CN105175382B - A kind of comprehensive processing and utilization method of purple potato - Google Patents

A kind of comprehensive processing and utilization method of purple potato Download PDF

Info

Publication number
CN105175382B
CN105175382B CN201510747216.9A CN201510747216A CN105175382B CN 105175382 B CN105175382 B CN 105175382B CN 201510747216 A CN201510747216 A CN 201510747216A CN 105175382 B CN105175382 B CN 105175382B
Authority
CN
China
Prior art keywords
filtrate
purple
potato
purple potato
anthocyanidin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201510747216.9A
Other languages
Chinese (zh)
Other versions
CN105175382A (en
Inventor
邹光友
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sichuan Guangyou Sweet Potato & Food Products Co Ltd
Original Assignee
Sichuan Guangyou Sweet Potato & Food Products Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sichuan Guangyou Sweet Potato & Food Products Co Ltd filed Critical Sichuan Guangyou Sweet Potato & Food Products Co Ltd
Priority to CN201510747216.9A priority Critical patent/CN105175382B/en
Publication of CN105175382A publication Critical patent/CN105175382A/en
Application granted granted Critical
Publication of CN105175382B publication Critical patent/CN105175382B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D311/00Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C07D311/60Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2
    • C07D311/62Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2 with oxygen atoms directly attached in position 3, e.g. anthocyanidins
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B30/00Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
    • C08B30/04Extraction or purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Preparation Of Fruits And Vegetables (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Cosmetics (AREA)

Abstract

The present invention provides a kind of comprehensive processing and utilization method of purple potato, comprises the following steps:Purple potato is cleaned, stripping and slicing, through defibrination, ultrasonic extraction, filtering, resin adsorption, filter to take to obtain resin and filtrate;Resin is through elution, concentration, dry anthocyanidin, concentrating filter liquor, dry starch.The present invention uses ultrasound assisted extraction technique, and uses resin adsorption, and obtained anthocyanidin purity is high-quality good, and anthocyanidin content is more than 9.1mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is more than 91%;Simultaneously using extract the waste liquid after anthocyanidin process starch in starch, gained purple sweet potato starch content be more than 98%, yield be purple potato total starch content more than 71%, improve the utilization rate of purple potato, more economic benefits can not only be brought, moreover it is possible to environmental protection.

