CN105076227A - Method for preparing mosquito eradication granules by virtue of wheat straws - Google Patents

Method for preparing mosquito eradication granules by virtue of wheat straws Download PDF

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Publication number
CN105076227A
CN105076227A CN201510539596.7A CN201510539596A CN105076227A CN 105076227 A CN105076227 A CN 105076227A CN 201510539596 A CN201510539596 A CN 201510539596A CN 105076227 A CN105076227 A CN 105076227A
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China
Prior art keywords
wheat stalk
add
particle
wheat
stalk particle
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CN201510539596.7A
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Chinese (zh)
Inventor
雷思宇
王志慧
宋国
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CHANGZHOU SIYU ENVIRONMENTAL PROTECTION MATERIAL TECHNOLOGY Co Ltd
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CHANGZHOU SIYU ENVIRONMENTAL PROTECTION MATERIAL TECHNOLOGY Co Ltd
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Priority to CN201510539596.7A priority Critical patent/CN105076227A/en
Publication of CN105076227A publication Critical patent/CN105076227A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to a method for preparing mosquito eradication granules by virtue of wheat straws, belongs to the field of mosquito prevention, and aims to overcome the shortcoming that diseases such as asthma are probably induced by substances harmful to human bodies in smoke produced by combustion of a conventional mosquito eradication substance. The method comprises the following steps of mixing and stirring carbonized wheat straw pellets and quisqualis indica in a sealing manner, adding absolute ethyl alcohol, permethrin, silica gel and lactic acid, adding carbon dioxide, and performing stirring, filtering and air-drying. The method is simple and convenient to operate, and the mosquito eradication granules have remarkable mosquito eradication effects, and are nontoxic and harmless to human bodies after being combusted.

