CN115089539A - Skin firming plant extract composition and preparation method and application thereof - Google Patents

Skin firming plant extract composition and preparation method and application thereof Download PDF

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Publication number
CN115089539A
CN115089539A CN202210901343.XA CN202210901343A CN115089539A CN 115089539 A CN115089539 A CN 115089539A CN 202210901343 A CN202210901343 A CN 202210901343A CN 115089539 A CN115089539 A CN 115089539A
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parts
plant extract
firming
extract composition
tremella
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CN115089539B (en
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乔卫东
吴题
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Xinrong Biological Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Veterinary Medicine (AREA)
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  • General Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Botany (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to a firming plant extract composition, and a preparation method and application thereof. The firming plant extract composition comprises plant extract, wherein the plant extract comprises the following raw materials in parts by weight: 15-40 parts of radix ophiopogonis, 5-20 parts of red dates, 5-25 parts of tremella, 10-30 parts of liquorice and 10-30 parts of myrobalan. The plant extract in the firming plant extract composition is extracted from five plant raw materials such as radix ophiopogonis, red dates, tremella, liquorice and myrobalan, has no irritant ingredient, has different effective ingredients of the plant raw materials, has a synergistic effect, has a good firming effect on skin, and has certain moisturizing and acne removing effects.

Description

Skin firming plant extract composition and preparation method and application thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a firming plant extract composition, and a preparation method and application thereof.
Background
Healthy skin should be smooth, moist and elastic, which is largely due to the moisture in the skin, and when the moisture content of the skin is sufficient, the skin is full of moisture, and particularly, the moisture content of the stratum corneum directly affects the apparent state of the skin. Whether the skin looks dry from the surface mainly depends on the water content of the horny layer of the epidermis, and when the water content is 10-20 percent, the skin looks moist, compact and elastic, and is the most ideal skin state; if the water content of the stratum corneum is less than 10%, the skin becomes dry and rough, and even cracks occur. For example, in autumn and winter, the weather is dry, if skin moisturizing is not focused, excessive moisture loss in the skin is caused, the skin may become dry, rough and aged, and in severe cases, the skin may have a peeling phenomenon, and the moisturized skin lacks softness and extensibility, so that the skin fat layer is broken, and then the eye marks and the lip marks are generated.
If the skin is dry but has no other symptoms, the skin can be properly applied with a moisturizing facial mask or a wiping moisturizing skin care product without irritation under the condition of well cleaning the skin only by paying attention to skin moisturizing at ordinary times so as to help the skin to replenish moisture; skin care products that help lock water may also be used to prevent water loss. However, the skin care products for removing acne and wrinkles in the market currently have various skin care varieties aiming at the situation that the skin has acne and fine lines, but most of the products use synthetic chemical substances as effective components, and some of the chemical synthetic effective components are hormones, so that the products can cause serious damage to human bodies after being used for a long time. Therefore, there is an urgent need to develop a skin care composition that is purely natural.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a firming plant extract composition as well as a preparation method and application thereof.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
in a first aspect, the firming plant extract composition provided by the invention comprises a plant extract, wherein the plant extract comprises the following raw materials in parts by weight: 15-40 parts of radix ophiopogonis, 5-20 parts of red dates, 5-25 parts of tremella, 10-30 parts of liquorice and 10-30 parts of myrobalan.
Preferably, the plant extract comprises the following raw materials in parts by weight: 25-35 parts of radix ophiopogonis, 8-12 parts of red dates, 8-12 parts of tremella, 15-25 parts of liquorice and 12-18 parts of myrobalan.
Preferably, the plant extract comprises the following raw materials in parts by weight: 30 parts of dwarf lilyturf tuber, 10 parts of red date, 10 parts of tremella, 20 parts of liquorice and 15 parts of myrobalan.
Preferably, the plant extract is prepared by the following method: adding radix Ophiopogonis, fructus Jujubae, Tremella, Glycyrrhrizae radix, and fructus Chebulae into water, soaking, heating, decocting, cooling, separating to obtain filtrate, standing, and refining to obtain plant extract.
Further preferably, the soaking time is 30-60 min; the heating and cooking temperature is 90-120 ℃, and the time is 20-60 min; the temperature of the separation after cooling is 50-60 ℃; the standing temperature is 4-10 ℃, and the standing time is 12-24 hours.
Further preferably, the ratio of the weight of the water to the total weight of the radix ophiopogonis, the red dates, the tremella, the liquorice and the myrobalan is (800-1500) to (45-145).
Preferably, the firming plant extract composition further comprises a preservative.
More preferably, the weight ratio of the preservative to the plant extracting solution is (0.1-0.4): 1.
In a second aspect, the present invention provides a method for preparing the firming plant extract composition according to the first aspect, comprising the steps of: mixing the plant extractive solution and antiseptic, sealing, and packaging.
In a third aspect, the present invention provides the use of the firming plant extract composition of the first aspect in cosmetics.
Compared with the prior art, the invention has the beneficial effects that:
the plant extract in the firming plant extract composition is extracted from five plant raw materials such as radix ophiopogonis, red dates, tremella, liquorice and myrobalan, has no irritant ingredient, has different effective ingredients, has a synergistic effect, has a good firming effect on skin, and has certain moisturizing and acne removing effects.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to the following examples. It will be understood by those skilled in the art that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
The reagents, methods and equipment adopted by the invention are conventional in the technical field if no special description is given.
Example 1
This example provides a firming plant extract composition, which is prepared by the following steps:
(1) weighing the following raw materials in parts by weight: 30 parts of radix ophiopogonis, 10 parts of red dates, 10 parts of tremella, 20 parts of liquorice, 15 parts of myrobalan and 1200 parts of water, wherein the radix ophiopogonis, the red dates, the tremella, the liquorice and the myrobalan are added into the water, soaked for 40min, heated to 100 ℃ at a constant speed within 20min, and subjected to heat preservation and steaming for 40 min; naturally cooling to 55 + -5 deg.C, filtering to obtain filtrate, standing at 5 deg.C for 15h, centrifuging at room temperature with high speed centrifuge, and filtering with 0.22 μm diameter filter membrane to obtain clear plant extractive solution;
