CN106038384A - Traditional Chinese medicine composition containing wild jujubes and used for sunscreen cosmetics - Google Patents

Traditional Chinese medicine composition containing wild jujubes and used for sunscreen cosmetics Download PDF

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CN106038384A
CN106038384A CN201610400550.1A CN201610400550A CN106038384A CN 106038384 A CN106038384 A CN 106038384A CN 201610400550 A CN201610400550 A CN 201610400550A CN 106038384 A CN106038384 A CN 106038384A
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extracting solution
chinese medicine
medicine composition
parts
ziziphi spinosae
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马殿伟
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/35Caprifoliaceae (Honeysuckle family)
    • A61K36/355Lonicera (honeysuckle)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/484Glycyrrhiza (licorice)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/71Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/72Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
    • A61K36/725Ziziphus, e.g. jujube
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/333Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/53Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

Abstract

The invention discloses traditional Chinese medicine composition containing wild jujubes and used for sunscreen cosmetics. The composition is prepared from raw materials in parts by weight as follows: 11-16 parts of tropaeolum majus, 24-28 parts of wild jujubes, 10-15 parts of medicine terminalia fruits, 6-10 parts of blackberries, 2-5 parts of liquorice and 4-8 parts of honeysuckle. Through optimization of matching of the raw materials, the medicinal raw materials have a synergistic interaction effect, the sunscreen effect of the composition is improved, and the composition has mild efficacy, is prepared from pure natural plant extracts, has few side effects and is wide in adaptability and low in cost.

Description

A kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae
Technical field
The present invention relates to cosmetic field, particularly to a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing.
Background technology
Solar radiation has two parts, the light of wavelength 290-320nm to be referred to as ultraviolet B to the ultraviolet on ground, and wavelength is 320- The light of 400nm is referred to as ultraviolet A.Ultraviolet B can suppress mitosis and DNA (deoxyribonucleic acid) (DNA), ribonucleic acid (RNA), albumen Matter synthesis, causing biomolecule chain rupture, cause DNA mutation induction skin carcinoma, the generation of stimulation melanin and causing referred to as " is shone Speckle " erythematous response.Ultraviolet A can significantly increase the weight of acute injury produced by ultraviolet B, adds carcinogenic probability, institute in case Shine and be not only the important means keeping human skin attractive in appearance, be also protection skin health and healthy key factor.
Sun-proof physical sunscreen and the chemical sunscreen of being divided into: physical sunscreen utilizes physics principle exactly, utilizes the atom of lamellar Microgranule reflection sunlight, reaches sun-proof purpose.Although physical sunscreen has so that ultraviolet cannot penetrate skin surface, can The advantage that thorough UVB protects is provided, but also has that to be not suitable for doing whole body sun-proof, skin is had bigger zest, it is impossible to whitening Skin, it is necessary to use makeup removal products to help removal totally to wait shortcomings;Chemical sunscreen is to come sun-proof by chemical composition, is to utilize The principle absorbed is come sun-proof, for a kind of transmission substance, absorbable ultraviolet so that it is be converted into molecular vibrational energy or heat energy reaches anti- The effect shone, such as para-amino benzoic acid and derivant thereof, cinnamic acid etc., after being coated on the face, Atomic Absorption sunlight, to prevent sunlight Contact skin.
It is chemical sunscreen product the most mostly at present, especially compound sunscreen product, although sun-proof result is good, cost Cheap, but its side effect is big, the easy allergy of skin, and sun-proof result is single, and existing small number of Chinese medicine based composition is prevented Although shining product to have no side effect, and skin is had multiple benefit effects, but it is poor to there is sun-proof result, the shortcoming that cost is high.
Summary of the invention
It is an object of the invention to overcome that the sun-proof result in the presence of existing sun-proof Chinese medicine composition is poor, cost is high not Foot, it is provided that a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae.The said composition compatibility by optimizing materials, makes Producing synergistic function between raw medicinal material, add the sun-proof result of compositions, drug effect is gentle;Said composition is by pure natural Plant extract combines, and has no side effect, and wide adaptability is with low cost.
In order to realize foregoing invention purpose, the invention provides a kind of Chinese drug-treated group for sun care preparations containing Ziziphi Spinosae Compound, said composition is to be prepared from by the raw material of following weight: nasturtium 11-16 part, Ziziphi Spinosae 24-28 part, scolds Sub-10-15 part, blackberry 6-10 part, Radix Glycyrrhizae 2-5 part, Flos Lonicerae 4-8 part.
