CN104758198A - Powerful antioxidant skin-care product containing blackberry extract and preparation method and application thereof - Google Patents
Powerful antioxidant skin-care product containing blackberry extract and preparation method and application thereof Download PDFInfo
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Abstract
The invention relates to the technical field of skin-care products, in particular to a powerful antioxidant skin-care product containing a blackberry extract. The powerful antioxidant skin-care product comprises the following ingredients: the blackberry extract, propylene glycol, hyaluronic acid, cyclopentasiloxane, xanthan gum, methyl cellulose, glycerol, polyoxyethylene-2 stearyl ether, methylparaben and deionized water. According to the powerful antioxidant skin-care product containing the blackberry extract, after the blackberry extract serves as an additive, excessive oxygen radicals in human skin can be efficiently removed, aging of the human skin and formation of facial splash are prevented or delayed, and the effects of skin whitening, moisture holding, skin repairing, ultraviolet protection, skin sterilization, inflammation diminishing, freckle and acne removal and the like can be achieved. Therefore, the powerful antioxidant skin-care product containing the blackberry extract can be widely applied to most products requiring antioxidant protection, such as facial masks, hand creams, sun creams, whitening creams, stimulating lotions, eye creams, anti-freezing creams and anti-dandruff products.
Description
Technical field
The present invention relates to technical field of skin care, especially relate to and a kind ofly there are the skin care item of strong anti-oxidation containing blackberry extract.
Background technology
Blackberry is a kind of local flavor and small berries that is best in quality, that be of high nutritive value, there is higher healthy nutritive value and economic worth, and be rich in special nutritional labeling, containing soluble solid 8.3%, total acid 1.3%, containing Vc9.3mg, Ve3.1mg in every 100g fresh fruit, aminoacid 829mg and multiple mineral element; Wherein the content of Ve be the 6-7 of Fructus Mali pumilae doubly, 4 times of mandarin orange, 3 times of Fructus Fragariae Ananssae; Zinc, selenium and amino acid whose content are also all apparently higher than Fructus Mali pumilae and mandarin orange.
In blackberry fruit, the content of cancer-resisting substance ellagic acid, defying age material superoxide dismutase (SOD) is all higher than other fruit.Superoxide dismutase (SOD) is free radical scavenger, and it is extensively present in the various tissues of organism, can scavenging free radicals O
2-(ultra-oxygen anion free radical), and O
2-have cytotoxicity, can make lipid peroxidation, damaging cells film, causes inflammation, tumor and autoimmune disease.Why people can be old and feeble, aging sign occurs little by little, as pigementation, flag, be similar to because produce in body the Oxidation got rusty, oxygen-derived free radicals cannot effectively be eliminated, and destroys collagen protein, elastic fibers albumen, makes skin moisture-keeping and maintain elastic afunction, wrinkle grows wild, and accelerates melanic precipitation.The growth at age and some extrinsic factor body and skin histology free radical can be caused to produce exceed the normal scavenging free radicals of body ability, thus skin histology is damaged, causes aging.Because SOD can scavenging free radicals, contribute to falling protoxydic speed, thus can slow down aging.SOD has certain curative effect to all kinds of autoimmune disease simultaneously.As lupus erythematosus, scleroderma, dermatomyositis etc.Should not form front use in acute stage pathological changes for rheumatoid arthritis patients, curative effect is better.To the personnel being likely subject to ionizing radiation, SOD also can be smeared as preventive measure.
Raspberry ketone or raspberry ketone glucoside is included in blackberry.The results showed, raspberry ketone glucoside is to the formation, the removing N that are oxidized lipoid
2o and control induced by ultraviolet irradiation skin erythema all have specially good effect.The ketenes element of Japanology Fructus Rubi also can dissolve body fat, efficiency or even capsaicin 3 times, plays slimming effect.
Blackberry development potentiality is huge, has developed into the emerging fruit of the third generation gradually at present.The cultivated area of global blackberry in 2007 is about 20035km
2, main converted products is quick-frozen fruit, canned food, fruit jam, fruit juice and fruit wine etc.; Between 10 years of nineteen ninety-five to 2005 year, global blackberry cultivated area adds 45%, and cultural area each continent all over the world, what wherein cultivated area was larger has the countries such as Serbia, Hungary, Mexico, the U.S., China and Costa Rica.According to investigation and analysis result, estimate that the cultivated area of blackberry in coming 10 years is by sustainable growth, wherein develop country faster and have Romania, Poland, Mexico, Chile, Hungary, China and the U.S., can 27032km be reached to whole world commercialization blackberry cultivated area in 2015
2.China is the main product state of Asia blackberry, and cultivated area is about 1550km
2world rankings the 3rd, Baima town, Nanjing Lishui County in 1986 under the guidance and help of Plant Research Inst., Jiangsu Prov. of the Chinese Academy of Sciences. start to carry out blackberry plantation, through the development of nearly 20 years, formed the planting scale in largest domestic, Asia first, Baima town becomes " township of Chinese blackberry ".