Description

A kind of comprehensive processing and utilization method of purple potato
Technical field
The present invention relates to a kind of comprehensive processing and utilization method of purple potato, extracted more specifically to one kind from purple potato The method of anthocyanidin and starch.
Background technology
Purple potato is called black potato, and potato meat is in purple to darkviolet.Due to its rich in have protein, starch, pectin, cellulose, Amino acid, vitamin and several mineral materials, at home and abroad in the market situation of selling well, are liked by masses.Purple potato is nutritious, also has special Different healthcare function, wherein protein, amino acid is all easily by human consumption and absorption.The selenium being rich in is cancer-resisting substance;Cyanine Element is a kind of organic active polyphenoils, with anti-oxidant, anti-aging, antitumor, reducing blood lipid, improves a variety of work(such as immunity Effect;Vitamin A can improve the mucomembranous epithelial cell of eyesight and skin, collagen protein can be made normally to synthesize, and prevent and treat scorbutic Occur.
Anthocyanidin is the water-soluble natural pigment that the class of nature one is widely present in plant, belongs to flavonoids. It is the main color-generation material in plant petals, the multicoloured color such as water fruits and vegetables, flowers is largely associated therewith.Research It was found that, anthocyan material also with anti-oxidant, anti-inflammatory, reducing blood lipid, suppresses tumour life in addition to assigning the abundant color of plant Into and beautifying face and moistering lotion, improve the physiological function such as the colour of skin.In Europe, anthocyanidin is referred to as " oral cosmetics for skin ".Meanwhile, Anthocyanidin or a kind of safer natural pigment.Therefore, anthocyanidin is largely developed, people can be not only met to it as medicine The demand of thing, cosmetics and health food, and the use of alternative harmful synthetic food color.
At present, although the extraction process of purple sweet potato anthocyanin has a lot, but there is no technique by purple sweet potato starch while carrying Take, such as patent document CN103896901A discloses " method of extraction purification anthocyanidin from purple potato ", patent document CN102993154A is disclosed " a kind of extracting method of purple sweet potato anthocyanin ", and patent document CN104926778A discloses " a kind of The extraction process of purple sweet potato anthocyanin ", the utilization of the purple potato disclosed in these documents is simple blue and white plain extraction, causes purple Potato value is not high, adds the production cost of purple potato deep processing product.
The content of the invention
It is an object of the invention to solve at least the above and/or defect, and provide at least will be described later excellent Point.
A further object of the invention is that the extraction efficiency of anthocyanidin and starch is improved by ultrasonic extracting method, so as to Obtain more preferable purple potato processing and utilization method.
In order to realize that there is provided a kind of comprehensive processing and utilization side of purple potato according to object of the present invention and further advantage Method, it is characterised in that comprise the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 3~5 times;Will cleaning Purple potato afterwards is cut into 2~6mm3Purple potato fourth;
Step 2: add in fiberizer and carry out defibrination purple potato fourth and water, during defibrination, with 1~3 parts by weight/ Mass concentration is added fiberizer, defibrination to obtained grinding slurry by min rate of addition for 0.6~0.9% citric acid solution The granularity of middle particle is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 55~65 DEG C, 30~45min of ultrasonic extraction;Obtain after ultrasound Slurries;
Step 4: the slurries after ultrasound are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, filter residue is diluted with water, And it is heated to 55~65 DEG C, then 30~45min of ultrasonic extraction obtains filtrate by 100 mesh filter-cloth filterings, filtrate will close twice And;
Step 5: the filtrate after merging is cooled into 50~53 DEG C, resin is then added, stirring and adsorbing 1~2 hour, so Resin is filtered out using the nylon cloth filter bag of 80 mesh afterwards, filtrate is collected;The nylon cloth bag for filling resin is put into 50 DEG C of distillations Eluted three times in water, collect eluent;The mixing speed of the stirring and adsorbing is 300~500r/min;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/9~1/11;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is 0.04~0.12MPa of pressure, temperature -45~-65 DEG C condition, freeze-drying to moisture≤8%.
Preferably, in the step 2, the weight ratio of purple potato fourth and water is 1:10~15, purple potato fourth and citric acid are molten The weight ratio of liquid is 1:5~8.
Preferably, in the step 3, the volume ratio of grinding slurry and water is 1:3~5.
Preferably, in the step 3 and step 4, ultrasonic power regulating range is in 800~1500W, supersonic frequency In 25~50KHz.
Preferably, between the step 3 and step 4, in addition to take step 3 ultrasound after slurries in add second Alcohol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 2~5mL/min flow velocitys, utilize high-voltage pulse Electric field pre-processes 30~90min;The ethanol of the addition accounts for the 1/5~1/3 of slurry volume, acetic acid account for slurry volume 1/5~ 1/3。
Preferably, the parameter of the high-pressure pulse electric pretreatment is:15~30kV/cm of pulse strength, pulse width 60~120 μ s, pulse number 10~30, pulse spacing 300-500ms.
Preferably, in the step 4, take and acetic acid and ethanol are added in the slurries after filter residue ultrasonic extraction, then with 2 ~5mL/min flow velocitys are delivered in high-voltage pulse electric field processing chamber through peristaltic pump, using high-pressure pulse electric pretreatment 10~ 30min;The parameter of high-pressure pulse electric pretreatment is:15~30kV/cm of pulse strength, the μ s of pulse width 60~120, arteries and veins Rush number 10~30, pulse spacing 300-500ms;The ethanol of the addition accounts for the 1/5~1/3 of slurry volume, and acetic acid accounts for slurry The 1/5~1/3 of liquid product.
Preferably, in the step 5, resin is D101 type macroporous absorbent resins;The resin of the addition with merge after Filtrate weight ratio be 1:5~10.
Preferably, in the step 5, the mode for adding resin is to drip resin with 1~3 parts by weight/min speed It is added in the filtrate after merging.
Preferably, in the step 6, pressure when vacuum decker works is in 0.03~0.05MPa.
The present invention at least includes following beneficial effect:
(1) present invention is comprehensively utilized purple potato, and technique is simple, not only substantially increases economic benefit, also helps Improve environment, substantial amounts of can economize on resources, improve productivity effect;
(2) method of the invention is that raw material has synchronously obtained anthocyanidin and starch by ultrasonic extraction using purple potato, it is to avoid Largely the waste of the materials with very high edibility, improves the utilization rate of purple potato, reduces purple potato deep processing product Production cost;
(3) extracting method being combined using ultrasound and high-pressure pulse electric, improves the recovery rate of anthocyanidin and starch, Simultaneously using the extraction of middle temperature, freeze-drying is dried, mild condition, is farthest retained anthocyanidin and is not destroyed.
(4) present invention is more than 98% using the content of starch in purple sweet potato starch obtained by ultrasonic extraction, and yield is that purple potato is total More than the 71% of content of starch;Anthocyanidin content is more than 9.1mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is more than 91%, the content using starch in purple sweet potato starch obtained by the ultrasonic method being combined with high-pressure pulse electric is more than 96%, yield For more than the 77% of purple potato total starch content;Anthocyanidin content is more than 9.7mg/g, anthocyanidin recovery rate in gained purple sweet potato anthocyanin More than 95%.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification Word can be implemented according to this.
It should be appreciated that such as " having ", "comprising" and " comprising " term used herein do not allot one or many The presence or addition of individual other elements or its combination.
Embodiment 1:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 3 times;After cleaning Purple potato be cut into 2mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 10kg water are added in fiberizer, during defibrination, by 5kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.6% citric acid solution in 30min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 55 DEG C, ultrasonic extraction 30min;Obtain the slurries after ultrasound; The power of ultrasound is 800W, and supersonic frequency is 25KHz;The volume ratio of the grinding slurry and water is 1:3;
Step 4: the slurries after ultrasound are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, filter residue is diluted with water, And it is heated to 55 DEG C, then ultrasonic extraction 30min obtains filtrate by 100 mesh filter-cloth filterings, filtrate will merge twice;Ultrasound Power be 800W, supersonic frequency is 25KHz;
Step 5: the filtrate after merging is cooled into 50 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing 1 are then added Hour, then resin is filtered out using the nylon cloth filter bag of 80 mesh, filtrate is collected;The nylon cloth bag for filling resin is put into 50 Eluted three times in DEG C distilled water, collect eluent;The mixing speed of the stirring and adsorbing is 300r/min;After the merging The weight ratio of filtrate and D101 type macroporous absorbent resins is 5:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/9;Pressure when vacuum decker works is in 0.03MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.04MPa, -45 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 94% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 72%;Anthocyanidin content is 9.1mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 91% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 2:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 6mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 15kg water are added in fiberizer, during defibrination, by 8kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.9% citric acid solution in 60min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 65 DEG C, ultrasonic extraction 45min;Obtain the slurries after ultrasound; The power of ultrasound is 1500W, and supersonic frequency is 50KHz;The volume ratio of the grinding slurry and water is 1:5;
Step 4: the slurries after ultrasound are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, filter residue is diluted with water, And it is heated to 65 DEG C, then ultrasonic extraction 45min obtains filtrate by 100 mesh filter-cloth filterings, filtrate will merge twice;Ultrasound Power be 1500W, supersonic frequency is 50KHz;
Step 5: the filtrate after merging is cooled into 53 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing 2 are then added Hour, then resin is filtered out using the nylon cloth filter bag of 80 mesh, filtrate is collected;The nylon cloth bag for filling resin is put into 50 Eluted three times in DEG C distilled water, collect eluent;The mixing speed of the stirring and adsorbing is 500r/min;Filter after the merging The weight ratio of liquid and D101 type macroporous absorbent resins is 10:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/11;Pressure when vacuum decker works is in 0.05MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.12MPa, -65 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 93% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 71.8%;Anthocyanidin content is 9.2mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet The 92% of anthocyanidin contained by potato (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 3:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 4mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 12kg water are added in fiberizer, during defibrination, by 6kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.8% citric acid solution in 40min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 60 DEG C, ultrasonic extraction 35min;Obtain the slurries after ultrasound; The power of ultrasound is 1200W, and supersonic frequency is 28KHz;The volume ratio of the grinding slurry and water is 1:4;
Step 4: the slurries after ultrasound are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, filter residue is diluted with water, And it is heated to 60 DEG C, then ultrasonic extraction 35min obtains filtrate by 100 mesh filter-cloth filterings, filtrate will merge twice;Ultrasound Power be 1200W, supersonic frequency is 28KHz;