Above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, wherein said nasturtium, returns spleen, liver Warp;There is effect of heat-clearing and toxic substances removing;It is mainly used in treating eye conjunctivitis, carbuncle furuncle and phyma poison.
Wherein said Ziziphi Spinosae, sour in the mouth, sweet;Property flat;Return lung, Liver Channel;There is tonifying liver, mind calming, arresting sweating, effect of promoting the production of body fluid; Being mainly used in treating restlessness of asrhenia type and insomnia, dreaminess of palpitating with fear, body void hyperhidrosis, Tianjin void is thirsty.
Wherein said blackberry, sweet in the mouth, acid;Warm in nature;Return liver, kidney, bladder warp;There is supplementing the kidney to control the nocturnal reducing urination, nourishing the liver to improve visual acuity Effect;Being mainly used in treating emission and spermatorrhea, enuresis frequent micturition, impotence and premature ejaculation, mesh is the most dim-sighted.
Wherein said Fructus Chebulae, bitter in the mouth, acid, puckery;Property flat;Return lung, large intestine channel;There is relieving diarrhea with astringents, astringing lung-QI and relieving cough, pathogenic fire reducing Effect of sore-throat relieving;Being mainly used in treating chronic diarrhea chronic dysentery, proctoptosis of having blood in stool, the deficiency of the lung is breathed with cough, and chronic cough is more than, pharyngalgia hoarseness.
Wherein said Radix Glycyrrhizae, sweet in the mouth;Property flat;Return spleen, stomach, lung meridian;There is QI invigorating invigorating middle warmer;Relieving spasm to stop pain;Nourishing the lung to arrest cough; Eliminating fire and detoxication;Effect of coordinating the actions of various ingredients in a prescription;Cure mainly asthenia lack of appetite;Leanness yellowish complexion;Shortness of breath and palpitation;Stomachache loose stool;Extremity contraction urgency pain; Hysteria;Cough and asthma;Laryngopharynx swelling and pain;Ulcerative carbuncle swells and ache;Infantile carbuncle;And medicine, alimentary toxicosis.For weakness of the spleen and stomach, asthenia is weary Power, shortness of breath and palpitation, cough with copious phlegm, gastral cavity abdomen, extremity contraction urgency pain, carbuncle sore tumefacting virus, cushion toxicity, strong.
Wherein said Flos Lonicerae, sweet in the mouth;Cold in nature;Return lung, the heart, stomach warp;Have heat-clearing and toxic substances removing, antiinflammatory, qi-restoratives treat wind it Effect;It is mainly used in treating disease under distension, epidemic febrile disease heating, pyretic toxicity carbuncle and ulcer and tumor.
Above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, it is preferred that said composition is by following The raw material of weight is prepared from: nasturtium 13-15 part, Ziziphi Spinosae 25-27 part, Fructus Chebulae's 12-15 part, and blackberry 6-8 part is sweet Grass 2-4 part, Flos Lonicerae 5-7 part;It is further preferred that said composition is to be prepared from by the raw material of following weight: Nasturtium 14 parts, Ziziphi Spinosae 25 parts, Fructus Chebulae 12 parts, blackberry 7 parts, 3 parts of Radix Glycyrrhizae, Flos Lonicerae 6 parts.By above-mentioned preferably, combination can be made The synergistic function of thing is maximum, and sun-proof result reaches optimal, and side effect is minimum.
Above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, in addition to above-mentioned necessary raw material, also Auxiliary material, such as, wetting agent, surfactant, ultraviolet ray-resistant material, alcohols, water etc. can be added according to actual needs.
Above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, can make with conventional base material by arbitrary proportion Cosmetics, State of cosmetics can be the one in solution, suspension, emulsion, paste, quintessence oil, spray.
Above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, said composition is natural by multiple gentleness Raw material is made, with Ziziphi Spinosae as monarch drug, nasturtium, Fructus Chebulae be ministerial drug, blackberry and Flos Lonicerae be adjuvant drug, Radix Glycyrrhizae for making medicine, each compatibility There is between medical material synergistic function, there is absorption ultraviolet, accelerate melanic decomposition, reduce melanin pigmentation, improve Skin is to effects such as the resistances of ultraviolet, thus reaches the most sun-proof and lasting sun-proof effect, and sun-proof result is more preferable, and medicine Imitate gentle, have no side effect, be suitable for all kinds of skin quality.
