CN105036849A - Bark-type traditional Chinese medicine mulberry root-bark production method - Google Patents
Bark-type traditional Chinese medicine mulberry root-bark production method Download PDFInfo
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- CN105036849A CN105036849A CN201510403212.9A CN201510403212A CN105036849A CN 105036849 A CN105036849 A CN 105036849A CN 201510403212 A CN201510403212 A CN 201510403212A CN 105036849 A CN105036849 A CN 105036849A
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Abstract
The invention discloses a production method of a bark-type traditional Chinese medicine, and relates to the field of traditional Chinese medicine production. According to the invention, nutrients are applied during a mulberry root-bark growth period: a, 3g of nucleotide salts and 2g of medium-trace elements are crushed and mixed; b, 5g of nucleotide salts and 5g of medium-trace elements are crushed and mixed; c, 8g of nucleotide salts, 10g of starch, 7g of cellulose and 5g of medium-trace elements are fetched; the nucleotide salts and medium-trace elements are crushed; starch and cellulose are added; and the materials are mixed; such that nutrients are obtained. The nucleotide salts are four 5'-mixed nucleotide potassium or sodium salts obtained after ribonucleic acid base hydrolysis. The medium-trace elements are Zn, Mn, Mg, Fe and B with a weight ratio of 2:2:2:1:2. The application method is that the nutrients are dissolved with water and then sprayed. The nutrient a is used during a seedling or germination period. The nutrient b is used in an early flowering period, and the nutrient c is used in a flowering period. The nutrients are respectively dissolved in 20L of water, and are respectively applied once. The method is simple, raw material-saving and cost-saving. With the method, mulberry root-bark yield and quality are improved.
Description
The application is application number 201310579812.1, the applying date: on November 19th, 2013, and denomination of invention is the divisional application of " production method of skin class Chinese medicine ".
Technical field
The present invention relates to the production method of skin class Chinese medicine, particularly the production method of skin class Chinese medicinal materials mulberry skin and medicine materical crude slice and extract.
Background technology
, there is composition activeconstituents more, do not save in the production method of existing skin class Chinese medicine, not rationally, not easily standing storage and preparation method are simple not for activeconstituents proportioning, and purposes is problem not widely.Authorization Notice No. CN102079672B, the patent No. is ZL201010514222.7's, name is called: a kind ofly promote the nutrient substance that skin class Chinese medicinal materials grows, described nutrient substance is by nucleosides hydrochlorate, glucose, amino acid and medium trace element composition, its weight percent is: nucleosides hydrochlorate 10-30%, glucose 20-70%, amino acid/11 0-20%, medium trace element 10-30%, described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) disodium or potassium, 5 '-bird adenylic acid (AMP) disodium or potassium, 5 '-cytidylic acid disodium or potassium, the sodium salt of 5 '-uridine monophosphate disodium or potassium four kinds of 5 '-mixed nucleotides or sylvite, described medium trace element refers to: Zn, Mn, Mg, Fe, B, specifically: zinc sulfate, manganous sulfate, magnesium sulfate, ferrous sulfate and borax.Just there are the problems referred to above.
Summary of the invention
Object of the present invention overcomes above-mentioned deficiency exactly, one is provided to decrease activeconstituents in composition, reasonable ratio, its effect still can meet or exceed the patent No. and be: a kind of production method promoting the skin class Chinese medicine of the patent of invention of the nutrient substance that skin class Chinese medicinal materials grows of " 201010514222.7 ".
