CN103613423B - The preparation method of the nutrient substance of fruit and seed class medicinal plant - Google Patents
The preparation method of the nutrient substance of fruit and seed class medicinal plant Download PDFInfo
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Abstract
The invention discloses the preparation method of the nutrient substance of fruit and seed class medicinal plant, belong to fertilizer or plant-growth regulator field, medicinal plant is cape jasmine; Step is: a. gets 2 grams or 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt respectively, trace element 2 grams or 4 grams; B. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mixing; Trace element refers to: Mn::B:Fe:Zn::Cu:Mo=5:3:3:3:2:1; Nucleotide sylvite and deoxynucleoside acid potassium salt refer to: the di-potassium of the di-potassium of four kinds of 5 '-mixed nucleotides and five kinds of 5 '-deoxidation mixed nucleotides.May also be: get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve.Also: nucleosides hydrochlorate is produced in the hydrolysis-decolouring of nucleic acid, drying-crystallization and deoxynucleoside hydrochlorate mixes with trace element again; The method is easy; After using, can reduce shedding 60-80%, stimulation ratio reaches more than 36%, jasminoidin and crocin content high.
Description
Technical field
The present invention relates to the preparation method for promoting the nutrient substance that fruit and seed class medicinal plant grows, the fertilizer particularly needed in a kind of fruit and seed class medicinal plant production or the preparation method of plant-growth regulator.
Background technology
Medicinal plant industry is a large industry of natural medicaments, greatly develop Chinese Medicine Industry, promote Chinese medicinal materials increasing both production and income, crude drug is made to move towards world market further, promote the modernization of Chinese medicine, it is the problem that China Chinese medicine scientist pays close attention to research, Chinese medicinal materials is fruit particularly, the growth of planting subclass Chinese medicinal materials be unable to do without and supplements corresponding nutrition, at present, fruit, the nutrient substance of planting the growth of subclass medicinal plant is exactly fertilizer, all be used in the very wide general fertilizer of planting range, even if present medicinal material fertilizer, main by executing nitrogen, phosphorus, potassic fertilizer and organic fertilizer and medium trace element carry out growth promoting effects, Chinese patent open (publication number CN1900028A) discloses a kind of fertilizer special for Chinese medicine material, and it adopts the big-and-middle microelement match of adjustment different, to adapt to different Chinese medicinal materialss, it remains a kind of common fertilizer, exist and use too much, the quality and flavor of fertilizer to Chinese medicinal materials has certain detrimentally affect, be unfavorable for the development of green agriculture and food safety and environmental protection, element proportioning is unreasonable, specific aim is not strong, usage quantity is large, the problem that valency is high.Application number 201010514241.X, applying date 2010.10.21, Authorization Notice No. CN102180721B, authorized announcement date 2013.03.27, denomination of invention is: the Chinese patent of " promoting the nutrient substance of fruit and seed class medicinal plant growth ", disclose the nutrient substance promoting the growth of fruit and seed class medicinal plant, it is made up of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, glucose, amino acid and trace element, its weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, glucose 20-70%, amino acid/11 0-20%, micro-10-30%.This patent exists that composition activeconstituents is more not to be saved, and not rationally, not easily standing storage and preparation method are simple not for activeconstituents proportioning, and purposes is problem not widely.
Summary of the invention
Object of the present invention overcomes above-mentioned deficiency exactly, one is provided to decrease activeconstituents in composition, composition proportion is reasonable, and its effect still can meet or exceed the patent No. and be: the preparation method of nutrient substance of the fruit and seed class medicinal plant of " 201010514241.X " and the purposes of this nutrient substance
The present invention is achieved in that
The preparation method of the nutrient substance of fruit and seed class medicinal plant, described fruit and seed class medicinal plant refers to cape jasmine;
Described method the steps include: that a. gets 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams;
B. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Or:
C. 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt is got, trace element 4 grams;
D. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Described trace element refers to: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn:B:Fe:Zn:Cu:Mo=5:3:3:3:2:1;
Described Nucleotide sylvite refers to: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, 5 '-uridylic acid dipotassium, the di-potassium of four kinds of 5 '-mixed nucleotides; Described deoxynucleoside acid potassium salt refers to: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, 5 '-deoxythymidylic acid dipotassium, the di-potassium of five kinds of 5 '-deoxidation mixed nucleotides.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, described fruit and seed class medicinal plant refers to cape jasmine;
Described nutrient substance is: 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams; Or:
5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 4 grams;
Method for making is: get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, described fruit and seed class medicinal plant refers to cape jasmine; Nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate 2 grams, trace element 2 grams of compositions; Or by: 5 grams of nucleosides hydrochlorates and deoxynucleoside hydrochlorate, trace element 4 grams of compositions; Not comprising glucose or/and amino acid in ideal nutrient composition, its preparation, take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside hydrochlorate is molten
Liquid, filters, and filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got; Nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieves.