But the period of maturation window of blackberry is little, the collection period allowed is shorter, fresh fruit listing peak period is concentrated, cause a lot of ripe fresh fruit unsalable, processing enterprise is also difficult to digestion, and its picking methods belongs to labour-intensive simultaneously, is difficult to mechanization and gathers, limit by objective condition, a large amount of mature fruits falls to the ground.According to statistics, the effective output that truly can be converted into economic benefit only has 4/5ths.The non-edible products of exploitation except freezing fruit, canned food, fruit jam, fruit juice and fruit wine has a extensive future, and also can fully utilize residual fruit, shedding, for blackberry industry increases income.
Summary of the invention
The technical problem to be solved in the present invention is: the invention provides a kind of skin care item with strong anti-oxidation function, skin tissue cell reparation containing blackberry extract, these skin care item be utilize contain in blackberry enrich the Multiple components such as SOD, vitamin, aminoacid, mineral, itself and other substance compatibility is in harmonious proportion, can make to be formed and transparent freeze shape skin care item, also can form emulsion or cream kind skin care item, there is strong anti-oxidation effect.
The technical solution adopted for the present invention to solve the technical problems is: a kind of strong anti-oxidation skin care item containing blackberry extract, its proportioning following (by mass percentage):
Containing a preparation method for the strong anti-oxidation skin care item of blackberry extract, comprise the steps:
1) preparation of blackberry extract: blackberry is removed impurity, cleaning, sterilization, be that the blackberry of 1:10-20 and water are 80-90 DEG C of reflux, extract, with solid-liquid ratio, extract 1-3 time, 1.5 hours extraction times are each, merge extractive liquid, and the residue fallen by filtered through gauze in extracting solution, extracting solution activated carbon decolorizing after filtration, distilling under reduced pressure is concentrated into paste, dries, pulverize, obtain blackberry extract;
2) according to amount of calculation, blackberry extract, propylene glycol, glycerol, methylcellulose, ring five polydimethylsiloxane are added to the water, are stirred at 75-85 DEG C without solid insoluble;
3) again to step 2) add xanthan gum, the stearic alcohol ether of polyoxyethylene-2 successively in solution, keep temperature-resistant, fully emulsified to uniform and stable cream state;
4) cooling step 3) solution to room temperature, then adds hyaluronic acid, methyl hydroxybenzoate stirs, and obtains a kind of strong anti-oxidation skin care item containing blackberry extract.
Containing a purposes for the strong anti-oxidation skin care item of blackberry extract, described a kind of strong anti-oxidation skin care item containing blackberry extract may be used for facial film, hand cream, sunscreen cream, skin whitener, skin dew of waking up, slow eye cream, antifreeze frost and dandruff product.
The invention has the beneficial effects as follows:
A kind of strong anti-oxidation skin care item containing blackberry extract of the present invention, using blackberry extract after additive use, it can have the ability of high-efficient cleaning except oxygen-derived free radicals excessive in human body skin, the aging of improvement or delaying human body skin, the formation of facial colour spot, and have, the effect such as whitening skin and preserving moisture, reparation skin, ultraviolet protection, inhibiting bacteria and diminishing inflammation, speckle removing, acne removing, experiment shows that blackberry extract has no side effect, safe and reliable; On the other hand, these skin care item are cheaper than common skin care item cost, and can resource be made full use of, expand the value of blackberry, facial film, hand cream, sunscreen cream, skin whitener, skin dew of waking up, most product needing anti-oxidation protection such as slow eye cream, antifreeze frost, dandruff product can be widely used in; Meanwhile, this invention overcomes the compatibility stability of natural materials and synthetic, and provides optimal proportion relation, makes to have good collaborative antiopxidant effect between each component.
The preparation method of a kind of strong anti-oxidation skin care item containing blackberry extract of the present invention, simple process, easy to implement the method, there is good adaptability.
Detailed description of the invention
Below in conjunction with specific embodiment, further the present invention is set forth, should be understood that and quote embodiment only for illustration of the present invention, and be not used in and limit the scope of the invention.
