CN105016867A - Application of fruit seed type medicinal plant nutrient - Google Patents
Application of fruit seed type medicinal plant nutrient Download PDFInfo
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- CN105016867A CN105016867A CN201510398461.3A CN201510398461A CN105016867A CN 105016867 A CN105016867 A CN 105016867A CN 201510398461 A CN201510398461 A CN 201510398461A CN 105016867 A CN105016867 A CN 105016867A
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Abstract
The invention discloses an application of fruit seed type medicinal plant nutrient. The medicinal plant is gardenia. The nutrient is obtained through the following steps: a, 2g or 5g of potassium nucleotide and potassium deoxynucleotide, and 2g or 4g of trace elements are respectively fetched; b, the potassium nucleotide, potassium deoxynucleotide and trace elements are crushed, sieved and well mixed; or, commercially available nucleotide salt and deoxynucleotide salt are mixed, commercially available trace elements are mixed into the mixture, and the mixture is crushed and sieved; or, nucleic acid is subjected to hydrolysis and decolorization, and drying and crystallization are carried out, such that nucleotide salt and deoxynucleotide salt are obtained, and the nucleotide salt and deoxynucleotide salt are mixed with trace elements. The nutrient can be applied as a fertilizer or a plant growth regulator in promoting the growth of the fruit seed type medicinal plant gardenia. The nutrient can also be used for producing gardenia fruit. With the nutrient, geniposide content is higher than 2.1%; geniposide and crocin contents are respectively higher by 20-36% than in current Pharmacopoeia standards; fruit drop can be reduced by 60-80%; yield increasing rate is higher than 36%; 80-90% of the fruits have uniform sizes; and effective component extraction yield is high.
Description
The application is application number: 201310579841.8, the applying date: on November 19th, 2013, and denomination of invention is the divisional application of " preparation method and its usage of the nutrient substance of fruit and seed class medicinal plant ".
Technical field
The present invention relates to the preparation method and its usage for promoting the nutrient substance that fruit and seed class medicinal plant grows, special
It not the preparation method and its usage of fertilizer or the plant-growth regulator needed during a kind of fruit and seed class medicinal plant is produced.
Background technology
Medicinal plant industry is a large industry of natural medicaments, greatly develop Chinese Medicine Industry, promote Chinese medicinal materials increasing both production and income, crude drug is made to move towards world market further, promote the modernization of Chinese medicine, it is the problem that China Chinese medicine scientist pays close attention to research, Chinese medicinal materials is fruit particularly, the growth of planting subclass Chinese medicinal materials be unable to do without and supplements corresponding nutrition, at present, fruit, the nutrient substance of planting the growth of subclass medicinal plant is exactly fertilizer, all be used in the very wide general fertilizer of planting range, even if present medicinal material fertilizer, main by executing nitrogen, phosphorus, potassic fertilizer and organic fertilizer and medium trace element carry out growth promoting effects, Chinese patent open (publication number CN 1900028A) discloses a kind of fertilizer special for Chinese medicine material, and it adopts the big-and-middle microelement match of adjustment different, to adapt to different Chinese medicinal materialss, it remains a kind of common fertilizer, exist and use too much, the quality and flavor of fertilizer to Chinese medicinal materials has certain detrimentally affect, be unfavorable for the development of green agriculture and food safety and environmental protection, element proportioning is unreasonable, specific aim is not strong, usage quantity is large, the problem that valency is high.Application number 201010514241.X, applying date 2010.10.21, Authorization Notice No. CN 102180721 B, authorized announcement date 2013.03.27, denomination of invention is: the Chinese patent of " promoting the nutrient substance of fruit and seed class medicinal plant growth ", disclose the nutrient substance promoting the growth of fruit and seed class medicinal plant, it is by nucleosides hydrochlorate and deoxynucleoside hydrochlorate, glucose, amino acid and trace element composition, its weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30 %, glucose 20-70%, amino acid/11 0-20%, trace element 10-30%.This patent exists that composition activeconstituents is more not to be saved, and not rationally, not easily standing storage and preparation method are simple not for activeconstituents proportioning, and purposes is problem not widely.
Summary of the invention
Object of the present invention overcomes above-mentioned deficiency exactly, provides one to decrease activeconstituents in composition, composition proportion
Rationally, its effect still can meet or exceed the patent No. and is: the fruit and seed class of " 201010514241.X " is medicinal plants
The preparation method of the nutrient substance of thing and the purposes of this nutrient substance.
