CN105191987A - Nano-titanium and biological-sulfur-zinc-manganese mixture for melon powdery mildew - Google Patents

Nano-titanium and biological-sulfur-zinc-manganese mixture for melon powdery mildew Download PDF

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Publication number
CN105191987A
CN105191987A CN201510589952.6A CN201510589952A CN105191987A CN 105191987 A CN105191987 A CN 105191987A CN 201510589952 A CN201510589952 A CN 201510589952A CN 105191987 A CN105191987 A CN 105191987A
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CN
China
Prior art keywords
zinc
titanium
manganese
powdery mildew
nano
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510589952.6A
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Chinese (zh)
Inventor
王猛
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Suzhou Keda Weilong Agricultural Technology Co Ltd
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Suzhou Keda Weilong Agricultural Technology Co Ltd
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Application filed by Suzhou Keda Weilong Agricultural Technology Co Ltd filed Critical Suzhou Keda Weilong Agricultural Technology Co Ltd
Priority to CN201510589952.6A priority Critical patent/CN105191987A/en
Publication of CN105191987A publication Critical patent/CN105191987A/en
Priority to PCT/CN2016/083490 priority patent/WO2017045432A1/en
Pending legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/20—Bacteria; Substances produced thereby or obtained therefrom
    • A01N63/22—Bacillus
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/20—Bacteria; Substances produced thereby or obtained therefrom

Abstract

The invention discloses a nano-titanium and biological-sulfur-zinc-manganese mixture for melon powdery mildew. The nano-titanium and biological-sulfur-zinc-manganese mixture for the melon powdery mildew is prepared from a first material and a second material. The first material comprises 35% of 60-nm-ball polymerization titanium, 15% of sulfur powder, 20% of zinc sulfate, 25% of manganese sulfate and 5% of chitin. The second material comprises 1 part of monascus, 1 part of bacillus subtilis, 1 part of bacillus megatherium, 1 part of lactobacillus thermophilus and 1 part of 25% brown sugar water. A preparing method of the nano-titanium and biological-sulfur-zinc-manganese mixture includes the steps that 1, the sulfur powder, the zinc sulfate and the manganese sulfate are added into the 60-nm-ball polymerization titanium and dissolved, and the mixture is arranged in the sun to be subjected to photodecomposition; 2, the microorganisms in the second material are arranged in the brown sugar water to be subjected to enriching culturing for 3 d; 3, the materials obtained after the step 1 are put into a microorganism bucket obtained after enriching culturing in the step 2, the chitin is put, secondary fermentation is carried out for 7 d, and the nano-titanium and biological-sulfur-zinc-manganese mixture for the melon powdery mildew is obtained. The nano-titanium and biological-sulfur-zinc-manganese mixture is sprayed to the blade surfaces of melons, cell membranes of pathogens are broken, and 95% of the powdery mildew is effectively inhibited.