Step 5: the filtrate after merging is cooled into 51 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing are then added 1.5 hours, then resin is filtered out using the nylon cloth filter bag of 80 mesh, collect filtrate;The nylon cloth bag for filling resin is put Enter in 50 DEG C of distilled water and elute three times, collect eluent;The mixing speed of the stirring and adsorbing is 400r/min;After the merging The weight ratio of filtrate and D101 type macroporous absorbent resins be 8:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/10;Pressure when vacuum decker works is in 0.04MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition be pressure 0.08MPa, -50 DEG C of conditions of temperature, it is cold It is lyophilized dry to moisture≤8%;Content of starch is 93.5% in gained purple sweet potato starch, and yield is purple potato total starch content The 72.3% of (the starch-containing 25g of the light violet potatos of 100g);Anthocyanidin content is 9.3mg/g in gained purple sweet potato anthocyanin, and anthocyanidin is extracted Rate is the 93% of anthocyanidin contained by light violet potato (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 4:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 5mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 13kg water are added in fiberizer, during defibrination, by 7kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.7% citric acid solution in 50min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 62 DEG C, ultrasonic extraction 40min;Obtain the slurries after ultrasound; The power of ultrasound is 1300W, and supersonic frequency is 40KHz;The volume ratio of the grinding slurry and water is 1:4;
Step 4: the slurries after ultrasound are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, filter residue is diluted with water, And it is heated to 58 DEG C, then ultrasonic extraction 40min obtains filtrate by 100 mesh filter-cloth filterings, filtrate will merge twice;Ultrasound Power be 1300W, supersonic frequency is 40KHz;
Step 5: the filtrate after merging is cooled into 52 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing are then added 1.8 hours, then resin is filtered out using the nylon cloth filter bag of 80 mesh, collect filtrate;The nylon cloth bag for filling resin is put Enter in 50 DEG C of distilled water and elute three times, collect eluent;The mixing speed of the stirring and adsorbing is 450r/min;After the merging The weight ratio of filtrate and D101 type macroporous absorbent resins be 7:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/10;Pressure when vacuum decker works is in 0.04MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.1MPa, -55 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 94% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 73%;Anthocyanidin content is 9.3mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 92% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 5:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 5mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 13kg water are added in fiberizer, during defibrination, by 7kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.7% citric acid solution in 50min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 62 DEG C, ultrasonic extraction 40min;Obtain the slurries after ultrasound; The power of ultrasound is 1300W, and supersonic frequency is 40KHz;The volume ratio of the grinding slurry and water is 1:4;Take the slurries after ultrasound Middle addition ethanol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 2mL/min flow velocitys, utilize high pressure Impulse electric field pre-processes 30min;The ethanol of the addition accounts for the 1/5 of slurry volume, and acetic acid accounts for the 1/5 of slurry volume;The height Pressure impulse electric field pretreatment parameter be:Pulse strength 15kV/cm, the μ s of pulse width 60, pulse number 10, pulse spacing 300ms;
Step 4: the slurries after being handled through high-pressure pulse electric are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, will Filter residue is diluted with water, and is heated to 58 DEG C, and then ultrasonic extraction 40min obtains filtrate by 100 mesh filter-cloth filterings, will twice Filtrate merges;The power of ultrasound is 1300W, and supersonic frequency is 40KHz;
Step 5: the filtrate after merging is cooled into 52 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing are then added 1.8 hours, then resin is filtered out using the nylon cloth filter bag of 80 mesh, collect filtrate;The nylon cloth bag for filling resin is put Enter in 50 DEG C of distilled water and elute three times, collect eluent;The mixing speed of the stirring and adsorbing is 450r/min;After the merging The weight ratio of filtrate and D101 type macroporous absorbent resins be 7:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/10;Pressure when vacuum decker works is in 0.04MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.1MPa, -55 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 96% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 78%;Anthocyanidin content is 9.7mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 95% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 6:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 5mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 13kg water are added in fiberizer, during defibrination, by 7kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.7% citric acid solution in 50min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 62 DEG C, ultrasonic extraction 40min;Obtain the slurries after ultrasound; The power of ultrasound is 1300W, and supersonic frequency is 40KHz;The volume ratio of the grinding slurry and water is 1:4;Take the slurries after ultrasound Middle addition ethanol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 2mL/min flow velocitys, utilize high pressure Impulse electric field pre-processes 30min;The ethanol of the addition accounts for the 1/5 of slurry volume, and acetic acid accounts for the 1/5 of slurry volume;The height Pressure impulse electric field pretreatment parameter be:Pulse strength 15kV/cm, the μ s of pulse width 60, pulse number 10, pulse spacing 300ms;
Step 4: the slurries after being handled through high-pressure pulse electric are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, will Filter residue is diluted with water, and is heated to 58 DEG C, ultrasonic extraction 40min, takes and ethanol and acetic acid are added in the slurries after ultrasound, then with 2mL/min flow velocitys are delivered in high-voltage pulse electric field processing chamber through peristaltic pump, and 10min is pre-processed using high-pressure pulse electric;Institute The ethanol for stating addition accounts for the 1/5 of slurry volume, and acetic acid accounts for the 1/5 of slurry volume;The parameter of the high-pressure pulse electric pretreatment For:Pulse strength 15kV/cm, the μ s of pulse width 60, pulse number 10, pulse spacing 300ms;Then slurries are passed through 100 Mesh filter-cloth filtering obtains filtrate, filtrate will merge twice;The power of ultrasound is 1300W, and supersonic frequency is 40KHz;