Described preparation method, is characterized in that, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
Promote the nutrient substance of fruit and seed class medicinal plant growth, screening formulation weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 40-60%, micro-40-60%.
Promote the nutrient substance of fruit and seed class medicinal plant growth,: nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, the sylvite of 5 '-uridylic acid dipotassium, four kinds of 5 '-mixed nucleotides.
Promote the nutrient substance of fruit and seed class medicinal plant growth, nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) disodium, 5 '-bird adenylic acid (AMP) disodium, 5 '-cytidylic acid disodium, the sodium salt of 5 '-uridine monophosphate disodium, four kinds of 5 '-mixed nucleotides.
Promote the nutrient substance of fruit and seed class medicinal plant growth, deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.
Promote the nutrient substance of fruit and seed class medicinal plant growth, it is characterized in that: trace element refers to: Mn, B, Fe, Zn, Cu, Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate.
Promote the nutrient substance of fruit and seed class medicinal plant growth, the weight ratio of trace element is: Mn: B: Fe: Zn: Cu: Mo=5: 3: 3: 3: 2: 1.
Promote the nutrient substance of fruit and seed class medicinal plant growth, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate.
Promote the nutrient substance of fruit and seed class medicinal plant growth, the weight percent of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, micro-10-30%, weighting agent 20-80%.
Promote the nutrient substance of fruit and seed class medicinal plant growth, weighting agent is: one or more of W-Gum, dextrin, Mierocrystalline cellulose, polyvidone, the weight percent of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 15-20%, trace element 15-20%, weighting agent 40-70%.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element composition, glucose is not comprised or/and amino acid in ideal nutrient composition, its weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 30-70%, trace element 30-70%, its preparation take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside acid salt solution, filters, and filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got;
, nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieve.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, screening formulation weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 40-60%, micro-40-60%.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, the potassium of 5 '-uridylic acid dipotassium or sodium four kinds of 5 '-mixed nucleotides or sodium salt.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, trace element refers to: Mn, B, Fe, Zn, Cu, Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, the weight ratio of trace element is: Mn: B: Fe: Zn: Cu: Mo=5: 3: 3: 3: 2: 1.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, composition also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weighting agent adding pulverizing mixes with nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element, the weight percent of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, trace element 10-30%, weighting agent 20-80%.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element composition, glucose is not comprised or/and amino acid in ideal nutrient composition, its weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 30-70%, trace element 30-70%, its preparation: be by weight percentage: nucleosides hydrochlorate 85-99%, deoxynucleoside hydrochlorate 1-15%, get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve.
The purposes of the nutrient substance of fruit and seed class medicinal plant, the application in the growth promoting fruit and seed class medicinal plant as fertilizer or plant-growth regulator; Or be applied to fruit and seed class medicinal plant and produce and can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The production method of fruit and seed class Chinese medicine, nutrient substance is used: described nutrient substance is: primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element composition in its process of growth, glucose is not comprised or/and amino acid in ideal nutrient composition, its weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 30-70%, micro-30-70%.
The application process of described nutrient substance is: spray with after water dissolution.
The production method of fruit and seed class Chinese medicine is 100-400ppm by the concentration sprayed after water dissolution.
The production method of fruit and seed class Chinese medicine, also weighting agent is comprised in described ideal nutrient composition, described weighting agent is one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nutrient compositions is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, trace element 10-30%, weighting agent 20-80%.
The production method of fruit and seed class Chinese medicine, the opportunity of using of described nutrient substance is: before the bud stage of fruit and seed class Chinese medicinal materials or/and initial bloom stage and full-bloom stage each once.
