CN103613426A - Production method of whole-grass traditional Chinese medicine - Google Patents
Production method of whole-grass traditional Chinese medicine Download PDFInfo
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- CN103613426A CN103613426A CN201310580012.1A CN201310580012A CN103613426A CN 103613426 A CN103613426 A CN 103613426A CN 201310580012 A CN201310580012 A CN 201310580012A CN 103613426 A CN103613426 A CN 103613426A
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Abstract
The invention discloses a production method of a whole-grass traditional Chinese medicine. The production method is characterized in that nutrients are used during the growth of the whole-grass traditional Chinese medicine, wherein the nutrients include the following components in percentage by weight: 30 to 70% of nucleotide salt and 30 to 70% of medium trace element, and exclude glucose or/and amino acid; the nucleotide salt is the sylvite or sodium salt of four 5'-mixed nucleotides and obtained by hydrolyzing ribonucleic acid alkaline, namely, wherein the four 5'-mixed nucleotides are namely 5'-adenylate dipotassium or sodium, 5'-guanylic dipotassium or sodium, 5'-cytidine monophosphate dipotassium or sodium, 5'-uridylic acid dipotassium or sodium; and the medium trace element includes Mn, B, Fe, Zn, Cu or Mo, namely manganese sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate or ammonium molybdate; and the nutrients are applied by being dissolved with water and then spraying. The production method of the whole-grass traditional Chinese medicine has the effect reaching or even exceeding the effect of a patent for invention with publication patent number of CN102079667B and patent number of ZL201010514233.5. The production method is simple, convenient, economic and environment-friendly, increases yield, improves resistance, improves and enhances quality, increases the output by 30 to 50%, and realizes extraction yield up to more than 90%.
Description
Technical field
The present invention relates to a kind of production method of traditional Chinese medicine of whole straw, particularly the production method of whole grass medicinal plant and medicine materical crude slice thereof and extract.
Background technology
The production method of existing promotion traditional Chinese medicine of whole straw, exists composition activeconstituents more, do not save, activeconstituents proportioning not rationally, be difficult for standing storage and preparation method is simple not, purposes is problem not widely.Granted publication CN 102079667 B, the patent No.: 201010514233.5 patent of invention, title is also: the nutrient substance that promotes the growth of whole grass medicinal plant, it is by nucleosides hydrochlorate, glucose, amino acid and middle trace element form, its weight percent is: nucleosides hydrochlorate 10-30%, glucose 20-70%, amino acid/11 0-20%, middle micro-10-30%, described nucleosides hydrochlorate refers to: after Yeast Nucleic Acid hydrolysis, obtain: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, the sylvite of four kind 5 '-mixed nucleotides of 5 '-cytidylic acid dipotassium or 5 '-uridylic acid dipotassium, described middle trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate, just there are the problems referred to above.
Summary of the invention
Object of the present invention overcomes above-mentioned deficiency exactly, a kind of activeconstituents in composition that reduced is provided, reasonable ratio, its effect still can meet or exceed the patent No. and be: the production method of the traditional Chinese medicine of whole straw of the patent of invention of the nutrient substance of the promotion whole grass medicinal plant growth of " 201010514233.5 ".
The present invention is achieved in that
Promote the nutrient substance of whole grass medicinal plant growth, it mainly by nucleosides hydrochlorate, in trace element form, do not comprise glucose or/and amino acid, weight percent is:; Nucleosides hydrochlorate 30-70%, middle micro-30-70%, described nucleosides hydrochlorate refers to: after Yeast Nucleic Acid basic hydrolysis, obtain: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, potassium or the sodium salt of 5 '-uridylic acid dipotassium or four kind 5 '-mixed nucleotides of sodium, described middle trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate or ammonium molybdate.
The nutrient substance that promotes the growth of whole grass medicinal plant, screening formulation weight percent is: nucleosides hydrochlorate 40-60%, middle micro-30-70%.