Step 5: the filtrate after merging is cooled into 52 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing are then added 1.8 hours, then resin is filtered out using the nylon cloth filter bag of 80 mesh, collect filtrate;The nylon cloth bag for filling resin is put Enter in 50 DEG C of distilled water and elute three times, collect eluent;The mixing speed of the stirring and adsorbing is 450r/min;After the merging The weight ratio of filtrate and D101 type macroporous absorbent resins be 7:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/10;Pressure when vacuum decker works is in 0.04MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.1MPa, -55 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 98% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 80%;Anthocyanidin content is 10mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 97% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 7:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 4mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 12kg water are added in fiberizer, during defibrination, by 6kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.8% citric acid solution in 40min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 60 DEG C, ultrasonic extraction 35min;Obtain the slurries after ultrasound; The power of ultrasound is 1200W, and supersonic frequency is 28KHz;The volume ratio of the grinding slurry and water is 1:4;Take the slurries after ultrasound Middle addition ethanol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 5mL/min flow velocitys, utilize high pressure Impulse electric field pre-processes 90min;The ethanol of the addition accounts for the 1/3 of slurry volume, and acetic acid accounts for the 1/3 of slurry volume;The height Pressure impulse electric field pretreatment parameter be:Pulse strength 30kV/cm, the μ s of pulse width 120, pulse number 30, pulse spacing 500ms;
Step 4: the slurries that high-pressure pulse electric is handled obtain filtrate and filter residue by 100 mesh filter-cloth filterings, by filter residue It is diluted with water, and is heated to 60 DEG C, then ultrasonic extraction 35min obtains filtrate by 100 mesh filter-cloth filterings, will filtrate twice Merge;The power of ultrasound is 1200W, and supersonic frequency is 28KHz;
Step 5: the filtrate after merging is cooled into 51 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing are then added 1.5 hours, then resin is filtered out using the nylon cloth filter bag of 80 mesh, collect filtrate;The nylon cloth bag for filling resin is put Enter in 50 DEG C of distilled water and elute three times, collect eluent;The mixing speed of the stirring and adsorbing is 400r/min;It is described to merge The weight ratio of filtrate afterwards and D101 type macroporous absorbent resins is 8:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/10;Pressure when vacuum decker works is in 0.04MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.08MPa, -50 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 96% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 77%;Anthocyanidin content is 9.8mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 97% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 8:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 4mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 12kg water are added in fiberizer, during defibrination, by 6kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.8% citric acid solution in 40min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 60 DEG C, ultrasonic extraction 35min;Obtain the slurries after ultrasound; The power of ultrasound is 1200W, and supersonic frequency is 28KHz;The volume ratio of the grinding slurry and water is 1:4;Take the slurries after ultrasound Middle addition ethanol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 5mL/min flow velocitys, utilize high pressure Impulse electric field pre-processes 90min;The ethanol of the addition accounts for the 1/3 of slurry volume, and acetic acid accounts for the 1/3 of slurry volume;The height Pressure impulse electric field pretreatment parameter be:Pulse strength 30kV/cm, the μ s of pulse width 120, pulse number 30, pulse spacing 500ms;
Step 4: the slurries that high-pressure pulse electric is handled obtain filtrate and filter residue by 100 mesh filter-cloth filterings, by filter residue It is diluted with water, and is heated to 60 DEG C, ultrasonic extraction 35min takes and ethanol and acetic acid are added in the slurries after ultrasound, then with 5mL/ Min flow velocitys are delivered in high-voltage pulse electric field processing chamber through peristaltic pump, and 30min is pre-processed using high-pressure pulse electric;It is described to add The ethanol entered accounts for the 1/3 of slurry volume, and acetic acid accounts for the 1/3 of slurry volume;The parameter of high-pressure pulse electric pretreatment is:Arteries and veins Rush intensity 30kV/cm, the μ s of pulse width 120, pulse number 30, pulse spacing 500ms;Then slurries are filtered by 100 mesh Cloth is filtrated to get filtrate, filtrate will merge twice;The power of ultrasound is 1200W, and supersonic frequency is 28KHz;
Step 5: the filtrate after merging is cooled into 51 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing are then added 1.5 hours, then resin is filtered out using the nylon cloth filter bag of 80 mesh, collect filtrate;The nylon cloth bag for filling resin is put Enter in 50 DEG C of distilled water and elute three times, collect eluent;The mixing speed of the stirring and adsorbing is 400r/min;After the merging The weight ratio of filtrate and D101 type macroporous absorbent resins be 8:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/10;Pressure when vacuum decker works is in 0.04MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.08MPa, -50 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 98% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 80%;Anthocyanidin content is 11mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 98% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 9:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 6mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 15kg water are added in fiberizer, during defibrination, by 8kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.9% citric acid solution in 60min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 65 DEG C, ultrasonic extraction 45min;Obtain the slurries after ultrasound; The power of ultrasound is 1500W, and supersonic frequency is 50KHz;The volume ratio of the grinding slurry and water is 1:5;Take the slurries after ultrasound Middle addition ethanol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 3mL/min flow velocitys, utilize high pressure Impulse electric field pre-processes 60min;The ethanol of the addition accounts for the 1/4 of slurry volume, and acetic acid accounts for the 1/4 of slurry volume;The height Pressure impulse electric field pretreatment parameter be:Pulse strength 20kV/cm, the μ s of pulse width 80, pulse number 20, pulse spacing 400ms;
Step 4: the slurries that high-pressure pulse electric is handled obtain filtrate and filter residue by 100 mesh filter-cloth filterings, by filter residue It is diluted with water, and is heated to 65 DEG C, then ultrasonic extraction 45min obtains filtrate by 100 mesh filter-cloth filterings, will filtrate twice Merge;The power of ultrasound is 1500W, and supersonic frequency is 50KHz;