The production method of fruit and seed class Chinese medicine, the opportunity of using of described nutrient substance is: respectively at the initial bloom stage of fruit and seed class Chinese medicinal materials and full-bloom stage once and at fruit development period and fruit expanding period respectively spray once or respectively spray once at fruit development period and fruit expanding period.
The production method of fruit and seed class Chinese medicine, the consumption of described nutrient substance is every mu of 2-8 gram, is every mu of 20-40 liter by water-soluble water consumption.
The production method of fruit and seed class Chinese medicine, the consumption of described nutrient substance is every mu of 15-30 gram, is every mu of 20-40 liter by water-soluble water consumption.
The production method of fruit and seed class Chinese medicine, nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, the dipotassium of 5 '-uridylic acid dipotassium or sodium four kinds of 5 '-mixed nucleotides or disodium salt; Deoxynucleoside hydrochlorate refers to: obtain after thymus nucleic acid basic hydrolysis: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, the disodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or di-potassium.
The production method of fruit and seed class Chinese medicine, trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn:B:Fe:Zn:Cu:Mo=5:3:3:3:2:1.
The production method of fruit and seed class Chinese medicine, the fruit and seed class Chinese medicinal materials 80%-90% size of results is even, its output is than the high 20-40% of produced in conventional processes, the fruit and seed class Chinese medicinal materials of results, than the high 20-50% of produced in conventional processes, is made high-quality medicine materical crude slice or the extracting effective components yield fruit and seed class Chinese medicinal materials height 15-49% than produced in conventional processes by its Contents of Main Components.
Weighting agent of the present invention: starch refers to: green starch, yam starch, wheat starch, sweet potato starch, W-Gum, water caltrop starch, Lotus Root Starch, Chinese Water Chestnut Starch etc., preferred W-Gum.Dextrin refers to: white dextrin, yellow starch gum and Britain glue, cyclodextrin.Mierocrystalline cellulose refers to: methylcellulose gum, Vltra tears, Natvosol, carboxymethyl cellulose etc.
The preparation method of the nutrient substance of Promoting plant growth provided by the present invention, concrete steps are as follows: take nucleic acid as raw material: one is for raw material with commercially available nucleic acid, two is adopt the nucleic acid of dry method or wet production to be raw material from the mycelium after fermentation plant fermentation: 1., the hydrolysis of nucleic acid is the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid of 1:20-30 according to nucleic acid, buck weight ratio, alkali lye is 5.5-7N, under 30-45 DEG C of condition, stir 10-14 hours, obtain nucleosides hydrochlorate and deoxynucleoside acid salt solution, filter, filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry: concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization: dissolve the nucleosides hydrochlorate after doing and deoxynucleoside hydrochlorate with clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate (from the mycelium after fermentation plant fermentation adopt the nucleic acid of dry method or wet production be raw material also containing water soluble mixt and impurity);
4., trace element is got;
, nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieve.
In nucleic acid hydrolysis process described in this preparation method, alkali lye used is sodium hydroxide or potassium hydroxide solution.
With commercially available nucleic acid for raw material, impure few after hydrolysis.
In the present invention, nucleosides hydrochlorate mainly refers to: 5 '-adenylic acid (AMP) disodium or potassium, 5 '-bird adenylic acid (AMP) disodium or potassium, 5 '-cytidylic acid disodium or potassium, the sodium salt of 5 '-uridine monophosphate disodium or potassium four kinds of 5 '-mixed nucleotides or sylvite; Deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.The source of nucleosides hydrochlorate and deoxynucleoside hydrochlorate is take nucleic acid as raw material, mainly the nucleic acid of dry method or wet production is adopted to be raw material from the mycelium after fermentation plant fermentation, this kind of nucleic acid is a small amount of thymus nucleic acid (DNA) of main mixing with Yeast Nucleic Acid (RNA), makes with alkali lye hydrolysis.
Beneficial effect of the present invention:
Because the present invention is not sugary or/and amino acid, decrease composition activeconstituents, so more economize in raw materials and cost.