(2) mixing antiseptic and plant extractive solution at weight ratio of 0.3:100, sealing, and packaging to obtain skin firming plant extract composition.
Example 2
This example provides a firming plant extract composition prepared by the method described in example 1, which differs from that described in example 1 in that: in this embodiment, the step (1) specifically includes: adding radix Ophiopogonis, fructus Jujubae, Tremella, Glycyrrhrizae radix, and fructus Chebulae into water, soaking for 60min, uniformly heating to 90 deg.C within 10min, keeping the temperature, steaming for 60min, naturally cooling to 55 + -5 deg.C, filtering to obtain filtrate, standing at 10 deg.C for 12h, centrifuging at room temperature with high speed centrifuge, and filtering with 0.22 micrometer filter membrane to obtain clear and transparent plant extract.
Example 3
This example provides a firming plant extract composition prepared by the method described in example 1, which differs from that described in example 1 in that: in this embodiment, the step (1) specifically includes: adding radix Ophiopogonis, fructus Jujubae, Tremella, Glycyrrhrizae radix, and fructus Chebulae into water, soaking for 30min, uniformly heating to 120 deg.C within 30min, keeping the temperature, steaming for 30min, naturally cooling to 55 + -5 deg.C, filtering to obtain filtrate, standing at 4 deg.C for 24h, centrifuging at room temperature with high speed centrifuge, filtering with 0.22 micrometer filter membrane to obtain clear plant extract.
Example 4
This example provides a firming plant extract composition prepared by the method described in example 1, which differs from that described in example 1 in that: in this example, the following raw materials in parts by weight are weighed in step (1): 35 parts of radix ophiopogonis, 12 parts of red dates, 8 parts of tremella, 15 parts of liquorice, 12 parts of myrobalan and 1200 parts of water.
Example 5
This example provides a firming plant extract composition prepared by the method described in example 1, which differs from that described in example 1 in that: in this example, the following raw materials in parts by weight are weighed in step (1): 25 parts of dwarf lilyturf tuber, 8 parts of red date, 12 parts of tremella, 25 parts of liquorice, 18 parts of myrobalan and 1200 parts of water.
Example 6
The preparation method of the firming plant extract composition provided in this example is different from that of example 1 in that: in this example, the following raw materials in parts by weight are weighed in step (1): 15 parts of radix ophiopogonis, 5 parts of red dates, 5 parts of tremella, 10 parts of liquorice, 10 parts of myrobalan and 800 parts of water.
Example 7
This example provides a firming plant extract composition prepared by the method described in example 1, which differs from that described in example 1 in that: in this example, the following raw materials in parts by weight are weighed in step (1): 40 parts of radix ophiopogonis, 20 parts of red dates, 25 parts of tremella, 30 parts of liquorice, 30 parts of myrobalan and 1200 parts of water.
Comparative example 1
This comparative example provides a plant extract composition, which was prepared by a method different from that of example 1 in that: this comparative example replaces "myrobalan" in example 1 with "gallnut".
Comparative example 2
This comparative example provides a plant extract composition, the preparation method of which differs from example 1 in that: in the comparative example, the following raw materials in parts by weight are weighed in step (1): 40 parts of radix ophiopogonis, 10 parts of tremella, 20 parts of liquorice, 15 parts of myrobalan and 1200 parts of water.
Comparative example 3
This comparative example provides a plant extract composition, which was prepared by a method different from that of example 1 in that: in the comparative example, the following raw materials in parts by weight were weighed in step (1): 30 parts of radix ophiopogonis, 10 parts of red dates, 10 parts of tremella, 35 parts of liquorice and 1200 parts of water.
Comparative example 4
This comparative example provides a plant extract composition, which was prepared by a method different from that of example 1 in that: in the comparative example, the following raw materials in parts by weight were weighed in step (1): 30 parts of dwarf lilyturf tuber, 20 parts of red date, 20 parts of liquorice, 15 parts of myrobalan and 1200 parts of water.
Application examples 1 to 11
The plant extract compositions provided in examples 1 to 7 and comparative examples 1 to 4 are respectively prepared into firming essence according to the following methods:
(1) weighing the following raw materials in percentage by weight: 1% of propylene glycol, 0.2% of carbomer, 0.05% of hyaluronic acid, 0.2% of triethanolamine, 3% of butanediol, 0.5% of p-hydroxyacetophenone, 0.5% of 1, 2-hexanediol and 94.55%.
(2) Weighing the plant extract composition and carbomer, mixing together, homogenizing for 3-5 minutes, heating to 80 ℃ while stirring, keeping the temperature and stirring for 30 minutes, cooling, adding triethanolamine when the temperature is reduced to 60 ℃, sequentially adding hyaluronic acid, propylene glycol, butanediol, p-hydroxyacetophenone and 1, 2-hexanediol when the temperature is reduced to 50 ℃, sampling and detecting when the temperature is reduced to 40 ℃, discharging after the product is qualified, standing for 48 hours, sampling, carrying out microbial detection, and filling into bottles after the product is qualified.
Effect example 1
Collecting 110 female volunteers, wherein the age of the volunteers is 18-45 years, randomly dividing the volunteers into 11 groups, using the products obtained in application examples 1-11 for each group of 10 persons, continuously using the products for 10 days, and then counting scoring results of the volunteers of each group on indexes such as appearance, smell, firming effect, moisturizing effect, skin feeling, overall satisfaction degree and acne removing satisfaction degree of the products, wherein each index value is 0-10 minutes, and 0 is the lowest value and represents extremely unsatisfactory; 10 is the highest value, indicating great satisfaction. The statistical results are shown in table 1 below.
TABLE 1
Figure BDA0003770980630000061
Figure BDA0003770980630000071
TABLE 2 statistical table of acne-removing satisfaction
Application example Source of extractive solution Satisfaction degree of acne removal
1 Example 1 8.5
2 Example 2 7.2
3 Example 3 7.4
4 Example 4 7.3
5 Example 5 7.6
6 Example 6 8.1
7 Example 7 8.3
8 Comparative example 1 6.9
9 Comparative example 2 7.1
10 Comparative example 3 5.8
11 Comparative example 4 6.3
According to the investigation result after the use of the consumer, the overall satisfaction degree of the consumer on the essence obtained by the use examples 1-7 is high, the skin tightening and moisturizing effects can be obviously felt within 10-20 minutes after the use, the skin is smooth and tender, and the overall satisfaction is relatively high; after one week of continuous use, the skin is obviously tender, smooth and elastic. The essence obtained in application examples 1-7 also has a certain acne removing effect on acne, has a certain acne removing effect after being continuously used for three days, and has a relatively obvious acne removing effect after being continuously used for 7-15 days.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (10)