Step 5: the filtrate after merging is cooled into 53 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing 2 are then added Hour, then resin is filtered out using the nylon cloth filter bag of 80 mesh, filtrate is collected;The nylon cloth bag for filling resin is put into 50 Eluted three times in DEG C distilled water, collect eluent;The mixing speed of the stirring and adsorbing is 500r/min;Filter after the merging The weight ratio of liquid and D101 type macroporous absorbent resins is 10:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/11;Pressure when vacuum decker works is in 0.05MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.12MPa, -65 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 96% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 78%;Anthocyanidin content is 9.9mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 97% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
Embodiment 10:
A kind of comprehensive processing and utilization method of purple potato, comprises the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 5 times;After cleaning Purple potato be cut into 6mm3Purple potato fourth;
Defibrination is carried out Step 2: 1kg purple potatos fourth and 15kg water are added in fiberizer, during defibrination, by 8kg matter Amount concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.9% citric acid solution in 60min Degree is less than 20 μm, obtains grinding slurry;
Step 3: grinding slurry is diluted with water, and it is heated to 65 DEG C, ultrasonic extraction 45min;Obtain the slurries after ultrasound; The power of ultrasound is 1500W, and supersonic frequency is 50KHz;The volume ratio of the grinding slurry and water is 1:5;Take the slurries after ultrasound Middle addition ethanol and acetic acid, are then delivered in high-voltage pulse electric field processing chamber through peristaltic pump with 3mL/min flow velocitys, utilize high pressure Impulse electric field pre-processes 60min;The ethanol of the addition accounts for the 1/4 of slurry volume, and acetic acid accounts for the 1/4 of slurry volume;The height Pressure impulse electric field pretreatment parameter be:Pulse strength 20kV/cm, the μ s of pulse width 80, pulse number 20, pulse spacing 400ms;
Step 4: the slurries that high-pressure pulse electric is handled obtain filtrate and filter residue by 100 mesh filter-cloth filterings, by filter residue It is diluted with water, and is heated to 65 DEG C, ultrasonic extraction 45min takes and ethanol and acetic acid are added in the slurries after ultrasound, then with 5mL/ Min flow velocitys are delivered in high-voltage pulse electric field processing chamber through peristaltic pump, and 20min is pre-processed using high-pressure pulse electric;It is described to add The ethanol entered accounts for the 1/4 of slurry volume, and acetic acid accounts for the 1/4 of slurry volume;The parameter of high-pressure pulse electric pretreatment is:Arteries and veins Rush intensity 20kV/cm, the μ s of pulse width 80, pulse number 20, pulse spacing 400ms;Then slurries are passed through into 100 mesh filter clothes Filtrate is filtrated to get, filtrate will be merged twice;The power of ultrasound is 1500W, and supersonic frequency is 50KHz;
Step 5: the filtrate after merging is cooled into 53 DEG C, D101 type macroporous absorbent resins, stirring and adsorbing 2 are then added Hour, then resin is filtered out using the nylon cloth filter bag of 80 mesh, filtrate is collected;The nylon cloth bag for filling resin is put into 50 Eluted three times in DEG C distilled water, collect eluent;The mixing speed of the stirring and adsorbing is 500r/min;Filter after the merging The weight ratio of liquid and D101 type macroporous absorbent resins is 10:1;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, condensation product Accumulate to original 1/11;Pressure when vacuum decker works is in 0.05MPa;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, the filtrate of concentration will be passed through Purple sweet potato starch is made by pneumatic conveying drying;The vacuum freeze drying condition is pressure 0.12MPa, -65 DEG C of conditions of temperature, freezing Dry to moisture≤8%;Content of starch is 98% in gained purple sweet potato starch, and yield is that (100g is fresh for purple potato total starch content The starch-containing 25g of purple potato) 81%;Anthocyanidin content is 10mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is light violet potato The 98% of contained anthocyanidin (the light violet potatos of 100g contain anthocyanidin 98mg).
It was found from embodiment 1~10, by the method for the present invention, the content of starch is more than 98% in gained purple sweet potato starch, Yield is more than the 71% of purple potato total starch content;Anthocyanidin content is more than 9.1mg/g in gained purple sweet potato anthocyanin, and anthocyanidin is carried Rate is taken to be more than 91%, it is worth mentioning at this point that, when consistent with method using other parameters, as embodiment 4 compares with embodiment 5 and 6 Compared with, the slurries after ultrasound are carried out after high-pressure pulse electric processing, content of starch is 96% in the gained purple sweet potato starch of embodiment 5, Yield is the 78% of purple potato total starch content (the starch-containing 25g of the light violet potatos of 100g);Anthocyanidin content is in gained purple sweet potato anthocyanin 9.7mg/g, anthocyanidin recovery rate is the 95% of anthocyanidin contained by light violet potato (the light violet potatos of 100g contain anthocyanidin 98mg), embodiment 6 Content of starch is 98% in gained purple sweet potato starch, and yield is the 80% of purple potato total starch content (the starch-containing 25g of the light violet potatos of 100g); Anthocyanidin content is 10mg/g in gained purple sweet potato anthocyanin, and anthocyanidin recovery rate is (the light violet potatos of 100g of anthocyanidin contained by light violet potato Containing anthocyanidin 98mg) 97%, its effect is apparently higher than embodiment 4;Same contrast exists in embodiment 3 and embodiment 7 Between 8, embodiment 2 and embodiment 9 and 10.It can be seen that use high-pressure pulse electric can improve starch and anthocyanidin in purple potato Recovery rate, is conducive to the comprehensive processing and utilization of purple potato.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed With.It can be applied to various suitable the field of the invention completely., can be easily for those skilled in the art Realize other modification.Therefore under the universal limited without departing substantially from claim and equivalency range, the present invention is not limited In specific details and shown here as the example with description.