The present invention is achieved in that
The purposes of the nutrient substance of fruit and seed class medicinal plant, described nutrient substance is in order to the standby nutrient substance of below legal system:
Described method the steps include: that a. gets 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams;
B. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Or:
C. 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt is got, trace element 4 grams;
D. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Described trace element refers to: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn::B:Fe: Zn::Cu: Mo=5:3:3:3:2:1;
Described Nucleotide sylvite refers to: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, 5 '-uridylic acid dipotassium, the di-potassium of four kinds of 5 '-mixed nucleotides; Described deoxynucleoside acid potassium salt refers to: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, 5 '-deoxythymidylic acid dipotassium, the di-potassium of five kinds of 5 '-deoxidation mixed nucleotides;
The application in the growth promoting fruit and seed class medicinal plant cape jasmine as fertilizer or plant-growth regulator of this nutrient substance;
Or be applied to fruit and seed class medicinal plant cape jasmine produce make described cape jasmine:
Determination of Gardenoside is greater than 2.1%;
Jasminoidin and crocin content are respectively higher than existing standards of pharmacopoeia 20-36%;
Cape jasmine can reduce shedding 60-80%, and stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size is even;
Cape jasmine extracting effective components yield can reach 149% of the cape jasmine than produced in conventional processes.
The purposes of the nutrient substance of fruit and seed class medicinal plant, described nutrient substance is in order to the standby nutrient substance of below legal system:
2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams; Or: 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 4 grams; Get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve;
The application in the growth promoting fruit and seed class medicinal plant cape jasmine as fertilizer or plant-growth regulator of this nutrient substance;
Or be applied to fruit and seed class medicinal plant cape jasmine produce make described cape jasmine:
Determination of Gardenoside is greater than 2.1%;
Jasminoidin and crocin content are respectively higher than existing standards of pharmacopoeia 20-36%;
Cape jasmine can reduce shedding 60-80%, and stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size is even;
Cape jasmine extracting effective components yield can reach 149% of the cape jasmine than produced in conventional processes.
The purposes of the nutrient substance of fruit and seed class medicinal plant, described nutrient substance is made up of nucleosides hydrochlorate and deoxynucleoside hydrochlorate 2 grams, trace element 2 grams; Or by: 5 grams of nucleosides hydrochlorates and deoxynucleoside hydrochlorate, trace element 4 grams of compositions; Not comprising glucose or/and amino acid in ideal nutrient composition, its preparation, take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside hydrochlorate is molten
Liquid, filters, and filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got; Nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieves;
The application in the growth promoting fruit and seed class medicinal plant cape jasmine as fertilizer or plant-growth regulator of this nutrient substance; Or be applied to fruit and seed class medicinal plant cape jasmine produce make described cape jasmine:
Determination of Gardenoside is greater than 2.1%;
Jasminoidin and crocin content are respectively higher than existing standards of pharmacopoeia 20-36%;
Cape jasmine can reduce shedding 60-80%, and stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size is even;
Cape jasmine extracting effective components yield can reach 149% of the cape jasmine than produced in conventional processes.
The purposes of the nutrient substance of fruit and seed class medicinal plant, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, described fruit and seed class medicinal plant refers to cape jasmine;
Described method the steps include: that a. gets 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams;
B. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Or:
C. 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt is got, trace element 4 grams;
D. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Described trace element refers to: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn::B:Fe: Zn::Cu: Mo=5:3:3:3:2:1;
Described Nucleotide sylvite refers to: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, 5 '-uridylic acid dipotassium, the di-potassium of four kinds of 5 '-mixed nucleotides; Described deoxynucleoside acid potassium salt refers to: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, 5 '-deoxythymidylic acid dipotassium, the di-potassium of five kinds of 5 '-deoxidation mixed nucleotides.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, described fruit and seed class medicinal plant refers to cape jasmine;
Described nutrient substance is: 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams; Or:
5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 4 grams;
Method for making is: get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, described fruit and seed class medicinal plant refers to cape jasmine; Nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate 2 grams, trace element 2 grams of compositions; Or by: 5 grams of nucleosides hydrochlorates and deoxynucleoside hydrochlorate, trace element 4 grams of compositions; Not comprising glucose or/and amino acid in ideal nutrient composition, its preparation, take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside hydrochlorate is molten
Liquid, filters, and filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got; Nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieves.
