing toner also comprise 0.1 ~ 4 part Radix Ophiopogonis extracting solution.
On the basis of technique scheme, described Fructus Lycopersici esculenti extracting solution is coated in microcapsule, and the cyst wall of this microcapsule adopts chitosan or Margarita powder to make, and this microcapsule is slow-release type microcapsule.
On the basis of technique scheme, the mass ratio of described Radix Rhodiolae extracting solution and Fructus Lycopersici esculenti extracting solution is 1:2.
On the basis of technique scheme, described toner/smoothing toner also comprises 0.1 ~ 0.5 portion of antiseptic.
A preparation method for Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner according to any one of claim 1 to 5, comprises the following steps:
S1: pure water is added in reactor, then successively 0.01 ~ 0.5 part of EDTA-2NA, 1 ~ 10 part of glycerol and 0.1 ~ 2 part of Radix Angelicae Sinensis extract are added reactor, low whipping speed is under the condition of 800 ~ 1000 turns/min, the speed being 3 ~ 5 DEG C/min by speed is warming up to 70 ~ 75 DEG C, 55 ~ 63 DEG C are cooled to after insulated and stirred 10 ~ 20min, reactor being evacuated to vacuum is-0.04 ~-0.06Mpa, in confined conditions, to 0.1 ~ 2 part of vitamin E of suction in reactor and 0.1 ~ 2 part of lact albumin hydrolysate/Herba bromi japonici amino acids;
S2: temperature of reaction kettle is reduced to lower than 45 DEG C, in confined conditions, suction 0.1 ~ 3 part of beet root extract, 0.1 ~ 3 part of Aloe extraction solution, 0.1 ~ 5 part of Radix Rhodiolae extracting solution, 0.2 ~ 10 part of Fructus Lycopersici esculenti extracting solution in reactor, be under the condition of-0.06 ~-0.08Mpa in reactor vacuum, after insulated and stirred 20 ~ 40min, filter and obtain Radix Rhodiolae toner/smoothing toner.
Compared with prior art, the invention has the advantages that:
(1) the Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner in the present invention, comprise Fructus Lycopersici esculenti extracting solution, Radix Rhodiolae extracting solution and Radix Angelicae Sinensis extracting solution, containing compositions such as vitamin C, carotene, vitamin B, glutathion in Fructus Lycopersici esculenti extracting solution, vitamin C has good antioxidation, effectively can avoid the oxidation deterioration of rhodioside, the skin effect after the uncork of effective guarantee skin care item.Radix Angelicae Sinensis can nurse one's health facial blood circulation, promotes that skin is to the absorption of the effective ingredient such as rhodioside, vitamin C, improves the utilization ratio of toner/smoothing toner.
(2) the Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner in the present invention, comprise Radix Ophiopogonis extracting solution, in Radix Ophiopogonis extracting solution containing luteolin, Radix Ophiopogonis element, isochlorogenic acid, caffeic acid, the composition such as luteolin-7-O-pair galactosides, wherein, the content of luteolin in toner/smoothing toner is greater than 0.001%, effectively can suppress the content of antibacterial in toner/smoothing toner, the effective ingredient avoiding bacterial multiplication in toner/smoothing toner to cause is decomposed, meanwhile, luteolin can also clear up the antibacterial of skin surface, alleviates scytitis.
(3) the Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner in the present invention; Fructus Lycopersici esculenti extract is coated in microcapsule; the cyst wall of this microcapsule adopts chitosan or Margarita powder to make; this microcapsule is slow-release type microcapsule; in use, microcapsule discharges Fructus Lycopersici esculenti extracting solution gradually, and vitamin C can be avoided oxidized fast; the effect of sustainable protection rhodioside can be reached, effectively can extend the shelf-life of rhodioside.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
The embodiment of the present invention provides a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner, by mass parts, in every 100 parts of toner/smoothing toners, containing following composition:
Surplus is pure water or mineral water.
In the embodiment of the present invention, in Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner containing comprise 0.1 ~ 4 part Radix Ophiopogonis extracting solution; And the mass ratio of Radix Rhodiolae extracting solution and Fructus Lycopersici esculenti extracting solution is 1:2.
In Radix Ophiopogonis extracting solution containing luteolin, Radix Ophiopogonis element, isochlorogenic acid, caffeic acid, the composition such as luteolin-7-O-pair galactosides, wherein, the content of luteolin in toner/smoothing toner is greater than 0.001%, effectively can suppress the content of antibacterial in toner/smoothing toner, the effective ingredient avoiding bacterial multiplication in toner/smoothing toner to cause is decomposed, meanwhile, luteolin can also clear up the antibacterial of skin surface, alleviates scytitis.