Coordinate nucleosides hydrochlorate and deoxynucleoside hydrochlorate, reasonable ratio because the present invention contains trace element, promote the growth of fruit and seed class medicinal plant more targeted specifically.
Although the present invention decreases activeconstituents, its effect does not still subtract and even produces better effect.
The present invention is not particularly containing glucose, glucose easily absorbs moisture deliquescence, nutrient substance containing glucose places the deliquescence that namely absorbs water more than a year under general condition of storage, there is product caking, nucleosides hydrochlorate and deoxynucleoside hydrochlorate are hydrolyzed further, cause quality product to reduce even to lose efficacy, so, the invention solves the problem of the not easily standing storage of nutrient substance.
Because the present invention also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc., the relevant regulations being generally not less than 20 grams as the foliage fertilizer minimum package of merchandise sales are adapted to the adding of weighting agent; Filler starch, dextrin, Mierocrystalline cellulose etc. also possess certain viscosity, make nutrient substance be attached to blade face after spraying and the plant surface time longer, make its action effect better; Weighting agent polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc. have dispersiveness and oilness, can extend the quality guaranteed period of nutrient substance.
Due to preparation method of the present invention: (1), the nucleic acid of dry method or wet production can be adopted to be raw material from byproduct (tankage) mycelium after fermentation plant (active sludge, petroleum fermentation etc. after Gourmet Powder Factory, brew-house, antibiotics plant, yeast factory, Amino Acid Factory, paper mill, sewage disposal) fermentation, its price of this nucleic acid is low, is easy to cost-saving; (2), can adopt the preparation method be hydrolyzed for raw material with commercially available nucleic acid, products pure degree is high, and the proportioning of Yeast Nucleic Acid and thymus nucleic acid can adjust, product suitability and better effects if; (3), also can directly with commercially available 5 '-adenylic acid (AMP) disodium or potassium, 5 '-Sodium guanylate or potassium, 5 '-cytidylic acid disodium or potassium, 5 '-uridine monophosphate disodium or potassium and 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite preparation; Add trace element again, form the present invention, be therefore suitable for more flexible, technique is simpler.
Purposes of the present invention is: as fertilizer particularly as foliage fertilizer or nutrient substance or the application of plant-growth regulator in the growth promoting fruit and seed class medicinal plant; Or be applied to fruit and seed class medicinal plant and produce and can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The present invention is applied to the growth promoting fruit and seed class medicinal plant, with strong points, can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
So product of the present invention: saving, environmental protection (nontoxic, harmless, noresidue, without any adverse side effect), comprehensive to fruit and seed class medicinal plant purposes, increase production, increase income, synergy, strengthen resistance, improve quality effective.
The present invention and 201010514241.X patent, traditional product and method contrast table 1
The present invention and 201010514241.X patent, traditional product and method contrast table 2
The present invention implements to spray agency part effect in table 3 to concrete crop
Note: content's index detection method is carried out with reference to national standard or industry standard, content is pressed dry product and is calculated
Embodiment:
Embodiment 1: get 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams, pulverizes Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element, sieves, mix.
Embodiment 2: get 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt trace element 4 grams, pulverizes Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element, sieves, mix, obtain nutrient substance.
Embodiment 3: take 7 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt (or sodium salt), trace element 5 grams, mixing, pulverizing, sieve, obtain nutrient substance.
Embodiment 4: get commercially available Nucleotide potassium or sodium salt and deoxynucleotide potassium or sodium salt 10 grams, trace element 10 grams, W-Gum 50 grams, Magnesium Stearate 30 grams, mix.
Embodiment 5: get Nucleotide potassium or sodium salt 90 grams, deoxynucleotide potassium or sodium salt 10 grams, mixing; Get trace element 100 grams again, Xylo-Mucine 800 grams, remix, pulverizing, excessively 90 mesh sieves.