The nutrient substance that promotes the growth of whole grass medicinal plant, is characterized in that: the weight ratio of middle trace element is: Mn:B: Fe: Zn:Cu: Mo=5:2:3:3:2:2.
The nutrient substance of whole grass medicinal plant growth, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate.
The nutrient substance of whole grass medicinal plant growth, the weight percent of nucleosides hydrochlorate, middle trace element and weighting agent is: nucleosides hydrochlorate 10-30 %, middle micro-10-30%, weighting agent 40-80%.
The nutrient substance of whole grass medicinal plant growth, weighting agent is: one or more of W-Gum, dextrin, Mierocrystalline cellulose, Magnesium Stearate, magnesium sulfate or zinc sulfate, the weight percent of nucleosides hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate 15-20%, middle micro-15-20%, weighting agent 40-70%.
Promote the preparation method of the nutrient substance of whole grass medicinal plant growth, it mainly by nucleosides hydrochlorate, in trace element form, do not comprise glucose or/and amino acid, weight percent is:; Nucleosides hydrochlorate 30-70%, middle micro-30-70%, described nucleosides hydrochlorate refers to: after Yeast Nucleic Acid basic hydrolysis, obtain: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, potassium or the sodium salt of 5 '-uridylic acid dipotassium or four kind 5 '-mixed nucleotides of sodium, described middle trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate or ammonium molybdate, by nucleosides hydrochlorate, middle trace element mixes, pulverizes, and crosses 50-150 mesh sieve.
The preparation method who promotes the nutrient substance of whole grass medicinal plant growth, screening formulation weight percent is: nucleosides hydrochlorate 40-60%, middle micro-30-70%.
The preparation method who promotes the nutrient substance of whole grass medicinal plant growth, the weight ratio of middle trace element is: Mn:B: Fe: Zn:Cu: Mo=5:2:3:3:2:2.
Promote the preparation method of the nutrient substance of whole grass medicinal plant growth, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nucleosides hydrochlorate, middle trace element and weighting agent is: nucleosides hydrochlorate 10-30 %, middle micro-10-30%, weighting agent 40-80%, adds the weighting agent of pulverizing to mix with nucleosides hydrochlorate, middle trace element.
Promote the preparation method of the nutrient substance of whole grass medicinal plant growth, it is characterized in that, weighting agent is: one or more of W-Gum, dextrin, Mierocrystalline cellulose, Magnesium Stearate, the weight percent of nucleosides hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate 15-20%, middle micro-15-20%, weighting agent 40-70%.
The production method of traditional Chinese medicine of whole straw, in its process of growth, use nutrient substance: described nutrient substance is mainly by nucleosides hydrochlorate, middle trace element forms, do not comprise glucose or/and amino acid, weight percent is: nucleosides hydrochlorate 30-70%, middle micro-30-70%, described nucleosides hydrochlorate refers to: after Yeast Nucleic Acid basic hydrolysis, obtain: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, potassium or the sodium salt of 5 '-uridylic acid dipotassium or four kind 5 '-mixed nucleotides of sodium, described middle trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate or ammonium molybdate, the application process of nutrient substance is: with spraying after water dissolution.
The production method of traditional Chinese medicine of whole straw is 100-400ppm by the concentration spraying after water dissolution.
The production method of traditional Chinese medicine of whole straw, the weight ratio of middle trace element is: Mn:B: Fe: Zn:Cu: Mo=5:2:3:3:2:2.
The production method of traditional Chinese medicine of whole straw, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nutrient substance composition is: nucleosides hydrochlorate 10-30 %, middle micro-10-30%, weighting agent 40-80%.
The production method of traditional Chinese medicine of whole straw, be the opportunity of using of described nutrient substance: in seedling stage of whole grass medicinal plant, bud stage or/and initial bloom stage, full-bloom stage each once.