Containing compositions such as vitamin C, carotene, vitamin B, glutathion in Fructus Lycopersici esculenti extracting solution, vitamin C has good antioxidation, effectively can avoid the oxidation deterioration of rhodioside, glutathion effectively can suppress melanic generation in skin, has good whitening function.And described Fructus Lycopersici esculenti extract is coated in microcapsule; the cyst wall of this microcapsule adopts chitosan or Margarita powder to make; this microcapsule is slow-release type microcapsule; in use; microcapsule discharges Fructus Lycopersici esculenti extracting solution gradually; vitamin C can be avoided oxidized fast, the effect of sustainable protection rhodioside can be reached, effectively can extend the shelf-life of rhodioside.
Radix Angelicae Sinensis can nurse one's health facial blood circulation, promotes that skin is to the absorption of the effective ingredient such as rhodioside, vitamin C, improves the utilization ratio of toner/smoothing toner.
The present invention also provides a kind of preparation method of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner, it is characterized in that, comprises the following steps:
S1: pure water is added in reactor, then successively 0.01 ~ 0.5 part of EDTA-2NA, 1 ~ 10 part of glycerol and 0.1 ~ 2 part of Radix Angelicae Sinensis extract are added reactor, low whipping speed is under the condition of 800 ~ 1000 turns/min, the speed being 3 ~ 5 DEG C/min by speed is warming up to 70 ~ 75 DEG C, 55 ~ 63 DEG C are cooled to after insulated and stirred 10 ~ 20min, reactor being evacuated to vacuum is-0.04 ~-0.06Mpa, in confined conditions, to 0.1 ~ 2 part of vitamin E of suction in reactor and 0.1 ~ 2 part of lact albumin hydrolysate/Herba bromi japonici amino acids.
S2: temperature of reaction kettle is reduced to lower than 45 DEG C, in confined conditions, in reactor suction 0.1 ~ 3 part of beet root extract, 0.1 ~ 3 part of Aloe extraction solution, 0.1 ~ 5 part of Radix Rhodiolae extracting solution, 0.2 ~ 10 part of Fructus Lycopersici esculenti extracting solution, 0.1 ~ 4 part Radix Ophiopogonis extracting solution, be under the condition of-0.06 ~-0.08Mpa in reactor vacuum, after insulated and stirred 20 ~ 40min, filter and obtain Radix Rhodiolae toner/smoothing toner.
Below, by 5 embodiments, the present invention is described in detail.
Embodiment 1
Pure water is added in reactor, then successively 0.01 part of EDTA-2NA, 1 part of glycerol and 0.1 part of Radix Angelicae Sinensis extract are added reactor, low whipping speed is under the condition of 1000 turns/min, the speed being 5 DEG C/min by speed is warming up to 75 DEG C, 55 DEG C are cooled to after insulated and stirred 20min, reactor is evacuated to vacuum for-0.04Mpa, in confined conditions, suction 2 parts of vitamin Es and 2 parts of lact albumin hydrolysate/Herba bromi japonici amino acidses in reactor.
Temperature of reaction kettle is reduced to 40 DEG C, in confined conditions, in reactor suction 3 parts of beet root extract, 0.1 part of Aloe extraction solution, 5 parts of Radix Rhodiolae extracting solution, 10 parts of Fructus Lycopersici esculenti extracting solution, 0.1 part Radix Ophiopogonis extracting solution, be under the condition of-0.08Mpa in reactor vacuum, after insulated and stirred 30min, filter and obtain Radix Rhodiolae toner/smoothing toner.
Embodiment 2
Pure water is added in reactor, then successively 0.5 part of EDTA-2NA, 10 parts of glycerol and 2 parts of Radix Angelicae Sinensis extracts are added reactor, low whipping speed is under the condition of 800 turns/min, the speed being 4 DEG C/min by speed is warming up to 70 DEG C, 60 DEG C are cooled to after insulated and stirred 15min, reactor is evacuated to vacuum for-0.06Mpa, in confined conditions, suction 0.1 part of vitamin E and 0.1 part of lact albumin hydrolysate/Herba bromi japonici amino acids in reactor.
Temperature of reaction kettle is reduced to 38 DEG C, in confined conditions, in reactor suction 0.1 part of beet root extract, 3 parts of Aloe extraction solution, 0.1 part of Radix Rhodiolae extracting solution, 0.2 part of Fructus Lycopersici esculenti extracting solution, 4 parts Radix Ophiopogonis extracting solution, be under the condition of-0.06Mpa in reactor vacuum, after insulated and stirred 40min, filter and obtain Radix Rhodiolae toner/smoothing toner.
