CN105174925A - Ceramic thin plate material and preparation method thereof - Google Patents

Ceramic thin plate material and preparation method thereof Download PDF

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Publication number
CN105174925A
CN105174925A CN201510552340.XA CN201510552340A CN105174925A CN 105174925 A CN105174925 A CN 105174925A CN 201510552340 A CN201510552340 A CN 201510552340A CN 105174925 A CN105174925 A CN 105174925A
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China
Prior art keywords
parts
slab
thin plate
preparation
ceramic thin
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CN201510552340.XA
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Chinese (zh)
Inventor
赵文刚
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TAICANG SHUNRUCHENG BUILDING MATERIALS Co Ltd
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TAICANG SHUNRUCHENG BUILDING MATERIALS Co Ltd
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Priority to CN201510552340.XA priority Critical patent/CN105174925A/en
Publication of CN105174925A publication Critical patent/CN105174925A/en
Pending legal-status Critical Current

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Abstract

The present invention discloses a ceramic thin plate material and a preparation method thereof, wherein the raw materials comprise, by weight, 30-40 parts of sodium sand, 15-25 parts of porcelain stone, 5-10 parts of limestone, 8-15 parts of kaolin, 1-10 parts of wollastonite, 1-5 parts of needle-like mullite, 3-8 parts of bentonite, 2-10 parts of potassium and sodium feldspar, and 0.5-3 parts of zinc oxide. The preparation method comprises: a, weighing various raw materials according to the weight part ratio, and crushing to prepare a powder material; b, carrying out vacuum extruding on the powder material prepared in the step a to form a plate billet; c, carrying out multiple rolling extruding on the obtained plate billet; d, carrying out microwave drying on the cut plate billet, and then carrying out low temperature biscuit firing; and e, carrying out late-stage processing on the fired plate billet, and then carrying out grading packaging. According to the present invention, the material has characteristics of reasonable formula, simple preparation, effective water absorption reducing, toughness improving, impact resistance improving and excellent mechanical property, and the method has characteristics of production efficiency improving, production cost reducing, and good market prospect.