The production method of traditional Chinese medicine of whole straw, be the opportunity of using of described nutrient substance: at the bud stage of whole grass medicinal plant or/and initial bloom stage, full-bloom stage each once.
The production method of traditional Chinese medicine of whole straw, the consumption of described nutrient substance is every mu of 2-8 gram, by water-soluble water consumption, is every mu of 20-40 liter.
The production method of traditional Chinese medicine of whole straw, the consumption of described nutrient substance is each every mu of 15-30 gram, by water-soluble water consumption, is each every mu of 20-40 liter.
The production method of described traditional Chinese medicine of whole straw, its output is than the high 30-50% of produced in conventional processes, its per mu yield product Contents of Main Components reaches as high as 93% than produced in conventional processes, the Chinese medicinal materials of results can be made to high-quality medicine materical crude slice or per mu yield product extracting effective components yield is reached as high as more than 90% than the Chinese medicinal materials of produced in conventional processes.
In the preparation of nutrient substance provided by the present invention, take nucleic acid as raw material: the one, take commercially available nucleic acid as raw material, 1., the hydrolysis of the nucleic acid ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid that is 1:20-30 according to nucleic acid, buck weight ratio the 2nd, it is raw material that the mycelium from fermentation plant fermentation adopts the nucleic acid of dry method or wet production:, alkali lye is 5.5-7N, under 30-45 ℃ of condition, stirs 10-14 hours, obtain nucleosides hydrochlorate and deoxynucleoside acid salt solution, filter, filtrate is adjusted pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry: concentrated solution is added to activated carbon decolorizing, suction filtration it, filtrate decompression is concentrated into moisture 10-25%;
3., crystallization: dissolve nucleosides hydrochlorate and the deoxynucleoside hydrochlorate after doing with clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, obtain white nucleosides hydrochlorate and deoxynucleoside hydrochlorate (it is impurity that the mycelium from fermentation plant fermentation adopts the water soluble mixt that also contains that the nucleic acid of dry method or wet production is raw material);
4., get middle trace element;
In nucleic acid hydrolysis process described in this preparation method, alkali lye used is sodium hydroxide or potassium hydroxide solution.
Take commercially available nucleic acid as raw material, impure few after hydrolysis.
The 3rd, commercially available: nucleosides hydrochlorate mainly refers to: 5 '-adenylic acid (AMP) disodium or potassium, 5 '-bird adenylic acid (AMP) disodium or potassium, 5 '-cytidylic acid disodium or potassium, sodium salt or the sylvite of four kind 5 '-mixed nucleotides of 5 '-uridine monophosphate disodium or potassium; Deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, sodium salt or the sylvite of five kind 5 '-deoxidation mixed nucleotides of 5 '-deoxythymidine acid disodium or potassium.
The source of nucleosides hydrochlorate and deoxynucleoside hydrochlorate is for take nucleic acid as raw material, that to adopt the nucleic acid of dry method or wet production be raw material for mycelium from fermentation plant fermentation, this kind of nucleic acid be take Yeast Nucleic Acid (RNA) as a small amount of thymus nucleic acid of main mixing (DNA), with alkali lye hydrolysis, makes.
Beneficial effect of the present invention:
Because the present invention has not reduced composition activeconstituents containing glucose, amino acid, so more economize in raw materials and cost.
Because the present invention contains middle trace element, coordinate nucleosides hydrochlorate, reasonable ratio, promotes the growth of traditional Chinese medicine of whole straw more targeted specifically.
Although the present invention has reduced activeconstituents, its effect does not still subtract and even produces better effect.
The present invention is not particularly containing glucose, glucose easily absorbs moisture deliquescence, the nutrient substance that contains glucose is placed the deliquescence that absorbs water about a year under general condition of storage, there is product caking, make nucleosides hydrochlorate, cause quality of products even to lose efficacy, so, the invention solves the problem that is difficult for standing storage of nutrient substance.