Embodiment 3
Pure water is added in reactor, then successively 0.01 part of EDTA-2NA, 3 parts of glycerol and 2 parts of Radix Angelicae Sinensis extracts are added reactor, low whipping speed is under the condition of 900 turns/min, the speed being 3 DEG C/min by speed is warming up to 73 DEG C, 60 DEG C are cooled to after insulated and stirred 13min, reactor is evacuated to vacuum for-0.05Mpa, in confined conditions, suction 1 part of vitamin E and 1 part of lact albumin hydrolysate/Herba bromi japonici amino acids in reactor.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, in reactor suction 1 part of beet root extract, 2 parts of Aloe extraction solution, 5 parts of Radix Rhodiolae extracting solution, 10 parts of Fructus Lycopersici esculenti extracting solution, 3 parts Radix Ophiopogonis extracting solution, be under the condition of-0.07Mpa in reactor vacuum, after insulated and stirred 30min, filter and obtain Radix Rhodiolae toner/smoothing toner.
The present embodiment is optimal proportion embodiment, adopt the toner/smoothing toner that this embodiment obtains, pH value is 6.3, after uncork, according to uncapping every day twice, each decap is the frequency of 2min, measuring the content of rhodioside in toner/smoothing toner, ascorbic content and total plate count, obtaining through measuring, 1 to July after uncapping, in toner/smoothing toner, the content of rhodioside and ascorbic content remain unchanged substantially, and total plate count does not exceed standard.
Embodiment 4
Pure water is added in reactor, then successively 0.01 part of EDTA-2NA, 3 parts of glycerol and 2 parts of Radix Angelicae Sinensis extracts are added reactor, low whipping speed is under the condition of 900 turns/min, the speed being 3 DEG C/min by speed is warming up to 73 DEG C, 60 DEG C are cooled to after insulated and stirred 13min, reactor is evacuated to vacuum for-0.05Mpa, in confined conditions, suction 1 part of vitamin E and 1 part of lact albumin hydrolysate/Herba bromi japonici amino acids in reactor.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, suction 1 part of beet root extract, 2 parts of Aloe extraction solution, 5 parts of Radix Rhodiolae extracting solution, 10 parts of Fructus Lycopersici esculenti extracting solution in reactor, be under the condition of-0.07Mpa in reactor vacuum, after insulated and stirred 30min, filter and obtain Radix Rhodiolae toner/smoothing toner.
Except not adding except Radix Ophiopogonis extract in the present embodiment, all the other are all identical with embodiment 3, after uncork, according to uncapping every day twice, each decap is the frequency of 2min, measure the content of rhodioside in toner/smoothing toner, ascorbic content and total plate count, obtain through measuring, 1 to March after uncapping, in toner/smoothing toner, the content of rhodioside and ascorbic content are all lower than embodiment 3, after 3 months, the total plate count in toner/smoothing toner exceeds standard, and the content of rhodioside and ascorbic content sharply reduce.
According to said determination result: interpolation Radix Ophiopogonis extract can suppress the antibacterial in toner/smoothing toner, effectively extends the shelf-life of toner/smoothing toner, the rhodioside in toner/smoothing toner and vitamin C is prevented to run off.
Embodiment 5
Pure water is added in reactor, then successively 0.01 part of EDTA-2NA, 3 parts of glycerol and 2 parts of Radix Angelicae Sinensis extracts are added reactor, low whipping speed is under the condition of 900 turns/min, the speed being 3 DEG C/min by speed is warming up to 73 DEG C, 60 DEG C are cooled to after insulated and stirred 13min, reactor is evacuated to vacuum for-0.05Mpa, in confined conditions, suction 1 part of vitamin E and 1 part of lact albumin hydrolysate/Herba bromi japonici amino acids in reactor.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, in reactor suction 1 part of beet root extract, 2 parts of Aloe extraction solution, 5 parts of Radix Rhodiolae extracting solution, 5 parts of Fructus Lycopersici esculenti extracting solution, 3 parts Radix Ophiopogonis extracting solution, be under the condition of-0.07Mpa in reactor vacuum, after insulated and stirred 30min, filter and obtain Radix Rhodiolae toner/smoothing toner.
The present embodiment is except Fructus Lycopersici esculenti extracting solution is different from embodiment 3, all the other are all identical with embodiment 3, after the toner/smoothing toner uncork of the present embodiment, according to uncapping every day twice, each decap is the frequency of 2min, measure the content of rhodioside in toner/smoothing toner, ascorbic content and total plate count, obtain through measuring, 1 to July after uncapping, ascorbic content is lower than content ascorbic in embodiment 3, and the content of rhodioside is also lower than embodiment 3, illustrate that Fructus Lycopersici esculenti extracting solution can effectively prevent rhodioside oxidized.
Embodiment 6
Pure water is added in reactor, then successively 0.01 part of EDTA-2NA, 3 parts of glycerol and 2 parts of Radix Angelicae Sinensis extracts are added reactor, low whipping speed is under the condition of 900 turns/min, the speed being 3 DEG C/min by speed is warming up to 73 DEG C, 60 DEG C are cooled to after insulated and stirred 13min, reactor is evacuated to vacuum for-0.05Mpa, in confined conditions, suction 1 part of vitamin E and 1 part of lact albumin hydrolysate/Herba bromi japonici amino acids in reactor.