Further, the invention provides the preparation side of a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Method, its concrete preparation process is as follows:
1, pulverize after nasturtium, Ziziphi Spinosae, Fructus Chebulae, blackberry, Radix Glycyrrhizae, Flos Lonicerae being separately dried, extract and concentrate, obtain non-irrigated gold Lotus extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extractive solution;
2, by the nasturtium extracting solution of step 1 gained, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extractive solution carries out maturation process respectively, carries out filtering, purifying to obtain each raw material essence, by each raw material essence after cooling Mix homogeneously, and again carry out filtering, purifying, obtain mixing essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing.
The preparation method of above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae is wherein right in step 1 Nasturtium, Ziziphi Spinosae, Fructus Chebulae, blackberry, Radix Glycyrrhizae, the extraction of Flos Lonicerae, method for concentration are conventional plant extract, method for concentration, energy Effective medical active composition in plant is separated, and increases activity component concentration, improve sun-proof result.
The preparation method of above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae is wherein right in step 2 Nasturtium extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extractive solution are carried out respectively Maturation process, i.e. carries out plant extraction liquid heating pressurized treatments, destroys the easy allergin in plant, reduce side effect, carry The high adaptability to different skin quality, and active ingredient breaks down bigger for molecular weight is become the active component of molecular weight, improve The absorption efficiency of skin.
Wherein, in described curing process, the cooking conditions to each raw material is different, can be the most anti-in farthest guarantee Shine under the reactive conditions of active substance, destroy the easy allergin in plant, reduce side effect, and by activity bigger for molecular weight Ingredient breakdown becomes the active component of molecular weight, improves the absorption efficiency of skin, its temperature, pressure and time specifically chosen As follows:
Material name Curing temperature (DEG C) Ripening pressure (MPa) Time (h)
Nasturtium 85-90 0.2-0.3 1-2
Ziziphi Spinosae 75-80 0.1-0.2 1-2
Blackberry 80-85 0.1-0.2 1-2
Fructus Chebulae 80-85 0.2-0.4 2-3
Flos Lonicerae 70-75 0.1-0.2 0.5-1
Radix Glycyrrhizae 75-80 0.2-0.3 2-3
The preparation method of above-mentioned a kind of Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, by extracting different material Liquid ripening at different conditions, inactivates the easy allergin in raw material extracting solution or decomposes, and retains energy Synergistic Effectively medicinal active ingredient, and active ingredient breaks down bigger for molecular weight is become the active component of molecular weight, thus not only Reduce the allergy probability of Chinese medicine composition, improve adaptability, moreover it is possible to improving the absorption efficiency of skin, sun-proof result is more preferable.
Compared with prior art, beneficial effects of the present invention:
1, the present composition passes through the rational compatibility of each raw material, makes different effective active compositions produce synergistic function, Exciting the property of medicine of effective active matter greatly, sun-proof result is more preferable.
2, the present composition selects multiple natural gentle raw material of Chinese medicine, and formulated by optimal compatibility, drug effect is gentle, nothing Side effect, with low cost.
3, Large molecule active substance decomposition is become small-molecule active substance by curing process by the present composition, to skin Permeability more preferable, be easily absorbed by the skin, the skin resistance to ultraviolet can be effectively increased.
4, the easy allergin in raw material extracting solution is processed by the present composition by curing process, reduces easily Anaphylaxis and side reaction, improve the adaptability of compositions.
Detailed description of the invention
Below in conjunction with test example and detailed description of the invention, the present invention is described in further detail.But this should not understood Scope for the above-mentioned theme of the present invention is only limitted to below example, and all technology realized based on present invention belong to this The scope of invention.