Described preparation method, is characterized in that, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
Promote the nutrient substance of fruit and seed class medicinal plant growth, it is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace unit
Element composition, do not comprise glucose or/and amino acid in ideal nutrient composition, its weight percent is: nucleosides hydrochlorate and deoxynucleoside
Hydrochlorate 30-70%, micro-30-70%.
Promote the nutrient substance of fruit and seed class medicinal plant growth, screening formulation weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 40-60%, micro-40-60%.
Promote the nutrient substance of fruit and seed class medicinal plant growth,: nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, the sylvite of 5 '-uridylic acid dipotassium, four kinds of 5 '-mixed nucleotides.
Promote the nutrient substance of fruit and seed class medicinal plant growth, nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) disodium, 5 '-bird adenylic acid (AMP) disodium, 5 '-cytidylic acid disodium, the sodium salt of 5 '-uridine monophosphate disodium, four kinds of 5 '-mixed nucleotides.
Promote the nutrient substance of fruit and seed class medicinal plant growth, deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.
Promote the nutrient substance of fruit and seed class medicinal plant growth, it is characterized in that: trace element refers to: Mn, B, Fe, Zn, Cu, Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate.
Promote the nutrient substance of fruit and seed class medicinal plant growth, the weight ratio of trace element is:
Mn ∶ B ∶ Fe ∶ Zn ∶ Cu ∶ Mo ＝ 5 ∶ 3 ∶ 3 ∶ 3 ∶ 2 ∶ 1。
Promote the nutrient substance of fruit and seed class medicinal plant growth, it also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate.
Promote the nutrient substance of fruit and seed class medicinal plant growth, the weight percent of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, micro-10-30%, weighting agent
20-80％。
Promote the nutrient substance of fruit and seed class medicinal plant growth, weighting agent is: one or more of W-Gum, dextrin, Mierocrystalline cellulose, polyvidone, the weight percent of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 15-20%, trace element 15-20%, weighting agent 40-70%.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element composition, glucose is not comprised or/and amino acid in ideal nutrient composition, its weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 30-70%, trace element 30-70%, its preparation take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside acid salt solution, mistake
Filter, filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got; , nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieve.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, screening formulation weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 40-60%, micro-40-60%.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-adenylic acid (AMP) dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, the potassium of 5 '-uridylic acid dipotassium or sodium four kinds of 5 '-mixed nucleotides or sodium salt.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, trace element refers to: Mn, B, Fe, Zn, Cu, Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, the weight ratio of trace element is: Mn: B: Fe: Zn: Cu: Mo=5: 3: 3: 3: 2: 1.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, composition also comprises weighting agent: one or more of starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weighting agent adding pulverizing mixes with nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element, the weight percent of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element and weighting agent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, trace element 10-30%, weighting agent 20-80%.
The preparation method of the nutrient substance of fruit and seed class medicinal plant, nutrient substance is primarily of nucleosides hydrochlorate and deoxynucleoside
Hydrochlorate, trace element composition, do not comprise glucose or/and amino acid in ideal nutrient composition, its weight percent is: nucleosides
Hydrochlorate and deoxynucleoside hydrochlorate 30-70%, micro-30-70%, its preparation: be by weight percentage: nucleosides hydrochlorate
85-99%, deoxynucleoside hydrochlorate 1-15%, get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again,
Remix, pulverize, sieve.
The purposes of the nutrient substance of fruit and seed class medicinal plant, the application in the growth promoting fruit and seed class medicinal plant as fertilizer or plant-growth regulator; Or be applied to fruit and seed class medicinal plant produce can improve its Yield and quality,
Quality, strengthen resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The production method of fruit and seed class Chinese medicine, uses nutrient substance: described nutrient substance is: main in its process of growth
Be made up of nucleosides hydrochlorate and deoxynucleoside hydrochlorate, trace element, in ideal nutrient composition, do not comprise glucose or/and amino acid, its
Weight percent is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 30-70%, micro-30-70%.
The application process of described nutrient substance is: spray with after water dissolution.
The production method of fruit and seed class Chinese medicine is 100-400ppm by the concentration sprayed after water dissolution.