Temperature of reaction kettle is reduced to 35 DEG C, in confined conditions, in reactor suction 1 part of beet root extract, 2 parts of Aloe extraction solution, 5 parts of Radix Rhodiolae extracting solution, 1 part of vitamin C (suitable with ascorbic content in 10 parts of Fructus Lycopersici esculenti extracting solution), 3 parts Radix Ophiopogonis extracting solution, be under the condition of-0.07Mpa in reactor vacuum, after insulated and stirred 30min, filter and obtain Radix Rhodiolae toner/smoothing toner.
This enforcement is except being replaced as except vitamin C by Fructus Lycopersici esculenti extracting solution, all the other are all identical with embodiment 3, according to uncapping every day twice, each decap is the frequency of 2min, measuring the content of rhodioside in toner/smoothing toner, ascorbic content and total plate count, obtaining, after February of uncapping through measuring, without vitamin C in toner/smoothing toner, and the content of rhodioside obviously reduces.Illustrate that Fructus Lycopersici esculenti extracting solution is coated in microcapsule by the present invention, carry out slow release, effectively can improve the utilization rate of Fructus Lycopersici esculenti extracting solution.
The present invention is not limited to above-mentioned embodiment, and for those skilled in the art, under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications are also considered as within protection scope of the present invention.The content be not described in detail in this description belongs to the known prior art of professional and technical personnel in the field.
Claims (6)
1. a Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner, is characterized in that: by mass parts, in every 100 parts of toner/smoothing toners, containing following composition:
Surplus is pure water or mineral water.
2. a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner as claimed in claim 1, is characterized in that: described toner/smoothing toner also comprise 0.1 ~ 4 part Radix Ophiopogonis extracting solution.
3. a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner as claimed in claim 1, is characterized in that: described Fructus Lycopersici esculenti extracting solution is coated in microcapsule, and the cyst wall of this microcapsule adopts chitosan or Margarita powder to make, and this microcapsule is slow-release type microcapsule.
4. a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner as claimed in claim 1, is characterized in that: the mass ratio of described Radix Rhodiolae extracting solution and Fructus Lycopersici esculenti extracting solution is 1:2.
5. a kind of Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner as claimed in claim 1, is characterized in that: described toner/smoothing toner also comprises 0.1 ~ 0.5 portion of antiseptic.
6. a preparation method for the Radix Angelicae Sinensis Radix Rhodiolae toner/smoothing toner according to any one of claim 1 to 5, is characterized in that: comprise the following steps:
S1: pure water is added in reactor, then successively 0.01 ~ 0.5 part of EDTA-2NA, 1 ~ 10 part of glycerol and 0.1 ~ 2 part of Radix Angelicae Sinensis extract are added reactor, low whipping speed is under the condition of 800 ~ 1000 turns/min, the speed being 3 ~ 5 DEG C/min by speed is warming up to 70 ~ 75 DEG C, 55 ~ 63 DEG C are cooled to after insulated and stirred 10 ~ 20min, reactor being evacuated to vacuum is-0.04 ~-0.06Mpa, in confined conditions, to 0.1 ~ 2 part of vitamin E of suction in reactor and 0.1 ~ 2 part of lact albumin hydrolysate/Herba bromi japonici amino acids;
S2: temperature of reaction kettle is reduced to lower than 45 DEG C, in confined conditions, suction 0.1 ~ 3 part of beet root extract, 0.1 ~ 3 part of Aloe extraction solution, 0.1 ~ 5 part of Radix Rhodiolae extracting solution, 0.2 ~ 10 part of Fructus Lycopersici esculenti extracting solution in reactor, be under the condition of-0.06 ~-0.08Mpa in reactor vacuum, after insulated and stirred 20 ~ 40min, filter and obtain Radix Rhodiolae toner/smoothing toner.
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| CN108186476A (en) * | 2018-03-25 | 2018-06-22 | 广州市卓多姿化妆品有限公司 | Facial mask and preparation method thereof is repaired in a kind of efficient skin care |
| CN109528602A (en) * | 2019-01-22 | 2019-03-29 | 广州睿森生物科技有限公司 | A kind of plant fermentation composition, preparation method and its application |
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| CN108186476A (en) * | 2018-03-25 | 2018-06-22 | 广州市卓多姿化妆品有限公司 | Facial mask and preparation method thereof is repaired in a kind of efficient skin care |
| CN109528602A (en) * | 2019-01-22 | 2019-03-29 | 广州睿森生物科技有限公司 | A kind of plant fermentation composition, preparation method and its application |
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