Embodiment 1
1, by nasturtium 14 parts, Ziziphi Spinosae 25 parts, Fructus Chebulae 12 parts, blackberry 7 parts, 3 parts of Radix Glycyrrhizae, Flos Lonicerae 6 parts be separately dried after pulverize, Extract with ethanol solution and concentrate, obtaining nasturtium extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae Extracting solution, Flos Lonicerae extractive solution;
2, by the nasturtium extracting solution of step 1 gained at 88 DEG C, carry out after carrying out ripening 2h under 0.2Mpa pressure filtering, purifying, Cool down to obtain nasturtium essence;By the Ziziphi Spinosae extracting solution of step 1 gained at 78 DEG C, carry out after carrying out ripening 1h under 0.2Mpa pressure Filter, purify, cool down to obtain Ziziphi Spinosae essence;By Fructus Chebulae's extracting solution of step 1 gained at 83 DEG C, under 0.3Mpa pressure, carry out ripening Carry out after 2h filtering, purifying, cool down to obtain Fructus Chebulae's essence;By the blackberry extracting solution of step 1 gained at 82 DEG C, under 0.1Mpa pressure Carry out after carrying out ripening 2h filtering, purifying, cool down to obtain blackberry essence;By the Radix Glycyrrhizae extract of step 1 gained at 73 DEG C, Carry out after carrying out ripening 3h under 0.2Mpa pressure filtering, purifying, cool down to obtain Radix Glycyrrhizae essence;The Flos Lonicerae of step 1 gained is carried Take liquid at 72 DEG C, carry out after carrying out ripening 1h under 0.1Mpa pressure filtering, purifying, cool down to obtain Flos Lonicerae essence;By gained The mixing of nasturtium essence, Ziziphi Spinosae essence, Fructus Chebulae's essence, blackberry essence, Radix Glycyrrhizae essence, Flos Lonicerae essence is all Even, and again purify, obtain mixing essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing;
4, sun-proof Chinese medicine composition that percentage by weight is 10%, the glycerol of 10%, the sorbitol olein of 2%, 3% olive are taken respectively Olive oil, 10% butanediol, the purified water of 65% make sunscreen cream.
It is good that this sunscreen cream has sun-proof result, can increase the skin resistance to ultraviolet, have no side effect, suitable various skins The advantage of skin quality.
Embodiment 2
1, by nasturtium 11 parts, Ziziphi Spinosae 24 parts, Fructus Chebulae 15 parts, blackberry 6 parts, 2 parts of Radix Glycyrrhizae, Flos Lonicerae 8 parts be separately dried after pulverize, Extract with ethanol solution and concentrate, obtaining nasturtium extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae Extracting solution, Flos Lonicerae extractive solution;
2, by the nasturtium extracting solution of step 1 gained at 85 DEG C, carry out after carrying out ripening 2h under 0.2Mpa pressure filtering, purifying, Cool down to obtain nasturtium essence;By the Ziziphi Spinosae extracting solution of step 1 gained at 80 DEG C, carry out after carrying out ripening 1h under 0.2Mpa pressure Filter, purify, cool down to obtain Ziziphi Spinosae essence;By Fructus Chebulae's extracting solution of step 1 gained at 85 DEG C, under 0.2Mpa pressure, carry out ripening Carry out after 3h filtering, purifying, cool down to obtain Fructus Chebulae's essence;By the blackberry extracting solution of step 1 gained at 85 DEG C, under 0.2Mpa pressure Carry out after carrying out ripening 1h filtering, purifying, cool down to obtain blackberry essence;By the Radix Glycyrrhizae extract of step 1 gained at 80 DEG C, Carry out after carrying out ripening 3h under 0.2Mpa pressure filtering, purifying, cool down to obtain Radix Glycyrrhizae essence;The Flos Lonicerae of step 1 gained is carried Take liquid at 70 DEG C, carry out after carrying out ripening 0.5h under 0.2Mpa pressure filtering, purifying, cool down to obtain Flos Lonicerae essence;By gained Nasturtium essence, Ziziphi Spinosae essence, Fructus Chebulae's essence, blackberry essence, Radix Glycyrrhizae essence, the mixing of Flos Lonicerae essence all Even, and again purify, obtain mixing essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing;
4, sun-proof Chinese medicine composition that percentage by weight is 10%, the glycerol of 10%, the sorbitol olein of 2%, 3% olive are taken respectively Olive oil, 10% butanediol, the purified water of 65% make sunscreen cream.
It is good that this sunscreen cream has sun-proof result, can increase the skin resistance to ultraviolet, have no side effect, suitable various skins The advantage of skin quality.