Summary of the invention
The present invention is achieved in that
The production method of skin class Chinese medicine mulberry skin, use nutrient substance at mulberry skin growing period, described nutrient substance is
A. get 3 grams of nucleosides hydrochlorates, medium trace element 2 grams, nucleosides hydrochlorate, medium trace element are pulverized, sieves, mix, the nutrient substance obtained;
B. take 5 grams of nucleosides hydrochlorates, medium trace element 5 grams, by nucleosides hydrochlorate, medium trace element mixing, pulverize, cross 100 mesh sieves, the nutrient substance obtained;
C. take 8 grams of nucleosides hydrochlorates, starch 10 grams, Mierocrystalline cellulose 7 grams, medium trace element 5 grams, nucleosides hydrochlorate, medium trace element are pulverized, sieves, add starch, Mierocrystalline cellulose, mix, the nutrient substance obtained;
Described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, 5 '-uridylic acid dipotassium or sodium, the potassium of four kinds of 5 '-mixed nucleotides or sodium salt;
Described medium trace element refers to: Zn, Mn, Mg, Fe, B, specifically: zinc sulfate, manganous sulfate, magnesium sulfate, ferrous sulfate and borax; Its weight ratio is: Zn:Mn:Mg:Fe:B=2:2:2:1:2;
The application process of nutrient substance is: spray with after water dissolution;
Described nutrient substance use opportunity and concentration is: at seedling or germination period a nutrient substance, initial bloom stage b nutrient substance, full-bloom stage c nutrient substance, is watered 20 liters respectively, respectively executes once.
The production method of skin class Chinese medicine, in its process of growth, use nutrient substance: described nutrient substance it primarily of nucleosides hydrochlorate, medium trace element composition, do not comprise glucose or/and amino acid, its weight percent is:; Nucleosides hydrochlorate 30-70%, medium trace element 30-70%, described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, the potassium of 5 '-uridylic acid dipotassium or sodium four kinds of 5 '-mixed nucleotides or sodium salt, described medium trace element refers to: Zn, Mn, Mg, Fe, B, specifically: zinc sulfate, manganous sulfate, magnesium sulfate, ferrous sulfate and borax, the application process of nutrient substance is: spray with after water dissolution.
The production method of skin class Chinese medicine is 100-400ppm by the concentration sprayed after water dissolution.
The production method of skin class Chinese medicine, the weight ratio of medium trace element is: Zn:Mn:Mg:Fe:B=2:2:2:1:2.
The production method of skin class Chinese medicine, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nutrient compositions is: nucleosides hydrochlorate 10-30%, medium trace element 10-30%, weighting agent 40-80%.
The production method of skin class Chinese medicine, the opportunity of using of described nutrient substance is: at seedling or germination period, initial bloom stage, full-bloom stage respectively once.
The production method of skin class Chinese medicine, the opportunity of using of described nutrient substance is: in seedling or germination period, treelet phase, become the tree phase respectively to spray 1-2 time every year.
The production method of skin class Chinese medicine, the consumption of described nutrient substance is every mu of 2-8 gram, is every mu of 20-40 liter by water-soluble water consumption.
The production method of skin class Chinese medicine, the consumption of described nutrient substance is at every turn every mu of 15-30 gram, is at every turn every mu of 20-40 liter by water-soluble water consumption.
The production method of skin class Chinese medicine, the Chinese medicinal materials of results, than the high 10%-20% of produced in conventional processes, can be made high-quality medicine materical crude slice extracting effective components yield and can reach more than 20% than the skin class Chinese medicinal materials of produced in conventional processes by its output.
In the preparation of nutrient substance provided by the present invention, take nucleic acid as raw material: one is for raw material with commercially available nucleic acid, two is adopt the nucleic acid of dry method or wet production to be raw material from the mycelium after fermentation plant fermentation: 1., the hydrolysis of nucleic acid is the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid of 1:20-30 according to nucleic acid, buck weight ratio, alkali lye is 5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtain nucleosides hydrochlorate and deoxynucleoside acid salt solution, filter, filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry: concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization: dissolve the nucleosides hydrochlorate after doing and deoxynucleoside hydrochlorate with clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate (from the mycelium after fermentation plant fermentation adopt the nucleic acid of dry method or wet production be raw material also containing water soluble mixt and impurity);
4., medium trace element is got;
, by nucleosides hydrochlorate medium trace element mix, pulverize, sieve.
In nucleic acid hydrolysis process described in this preparation method, alkali lye used is sodium hydroxide or potassium hydroxide solution.
With commercially available nucleic acid for raw material, impure few after hydrolysis.