Description

A kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture
Technical field
The present invention relates to a kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture, belong to the technical field of agro-ecology type control of plant disease.
Background technology
In Muskmelon Planting, especially in the planting environment of facility plastic greenhouse, due to the temperature of facility plastic greenhouse, the control of humidity is improper, the element at N P and K is focused on during fertilising, ignore the zinc in trace element, manganese, magnesium, the use of boron, add irrigation improper, the muskmelon of planting in facility plastic greenhouse, the resistance of itself is poor, add environmental management improper, cause the applicable environment of the pathogenic growth of melon powdery mildew, melon powdery mildew is in plant growth whole process, as long as fitness of environment all can be fallen ill, especially in the end of spring and the beginning of summer, autumn late summer the most easily causes the generation of powdery mildew at the beginning, the blade of powdery mildew main harm crop, stem is climing, although be not easy the death causing crop, but whole blade can be covered when its mildew is serious, have a strong impact on photosynthesis, form the malnutrition of crop, cause plant early ageing, change melon, the lighter affects the 30-40% of harvest, time serious, even No kernels or seeds are gathered, as in a year of scarcity, cause serious economic loss, the chemical prevention and control method used on the market at present has second phonetic phenol bacterium fat, thiophanate methyl, the chemical agents such as tpn, these chemical agents are used easily to produce the residual of medicament, soil digestion not easily, the problems such as powdery mildew substance develops immunity to drugs.
Present consumer payes attention to gradually for nuisanceless, green food, requirement for Detecting Pesticide standard is more and more higher, how a kind of control agent of powdery mildew of nontoxic, harmless boilogical type is provided, not only can suppress the growth of melon powdery mildew, the trace element of muskmelon growing period can be provided again to supplement, not developing immunity to drugs after using, easily by the organic-biological control agent that soil and plant absorption decompose, is a solution being badly in need of at present wanting on agricultural planting.
Summary of the invention
Technical problem to be solved by this invention is to provide one and carries out photocatalytic oxidation decomposition sulphur with 60nm ball polymerization titanium, zinc sulphate, the sulphur of manganese sulphate, zinc, the main component of manganese, then via monascus, bacillus subtilis, bacillus megaterium, lactobacillus Beijerinc absorbs zinc, manganese, the element of sulphur, changes into the zinc of biotype, manganese, the kenel of sulphur exists, and application powdery mildew pathogene is to zinc, manganese, the sensitivity characteristic of sulphur, its mechanism of action is the forbidden band electrolysis generation heat via 60nm ball polymerization titanium, and carry out damage and failure to the cell membrane of powdery mildew pathogen, application powdery mildew pathogene is to zinc, manganese, the sensitivity characteristic of sulphur, by zinc, manganese, the composition of sulphur is brought in the cyton of pathogene, destroy the organized enzyme conversion of pathogene, and then the growth of the pathogene of suppression powdery mildew, the generation of effective suppression powdery mildew, the present invention does not only produce environment and pollutes, the nutrient that the composition used is plant demand, easily degrade at occurring in nature, not only play the morbidity suppressing powdery mildew, more can increase sugariness and the mouthfeel of melon fruit, be a kind of biocontrol agent that can become economic worth, solve the technical barrier of residue of pesticide and pathogene disease resistance.
The present invention is that to solve the problems of the technologies described above the technical scheme adopted be a kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture, its material mixture ratio and processing step as follows:
1, material:
(1), material I: 60nm ball polymerization titanium 35%, sofril 15%, zinc sulphate 20%, manganese sulphate 25%, chitin 5%;
(2), material II: monascus is a, bacillus subtilis is a, bacillus megaterium is a, lactobacillus Beijerinc is a, 25% brown sugar water is a;
2, processing step:
(1), by Cosan, zinc sulphate, manganese sulphate put into after 60nm ball polymerization titanium dissolves, be positioned over photocatalysis Decomposition 2.5h under sunshine;
(2), the microorganism in material II is put into brown sugar water and carry out enrichment culture 3d;
(3), step 1 is completed after output object, putting in the fermentation cauldron of step 2, then add the chitin in material I, carry out secondary fermentation, is 7d between yeast phase;
(4), fermented rear filtration residue, obtains a kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture.
Advantage of the present invention:
The present invention contrasts prior art following effect: one provided by the invention is by inorganic compound, the element of the sulphur of ionic state, zinc, manganese element, recycling monascus, bacillus subtilis, bacillus megaterium absorption ionic state is formed after photocatalysis Decomposition via 60nm ball polymerization titanium, produce the compound of the sulphur of biotype, zinc, manganese state, chitin changes into high fat film via microbial enzyme, in order to be polymerized various trace elements.Spray on the blade face of muskmelon, not only on blade face, form layer protecting film, the pathogene of isolation powdery mildew is adsorbed on blade face, there is sulphur to powdery mildew pathogen susceptibility in addition, zinc, manganese element, when pathogene is adsorbed on blade, being polymerized titanium by nanosphere produces electrolysis high hot, destroy the cell membrane of pathogene, by the element to powdery mildew pathogen sensitivity, invade in its cytoplasm, destroy the organized enzyme of pathogene, and then the growth of the pathogene of deactivation powdery mildew, element used is in addition that muskmelon increases sweet element, increase commodity fruit sweetness quality, the material that the present invention uses is via after photocatalysis Decomposition, be applicable to large-scale promotion application.
Accompanying drawing explanation
The process flow diagram of Fig. 1 a kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture
Embodiment
1, case one: farm, Zhangjiagang, Suzhou City of Jiangsu Province, plantation Melon 30 mu of ground, in the facility plastic greenhouse of discovery by the end of May then, there is white powder thing in melon leaf, through studying and judging the stage of the cleistothecium being powdery mildew, as unsuitable treatment, in 7 days, the muskmelon on 30 mu of ground will occur that a large amount of tendrils is dead; Apply a kind of melon powdery mildew nano-titanium of the present invention and biological sulphur zinc-manganese mixture 500 times of liquid, first day sprays in blade face, within second day, spray with clear water, within 3rd day, spray 750 times of liquid, within 4th day, again with clear water spray, treat rear new climing regeneration in 7 days, sprayed 1000 times of liquid every 10 days and carry out maintenance work, start to yield positive results after 20 days, to the symptom of non-goodbye powdery mildew at the end of gathering;
2, case two: plantation family, Pro Lake Town, Suzhou City of Jiangsu Province, 15 mu, muskmelon planted by the sweet treasured of application simple plastic greenhouse plantation Japan, after melon is overgrow and is grown to 5 joints, within every 7 days, spray a kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture 1000 times of liquid, as powdery mildew prevention work, have powdery mildew to occur to having no in melon canopy after gathering, sugariness is 17 degree after tested, increases 2-3 degree than normal muskmelon sugariness;
3, case three: Nan Gang town, Zhangjiagang, Suzhou City of Jiangsu Province, application green house plantation Elizabethan Melon, when patrolling in field, find a part of blade to occur white powder point, apply a kind of melon powdery mildew nano-titanium of the present invention and biological sulphur zinc-manganese mixture 700 times of liquid spray, sprayed once every 7 days, spread generation to what have no powdery mildew after having gathered, detect residue of pesticide through local agriculture test department, do not occur residue of pesticide.
By above actual in the application in land for growing field crops, when between the powdery mildew high-incidence season, apply a kind of melon powdery mildew nano-titanium of the present invention and biological sulphur zinc-manganese mixture, control or treatment melon powdery mildew all work to obtain effect, and the element of the present invention's use is the nutrient needed for muskmelon growth, the photosynthesis under low light photograph can be increased in, nutrient is changed into the sugariness of muskmelon, and then increase the sugariness 1-2 degree of muskmelon, increasing the value of commodity fruit, is the solution of a kind of green non-poisonous controlling powdery mildew be worthy to be popularized; Although the present invention discloses as above with preferred embodiments; so itself and be not used to limit the present invention, any those skilled in the art, without departing from the spirit and scope of the present invention; when doing a little amendment and perfect, therefore protection scope of the present invention is when being as the criterion of defining with claims.