Embodiment 3
1, by nasturtium 11 parts, Ziziphi Spinosae 28 parts, Fructus Chebulae 10 parts, blackberry 10 parts, 5 parts of Radix Glycyrrhizae, Flos Lonicerae 4 parts is separately dried rear powder Broken, extract with ethanol solution and concentrate, obtain nasturtium extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extractive solution;
2, by the nasturtium extracting solution of step 1 gained at 90 DEG C, carry out after carrying out ripening 1h under 0.3Mpa pressure filtering, purifying, Cool down to obtain nasturtium essence;By the Ziziphi Spinosae extracting solution of step 1 gained at 75 DEG C, carry out after carrying out ripening 2h under 0.1Mpa pressure Filter, purify, cool down to obtain Ziziphi Spinosae essence;By Fructus Chebulae's extracting solution of step 1 gained at 80 DEG C, under 0.4Mpa pressure, carry out ripening Carry out after 2h filtering, purifying, cool down to obtain Fructus Chebulae's essence;By the blackberry extracting solution of step 1 gained at 85 DEG C, under 0.2Mpa pressure Carry out after carrying out ripening 1h filtering, purifying, cool down to obtain blackberry essence;By the Radix Glycyrrhizae extract of step 1 gained at 75 DEG C, Carry out after carrying out ripening 2h under 0.3Mpa pressure filtering, purifying, cool down to obtain Radix Glycyrrhizae essence;The Flos Lonicerae of step 1 gained is carried Take liquid at 75 DEG C, carry out after carrying out ripening 1h under 0.1Mpa pressure filtering, purifying, cool down to obtain Flos Lonicerae essence;By gained The mixing of nasturtium essence, Ziziphi Spinosae essence, Fructus Chebulae's essence, blackberry essence, Radix Glycyrrhizae essence, Flos Lonicerae essence is all Even, and again purify, obtain mixing essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing;
4, sun-proof Chinese medicine composition that percentage by weight is 10%, the glycerol of 10%, the sorbitol olein of 2%, 3% olive are taken respectively Olive oil, 10% butanediol, the purified water of 65% make sunscreen cream.
It is good that this sunscreen cream has sun-proof result, can increase the skin resistance to ultraviolet, have no side effect, suitable various skins The advantage of skin quality.
Comparative example 1
1, by nasturtium 14 parts, Fructus Chebulae 12 parts, blackberry 7 parts, 3 parts of Radix Glycyrrhizae, Flos Lonicerae 6 parts is pulverized after being separately dried, molten with ethanol Liquid extracts and concentrates, and obtains nasturtium extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extraction Liquid;
2, by the nasturtium extracting solution of step 1 gained at 88 DEG C, carry out after carrying out ripening 2h under 0.2Mpa pressure filtering, purifying, Cool down to obtain nasturtium essence;By Fructus Chebulae's extracting solution of step 1 gained at 83 DEG C, carry out after carrying out ripening 2h under 0.3Mpa pressure Filter, purify, cool down to obtain Fructus Chebulae's essence;By the blackberry extracting solution of step 1 gained at 82 DEG C, under 0.1Mpa pressure, carry out ripening Carry out after 2h filtering, purifying, cool down to obtain blackberry essence;By the Radix Glycyrrhizae extract of step 1 gained at 73 DEG C, under 0.2Mpa pressure Carry out after carrying out ripening 3h filtering, purifying, cool down to obtain Radix Glycyrrhizae essence;By the Flos Lonicerae extractive solution of step 1 gained at 72 DEG C, Carry out after carrying out ripening 1h under 0.1Mpa pressure filtering, purifying, cool down to obtain Flos Lonicerae essence;By the nasturtium elite of gained Liquid, Fructus Chebulae's essence, blackberry essence, Radix Glycyrrhizae essence, Flos Lonicerae essence mix homogeneously, and again purify, obtain mixed Close essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations;
4, sun-proof Chinese medicine composition that percentage by weight is 10%, the glycerol of 10%, the sorbitol olein of 2%, 3% olive are taken respectively Olive oil, 10% butanediol, the purified water of 65% make sunscreen cream.