Embodiment 1
1, a kind of strong anti-oxidation skin care item formula containing blackberry extract: blackberry extract 10%, propylene glycol 2%, hyaluronic acid 0.5%, ring five polydimethylsiloxane 1%, xanthan gum 0.01%, methylcellulose 5%, glycerol 1%, the stearic alcohol ether 1% of polyoxyethylene-2, methyl hydroxybenzoate 0.5%, surplus is water.
2, a kind of preparation method of the strong anti-oxidation skin care item containing blackberry extract
1) preparation of blackberry extract: blackberry is removed impurity, cleaning, sterilization, be that the blackberry of 1:10 and water are 80-90 DEG C of reflux, extract, with solid-liquid ratio, extract 3 times, 1.5 hours extraction times are each, merge extractive liquid, and the residue fallen by filtered through gauze in extracting solution, extracting solution activated carbon decolorizing after filtration, distilling under reduced pressure is concentrated into paste, dries, pulverize, obtain blackberry extract;
2) according to amount of calculation, blackberry extract, propylene glycol, glycerol, methylcellulose, ring five polydimethylsiloxane are added to the water, are stirred at 75-85 DEG C without solid insoluble;
3) again to step 2) add xanthan gum, the stearic alcohol ether of polyoxyethylene-2 successively in solution, keep temperature-resistant, fully emulsified to uniform and stable cream state;
4) cooling step 3) solution to room temperature, then adds hyaluronic acid, methyl hydroxybenzoate stirs, and obtains a kind of strong anti-oxidation skin care item containing blackberry extract.
DPPH radical scavenging activity test experiments:
1, with the DPPH solution of dehydrated alcohol preparation 0.1mmol/L, keep in Dark Place.The detected solution solution of preparation 0.5mg/mL (respectively this formulation product, blackberry extract, not containing same formulation product, the commercially available similar oxidation resistant product of blackberry extract).Test sample is diluted to variable concentrations.
2,2mL is tested sample solution and 2mL DPPH solution joins in same test tube, shake up, under room temperature, dark place measures its absorbance A 1 after leaving standstill 30min, Simultaneously test 2mL DPPH solution and 2mL solvent (distilled water or corresponding buffer solution) mixed absorbance A 3, and 2mL tests sample solution and the mixed absorbance A 2 of 2mL dehydrated alcohol.
3, the expression of radical scavenging activity:
Clearance rate (%)=[1-(A1-A2)/A3] × 100%
Clearance rate shows that more greatly oxidation resistance is stronger
Result shows: this formulation product than being used alone blackberry extract, all not good, also effective than commercial like product containing the same formulation product effect of blackberry extract, and makes to have good collaborative antiopxidant effect between each component.
And respectively skin test is carried out to the crowd of Different age group:
Carry out skin care item test to child, middle age, old people respectively, all select facial skin test, the time is one month.
Embodiment 2
1, a kind of strong anti-oxidation skin care item formula containing blackberry extract: blackberry extract 1%, propylene glycol 1%, hyaluronic acid 0.01%, ring five polydimethylsiloxane 10%, xanthan gum 0.5%, methylcellulose 1%, glycerol 5%, the stearic alcohol ether 3% of polyoxyethylene-2, methyl hydroxybenzoate 0.1%, surplus is water.
2, a kind of preparation method of the strong anti-oxidation skin care item containing blackberry extract
1) preparation of blackberry extract: blackberry is removed impurity, cleaning, sterilization, be that the blackberry of 1:20 and water are 80-90 DEG C of reflux, extract, with solid-liquid ratio, extract 1 time, 1.5 hours extraction times are each, merge extractive liquid, and the residue fallen by filtered through gauze in extracting solution, extracting solution activated carbon decolorizing after filtration, distilling under reduced pressure is concentrated into paste, dries, pulverize, obtain blackberry extract;
2) according to amount of calculation, blackberry extract, propylene glycol, glycerol, methylcellulose, ring five polydimethylsiloxane are added to the water, are stirred at 75-85 DEG C without solid insoluble;
3) again to step 2) add xanthan gum, the stearic alcohol ether of polyoxyethylene-2 successively in solution, keep temperature-resistant, fully emulsified to uniform and stable cream state;
4) cooling step 3) solution to room temperature, then adds hyaluronic acid, methyl hydroxybenzoate stirs, and obtains a kind of strong anti-oxidation skin care item containing blackberry extract.