Three is commercially available: nucleosides hydrochlorate mainly refers to: 5 '-adenylic acid (AMP) disodium or potassium, 5 '-bird adenylic acid (AMP) disodium or potassium, 5 '-cytidylic acid disodium or potassium, the sodium salt of 5 '-uridine monophosphate disodium or potassium four kinds of 5 '-mixed nucleotides or sylvite; Deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.
The source of nucleosides hydrochlorate and deoxynucleoside hydrochlorate is take nucleic acid as raw material, adopt the nucleic acid of dry method or wet production to be raw material from the mycelium after fermentation plant fermentation, this kind of nucleic acid is a small amount of thymus nucleic acid (DNA) of main mixing with Yeast Nucleic Acid (RNA), makes with alkali lye hydrolysis.
Beneficial effect of the present invention:
Because the present invention does not decrease composition activeconstituents, so more economize in raw materials and cost containing glucose, amino acid.
Coordinate nucleosides hydrochlorate, reasonable ratio because the present invention contains medium trace element, promote the growth of skin class Chinese medicine more targeted specifically.
Although the present invention decreases activeconstituents, its effect does not still subtract and even produces better effect.
The present invention is not particularly containing glucose, glucose easily absorbs moisture deliquescence, nutrient substance containing glucose places the deliquescence that namely absorbs water for about a year under general condition of storage, there is product caking, make nucleosides hydrochlorate, cause quality product to reduce even to lose efficacy, so, the invention solves the problem of the not easily standing storage of nutrient substance.
. because the present invention also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc., adapt to the adding of weighting agent the relevant regulations being generally not less than 20 grams as the foliage fertilizer minimum package of merchandise sales; Filler starch, dextrin, Mierocrystalline cellulose etc. also possess certain viscosity, make nutrient substance be attached to blade face after spraying and the plant surface time longer, make its action effect better; Weighting agent polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc. have dispersiveness and oilness, can extend the quality guaranteed period of nutrient substance.
Purposes of the present invention is: as fertilizer particularly as foliage fertilizer or nutrient substance or the application of plant-growth regulator in the growth promoting skin class Chinese medicine; Or the production being applied to skin class Chinese medicine can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The present invention is applied to the production of skin class Chinese medicine, with strong points, can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
So product of the present invention: saving, environmental protection, nontoxic, harmless, noresidue, without any adverse side effect, comprehensive to the purposes of skin class Chinese medicine, increase production, increase income, synergy, strengthen resistance, improve quality effective.
The present invention and No. 201010514222.7 patents, traditional product and method contrast tables 1
The present invention and No. 201010514222.7 patents, traditional product and method contrast tables 2
Embodiment:
Embodiment 1: get 3 grams of nucleosides hydrochlorates, medium trace element 2 grams, pulverizes nucleosides hydrochlorate, medium trace element, sieves, mix.
Embodiment 2: take 5 grams of nucleosides hydrochlorates, medium trace element 5 grams, by nucleosides hydrochlorate, medium trace element mixing, pulverizes, crosses 100 mesh sieves, obtain nutrient substance.
Embodiment 3: take 8 grams of nucleosides hydrochlorates, starch 10 grams, Mierocrystalline cellulose 7 grams, medium trace element 5 grams, pulverizes nucleosides hydrochlorate, medium trace element, sieves, add starch, Mierocrystalline cellulose, mix, obtain nutrient substance.
Embodiment 4: the bark of eucommia: first time is seedling stage, in April, with embodiment 1 nutrient substance, is watered 20 liters, evenly sprays in one mu of bark of eucommia; Second time is the treelet phase, and the annual 3-4 month and the 5-6 month respectively spray once; Third time is
Become the tree phase: annual 4-5 month and respectively spraying once the 7-8 month.
Embodiment 5: golden cypress: first time is nursery stage, with embodiment 2 grams of nutrient substances, is watered 20 liters, evenly sprays on one mu of golden cypress seedling; Second time is setting date, and spray once; Third time is for becoming the tree phase: annual 4-5 month and respectively spraying once the 7-8 month.
Embodiment 6: mulberry skin: use the method for embodiment 1, embodiment 2 and embodiment 3 each once respectively at seedling or germination period, initial bloom stage, full-bloom stage.