Embodiment 6: by 100 grams, the crude product Yeast Nucleic Acid (RNA) obtained from the mycelium of fermentation plant's byproduct by dry method or wet method, be dissolved in the sodium hydroxide solution of 3 liters of 6.3N, under 37 DEG C of conditions, stir 12 hours, obtain and mainly refer to contain: 5 '-adenylic acid (AMP) disodium, 5 '-bird adenylic acid (AMP) disodium, 5 '-cytidylic acid disodium, the sodium salt of 5 '-uridine monophosphate disodium, four kinds of 5 '-mixed nucleotides (also has deoxynucleoside hydrochlorate: 5 '-Desoxyadenosine acid disodium, 5 '-deoxidation bird adenylic acid (AMP) disodium, 5 '-Deoxyribose cytidine acid disodium, 5 '-deoxyuridine acid disodium, , the sodium salt of 5 '-deoxythymidine acid disodium, five kinds of 5 '-deoxidation mixed nucleotides and the solution of impurity), filter, filtrate is neutralized to pH8-8.5, be evaporated to appropriate, concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 15%, nearly dry new-nucleo and Sodium Deoxyribomuleotide is dissolved by proper amount of clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, about obtain 85-90 grams, white core thuja acid salt and deoxynucleoside hydrochlorate and water soluble mixt impurity, get 90 grams of trace elements again to mix with it, mixture is pulverized, cross 100 mesh sieves.
Embodiment 7: by 100 grams, the crude product Yeast Nucleic Acid (RNA) obtained from the mycelium of fermentation plant's byproduct by dry method or wet method, be dissolved in the potassium hydroxide solution of 2.5 liters of 6N, under 40 DEG C of conditions, stir 10 hours, obtain and mainly refer to contain: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, the sylvite of 5 '-uridylic acid dipotassium, four kinds of 5 '-mixed nucleotides, also has deoxynucleoside hydrochlorate: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, , the sylvite of 5 '-deoxythymidylic acid dipotassium, five kinds of 5 '-deoxidation mixed nucleotides and impurity (amino acid, sugar part and nitrogen, phosphorus, potassium, iron, calcium, magnesium, zinc, copper, manganese etc.) solution, filter, filtrate is neutralized to pH8-8.5, be evaporated to appropriate, concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume to 20%, nearly dry Nucleotide potassium and deoxynucleotide potassium is dissolved by proper amount of clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, about 88-93 grams of white core thuja acid sylvite and deoxynucleoside acid potassium salt and water soluble mixt impurity, get 80 grams of trace elements again to mix with it, mixture is pulverized, cross 80 mesh sieves.
Embodiment 7: by commercially available nucleosides hydrochlorate 90 grams, deoxynucleoside hydrochlorate 10 grams, mixing, be dissolved in the potassium hydroxide solution of 2.5 liters of 6N, under 40 DEG C of conditions, stir 10 hours, must contain: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, the sylvite of 5 '-uridylic acid dipotassium, four kinds of 5 '-mixed nucleotides, also has deoxynucleoside hydrochlorate: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, , the solution of the sylvite of 5 '-deoxythymidylic acid dipotassium, five kinds of 5 '-deoxidation mixed nucleotides, filter, filtrate is neutralized to pH8-8.5, be evaporated to appropriate, concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume to 20%, nearly dry Nucleotide potassium and deoxynucleotide potassium is dissolved by proper amount of clear water, its solution adds alcohol and separates out, and crystallization suction filtration is dry, about obtains 95-98 grams of white core thuja acid sylvite and deoxynucleoside acid potassium salt, get 120 grams of trace elements again to mix with it, mixture is pulverized, cross 120 mesh sieves.
Embodiment 8: snakegourd: perennial herbaceous stem rattan wood, after cultivation, Second Year sprays three times every year, and first time, at stem climing length 30 cm, with 4 grams of nutrient substances, is watered 20 liters, evenly sprays on snakegourd rattan leaf; Second time, at the plant blossom initial stage, is filled a prescription by embodiment 3, is watered 30 liters, evenly spray on one mu of snakegourd, and third time, at full-bloom stage, fills a prescription by embodiment 2, is watered 40 liters, evenly spray on one mu of snakegourd.Snakegourd can increase production 20%-30%, and the root (Snakegourd Root) of snakegourd also can increase production more than 30% simultaneously.
Embodiment 9: cape jasmine: respectively spray once at initial bloom stage and full-bloom stage, fill a prescription by embodiment 1, be watered 30 liters, evenly sprays on one mu of cape jasmine; Respectively spray once again at fruit development period and fruit expanding period: fill a prescription by embodiment 2, convert 30 premium on currency, evenly spray on one mu of cape jasmine; Can reduce shedding 60-80%, stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size evenly, jasminoidin and crocin content is respectively higher than existing standards of pharmacopoeia 20-36%.