Embodiment 3
1, a kind of strong anti-oxidation skin care item formula containing blackberry extract: blackberry extract 10%, propylene glycol 5%, hyaluronic acid 0.5%, ring five polydimethylsiloxane 10%, xanthan gum 0.5%, methylcellulose 5%, glycerol 5%, the stearic alcohol ether 3% of polyoxyethylene-2, methyl hydroxybenzoate 0.5%, surplus is water.
2, a kind of preparation method of the strong anti-oxidation skin care item containing blackberry extract
1) preparation of blackberry extract: blackberry is removed impurity, cleaning, sterilization, be that the blackberry of 1:15 and water are 80-90 DEG C of reflux, extract, with solid-liquid ratio, extract 2 times, 1.5 hours extraction times are each, merge extractive liquid, and the residue fallen by filtered through gauze in extracting solution, extracting solution activated carbon decolorizing after filtration, distilling under reduced pressure is concentrated into paste, dries, pulverize, obtain blackberry extract;
2) according to amount of calculation, blackberry extract, propylene glycol, glycerol, methylcellulose, ring five polydimethylsiloxane are added to the water, are stirred at 75-85 DEG C without solid insoluble;
3) again to step 2) add xanthan gum, the stearic alcohol ether of polyoxyethylene-2 successively in solution, keep temperature-resistant, fully emulsified to uniform and stable cream state;
4) cooling step 3) solution to room temperature, then adds hyaluronic acid, methyl hydroxybenzoate stirs, and obtains a kind of strong anti-oxidation skin care item containing blackberry extract.
With above-mentioned according to desirable embodiment of the present invention for enlightenment, by above-mentioned description, relevant staff in the scope not departing from this invention technological thought, can carry out various change and amendment completely.The technical scope of this invention is not limited to the content in description, must determine its technical scope according to right.
Claims (3)
1. containing strong anti-oxidation skin care item for blackberry extract, it is characterized in that, its proportioning following (by mass percentage):
2. the preparation method of a kind of strong anti-oxidation skin care item containing blackberry extract as claimed in claim 1, is characterized in that comprising the steps:
1) preparation of blackberry extract: blackberry is removed impurity, cleaning, sterilization, be that the blackberry of 1:10-20 and water are 80-90 DEG C of reflux, extract, with solid-liquid ratio, extract 1-3 time, 1.5 hours extraction times are each, merge extractive liquid, and the residue fallen by filtered through gauze in extracting solution, extracting solution activated carbon decolorizing after filtration, distilling under reduced pressure is concentrated into paste, dries, pulverize, obtain blackberry extract;
2) according to amount of calculation, blackberry extract, propylene glycol, glycerol, methylcellulose, ring five polydimethylsiloxane are added to the water, are stirred at 75-85 DEG C without solid insoluble;
3) again to step 2) add xanthan gum, the stearic alcohol ether of polyoxyethylene-2 successively in solution, keep temperature-resistant, fully emulsified to uniform and stable cream state;
4) cooling step 3) solution to room temperature, then adds hyaluronic acid, methyl hydroxybenzoate stirs, and obtains a kind of strong anti-oxidation skin care item containing blackberry extract.
3. the purposes of a kind of strong anti-oxidation skin care item containing blackberry extract as claimed in claim 1, is characterized in that: described a kind of strong anti-oxidation skin care item containing blackberry extract may be used for facial film, hand cream, sunscreen cream, skin whitener, skin dew of waking up, slow eye cream, antifreeze frost and dandruff product.