Claims (1)
1. the production method of skin class Chinese medicine mulberry skin, is characterized in that: use nutrient substance at mulberry skin growing period, described nutrient substance is
A. get 3 grams of nucleosides hydrochlorates, medium trace element 2 grams, nucleosides hydrochlorate, medium trace element are pulverized, sieves, mix, the nutrient substance obtained;
B. take 5 grams of nucleosides hydrochlorates, medium trace element 5 grams, by nucleosides hydrochlorate, medium trace element mixing, pulverize, cross 100 mesh sieves, the nutrient substance obtained;
C. take 8 grams of nucleosides hydrochlorates, starch 10 grams, Mierocrystalline cellulose 7 grams, medium trace element 5 grams, nucleosides hydrochlorate, medium trace element are pulverized, sieves, add starch, Mierocrystalline cellulose, mix, the nutrient substance obtained;
Described nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, 5 '-uridylic acid dipotassium or sodium, the potassium of four kinds of 5 '-mixed nucleotides or sodium salt;
Described medium trace element refers to: Zn, Mn, Mg, Fe, B, specifically: zinc sulfate, manganous sulfate, magnesium sulfate, ferrous sulfate and borax; Its weight ratio is: Zn:Mn:Mg:Fe:B=2:2:2:1:2;
The application process of nutrient substance is: spray with after water dissolution;
Described nutrient substance use opportunity and concentration is: at seedling or germination period a nutrient substance, initial bloom stage b nutrient substance, full-bloom stage c nutrient substance, is watered 20 liters respectively, respectively executes once.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310579812.1A CN103613422B (en) | 2013-11-19 | 2013-11-19 | The production method of skin class Chinese medicine |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310579812.1A Division CN103613422B (en) | 2013-11-19 | 2013-11-19 | The production method of skin class Chinese medicine |
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| CN105036849A true CN105036849A (en) | 2015-11-11 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510403212.9A Withdrawn CN105036849A (en) | 2013-11-19 | 2013-11-19 | Bark-type traditional Chinese medicine mulberry root-bark production method |
| CN201310579812.1A Expired - Fee Related CN103613422B (en) | 2013-11-19 | 2013-11-19 | The production method of skin class Chinese medicine |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310579812.1A Expired - Fee Related CN103613422B (en) | 2013-11-19 | 2013-11-19 | The production method of skin class Chinese medicine |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102079672A (en) * | 2010-10-21 | 2011-06-01 | 高旌 | Nutrient for promoting growth of bark traditional Chinese medicinal materials |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102241541A (en) * | 2010-05-11 | 2011-11-16 | 林光德 | Method for producing foliar fertilizer of tea |
| CN102311289B (en) * | 2010-07-02 | 2014-04-30 | 王祥林 | Organic water soluble fertilizer |
| CN103332999B (en) * | 2010-10-21 | 2014-09-10 | 高旌 | Method for producing high-quality high-yield bark type traditional Chinese medicinal material eucommia bark |
| CN103332998B (en) * | 2010-10-21 | 2014-09-10 | 高旌 | Method for producing bark type traditional Chinese medicinal material |
| CN102515948B (en) * | 2011-12-09 | 2013-12-11 | 大千生态景观股份有限公司 | Plant antifreezer and its preparation method |
| CN102746060B (en) * | 2012-06-18 | 2014-08-06 | 湖南中烟工业有限责任公司 | Root growth promoting agent for tobacco, its preparation and application |
| CN103058785A (en) * | 2013-02-05 | 2013-04-24 | 河南誉中奥农业科技有限公司 | Environment-friendly ecological full-nutrient fertilizer and production method of environment-friendly ecological full-nutrient fertilizer |
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- 2013-11-19 CN CN201510403212.9A patent/CN105036849A/en not_active Withdrawn
- 2013-11-19 CN CN201310579812.1A patent/CN103613422B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102079672A (en) * | 2010-10-21 | 2011-06-01 | 高旌 | Nutrient for promoting growth of bark traditional Chinese medicinal materials |
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| CN103613422B (en) | 2016-04-20 |
| CN103613422A (en) | 2014-03-05 |
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