Claims (5)

1. a kind of comprehensive processing and utilization method of purple potato, it is characterised in that comprise the following steps:
Step 1: taking fresh purple potato to remove small holes caused by worms, damage, dirt and miscellaneous palpus, then cleaned with water 3~5 times;After cleaning Purple potato is cut into 2~6mm3Purple potato fourth;
Step 2: being 1 by weight ratio:10~15 purple potato fourth and water adds in fiberizer and carries out defibrination, during defibrination, Mass concentration is added dropwise to fiberizer, the particle of defibrination particle into obtained grinding slurry for 0.6~0.9% citric acid solution Degree is less than 20 μm, obtains grinding slurry;The time for adding of the citric acid solution is 30~60min;The purple potato fourth and citric acid The weight ratio of solution is 1:5~8;
Step 3: grinding slurry is diluted with water, and it is heated to 55~65 DEG C, 30~45min of ultrasonic extraction;Obtain the slurry after ultrasound Liquid;Take and ethanol and acetic acid are added in the slurries after ultrasound, high-voltage pulse is then delivered to through peristaltic pump with 2~5mL/min flow velocitys In electric field processing chamber, 30~90min is pre-processed using high-pressure pulse electric;The ethanol of the addition account for slurry volume 1/5~ 1/3, acetic acid accounts for the 1/5~1/3 of slurry volume;The parameter of high-pressure pulse electric pretreatment is:15~30kV/ of pulse strength Cm, the μ s of pulse width 60~120, pulse number 10~30, pulse spacing 300-500ms;The volume of the grinding slurry and water Than for 1:3~5;The power regulating range of ultrasound is in 800~1500W, and supersonic frequency is in 25~50KHz;
Step 4: the slurries after ultrasound are obtained into filtrate and filter residue by 100 mesh filter-cloth filterings, filter residue is diluted with water, and added Heat is to 55~65 DEG C, and then 30~45min of ultrasonic extraction obtains filtrate by 100 mesh filter-cloth filterings, filtrate will merge twice; The power regulating range of ultrasound is in 800~1500W, and supersonic frequency is in 25~50KHz;
Step 5: the filtrate after merging is cooled into 50~53 DEG C, resin is then added, then stirring and adsorbing 1~2 hour adopts Resin is filtered out with the nylon cloth filter bag of 80 mesh, filtrate is collected;The nylon cloth bag for filling resin is put into 50 DEG C of distilled water Elution three times, collects eluent;The mixing speed of the stirring and adsorbing is 300~500r/min;
Step 6: the filtrate that step 5 is collected and eluent are concentrated inside vacuum decker respectively, concentration volume is extremely Originally 1/9~1/11;
Step 7: purple sweet potato anthocyanin will be made by the eluent vacuum freeze drying of concentration, it will be passed through by the filtrate of concentration Purple sweet potato starch is made in pneumatic conveying drying;The vacuum freeze drying condition is 0.04~0.12MPa of pressure, temperature -45~-65 DEG C bar Part, freeze-drying to moisture≤8%.
2. the comprehensive processing and utilization method of purple potato as claimed in claim 1, it is characterised in that in the step 4, takes filter residue to surpass Ethanol and acetic acid are added in slurries after sound extraction, high-pressure pulse electric is then delivered to through peristaltic pump with 2~5mL/min flow velocitys In process chamber, 10~30min is pre-processed using high-pressure pulse electric;The parameter of high-pressure pulse electric pretreatment is:Pulse 15~30kV/cm of intensity, the μ s of pulse width 60~120, pulse number 10~30, pulse spacing 300-500ms;It is described to add Ethanol account for the 1/5~1/3 of slurry volume, acetic acid accounts for the 1/5~1/3 of slurry volume.
3. the comprehensive processing and utilization method of purple potato as claimed in claim 1, it is characterised in that in the step 5, resin is D101 type macroporous absorbent resins;The resin of the addition with merge after filtrate weight ratio be 1:5~10.
4. the comprehensive processing and utilization method of purple potato as claimed in claim 1, it is characterised in that in the step 5, adds resin Mode be by resin be added drop-wise to merge after filtrate in;The time for adding of the resin is 20~50min.
5. the comprehensive processing and utilization method of purple potato as claimed in claim 1, it is characterised in that in the step 6, is concentrated in vacuo Pressure when machine works is in 0.03~0.05MPa.
CN201510747216.9A 2015-11-06 2015-11-06 A kind of comprehensive processing and utilization method of purple potato Active CN105175382B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510747216.9A CN105175382B (en) 2015-11-06 2015-11-06 A kind of comprehensive processing and utilization method of purple potato