Comparative example 2
1, by nasturtium 14 parts, Ziziphi Spinosae 25 parts, Fructus Chebulae 12 parts, 3 parts of Radix Glycyrrhizae, Flos Lonicerae 6 parts is pulverized after being separately dried, molten with ethanol Liquid extracts and concentrates, and obtains nasturtium extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extraction Liquid;
2, by the nasturtium extracting solution of step 1 gained at 88 DEG C, carry out after carrying out ripening 2h under 0.2Mpa pressure filtering, purifying, Cool down to obtain nasturtium essence;By the Ziziphi Spinosae extracting solution of step 1 gained at 78 DEG C, carry out after carrying out ripening 1h under 0.2Mpa pressure Filter, purify, cool down to obtain Ziziphi Spinosae essence;By Fructus Chebulae's extracting solution of step 1 gained at 83 DEG C, under 0.3Mpa pressure, carry out ripening Carry out after 2h filtering, purifying, cool down to obtain Fructus Chebulae's essence;By the Radix Glycyrrhizae extract of step 1 gained at 73 DEG C, under 0.2Mpa pressure Carry out after carrying out ripening 3h filtering, purifying, cool down to obtain Radix Glycyrrhizae essence;By the Flos Lonicerae extractive solution of step 1 gained at 72 DEG C, Carry out after carrying out ripening 1h under 0.1Mpa pressure filtering, purifying, cool down to obtain Flos Lonicerae essence;By the nasturtium elite of gained Liquid, Ziziphi Spinosae essence, Fructus Chebulae's essence, Radix Glycyrrhizae essence, Flos Lonicerae essence mix homogeneously, and again purify, obtain mixed Close essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing;
4, sun-proof Chinese medicine composition that percentage by weight is 10%, the glycerol of 10%, the sorbitol olein of 2%, 3% olive are taken respectively Olive oil, 10% butanediol, the purified water of 65% make sunscreen cream.
Comparative example 3
1, by nasturtium 10 parts, Ziziphi Spinosae 15 parts, Fructus Chebulae 20 parts, blackberry 7 parts, 3 parts of Radix Glycyrrhizae, Flos Lonicerae 6 parts be separately dried after pulverize, Extract with ethanol solution and concentrate, obtaining nasturtium extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae Extracting solution, Flos Lonicerae extractive solution;
2, by the nasturtium extracting solution of step 1 gained at 88 DEG C, carry out after carrying out ripening 2h under 0.2Mpa pressure filtering, purifying, Cool down to obtain nasturtium essence;By the Ziziphi Spinosae extracting solution of step 1 gained at 78 DEG C, carry out after carrying out ripening 1h under 0.2Mpa pressure Filter, purify, cool down to obtain Ziziphi Spinosae essence;By Fructus Chebulae's extracting solution of step 1 gained at 83 DEG C, under 0.3Mpa pressure, carry out ripening Carry out after 2h filtering, purifying, cool down to obtain Fructus Chebulae's essence;By the blackberry extracting solution of step 1 gained at 82 DEG C, under 0.1Mpa pressure Carry out after carrying out ripening 2h filtering, purifying, cool down to obtain blackberry essence;By the Radix Glycyrrhizae extract of step 1 gained at 73 DEG C, Carry out after carrying out ripening 3h under 0.2Mpa pressure filtering, purifying, cool down to obtain Radix Glycyrrhizae essence;The Flos Lonicerae of step 1 gained is carried Take liquid at 72 DEG C, carry out after carrying out ripening 1h under 0.1Mpa pressure filtering, purifying, cool down to obtain Flos Lonicerae essence;By gained The mixing of nasturtium essence, Ziziphi Spinosae essence, Fructus Chebulae's essence, blackberry essence, Radix Glycyrrhizae essence, Flos Lonicerae essence is all Even, and again purify, obtain mixing essence;
3, mixing essence step 2 obtained carries out homogenizing, obtains the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae Thing;
4, sun-proof Chinese medicine composition that percentage by weight is 10%, the glycerol of 10%, the sorbitol olein of 2%, 3% olive are taken respectively Olive oil, 10% butanediol, the purified water of 65% make sunscreen cream.
The sun care preparations that above-described embodiment 1-3 and comparative example 1-3 obtain is detected, testing result, records as follows: (wherein matched group is the chemical sunscreen cosmetics that on market, existing sales volume is maximum)
Group SPF (sun protection factor) (SPF) To absorption of UV (%)
Embodiment 1 13 63
Embodiment 2 12 61
Embodiment 3 12 62
Comparative example 1 3 24
Comparative example 2 5 35
Comparative example 3 5 34
Matched group 8 48
From above proof test data, embodiment 1-3 have employed present composition raw material composition and formula is prepared into The sun-proof Chinese medicine composition arrived, has synergistic function, and sun-proof result is notable, and SPF (sun protection factor) is high, the absorbance to ultraviolet Greatly, and drug effect is gentle, has no side effect, and to skin not allergy, is suitable for various people and uses;Comparative example 1 does not adds monarch drug Ziziphi Spinosae, Compositions compatibility changes completely, and sun-proof result is very poor;Comparative example 2 does not adds adjuvant drug blackberry, and compositions compatibility changes, between medical material Losing synergistic function, sun-proof result is deteriorated;Comparative example 3 does not use the raw material number of the present composition, and compatibility changes Becoming, Fructus Chebulae becomes monarch drug, and Ziziphi Spinosae becomes ministerial drug, and the overall property of medicine of compositions prepared changes, and also loses collaborative between medical material Potentiation, sun-proof result is deteriorated;Matched group is existing sun care preparations testing result, obtains prepared by the embodiment of the present invention Sun care preparations SPF (sun protection factor) and absorption of UV significant difference.

