CN103099759B - Extraction of active components from blackberry seeds, hawthorn seeds and pomegranate seeds and preparation of applying mask - Google Patents
Extraction of active components from blackberry seeds, hawthorn seeds and pomegranate seeds and preparation of applying mask Download PDFInfo
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- CN103099759B CN103099759B CN201310061163.6A CN201310061163A CN103099759B CN 103099759 B CN103099759 B CN 103099759B CN 201310061163 A CN201310061163 A CN 201310061163A CN 103099759 B CN103099759 B CN 103099759B
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Abstract
The invention discloses an applying mask of active antioxidant extracts from blackberry seeds, hawthorn seeds, pomegranate seeds and other fruit seeds. According to a formula, the mask comprises the following components: 20%-40% of polyvinylpyrrolidone (PVP), 4%-10% of glycerol, 14%-50% of an extract solution containing blackberry seed powder, hawthorn seed powder and pomegranate seed powder, 10%-60% of pure water, and 3%-10% of a toughening agent. The preparation method consists of: subjecting the raw materials to mixing and heating, stirring them uniformly, conducting cooling and sealing packaging, thus obtaining the mask product. The mask produced by the formula involved in the invention has a soft texture and good touch sense with skin, and can absorb and release a lot of nutritional ingredients to make skin fair, smoother and full of resilience and reduce skin wrinkles. Meanwhile, the applying mask makes use of the high content polyphenol compounds, flavones, anthocyanins, vitamin C and other natural active substances contained in the blackberry seeds, hawthorn seeds, pomegranate seeds and other fruit seeds, and has the efficacy of eliminating active free radicals, preventing aging and resisting oxidation, etc.
Description
Technical field
The invention belongs to Cosmetic Manufacture field, be specifically related to the extraction process of oxidation-resistant active ingredient and the preparation method of smearing mask in a kind of blackberry seed, seed of Fructus Crataegi, Semen Granati.
Background technology
The mankind use facial film with a long history as cosmetic tool, can trace back to ancient Egypt and Chinese Tang Dynasty.The principle of facial film is to adopt the dressing of a thick layer of not same-action and composition to apply in face, and obstruct skin contacts with air.When this one deck dressing tightly be attached on skin time, can be because suppressing the secretion of sebum and antiperspirant evaporation of water but skin temperature rise; Those moisture that cannot evaporate of skin surface can be deposited in epidermal area, and the moisture of epidermal area is full, and it is will smoother tight that skin seems, it is light that microgroove also can become; In addition, temperature and warm meeting make cutin softening, pore expansion; Pore expansion, the sweat mixed with dirt that is deposited in the inside just can be seized the opportunity eliminating, and therefore facial film can more thoroughly clean skin.
In several fruit seeds such as blackberry seed, seed of Fructus Crataegi, Semen Granati, self high-load has multiple polyphenol compound, flavone, anthocyanidin, vitamin C etc. a series ofly to have defying age, removes the natural active matters such as free radical physiologically active, antioxidant content.The inhibitor that can be used as many enzyme systems of polyphenol compound or activator, metal-chelator and free radical scavenger, its dissociation by phenolic hydroxyl group and free radical, by way of producing antioxidation, are the very promising class Natural antioxidant and free radical scavengers in medicine, food, cosmetics; Flavone is a kind of very strong antioxidant, can effectively remove the oxygen-derived free radicals in body, it stops the ability of oxidation is the more than ten times of vitamin E, and can stop degeneration, the aging of cell, also can stop the generation of cancer, it can also suppress oozing out of inflammatory enzyme, can promote healing and the pain relieving of wound; Anthocyanidin is the antidotal supplementary of pure natural, studies have shown that it is that mankind nowadays is found the most effective antioxidant, it can protect human body to avoid the damage of the harmful substances such as free radical, its antioxygenic property exceeds 50 times than vitamin E, it can also be by making skin become smooth and high resilience to the inhibition of elastoser and Collagenase, can prevent that inflammation-inhibiting and allergy, have radiation-resistant effect due to the skin injury that excessively Exposure to Sunlight causes; Vitamin C has antioxidation, can protect other antioxidants, prevents the injury of radical pair human body.It can also make, and dermal melanin is calm to be reduced, thereby reduces black speck and freckle, makes whitening skin.In daily life, blackberry seed, seed of Fructus Crataegi, Semen Granati all belong to garbage, now its active component are extracted, and can realize the recycling of waste resource, and existing economic worth, has again social meaning.
So far, not yet there is antioxidant activity thing in fruit seeds such as extracting blackberry seed, seed of Fructus Crataegi, Semen Granati and prepare the technology of facial film.
Summary of the invention
1, goal of the invention
The object of the invention is to provide a kind of active polyphenoils in several fruit seeds such as blackberry seed, seed of Fructus Crataegi, Semen Granati that extracts, prepare there is nourishing and whitening, the method for the nourishing pack of the function such as anti-aging, antioxidation.