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510747216.9A CN105175382B (en) 2015-11-06 2015-11-06 A kind of comprehensive processing and utilization method of purple potato

Publications (2)

Publication Number Publication Date
CN105175382A CN105175382A (en) 2015-12-23
CN105175382B true CN105175382B (en) 2017-08-22

Family

ID=54897900

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510747216.9A Active CN105175382B (en) 2015-11-06 2015-11-06 A kind of comprehensive processing and utilization method of purple potato

Country Status (1)

Country Link
CN (1) CN105175382B (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106579423A (en) * 2016-11-24 2017-04-26 青岛大学 Comprehensive extraction method for various effective components in purple sweet potatoes
CN110651894A (en) * 2019-10-31 2020-01-07 上海耐威克宠物用品有限公司 Pet health product for improving immunity and preparation method thereof
CN114107417A (en) * 2021-12-02 2022-03-01 武汉轻工大学 Blood sugar reducing polypeptide based on enzymolysis of purple sweet potato protein polyphenol compound, preparation method and application
CN114098083A (en) * 2021-12-02 2022-03-01 武汉轻工大学 Purple sweet potato ingredient and preparation method and application thereof
CN113951519A (en) * 2021-12-03 2022-01-21 武汉轻工大学 Purple sweet potato protein polyphenol compound and preparation method and application thereof

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102174606B (en) * 2011-03-07 2014-01-29 江苏省农业科学院 Combined extraction method of blackberry seed oil and anthocyanin in blackberry juice production byproducts
CN102786506B (en) * 2011-05-19 2015-04-22 长沙康隆生物制品有限公司 Technology for rapidly preparing 25% anthocyanidins from cowberry
CN103896901A (en) * 2013-12-24 2014-07-02 合肥中科小陶食品有限公司 Method for extracting purified anthocyanin from purple sweet potatoes
CN103880804B (en) * 2014-03-20 2015-12-02 江苏大学 A kind of method of anthocyanidin in extraction and isolation purple sweet potato powder
CN104130333B (en) * 2014-07-21 2016-09-07 天津商业大学 Utilize purple potato synchronous production anthocyanidin, starch, cellulose and method of protein

Also Published As

Publication number Publication date
CN105175382A (en) 2015-12-23

Similar Documents

Publication Publication Date Title
CN105175382B (en) A kind of comprehensive processing and utilization method of purple potato
CN102675317B (en) Method for extracting a plurality of kinds of active ingredients from tea leaves simultaneously
CN105011160A (en) Eucommia ulmoides leaf and wild chrysanthemum flower nutritional powder processing method
CN105111325B (en) A kind of continuous method for extracting polysaccharide, protein and dietary fiber in pin from needle mushroom
CN104829734B (en) A kind of method of utilization dried thin mushroom production pigment, albumen, polysaccharide and dietary fiber
CN105998139B (en) A method of flavones is extracted from Sweet Potato Leaf
CN105111177B (en) Method for extracting procyanidine from peony hulls
CN104490954B (en) A kind of extracting method of Moringa
CN105037572B (en) A kind of method that burdock polysaccharide is extracted from radix bardanae
CN101319095B (en) Microwave extraction method for purple cabbage haematochrome
CN103783236A (en) Low-sugar preserved plum preparation method
CN103788218A (en) Decomposition and extraction method of active ingredients in purple sweet potatoes
CN103073914B (en) Method for extracting maize yellow pigment from maize protein
CN109134691A (en) A kind of method of high efficiency extraction Polysaccharide in Pleurotus eryngii
CN107573438A (en) A kind of method that polysaccharide is extracted in the pericarp from passion fruit
CN102911514B (en) Method for extracting pigment from tangerine peel
CN108570031A (en) A kind of extracting method of lycium ruthenicum anthocyanidin
CN105838106A (en) Ultrahigh-pressure extraction method for pigment in fruit and vegetable
CN103194346A (en) Production method of pitaya and grape composite fruit vine
CN101444318B (en) Process for producing high-luminousness olive clear-juice beverage
CN109180829A (en) A kind of preparation method and application of Pueraria Flavonid and polyoses extract
CN110180216B (en) Method and device for extracting and purifying anthocyanin by ultrasonic-enhanced fluidized bed type resin adsorption-desorption
CN104131060B (en) Corbicula fluminea anti-oxidative peptide and preparation method thereof
CN101973920B (en) Method for extracting carotenoid from physalis persistent calyx
CN101433322B (en) Functional food rich in anthocyanidin and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Comprehensive processing and utilization method of purple sweet potatoes

Effective date of registration: 20180620

Granted publication date: 20170822

Pledgee: Agricultural Bank of China, Limited by Share Ltd, Mianyang branch

Pledgor: Sichuan Guangyou Sweet Potato & Food Products Co., Ltd.|Zou Guangyou

Registration number: 2018510000063

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20190815

Granted publication date: 20170822

Pledgee: Agricultural Bank of China, Limited by Share Ltd, Mianyang branch

Pledgor: Sichuan Guangyou Sweet Potato & Food Products Co., Ltd.

Registration number: 2018510000063