Description

A kind of method utilizing wheat stalk to prepare killing mosquitoes particle
Technical field
The present invention relates to a kind of method utilizing wheat stalk to prepare killing mosquitoes particle, belong to insect protected field.
Background technology
The annual summer harvest in recent years and when the autumn and winter, always has the stalks such as a large amount of wheats, corn to burn in field, creates a large amount of heavy smog, not only become the bottleneck problem of rural environmental protection, even become the arch-criminal of bringing disaster to urban environment.Especially, after wheat harvest, a large amount of wheat straws is had to pile up between field or in courtyard.Such one is hold fire hazardous; Two is that wheat straw chance rain can go rotten, and contaminated environment, affects health.So wheat stalk industrialization used, can be used as the raw material etc. of insulation material, paper pulp raw material, all kinds of light weight board and packaging material.These comprehensive utilizations, have not only transformed a large amount of waste straw, have eliminated potential environmental pollution, and had good economic benefit, achieve the circulation of natural matter and energy.
General mosquito to start to occur annual April, reaches activity peak to mid or late August.Mosquito can propagate various diseases, and as Anopheles sinensis propagates malaria, Culex tritaeniorhynchus, Culex pipiens pallens propagate encephalitis, and Aedes aegypti, aedes albopictus propagate dengue fever, and Anopheles arthropophagus propagates filariosis etc., very harmful to the mankind.The entomologist Da Liai covering Billy's dust centre of research and development says, mosquito can tell some molecule that human cellular activity produces well, the lactic acid produced when the carbonic acid gas produced during as breathed and strenuous exercise, and the material of some people secretion is more than others.Therefore, those secretions and breathe vigorous people, just more easily become the target of mouth under mosquito.
Summary of the invention
The technical problem that the present invention mainly solves: contain many harmful materials in the cigarette of the substance combustion of current killing mosquitoes, likely bring out the drawback that the diseases such as asthma mostly are, provide a kind of method utilizing wheat stalk to prepare killing mosquitoes particle, wheat stalk particle after charing and fruit of Rangoon creeper's mixing are sealed stirring by the method, add absolute ethyl alcohol, permethrin, silica gel, after lactic acid, stir after adding carbon dioxide again, filter, air-dry, the method preparation method is simple, easy to operate, killing mosquitoes Be very effective, and it is harmless to human non-toxic after burning.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
(1) get wheat stalk to put into cracker and pulverize, be ground into 10 ~ 30 order particles, obtained particle is put into water, add the phosphoric acid solution that mass fraction is 80 ~ 85% more wherein, its addition is 15 ~ 18% of wheat stalk particle quality, soak 12 ~ 15min, then filter, filtered fluid is collected for subsequent use;
(2) above-mentioned filtrate is put into retort and carry out charing 2 ~ 3h, temperature is set to 450 ~ 500 DEG C, is then taken out by the wheat stalk particle after charing, is cooled to 28 ~ 35 DEG C, washing is carried out 2 ~ 4 times with the filtered fluid collected by above-mentioned steps, then by its natural air drying;
(3) the wheat stalk particle after air-dry is put into container, add the fruit of Rangoon creeper wherein, its addition is 40 ~ 50% of wheat stalk particle quality, seal slow heating to it to stir simultaneously, every 10min heats up 3 DEG C, when being warming up to 55 ~ 60 DEG C, stops heating up, insulation 40 ~ 50min, is then taken out and is cooled to room temperature;
(4) the wheat stalk particle obtained by step (3) is put into container, add absolute ethyl alcohol wherein to flood wheat stalk particle, add the permethrin of Wheat Straw granular mass 5 ~ 9%, add the silica gel of Wheat Straw granular mass 8 ~ 10% and add the lactic acid of Wheat Straw granular mass 7 ~ 10%, airtight container, carbonic acid gas is used to remove the gas of internal tank, keep temperature 55 ~ 60 DEG C, stir 30 ~ 35min, then filter, the wheat stalk particle natural air drying after filtration.
Application method of the present invention: the mosquito grabbing 100 work, puts in closed mosquito net, then mosquito particle the present invention prepared burns, and puts into mosquito net, quiet put one hour after, open mosquito net, find the mosquito that almost do not survive, except mosquito rate reaches 99%.
The invention has the beneficial effects as follows:
(1) the method manufacture craft is simple, and easy to operate, cost is low;
(2) the particle killing mosquitoes Be very effective that the method is obtained, and human body is safe from harm, natural safety.
Embodiment