Description

A kind of ceramic thin plate material and preparation method thereof
Technical field
The present invention relates to architectural decoration material field, be specifically related to a kind of ceramic thin plate material and preparation method thereof.
Background technology
In modern architecture repairs profession, along with the raising of housing industrialization and living standards of the people, the share of market of high-quality, multifunction green building material product will expand gradually, the diversification of production development trend, personalization, fashion-orientation, environment protection health.For adapting to the requirement of society people, various Novel decoration material arises at the historic moment, and each product is more and more tending towards nature, elegance, tool personality elements from early stage ornamental decorative effect to today.
Ceramic thin plate is a kind of high-quality green building material, and it has, and various in style, pattern is abundant, good decorating effect, easily maintain, and product pattern is naturally true to nature, is deeply subject to consumers.Wherein large-sized ceramic tiles is due to economical, attractive in appearance, and color is wide in variety and be widely adopted on decorative wall, cylinder.Occupy very large market ratio in developed countries such as America and Europes, but in China, existing market acceptance level is still not high.Major cause is because current commercially ceramic thin plate can not get good guarantee in toughness and intensity, and complex manufacturing, and cost drops into high, therefore product price, human consumer can not accept.
Therefore, for the problems referred to above, the present invention proposes a kind of new technical scheme.
Summary of the invention
The object of this invention is to provide a kind of intensity good, technique advantages of simple, ceramic thin plate material reducing production cost and preparation method thereof.
The present invention is achieved through the following technical solutions:
A kind of ceramic thin plate material, comprises the raw material composition of following parts by weight: 30 ~ 40 parts, sodium sand, porcelain stone 15 ~ 25 parts, 5 ~ 10 parts, Wingdale, kaolin 8 ~ 15 parts, wollastonite 1 ~ 10 part, acicular mullite 1 ~ 5 part, wilkinite 3 ~ 8 parts, potassium albite 2 ~ 10 parts, 0.5 ~ 3 part, zinc oxide.
A preparation method for ceramic thin plate material, comprises the following steps:
A, take various raw material according to above-mentioned raw materials parts by weight proportioning, by described various raw material pulverizing, then Homogeneous phase mixing, makes powder;
B, vacuum extrusion is carried out to the powder prepared in step a become slab;
C, vacuum extrusion complete, carry out edging pressure to gained slab, first time is 18 ~ 25mm to the thickness of slab after edging pressure, second time is 8 ~ 12mm to the thickness of slab after edging pressure, after 3rd pair of edging pressure, the thickness of slab is 5 ~ 8mm, after edging pressure is terminated, slab is cut into required length and width;
D, carry out microwave drying to the slab of well cutting, after dry, base substrate moisture controlled is 2 ~ 8%, and dried slab is carried out low temperature biscuiting, and temperature controls at 800 ~ 900 DEG C, and the biscuiting time is 45 ~ 60min;
E, post-production is carried out to the slab of biscuiting, then carry out secondary cut, finally divide grade packaged.
Further, described zinc oxide available alumina replaces.
Further, described slab is no less than to three times rolling extrusion process.
Further, described post-treatment comprises pouring glaze, stamp, glaze firing and cutting and polishing.
The invention has the beneficial effects as follows: the present invention fills a prescription rationally, preparation is simple, significantly reduces the water-intake rate of material, improve toughness and the shock resistance of material simultaneously, have excellent mechanical property, and improve preparation efficiency, reduce production cost, there are good market outlook.
Embodiment
Below in conjunction with embodiment, the present invention is described further.
Embodiment 1
A kind of ceramic thin plate material, comprises the raw material composition of following parts by weight: husky 30 parts of sodium, porcelain stone 15 parts, 5 parts, Wingdale, kaolin 8 parts, wollastonite 1 part, acicular mullite 1 part, wilkinite 3 parts, potassium albite 2 ~ 10 parts, 0.5 part, zinc oxide.
A preparation method for ceramic thin plate material, comprises the following steps:
A, take various raw material according to above-mentioned raw materials parts by weight proportioning, by described various raw material pulverizing, then Homogeneous phase mixing, makes powder;
B, vacuum extrusion is carried out to the powder prepared in step a become slab;
C, vacuum extrusion complete, and carry out edging pressure to gained slab, and first time is 18mm to the thickness of slab after edging pressure, second time is 8mm to the thickness of slab after edging pressure, after 3rd pair of edging pressure, the thickness of slab is 5mm, after terminating, slab is cut into required length and width to edging pressure;
D, carry out microwave drying to the slab of well cutting, after dry, base substrate moisture controlled is 2%, and dried slab is carried out low temperature biscuiting, and temperature controls at 800 DEG C, and the biscuiting time is 45min;
E, post-production is carried out to the slab of biscuiting, then carry out secondary cut, finally divide grade packaged.
Embodiment 2
A kind of ceramic thin plate material, comprises the raw material composition of following parts by weight: husky 35 parts of sodium, porcelain stone 20 parts, 8 parts, Wingdale, kaolin 10 parts, wollastonite 5 parts, acicular mullite 3 parts, wilkinite 5 parts, potassium albite 6 parts, 1.5 parts, aluminum oxide.
A preparation method for ceramic thin plate material, comprises the following steps:
A, take various raw material according to above-mentioned raw materials parts by weight proportioning, by described various raw material pulverizing, then Homogeneous phase mixing, makes powder;
B, vacuum extrusion is carried out to the powder prepared in step a become slab;
C, vacuum extrusion complete, carry out edging pressure to gained slab, first time is 20mm to the thickness of slab after edging pressure, second time is 10mm to the thickness of slab after edging pressure, after 3rd pair of edging pressure, the thickness of slab is 6mm, after edging pressure is terminated, slab is cut into required length and width;
D, carry out microwave drying to the slab of well cutting, after dry, base substrate moisture controlled is 5%, and dried slab is carried out low temperature biscuiting, and temperature controls at 850 DEG C, and the biscuiting time is 50min;
E, post-production is carried out to the slab of biscuiting, then carry out secondary cut, finally divide grade packaged.
Embodiment 3
A kind of ceramic thin plate material, comprises the raw material composition of following parts by weight: husky 40 parts of sodium, porcelain stone 25 parts, 10 parts, Wingdale, kaolin 15 parts, wollastonite 10 parts, acicular mullite 5 parts, wilkinite 8 parts, potassium albite 10 parts, 3 parts, zinc oxide.
A preparation method for ceramic thin plate material, comprises the following steps:
A, take various raw material according to above-mentioned raw materials parts by weight proportioning, by described various raw material pulverizing, then Homogeneous phase mixing, makes powder;
B, vacuum extrusion is carried out to the powder prepared in step a become slab;
C, vacuum extrusion complete, carry out edging pressure to gained slab, first time is 25mm to the thickness of slab after edging pressure, second time is 12mm to the thickness of slab after edging pressure, after 3rd pair of edging pressure, the thickness of slab is 8mm, after edging pressure is terminated, slab is cut into required length and width;
D, carry out microwave drying to the slab of well cutting, after dry, base substrate moisture controlled is 8%, and dried slab is carried out low temperature biscuiting, and temperature controls at 900 DEG C, and the biscuiting time is 60min;
E, post-production is carried out to the slab of biscuiting, then carry out secondary cut, finally divide grade packaged.
The present invention fills a prescription rationally, and preparation is simple, significantly reduces the water-intake rate of material, improves toughness and the shock resistance of material simultaneously, has excellent mechanical property, and improves preparation efficiency, reduce production cost, have good market outlook.
Although above-mentioned, the specific embodiment of the present invention is described; but not limiting the scope of the invention; on the basis of technical scheme of the present invention, those skilled in the art do not need to pay various amendment or distortion that creative work can make still within protection scope of the present invention.