2, technical scheme
For achieving the above object, in its formula, each component is: 20%-40% polyvinylpyrrolidone (PVP), 4%-10% glycerol, several fruit seed powder extracting solution such as 14%-50% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, 10%-50% pure water, 3%-10% flexibilizer, each component sum is 100%.Wherein, extracting solution is for taking charge ratio several fruit seed powder such as (: extractant) blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder as 1: ratio (10-20), accurately taking the concentration that several fruit seed powder such as a blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder join 10-20 times of quality is in 30-100% alcoholic solution, at 15 DEG C-60 DEG C of temperature, extract 0.5h-7h, filter and obtain extracting solution.
In several fruit seeds such as blackberry seed of the present invention, seed of Fructus Crataegi, Semen Granati, preparation method and the step of active antioxidant extract facial film are as follows:
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): 1: ratio (10-20), accurately taking the concentration that several fruit seed powder such as a blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder join 10-20 times of quality is in 30-100% alcoholic solution, at 15 DEG C-60 DEG C of temperature, extract 3.5h-5.5h, filter and obtain extracting solution.
(2) preparation of facial film: accurately weigh 20%-40% polyvinylpyrrolidone (PVP), 4%-10% glycerol, 14%-50% extracting solution, 10%-60% pure water, the micro-heated and stirred of 3%-10% flexibilizer is dissolved polyvinylpyrrolidone (PVP) completely, fully mix rear coolingly, prepare facial film finished product.
3, beneficial effect of the present invention
By the facial film quality softness of formula of the present invention, explained hereafter, good with the applying ointment or plaster property of skin, can absorb and discharge more nutritional labeling, and whitening effect is good, makes skin smooth high resilience, desalination wrinkle of skin.In addition in conjunction with a series of materials such as the polyphenol containing in fruit seed, flavone, anthocyanidin, vitamin Cs, be prepared into there is nourishing and whitening, the nourishing pack of the many integration function such as anti-aging, antioxidation.
Detailed description of the invention
Embodiment 1
Formula: each component is: 20% polyvinylpyrrolidone (PVP), 6% glycerol, several fruit seed powder extracting solution such as 14% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, 57% pure water, 3% flexibilizer.
Preparation process
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): the ratio of 1: 10, accurately taking quality and be several fruit seed powder such as the blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder of 5 weight portions adds in 75% alcoholic solution of 50 weight portions, ultrasound wave assisted extraction 5.5h at 37 DEG C of temperature, filters and obtains extracting solution by sucking filtration mode.
(2) preparation of facial film: the polyvinylpyrrolidone (PVP) that accurately weighs 7 weight portions, the glycerol of 2 weight portions, the pure water of the extracting solution of 5 weight portions and 20 weight portions, the flexibilizer of 1 weight portion, micro-heated and stirred is dissolved polyvinylpyrrolidone (PVP) completely, fully mix rear coolingly, prepare facial film finished product.
Embodiment 2
Formula: each component is: 30% polyvinylpyrrolidone (PVP), 4% glycerol, several fruit seed powder extracting solution such as 47% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, 13% pure water, 6% flexibilizer.
Preparation process
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): the ratio of 1: 15, accurately take 75% alcoholic solution that several fruit seed powder such as the blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder of 5 mass parts add 75 mass parts, under temperature 60 C, ultrasound wave assisted extraction 4.5h, filters and obtains extracting solution by sucking filtration mode.
(2) preparation of facial film: the polyvinylpyrrolidone (PVP) that accurately weighs 22 mass parts, the glycerol of 3 mass parts, the extracting solution of 35 mass parts, the pure water of 10 mass parts, the flexibilizer of 4 mass parts, micro-heated and stirred is dissolved polyvinylpyrrolidone (PVP) completely, fully mixes rear coolingly, prepares facial film finished product.
Embodiment 3
Formula: each component is: 40% polyvinylpyrrolidone (PVP), 10% glycerol, several fruit seed powder extracting solution such as 30% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, 10% pure water, 10% flexibilizer.
Preparation process
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): the ratio of 1: 20, accurately taking several fruit seed powder such as the blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder of 1 mass parts adds in 75% alcoholic solution of 20 mass parts, ultrasound wave assisted extraction 3.5h at 15 DEG C of temperature, filters and obtains extracting solution by sucking filtration mode.
(2) preparation of facial film: the polyvinylpyrrolidone (PVP) that accurately weighs 4 mass parts, the glycerol of 1 mass parts, the extracting solution of 3 mass parts, the pure water of 1 mass parts, the flexibilizer of 1 mass parts, micro-heated and stirred is dissolved polyvinylpyrrolidone (PVP) completely, fully mixes rear coolingly, prepares facial film finished product.