. because the present invention also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc., the adding to have adapted to of weighting agent are generally not less than the relevant regulations of 20 grams as the foliage fertilizer minimum package of merchandise sales; Filler starch, dextrin, Mierocrystalline cellulose etc. also possess certain viscosity, after spraying, make nutrient substance be attached to blade face and the plant surface time longer, make its action effect better; Weighting agent polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc. have dispersiveness and oilness, can extend the quality guaranteed period of nutrient substance.
Purposes of the present invention is: as fertilizer sources is particularly as foliage fertilizer or nutrient substance or the application of plant-growth regulator in the growth that promotes traditional Chinese medicine of whole straw; Or the production that is applied to traditional Chinese medicine of whole straw can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The present invention is applied to the production of traditional Chinese medicine of whole straw, with strong points, can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
So product of the present invention: saving, environmental protection, nontoxic, harmless, noresidue, without any adverse side effect, comprehensive to the purposes of herb Chinese medicine, increase production, increase income, synergy, strengthen resistance, improve quality effective.
The present invention and No. 201010514233.5 patents, traditional product and method contrast tables 1
The present invention and No. 201010514233.5 patents, traditional product and method contrast tables 2
The present invention implements to spray agency part effect in Table 3 to concrete crop
Note: content's index detection method is carried out with reference to national standard or industry standard, content is pressed dry product and is calculated
Embodiment:
Embodiment 1: get 3 grams of Nucleotide sylvite, and middle micro-2 grams, nucleosides hydrochlorate, middle trace element are pulverized, sieve, mix.
Embodiment 2: get 5 grams of ribonucleotide sodium salts, and middle micro-5 grams, nucleosides hydrochlorate, middle trace element are pulverized, sieve, mix, obtain nutrient substance.
Embodiment 3: take 8 grams of Nucleotide sylvite, and middle micro-5 grams, nucleosides hydrochlorate, middle trace element are pulverized, sieve, mix, obtain nutrient substance.
Embodiment 4: take 4 grams of ribonucleotide sodium salts, middle micro-4 grams, 12 grams of W-Gums, pulverize nucleosides hydrochlorate, middle trace element, sieve, then mix with W-Gum, obtain nutrient substance.
Embodiment 5: take 6 grams of Nucleotide sylvite, and middle micro-8 grams, 12 grams of Xylo-Mucines, 4 grams of Magnesium Stearates, mix nucleosides hydrochlorate, middle trace element, Magnesium Stearate, Xylo-Mucine, pulverize, and sieve, and obtain nutrient substance.
(embodiment 1-embodiment 5 is the mu amount of spraying)
Embodiment 6; Spica Prunellae; Be seedling stage for the first time, with embodiment 4 nutrient substances, be watered 20 liters, evenly spray on one mu of Spica Prunellae; Reflorescence the balling initial stage, by embodiment 3 formulas, be watered 30 liters, evenly spray on one mu of Spica Prunellae.Mu Spica Prunellae and XIAKUQIU volume increase 20%-30%.
Embodiment 7, peppermint: due to 1 year results several of peppermint, the turnout of plant is large, needs to consume larger nutrient, sprays for the first time as seedling growth stage, with embodiment 4 nutrient substances, is watered 30 liters, evenly sprays on one mu of peppermint seedling; Spray for the second time as branch animated period: by embodiment 5 nutrient substances, convert 30 premium on currency, evenly spray on one mu of peppermint seedling; Pregnant flower bud flowering period besides: press respectively embodiment 1, embodiment 2, embodiment 3 formulas in August, September, October, be watered respectively 20,30,40 liters, according to the growing state of peppermint in bud stage, initial bloom stage, each spray of full-bloom stage once.According in Hui nationality, the head of boundary field experiment situation and former experimental result at Nanping, Fujian, the head of circle, Anhui basic identical: can make peppermint oil offtake nearly double, simultaneously to improving the large containing alcohol amount and specific rotation effect of crude peppermint oil bu.