Claims (5)

1. a ceramic thin plate material, it is characterized in that: the raw material composition comprising following parts by weight: 30 ~ 40 parts, sodium sand, porcelain stone 15 ~ 25 parts, 5 ~ 10 parts, Wingdale, kaolin 8 ~ 15 parts, wollastonite 1 ~ 10 part, acicular mullite 1 ~ 5 part, wilkinite 3 ~ 8 parts, potassium albite 2 ~ 10 parts, 0.5 ~ 3 part, zinc oxide.
2. the preparation method of a kind of ceramic thin plate material according to claim 1, is characterized in that: comprise the following steps:
A, take various raw material according to above-mentioned raw materials parts by weight proportioning, by described various raw material pulverizing, then Homogeneous phase mixing, makes powder;
B, vacuum extrusion is carried out to the powder prepared in step a become slab;
C, vacuum extrusion complete, carry out edging pressure to gained slab, first time is 18 ~ 25mm to the thickness of slab after edging pressure, second time is 8 ~ 12mm to the thickness of slab after edging pressure, after 3rd pair of edging pressure, the thickness of slab is 5 ~ 8mm, after edging pressure is terminated, slab is cut into required length and width;
D, carry out microwave drying to the slab of well cutting, after dry, base substrate moisture controlled is 2 ~ 8%, and dried slab is carried out low temperature biscuiting, and temperature controls at 800 ~ 900 DEG C, and the biscuiting time is 45 ~ 60min;
E, post-production is carried out to the slab of biscuiting, then carry out secondary cut, finally divide grade packaged.
3. a kind of ceramic thin plate material according to claim 1, is characterized in that: described zinc oxide available alumina replaces.
4. the preparation method of a kind of ceramic thin plate material according to claim 2, is characterized in that: described slab is no less than to three times rolling extrusion process.
5. the preparation method of a kind of ceramic thin plate material according to claim 2, is characterized in that: described post-treatment comprises and drenches glaze, stamp, glaze firing and cutting and polishing.
CN201510552340.XA 2015-09-02 2015-09-02 Ceramic thin plate material and preparation method thereof Pending CN105174925A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108238783A (en) * 2016-12-27 2018-07-03 中磊企业集团装饰有限公司 A kind of production technology of artificial marble ceramic glazed thin plate
CN109020212A (en) * 2018-09-20 2018-12-18 河南省钧艺照明灯具有限公司 It is a kind of to watch lamps and lanterns and preparation method thereof suitable for outdoor ceramics
CN111098400A (en) * 2019-12-27 2020-05-05 深圳须弥云图空间科技有限公司 Manufacturing method of wave wire bonding floor tile and wave wire bonding floor tile
CN112062546A (en) * 2020-08-11 2020-12-11 广东嘉联企业陶瓷有限公司 6 mm porcelain thin rock plate and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102173760A (en) * 2011-02-17 2011-09-07 山东德惠来装饰瓷板有限公司 Method for manufacturing large silicon oxide ceramic sheet
CN104355607A (en) * 2014-10-16 2015-02-18 佛山市禾才科技服务有限公司 High-strength semitransparent ceramic sheet and preparation method thereof
CN104355651A (en) * 2014-10-16 2015-02-18 佛山市禾才科技服务有限公司 High-strength semitransparent ceramic material and preparation method of ceramic sheet

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102173760A (en) * 2011-02-17 2011-09-07 山东德惠来装饰瓷板有限公司 Method for manufacturing large silicon oxide ceramic sheet
CN104355607A (en) * 2014-10-16 2015-02-18 佛山市禾才科技服务有限公司 High-strength semitransparent ceramic sheet and preparation method thereof
CN104355651A (en) * 2014-10-16 2015-02-18 佛山市禾才科技服务有限公司 High-strength semitransparent ceramic material and preparation method of ceramic sheet

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
中国硅酸盐学会陶瓷分会建筑卫生陶瓷专业委员会: "《现代建筑卫生陶瓷工程师手册》", 31 August 1998, 中国建材工业出版社 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108238783A (en) * 2016-12-27 2018-07-03 中磊企业集团装饰有限公司 A kind of production technology of artificial marble ceramic glazed thin plate
CN109020212A (en) * 2018-09-20 2018-12-18 河南省钧艺照明灯具有限公司 It is a kind of to watch lamps and lanterns and preparation method thereof suitable for outdoor ceramics
CN111098400A (en) * 2019-12-27 2020-05-05 深圳须弥云图空间科技有限公司 Manufacturing method of wave wire bonding floor tile and wave wire bonding floor tile
CN111098400B (en) * 2019-12-27 2022-02-08 深圳须弥云图空间科技有限公司 Manufacturing method of wave wire bonding floor tile and wave wire bonding floor tile
CN112062546A (en) * 2020-08-11 2020-12-11 广东嘉联企业陶瓷有限公司 6 mm porcelain thin rock plate and preparation method thereof

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Application publication date: 20151223