Claims (3)

1. melon powdery mildew nano-titanium and a biological sulphur zinc-manganese mixture, is characterized in that: be polymerized by 60nm ball the composition that titanium utilizes the sulphur of sunshine photodissociation sulphur, zinc sulphate, manganese sulphate, zinc, manganese; Via monascus, bacillus subtilis, bacillus megaterium, lactobacillus Beijerinc, absorb the composition after photodissociation, form biological sulphur zinc-manganese, then after adding chitin, resolve into a kind of melon powdery mildew nano-titanium of colloidal and biological sulphur zinc-manganese mixture.
2. the material of a kind of melon powdery mildew nano-titanium as claimed in claim 1 and the employing of biological sulphur zinc-manganese mixture is as follows:
1), material 1:60nm ball polymerization titanium 35%, sofril 15%, zinc sulphate 20%, manganese sulphate 25%, chitin 5%;
2), material 2: monascus is a, bacillus subtilis is a, bacillus megaterium is a, lactobacillus Beijerinc is a, 25% brown sugar water is a.
3. a kind of melon powdery mildew nano-titanium as claimed in claim 1 and biological sulphur zinc-manganese mixture adopt following processing step to make:
(A1), by Cosan, zinc sulphate, manganese sulphate put into after 60nm ball polymerization titanium dissolves, be positioned over photocatalysis Decomposition 2.5h under sunshine;
(A2), the microorganism of material 2 is put into brown sugar water and carry out enrichment culture 3d;
(A3), further by step 1) complete the material of photodissociation, put into step 2) complete in the fermentable still after enrichment culture; Drop into chitin again and carry out secondary fermentation, fermentation time is 7d; Namely a kind of melon powdery mildew nano-titanium and biological sulphur zinc-manganese mixture is obtained after having fermented.
CN201510589952.6A 2015-09-16 2015-09-16 Nano-titanium and biological-sulfur-zinc-manganese mixture for melon powdery mildew Pending CN105191987A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201510589952.6A CN105191987A (en) 2015-09-16 2015-09-16 Nano-titanium and biological-sulfur-zinc-manganese mixture for melon powdery mildew
PCT/CN2016/083490 WO2017045432A1 (en) 2015-09-16 2016-05-26 Nano-titanium and biological-sulfur-zinc-manganese mixture for melon powdery mildew

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Application Number Priority Date Filing Date Title
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CN113498781A (en) * 2021-08-16 2021-10-15 中国农业大学 Application of nano manganese dioxide in preventing and treating bacterial leaf blight of rice

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