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Cited By (14)
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| CN104982860A (en) * | 2015-07-22 | 2015-10-21 | 湖北中烟工业有限责任公司 | Preparation method of blackberry extract |
| CN105055197A (en) * | 2015-08-26 | 2015-11-18 | 湖州旭龙生物化学有限公司 | Orange peel oil skin care product and preparation method thereof |
| CN105997619A (en) * | 2016-05-18 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Preparation method and application of hericium erinaceus extracting solution |
| CN106038384A (en) * | 2016-06-08 | 2016-10-26 | 马殿伟 | Traditional Chinese medicine composition containing wild jujubes and used for sunscreen cosmetics |
| CN106074281A (en) * | 2016-07-12 | 2016-11-09 | 广州丹奇日用化工厂有限公司 | A kind of preparation method and applications of Hericium erinaceus (Bull. Ex Fr.) Pers. extracting solution |
| KR20170080094A (en) * | 2015-12-31 | 2017-07-10 | 주식회사 엘지생활건강 | Composition for improving skin conditions comprising 4-(4-Hydroxyphenyl)-2-butanone |
| CN107184464A (en) * | 2017-05-25 | 2017-09-22 | 上海悦目化妆品有限公司 | A kind of Compound Black plant fermentation composition with white-skinned face function and preparation method thereof and the application in facial mask class product |
| CN107569432A (en) * | 2017-08-29 | 2018-01-12 | 皖南医学院 | A kind of draft nourishes hand lotion of the white moisturizing of releiving of profit and preparation method thereof |
| CN108158850A (en) * | 2018-02-23 | 2018-06-15 | 国妆汉美（广州）化妆品有限公司 | A kind of composite skin care product with efficient replenishing water and preserving moisture effect and preparation method thereof |
| CN108272727A (en) * | 2018-04-08 | 2018-07-13 | 上海粉蝶化妆品有限公司 | A kind of rain lily meat lip orchid face cream |
| CN108309835A (en) * | 2018-04-25 | 2018-07-24 | 山东省农业科学院农产品研究所 | A kind of strong anti-oxidation skin care item of the anti-oxidation peptide containing peony seeds and preparation method thereof |
| CN108721174A (en) * | 2018-08-24 | 2018-11-02 | 项佳红 | A kind of anti-aging skin care product and preparation method thereof of addition Fructus Cannabis extract |
| CN110139569A (en) * | 2017-08-09 | 2019-08-16 | 奥比托有限公司 | Black raspberry extract, the whitening agent containing black raspberry extract and diet product, the manufacturing method of black raspberry extract and the method for whitening for having used black raspberry extract |
| CN115670985A (en) * | 2022-10-26 | 2023-02-03 | 浙江兰树化妆品有限公司 | Antioxidant method for preparing skin care product by using herbal plant extract |
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| CN104982860B (en) * | 2015-07-22 | 2018-09-21 | 湖北中烟工业有限责任公司 | The preparation method of blackberry extract |
| CN104982860A (en) * | 2015-07-22 | 2015-10-21 | 湖北中烟工业有限责任公司 | Preparation method of blackberry extract |
| CN105055197A (en) * | 2015-08-26 | 2015-11-18 | 湖州旭龙生物化学有限公司 | Orange peel oil skin care product and preparation method thereof |
| KR20170080094A (en) * | 2015-12-31 | 2017-07-10 | 주식회사 엘지생활건강 | Composition for improving skin conditions comprising 4-(4-Hydroxyphenyl)-2-butanone |
| KR102261933B1 (en) | 2015-12-31 | 2021-06-04 | 주식회사 엘지생활건강 | Composition for improving skin conditions comprising 4-(4-Hydroxyphenyl)-2-butanone |
| CN105997619A (en) * | 2016-05-18 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Preparation method and application of hericium erinaceus extracting solution |
| CN106038384A (en) * | 2016-06-08 | 2016-10-26 | 马殿伟 | Traditional Chinese medicine composition containing wild jujubes and used for sunscreen cosmetics |
| CN106074281A (en) * | 2016-07-12 | 2016-11-09 | 广州丹奇日用化工厂有限公司 | A kind of preparation method and applications of Hericium erinaceus (Bull. Ex Fr.) Pers. extracting solution |
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| CN107184464A (en) * | 2017-05-25 | 2017-09-22 | 上海悦目化妆品有限公司 | A kind of Compound Black plant fermentation composition with white-skinned face function and preparation method thereof and the application in facial mask class product |
| CN110139569A (en) * | 2017-08-09 | 2019-08-16 | 奥比托有限公司 | Black raspberry extract, the whitening agent containing black raspberry extract and diet product, the manufacturing method of black raspberry extract and the method for whitening for having used black raspberry extract |
| CN107569432A (en) * | 2017-08-29 | 2018-01-12 | 皖南医学院 | A kind of draft nourishes hand lotion of the white moisturizing of releiving of profit and preparation method thereof |
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| CN108272727A (en) * | 2018-04-08 | 2018-07-13 | 上海粉蝶化妆品有限公司 | A kind of rain lily meat lip orchid face cream |
| CN108309835A (en) * | 2018-04-25 | 2018-07-24 | 山东省农业科学院农产品研究所 | A kind of strong anti-oxidation skin care item of the anti-oxidation peptide containing peony seeds and preparation method thereof |
| CN108721174A (en) * | 2018-08-24 | 2018-11-02 | 项佳红 | A kind of anti-aging skin care product and preparation method thereof of addition Fructus Cannabis extract |
| CN115670985A (en) * | 2022-10-26 | 2023-02-03 | 浙江兰树化妆品有限公司 | Antioxidant method for preparing skin care product by using herbal plant extract |
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