Claims (9)
1. the production method of traditional Chinese medicine of whole straw, it is characterized in that using nutrient substance in its process of growth: described nutrient substance is mainly by nucleosides hydrochlorate, middle trace element forms, do not comprise glucose or/and amino acid, weight percent is: nucleosides hydrochlorate 30-70%, middle micro-30-70%, described nucleosides hydrochlorate refers to: after Yeast Nucleic Acid basic hydrolysis, obtain: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, potassium or the sodium salt of 5 '-uridylic acid dipotassium or four kind 5 '-mixed nucleotides of sodium, described middle trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate or ammonium molybdate, the application process of nutrient substance is: with spraying after water dissolution.
2. the production method of traditional Chinese medicine of whole straw according to claim 1, its feature is being: by the concentration spraying after water dissolution, be 100-400ppm.
3. the production method of traditional Chinese medicine of whole straw according to claim 1, is characterized in that: the weight ratio of middle trace element is: Mn:B: Fe: Zn:Cu: Mo=5:2:3:3:2:2.
4. the production method of traditional Chinese medicine of whole straw according to claim 1, it is characterized in that, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nutrient substance composition is: nucleosides hydrochlorate 10-30 %, middle micro-10-30%, weighting agent 40-80%.
5. the production method of traditional Chinese medicine of whole straw according to claim 1, its feature is being: be the opportunity of using of described nutrient substance: in seedling stage of whole grass medicinal plant, bud stage or/and initial bloom stage, full-bloom stage each once.
6. the production method of traditional Chinese medicine of whole straw according to claim 1, its feature is being: be the opportunity of using of described nutrient substance: at the bud stage of whole grass medicinal plant or/and initial bloom stage, full-bloom stage each once.
7. according to the production method of traditional Chinese medicine of whole straw described in claim 1,2,3,5 or 6, its feature is being: the consumption of described nutrient substance is every mu of 2-8 gram, by water-soluble water consumption, is every mu of 20-40 liter.
8. the production method of traditional Chinese medicine of whole straw according to claim 4, its feature is being: the consumption of described nutrient substance is each every mu of 15-30 gram, by water-soluble water consumption, is each every mu of 20-40 liter.
9. piece according to the production method of traditional Chinese medicine of whole straw described in claim 1,2,3,4,5,6 or 8, its feature is being: its output can be up to 30-50% than produced in conventional processes, its per mu yield product Contents of Main Components reaches as high as 93% than produced in conventional processes, the Chinese medicinal materials of results can be made to high-quality medicine materical crude slice or per mu yield product extracting effective components yield is reached as high as more than 90% than the Chinese medicinal materials of produced in conventional processes.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1376654A (en) * | 2002-04-29 | 2002-10-30 | 孙永林 | Fertilizer dedicated for graminous plants and its application method |
| JP2004196679A (en) * | 2002-12-17 | 2004-07-15 | Sanin Kensetsu Kogyo Kk | Plant growth promoter |
| CN103274787A (en) * | 2010-10-21 | 2013-09-04 | 高旌 | High-quality and high-yield production method of whole grass medicinal plant |
| CN103332976A (en) * | 2010-10-21 | 2013-10-02 | 高旌 | Preparation method of nutrient for promoting growth of medicinal whole-grass plant |
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- 2013-11-19 CN CN201310580012.1A patent/CN103613426A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1376654A (en) * | 2002-04-29 | 2002-10-30 | 孙永林 | Fertilizer dedicated for graminous plants and its application method |
| JP2004196679A (en) * | 2002-12-17 | 2004-07-15 | Sanin Kensetsu Kogyo Kk | Plant growth promoter |
| CN103274787A (en) * | 2010-10-21 | 2013-09-04 | 高旌 | High-quality and high-yield production method of whole grass medicinal plant |
| CN103332976A (en) * | 2010-10-21 | 2013-10-02 | 高旌 | Preparation method of nutrient for promoting growth of medicinal whole-grass plant |
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Application publication date: 20140305 |