The preparation of the extraction of active component and smearing mask in blackberry seed, seed of Fructus Crataegi, Semen Granati
Technical field
The invention belongs to the Cosmetic Manufacture field, be specifically related to the extraction process of oxidation-resistant active ingredient in a kind of blackberry seed, seed of Fructus Crataegi, Semen Granati and the preparation method of smearing mask.
Background technology
The mankind use facial film with a long history as cosmetic tool, can trace back to ancient Egypt and Chinese Tang Dynasty.The principle of facial film is to adopt the dressing of a thick layer of not same-action and composition to apply in face, and the obstruct skin contacts with air.When this one deck dressing tightly be attached on skin the time, can be because of the evaporation of the secretion that suppresses sebum and sweat but the rising of skin temperature; Those moisture that can't evaporate of skin surface can be deposited in epidermal area, and the moisture of epidermal area is full, and it is will smoother tight that skin seems, it is light that microgroove also can become; In addition, temperature and warm meeting make cutin softening, the pore expansion; The pore expansion, the sweat mixed with dirt that is deposited in the inside just can be seized the opportunity eliminating, so facial film can more thoroughly clean skin.
In several fruit seeds such as blackberry seed, seed of Fructus Crataegi, Semen Granati, self high-load has multiple polyphenol compound, flavone, anthocyanidin, vitamin C etc. a series ofly to have defying age, removes the natural active matters such as free radical physiologically active, antioxidant content.The inhibitor that can be used as many enzyme systems of polyphenol compound or activator, metal-chelator and free radical scavenger, it by phenolic hydroxyl group from separate and free radical by way of the generation antioxidation, be the very promising class Natural antioxidant and a free radical scavenger in medicine, food, cosmetics; Flavone is a kind of very strong antioxidant, can effectively remove the oxygen-derived free radicals in body, it stops the ability of oxidation is more than ten times of vitamin E, and can stop degeneration, the aging of cell, also can stop the generation of cancer, it can also suppress oozing out of inflammatory enzyme, can promote healing and the pain relieving of wound; Anthocyanidin is the antidotal supplementary of pure natural, studies have shown that it is that mankind nowadays is found the most effective antioxidant, it can protect human body to avoid the damage of the harmful substances such as free radical, its antioxygenic property exceeds 50 times than vitamin E, it can also be by making skin become smooth and high resilience to elastoser and collagen protein enzymeinhibition, can prevent the skin injury that causes due to excessive Exposure to Sunlight, inflammation-inhibiting and allergy have radiation-resistant effect; Vitamin C has antioxidation, can protect other antioxidants, prevents the injury of radical pair human body.It can also make, and dermal melanin is calm to be reduced, thereby reduces black speck and freckle, makes whitening skin.In daily life, blackberry seed, seed of Fructus Crataegi, Semen Granati all belong to garbage, now its active component are extracted, and can realize the recycling of waste resource, and existing economic worth has again social meaning.
So far, antioxidant activity thing in fruit seeds such as extracting blackberry seed, seed of Fructus Crataegi, Semen Granati is not yet arranged and prepare the technology of facial film.
Summary of the invention
1, goal of the invention
The object of the invention is to provide active polyphenoils in several fruit seeds such as a kind of extraction blackberry seed, seed of Fructus Crataegi, Semen Granati, prepare have nourishing and whitening, the method for the nourishing pack of the function such as anti-aging, antioxidation.
2, technical scheme
For achieving the above object, in its formula, each component is: 20%-40% polyvinylpyrrolidone (PVP), 4%-10% glycerol, the youngsters such as 14%-50% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder plant fruit seed powder extracting solution, the 10%-50% pure water, 3%-10% flexibilizer, each component sum are 100%.Wherein, extracting solution is for (youngsters such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder plant fruit seed powder: extractant) as 1: ratio (10-20) take charge ratio, accurately taking the concentration that several fruit seed powder such as a blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder join 10-20 times of quality is in the 30-100% alcoholic solution, extract 0.5h-7h at 15 ℃-60 ℃ of temperature, filter and obtain extracting solution.