Get wheat stalk to put into cracker and pulverize, be ground into 10 ~ 30 order particles, obtained particle is put into water, add the phosphoric acid solution that mass fraction is 80 ~ 85% more wherein, its addition is 15 ~ 18% of wheat stalk particle quality, soak 12 ~ 15min, then filter, filtered fluid is collected for subsequent use; Above-mentioned filtrate is put into retort and carries out charing 2 ~ 3h, temperature is set to 450 ~ 500 DEG C, is then taken out by the wheat stalk particle after charing, is cooled to 28 ~ 35 DEG C, washing is carried out 2 ~ 4 times with the filtered fluid collected by above-mentioned steps, then by its natural air drying; Wheat stalk particle after air-dry is put into container, add the fruit of Rangoon creeper wherein, its addition is 40 ~ 50% of wheat stalk particle quality, seal slow heating to it to stir simultaneously, every 10min heats up 3 DEG C, when being warming up to 55 ~ 60 DEG C, stops heating up, insulation 40 ~ 50min, is then taken out and is cooled to room temperature; Obtained wheat stalk particle is put into container, add absolute ethyl alcohol wherein to flood wheat stalk particle, add the permethrin of Wheat Straw granular mass 5 ~ 9%, add the silica gel of Wheat Straw granular mass 8 ~ 10% and add the lactic acid of Wheat Straw granular mass 7 ~ 10%, airtight container, carbonic acid gas is used to remove the gas of internal tank, keep temperature 55 ~ 60 DEG C, stir 30 ~ 35min, then filter, the wheat stalk particle natural air drying after filtration.
Application method of the present invention: the mosquito grabbing 100 work, puts in closed mosquito net, then mosquito particle the present invention prepared burns, and puts into mosquito net, quiet put one hour after, open mosquito net, find the mosquito that almost do not survive, except mosquito rate reaches 99%.
The wheat stalk getting 1Kg is put into cracker and is pulverized, and is ground into 10 order particles, obtained particle is put into water, add the phosphoric acid solution that mass fraction is 80% more wherein, its addition is 150g, soaks 12min, then filter, filtered fluid is collected for subsequent use; Above-mentioned filtrate is put into retort and carries out charing 2h, temperature is set to 450 DEG C, is then taken out by the wheat stalk particle after charing, is cooled to 28 DEG C, carries out washing 2 times with the filtered fluid collected by above-mentioned steps, then by its natural air drying; Wheat stalk particle after air-dry is put into container, adds the fruit of Rangoon creeper wherein, its addition is 400g, seal slow heating to it to stir, every 10min heats up 3 DEG C, when being warming up to 55 DEG C simultaneously, stop heating up, insulation 40min, is then taken out and is cooled to room temperature; Obtained wheat stalk particle is put into container, add absolute ethyl alcohol wherein to flood wheat stalk particle, add permethrin that quality is 50g, add the silica gel of 80g and add the lactic acid of 70g, airtight container, carbonic acid gas is used to remove the gas of internal tank, keep temperature 55 DEG C, stir 30min, then filter, the wheat stalk particle natural air drying after filtration.
The method manufacture craft is simple, and easy to operate, cost is low; Obtained particle is safe from harm to human body, and natural safety, killing mosquitoes Be very effective, except mosquito rate reaches 99%.
The wheat stalk getting 2Kg is put into cracker and is pulverized, and be ground into 20 order particles, obtained particle is put into water, then add the phosphoric acid solution that mass fraction is 83% wherein, addition is 300g, soaks 13min, then filters, and filtered fluid is collected for subsequent use; Above-mentioned filtrate is put into retort and carries out charing 2.5h, temperature is set to 475 DEG C, is then taken out by the wheat stalk particle after charing, is cooled to 30 DEG C, carries out washing 3 times with the filtered fluid collected by above-mentioned steps, then by its natural air drying; Wheat stalk particle after air-dry is put into container, adds the fruit of Rangoon creeper wherein, its addition is 900g, seal slow heating to it to stir, every 10min heats up 3 DEG C, when being warming up to 58 DEG C simultaneously, stop heating up, insulation 45min, is then taken out and is cooled to room temperature; Obtained wheat stalk particle is put into container, add the lactic acid that absolute ethyl alcohol floods wheat stalk particle, adds the permethrin of 100g, adds the silica gel of 160g and 140g wherein, airtight container, carbonic acid gas is used to remove the gas of internal tank, keep temperature 57 DEG C, stir 33min, then filter, the wheat stalk particle natural air drying after filtration.
The method manufacture craft is simple, and easy to operate, cost is low; Obtained particle is safe from harm to human body, and natural safety, killing mosquitoes Be very effective, except mosquito rate reaches 99%.
Get 3Kg wheat stalk to put into cracker and pulverize, be ground into 30 order particles, obtained particle is put into water, then add the phosphoric acid solution that mass fraction is 85% wherein, its addition is 450g, soaks 15min, then filters, and filtered fluid is collected for subsequent use; Above-mentioned filtrate is put into retort and carries out charing 3h, temperature is set to 500 DEG C, is then taken out by the wheat stalk particle after charing, is cooled to 35 DEG C, carries out washing 4 times with the filtered fluid collected by above-mentioned steps, then by its natural air drying; Wheat stalk particle after air-dry is put into container, adds the fruit of Rangoon creeper wherein, its addition is 1500g, seal slow heating to it to stir, every 10min heats up 3 DEG C, when being warming up to 60 DEG C simultaneously, stop heating up, insulation 50min, is then taken out and is cooled to room temperature; Obtained wheat stalk particle is put into container, add absolute ethyl alcohol wherein to flood wheat stalk particle, add the permethrin of 270g, add the silica gel of 300g and add the lactic acid of 300g, airtight container, carbonic acid gas is used to remove the gas of internal tank, keep temperature 60 C, stir 35min, then filter, the wheat stalk particle natural air drying after filtration.
The method manufacture craft is simple, and easy to operate, cost is low; Obtained particle is safe from harm to human body, and natural safety, killing mosquitoes Be very effective, except mosquito rate reaches 99%.