1. The skin-firming plant extract composition is characterized by comprising plant extract, wherein the plant extract comprises the following raw materials in parts by weight: 15-40 parts of radix ophiopogonis, 5-20 parts of red dates, 5-25 parts of tremella, 10-30 parts of liquorice and 10-30 parts of myrobalan.
2. The firming plant extract composition of claim 1, wherein the plant extract comprises the following raw materials in parts by weight: 25-35 parts of radix ophiopogonis, 8-12 parts of red dates, 8-12 parts of tremella, 15-25 parts of liquorice and 12-18 parts of myrobalan.
3. The firming plant extract composition of claim 1, wherein the plant extract comprises the following raw materials in parts by weight: 30 parts of dwarf lilyturf tuber, 10 parts of red date, 10 parts of tremella, 20 parts of liquorice and 15 parts of myrobalan.
4. The firming plant extract composition according to claim 1, wherein said plant extract is prepared by the following method: adding radix Ophiopogonis, fructus Jujubae, Tremella, Glycyrrhrizae radix, and fructus Chebulae into water, soaking, heating, decocting, cooling, separating to obtain filtrate, standing, and refining to obtain plant extract.
5. The firming plant extract composition according to claim 4, wherein the soaking time is 30 to 60 min; the heating and cooking temperature is 90-120 ℃, and the time is 20-60 min; the temperature of the separation after cooling is 50-60 ℃; the standing temperature is 4-10 ℃, and the standing time is 12-24 hours.
6. The firming plant extract composition of claim 4, wherein the weight ratio of the water to the total weight of the radix Ophiopogonis, the red dates, the tremella, the liquorice and the myrobalan is (800-1500) to (45-145).
7. The firming plant extract composition of claim 1, further comprising a preservative.
8. The firming plant extract composition of claim 7, wherein the weight ratio of said preservative to said plant extract is (0.1-0.4): 1.
9. A process for preparing the firming plant extract composition of claim 8, comprising the steps of: mixing the plant extractive solution and antiseptic, sealing, and packaging.
10. Use of the firming plant extract composition of any one of claims 1 to 8 in cosmetics.
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