Claims (4)
1. the preparation method of the nutrient substance of fruit and seed class medicinal plant, is characterized in that: described fruit and seed class medicinal plant refers to cape jasmine;
Described method the steps include: that a. gets 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams;
B. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Or:
C. 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt is got, trace element 4 grams;
D. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Described trace element refers to: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn:B:Fe:Zn:Cu:Mo=5:3:3:3:2:1;
Described Nucleotide sylvite refers to: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, 5 '-uridylic acid dipotassium, the di-potassium of four kinds of 5 '-mixed nucleotides; Described deoxynucleoside acid potassium salt refers to: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, 5 '-deoxythymidylic acid dipotassium, the di-potassium of five kinds of 5 '-deoxidation mixed nucleotides.
2. the preparation method of the nutrient substance of fruit and seed class medicinal plant, is characterized in that: described fruit and seed class medicinal plant refers to cape jasmine;
Described nutrient substance is: 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams; Or:
5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 4 grams;
Method for making is: get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve.
3. the preparation method of the nutrient substance of fruit and seed class medicinal plant, is characterized in that: described fruit and seed class medicinal plant refers to cape jasmine; Nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate 2 grams, trace element 2 grams of compositions; Or by: 5 grams of nucleosides hydrochlorates and deoxynucleoside hydrochlorate, trace element 4 grams of compositions; Not comprising glucose or/and amino acid in ideal nutrient composition, its preparation, take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside hydrochlorate is molten
Liquid, filters, and filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got; Nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieves.
4. preparation method according to claim 3, is characterized in that, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
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| CN201510398461.3A CN105016867A (en) | 2013-11-19 | 2013-11-19 | Application of fruit seed type medicinal plant nutrient |
| CN201310579841.8A CN103613423B (en) | 2013-11-19 | 2013-11-19 | The preparation method of the nutrient substance of fruit and seed class medicinal plant |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000063138A1 (en) * | 1999-04-16 | 2000-10-26 | Miller Chemical & Fertilizer Corporation | Soluble fertilizer formulation |
| CN102180721A (en) * | 2010-10-21 | 2011-09-14 | 高旌 | Nutrient for promoting growth of fruit seed medicinal plant |
| CN103113166A (en) * | 2010-10-21 | 2013-05-22 | 高旌 | Production method with good quality and high yield for medicinal plants trichosanthes kirilowii maxim and radices trichosanthis |
| CN103141201A (en) * | 2010-10-21 | 2013-06-12 | 高旌 | Good-quality and high-yield production method of fruit and seed medicinal plants |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102079665B (en) * | 2010-10-21 | 2013-06-12 | 高旌 | Nutrient for enhancing plant growth and preparation method thereof |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000063138A1 (en) * | 1999-04-16 | 2000-10-26 | Miller Chemical & Fertilizer Corporation | Soluble fertilizer formulation |
| US6241795B1 (en) * | 1999-04-16 | 2001-06-05 | Miller Chemical And Fertilizer Corporation | Soluble fertilizer formulation |
| CN102180721A (en) * | 2010-10-21 | 2011-09-14 | 高旌 | Nutrient for promoting growth of fruit seed medicinal plant |
| CN103113166A (en) * | 2010-10-21 | 2013-05-22 | 高旌 | Production method with good quality and high yield for medicinal plants trichosanthes kirilowii maxim and radices trichosanthis |
| CN103141201A (en) * | 2010-10-21 | 2013-06-12 | 高旌 | Good-quality and high-yield production method of fruit and seed medicinal plants |
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| CN105016867A (en) | 2015-11-04 |
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Effective date of registration: 20170328 Address after: 236800 Anhui Province, Bozhou City Industrial Park, Anhui road vibration Qiao e g Chinese herbal medicine limited liability company Patentee after: Anhui Chinese Medicine Co., Ltd. Address before: 230001 Luyang, Anhui Province, Taoyuan Road, No. 66, No. 107, China Railway Park, room, room 3 Patentee before: Hefei Kaige Information Technology Co., Ltd. |
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