Claims (5)
1. a preparation technology for the facial film extracting based on active matter in blackberry seed, seed of Fructus Crataegi and Semen Granati, is characterized in that carrying out according to the following steps:
(1) blackberry seed, seed of Fructus Crataegi and Semen Granati active matter extract: with charge ratio, blackberry seed powder, seed of Fructus Crataegi powder and Semen Granati powder: extractant is the mass ratio of 1:10-20, accurately taking the concentration that a blackberry seed powder, seed of Fructus Crataegi powder and Semen Granati powder join 10-20 times of quality is in 30-100% alcoholic solution, extract at a certain temperature, filter and obtain extracting solution;
(2) preparation of facial film: accurately weigh 20%-40% polyvinylpyrrolidone, 4%-10% glycerol, extracting solution described in 14%-50% step (1), 10%-60% pure water, 3%-10% flexibilizer, the mass percent sum of each component is 100%, micro-heated and stirred is dissolved polyvinylpyrrolidone completely, fully mix rear coolingly, prepare facial film finished product.
2. the preparation technology of the facial film extracting based on active matter in blackberry seed, seed of Fructus Crataegi and Semen Granati according to claim 1, is characterized in that, blackberry seed, seed of Fructus Crataegi and Semen Granati are pulverized for after drying.
3. the preparation technology of the facial film extracting based on active matter in blackberry seed, seed of Fructus Crataegi and Semen Granati according to claim 1, is characterized in that, in blackberry seed powder, seed of Fructus Crataegi powder and Semen Granati powder, active matter extraction temperature is 15-60 DEG C.
4. the preparation technology of the facial film extracting based on active matter in blackberry seed, seed of Fructus Crataegi and Semen Granati according to claim 1, is characterized in that, in blackberry seed powder, seed of Fructus Crataegi powder and Semen Granati powder, active matter extraction time is 0.5h-7h.
5. the preparation technology of the facial film extracting based on active matter in blackberry seed, seed of Fructus Crataegi and Semen Granati according to claim 4, is characterized in that, the facial film preparation temperature that adopts is 10-60 DEG C.
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| CN201310061163.6A CN103099759B (en) | 2013-02-27 | 2013-02-27 | Extraction of active components from blackberry seeds, hawthorn seeds and pomegranate seeds and preparation of applying mask |
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| CN201310061163.6A CN103099759B (en) | 2013-02-27 | 2013-02-27 | Extraction of active components from blackberry seeds, hawthorn seeds and pomegranate seeds and preparation of applying mask |
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| CN103099759B true CN103099759B (en) | 2014-07-09 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104758198B (en) * | 2014-01-08 | 2017-11-21 | 南京美纯生物科技有限公司 | A kind of strong anti-oxidation skin care item containing blackberry extract and its production and use |
| CN107334693A (en) * | 2016-04-29 | 2017-11-10 | 伽蓝（集团）股份有限公司 | Compound seed extract and preparation method thereof |
| CN106265303A (en) * | 2016-08-24 | 2017-01-04 | 刘艺鹏 | Semen Granati cosmetics and skincare product |
| CN106983691B (en) * | 2017-05-18 | 2020-03-27 | 广州娇漾生物科技有限公司 | Lotus polyphenol-containing anti-oxidation pore-shrinking sleeping mask and preparation method thereof |
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| CN1633981A (en) * | 2004-11-24 | 2005-07-06 | 黄天军 | Ion water beauty product and its face pack |
| CN102370591A (en) * | 2010-08-24 | 2012-03-14 | 上海博天尼化妆品有限公司 | Pomegranate rind extract method and application of pomegranate rind extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO1997039632A1 (en) * | 1996-04-22 | 1997-10-30 | Henkel Corporation | Natural antioxidant composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1633981A (en) * | 2004-11-24 | 2005-07-06 | 黄天军 | Ion water beauty product and its face pack |
| CN102370591A (en) * | 2010-08-24 | 2012-03-14 | 上海博天尼化妆品有限公司 | Pomegranate rind extract method and application of pomegranate rind extract |
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Effective date of registration: 20180329 Address after: 201612 Shanghai City, Songjiang District new town new grid No. 758 Building 2 Patentee after: SHANGHAI FOREST CABIN BIOLOGICAL-TECH Co.,Ltd. Address before: 210007 Jiangsu Province, Nanjing City Guanghua Road stonegateway No. 104 Patentee before: Jiang Caiyun |
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Address after: 201600 Building 2, 758 Xinge Road, Xinqiao Town, Songjiang District, Shanghai Patentee after: Shanghai linqingxuan Biotechnology Co.,Ltd. Address before: 201612 Building 2, 758 Xinge Road, Xinqiao Town, Songjiang District, Shanghai Patentee before: SHANGHAI FOREST CABIN BIOLOGICAL-TECH Co.,Ltd. |