In several fruit seeds such as blackberry seed of the present invention, seed of Fructus Crataegi, Semen Granati, preparation method and the step of active antioxidant extract facial film are as follows:
(1) preparation of extracting solution: (youngsters such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder plant fruit seed powder: extractant): 1: ratio (10-20) with charge ratio, accurately taking the youngsters such as a blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, to plant the concentration that fruit seed powder joins 10-20 times of quality be in the 30-100% alcoholic solution, extract 3.5h-5.5h at 15 ℃-60 ℃ of temperature, filter and obtain extracting solution.
(2) preparation of facial film: accurate weighing 20%-40% polyvinylpyrrolidone (PVP), 4%-10% glycerol, the 14%-50% extracting solution, the 10%-60% pure water, the little heated and stirred of 3%-10% flexibilizer is dissolved polyvinylpyrrolidone (PVP) fully, fully cooling after mixing, prepare the facial film finished product.
3, beneficial effect of the present invention
Facial film quality with formula of the present invention, explained hereafter is soft, and is good with the applying ointment or plaster property of skin, can absorb and discharge more nutritional labeling, and whitening effect is good, makes the skin smooth high resilience, the desalination wrinkle of skin.In addition in conjunction with a series of materials such as the polyphenol that contains in the fruit seed, flavone, anthocyanidin, vitamin Cs, be prepared into have nourishing and whitening, the nourishing pack of the many integration function such as anti-aging, antioxidation.
The specific embodiment
Embodiment 1
Formula: each component is: 20% polyvinylpyrrolidone (PVP), 6% glycerol, several fruit seed powder extracting solution such as 14% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, 57% pure water, 3% flexibilizer.
Preparation process
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): the ratio of 1: 10, several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder that accurately take quality and be 5 weight portions add in 75% alcoholic solution of 50 weight portions, at 37 ℃ of lower ultrasound wave assisted extraction 5.5h of temperature, filter with the sucking filtration mode and obtain extracting solution.
(2) preparation of facial film: the polyvinylpyrrolidone (PVP) of accurate weighing 7 weight portions, the glycerol of 2 weight portions, the pure water of the extracting solution of 5 weight portions and 20 weight portions, the flexibilizer of 1 weight portion, little heated and stirred is dissolved polyvinylpyrrolidone (PVP) fully, fully cooling after mixing, prepare the facial film finished product.
Embodiment 2
Formula: each component is: 30% polyvinylpyrrolidone (PVP), and 4% glycerol, the youngsters such as 47% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder plant fruit seed powder extracting solution, 13% pure water, 6% flexibilizer.
Preparation process
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): the ratio of 1: 15, the youngster such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder who accurately takes 5 mass parts plants 75% alcoholic solution that fruit seed powder adds 75 mass parts, ultrasound wave assisted extraction 4.5h under temperature 60 C filters with the sucking filtration mode and obtains extracting solution.
(2) preparation of facial film: the polyvinylpyrrolidone (PVP) of accurate weighing 22 mass parts, the glycerol of 3 mass parts, the extracting solution of 35 mass parts, the pure water of 10 mass parts, the flexibilizer of 4 mass parts, little heated and stirred is dissolved polyvinylpyrrolidone (PVP) fully, and is fully cooling after mixing, prepares the facial film finished product.
Embodiment 3
Formula: each component is: 40% polyvinylpyrrolidone (PVP), 10% glycerol, several fruit seed powder extracting solution such as 30% blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder, 10% pure water, 10% flexibilizer.
Preparation process
(1) preparation of extracting solution: with charge ratio (several fruit seed powder such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder: extractant): the ratio of 1: 20, the youngster such as blackberry seed powder, seed of Fructus Crataegi powder, Semen Granati powder who accurately takes 1 mass parts plants fruit seed powder and adds in 75% alcoholic solution of 20 mass parts, at 15 ℃ of lower ultrasound wave assisted extraction 3.5h of temperature, filter with the sucking filtration mode and obtain extracting solution.
(2) preparation of facial film: the polyvinylpyrrolidone (PVP) of accurate weighing 4 mass parts, the glycerol of 1 mass parts, the extracting solution of 3 mass parts, the pure water of 1 mass parts, the flexibilizer of 1 mass parts, little heated and stirred is dissolved polyvinylpyrrolidone (PVP) fully, and is fully cooling after mixing, prepares the facial film finished product.