Claims (10)

1. the Chinese medicine composition for sun care preparations containing Ziziphi Spinosae, it is characterised in that described compositions is by following The raw material of weight is prepared from: nasturtium 11-16 part, Ziziphi Spinosae 24-28 part, Fructus Chebulae's 10-15 part, blackberry 6-10 part, Radix Glycyrrhizae 2-5 part, Flos Lonicerae 4-8 part.
Chinese medicine composition the most according to claim 1, it is characterised in that described compositions is former by following weight Material is prepared from: nasturtium 13-15 part, Ziziphi Spinosae 25-27 part, Fructus Chebulae's 12-15 part, blackberry 6-8 part, Radix Glycyrrhizae 2-4 part, Flos Lonicerae 5-7 part.
Chinese medicine composition the most according to claim 2, it is characterised in that described compositions is former by following weight Material is prepared from: nasturtium 14 parts, Ziziphi Spinosae 25 parts, Fructus Chebulae 12 parts, blackberry 7 parts, 3 parts of Radix Glycyrrhizae, Flos Lonicerae 6 parts.
4. according to Chinese medicine composition described in any one of claim 1-3, it is characterised in that the preparation side of described Chinese medicine composition Method, its concrete preparation process is as follows:
(1), nasturtium, Ziziphi Spinosae, Fructus Chebulae, blackberry, Radix Glycyrrhizae, Flos Lonicerae are separately dried after pulverize, extract and concentrate, obtain non-irrigated Lily feet extracting solution, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae extract, Flos Lonicerae extractive solution;
(2), the nasturtium extracting solution of step 1 gained, Ziziphi Spinosae extracting solution, Fructus Chebulae's extracting solution, blackberry extracting solution, Radix Glycyrrhizae are extracted Liquid, Flos Lonicerae extractive solution carry out maturation process respectively, carry out filtering, purifying to obtain each raw material essence after cooling, by each raw material essence China's liquid mix homogeneously, and again carry out filtering, purifying, obtain mixing essence;
(3) the mixing essence, by step 2 obtained carries out homogenizing, obtains the Chinese drug-treated group for sun care preparations containing Ziziphi Spinosae Compound.
Chinese medicine composition the most according to claim 4, it is characterised in that in the preparation method step 2 of described compositions, drought gold The curing temperature of lotus extracting solution is 85-90 DEG C, pressure is 0.2-0.3Mpa, the time is 1-2h.
Chinese medicine composition the most according to claim 4, it is characterised in that in the preparation method step 2 of described compositions, Ziziphi Spinosae The curing temperature of extracting solution is 75-80 DEG C, pressure is 0.1-0.2Mpa, the time is 1-2h.
Chinese medicine composition the most according to claim 4, it is characterised in that in the preparation method step 2 of described compositions, blackberry The curing temperature of extract is 80-85 DEG C, pressure is 0.1-0.2Mpa, the time is 1-2h.
Chinese medicine composition the most according to claim 4, it is characterised in that in the preparation method step 2 of described compositions, Fructus Chebulae The curing temperature of extracting solution is 80-85 DEG C, pressure is 0.2-0.4Mpa, the time is 2-3h.
Chinese medicine composition the most according to claim 4, it is characterised in that in the preparation method step 2 of described compositions, gold silver To spend the curing temperature of extracting solution be 70-75 DEG C, pressure is 0.1-0.2Mpa, the time is 0.5-1h.
Chinese medicine composition the most according to claim 4, it is characterised in that in the preparation method step 2 of described compositions, sweet The curing temperature of grass extracting solution is 75-80 DEG C, pressure is 0.2-0.3Mpa, the time is 2-3h.
CN201610400550.1A 2016-06-08 2016-06-08 Traditional Chinese medicine composition containing wild jujubes and used for sunscreen cosmetics Pending CN106038384A (en)

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Application publication date: 20161026