Claims (1)

1. utilize wheat stalk to prepare a method for killing mosquitoes particle, it is characterized in that concrete preparation process is:
(1) get wheat stalk to put into cracker and pulverize, be ground into 10 ~ 30 order particles, obtained particle is put into water, add the phosphoric acid solution that mass fraction is 80 ~ 85% more wherein, its addition is 15 ~ 18% of wheat stalk particle quality, soak 12 ~ 15min, then filter, filtered fluid is collected for subsequent use;
(2) above-mentioned filtrate is put into retort and carry out charing 2 ~ 3h, temperature is set to 450 ~ 500 DEG C, is then taken out by the wheat stalk particle after charing, is cooled to 28 ~ 35 DEG C, washing is carried out 2 ~ 4 times with the filtered fluid collected by above-mentioned steps, then by its natural air drying;
(3) the wheat stalk particle after air-dry is put into container, add the fruit of Rangoon creeper wherein, its addition is 40 ~ 50% of wheat stalk particle quality, seal slow heating to it to stir simultaneously, every 10min heats up 3 DEG C, when being warming up to 55 ~ 60 DEG C, stops heating up, insulation 40 ~ 50min, is then taken out and is cooled to room temperature;
(4) the wheat stalk particle obtained by step (3) is put into container, add absolute ethyl alcohol wherein to flood wheat stalk particle, add the permethrin of Wheat Straw granular mass 5 ~ 9%, add the silica gel of Wheat Straw granular mass 8 ~ 10% and add the lactic acid of Wheat Straw granular mass 7 ~ 10%, airtight container, carbonic acid gas is used to remove the gas of internal tank, keep temperature 55 ~ 60 DEG C, stir 30 ~ 35min, then filter, the wheat stalk particle natural air drying after filtration.
CN201510539596.7A 2015-08-30 2015-08-30 Method for preparing mosquito eradication granules by virtue of wheat straws Pending CN105076227A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105519593A (en) * 2015-12-12 2016-04-27 常州大学 Preparation method of natural solid granular insecticide

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103461325A (en) * 2013-06-06 2013-12-25 黄山市迎客松生物科技有限公司 Straw-based drug liquid controlled release agent and preparation method thereof
CN103688927A (en) * 2013-11-27 2014-04-02 绵阳市美日佳日化用品有限责任公司 Mosquito repellent incense blank
CN103766423A (en) * 2014-02-26 2014-05-07 泗洪新创源木业有限公司 Composite biomass mosquito repellent material

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103461325A (en) * 2013-06-06 2013-12-25 黄山市迎客松生物科技有限公司 Straw-based drug liquid controlled release agent and preparation method thereof
CN103688927A (en) * 2013-11-27 2014-04-02 绵阳市美日佳日化用品有限责任公司 Mosquito repellent incense blank
CN103766423A (en) * 2014-02-26 2014-05-07 泗洪新创源木业有限公司 Composite biomass mosquito repellent material

Non-Patent Citations (2)

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Title
汪明性: "《新编实用药物学》", 30 June 2000 *
钟敏等: "植物防治蚊虫的应用研究进展", 《中华卫生杀虫药械》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105519593A (en) * 2015-12-12 2016-04-27 常州大学 Preparation method of natural solid granular insecticide

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Application publication date: 20151125