The production method of fruit and seed class Chinese medicine, also comprises weighting agent in described ideal nutrient composition, and described weighting agent forms sediment
One or more of powder, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate, the weight percent of nutrient compositions is: nucleosides hydrochlorate and deoxynucleoside hydrochlorate 10-30%, micro-10-30%, weighting agent 20-80%.
The production method of fruit and seed class Chinese medicine, the opportunity of using of described nutrient substance is: at fruit and seed class Chinese medicinal materials
Before bud stage or/and initial bloom stage and full-bloom stage each once.
The production method of fruit and seed class Chinese medicine, the opportunity of using of described nutrient substance is: at the initial bloom stage of fruit and seed class Chinese medicinal materials and full-bloom stage is each once and at fruit development period and fruit expanding period respectively to spray once or fruit development period and fruit again
Real expanding stage respectively sprays once.
The production method of fruit and seed class Chinese medicine, the consumption of described nutrient substance is every mu of 2-8 gram, with water-soluble water
Amount is every mu of 20-40 liter.
The production method of fruit and seed class Chinese medicine, the consumption of described nutrient substance is every mu of 15-30 gram, is every mu of 20-40 liter by water-soluble water consumption.
The production method of fruit and seed class Chinese medicine, nucleosides hydrochlorate refers to: obtain after Yeast Nucleic Acid basic hydrolysis: 5 '-gland
Thuja acid dipotassium or sodium, 5 '-bird adenylic acid (AMP) dipotassium or sodium, 5 '-cytidylic acid dipotassium or sodium, the dipotassium of 5 '-uridylic acid dipotassium or sodium four kinds of 5 '-mixed nucleotides or disodium salt; Deoxynucleoside hydrochlorate refers to: obtain after thymus nucleic acid basic hydrolysis
: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, the disodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or di-potassium.
The production method of fruit and seed class Chinese medicine, trace element refers to: Mn, B, Fe, Zn, Cu or Mo, specifically: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn:B:Fe:
Zn:Cu:Mo=5:3:3:3:2:1。
The production method of fruit and seed class Chinese medicine, the fruit and seed class Chinese medicinal materials 80%-90% size of results is even, and it produces
Measure than the high 20-40% of produced in conventional processes, its Contents of Main Components than the high 20-50% of produced in conventional processes, by the fruit of results
High-quality medicine materical crude slice or the extracting effective components yield fruit and seed class Chinese medicinal materials than produced in conventional processes made by real subclass Chinese medicinal materials of planting
High 15-49%.
Weighting agent of the present invention: starch refers to: green starch, yam starch, wheat starch, sweet potato starch, W-Gum, water caltrop starch, Lotus Root Starch, Chinese Water Chestnut Starch etc., preferred W-Gum.Dextrin refers to: white dextrin, yellow starch gum and Britain glue, cyclodextrin.Mierocrystalline cellulose refers to: methylcellulose gum, Vltra tears, Natvosol, carboxymethyl cellulose etc.
The preparation method of the nutrient substance of Promoting plant growth provided by the present invention, concrete steps are as follows: be former with nucleic acid
Material: one is with commercially available nucleic acid for raw material, two is the core adopting dry method or wet production from the mycelium after fermentation plant fermentation
Acid is for raw material: 1., the hydrolysis of nucleic acid is the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid of 1:20-30 according to nucleic acid, buck weight ratio, alkali lye is 5.5-7N, under 30-45 DEG C of condition, stir 10-14 hours, obtain nucleosides hydrochlorate and deoxynucleoside acid salt solution, filter, filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry: concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization: dissolve the nucleosides hydrochlorate after doing and deoxynucleoside hydrochlorate with clear water, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate (the mycelium employing dry method after fermenting from fermentation plant or wet method life
The nucleic acid produced be raw material also containing water soluble mixt and impurity);
4., trace element is got;
, nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieve.
In nucleic acid hydrolysis process described in this preparation method, alkali lye used is sodium hydroxide or potassium hydroxide solution.
With commercially available nucleic acid for raw material, impure few after hydrolysis.
In the present invention, nucleosides hydrochlorate mainly refers to: 5 '-adenylic acid (AMP) disodium or potassium, 5 '-bird adenylic acid (AMP) disodium or potassium,
5 '-cytidylic acid disodium or potassium, the sodium salt of 5 '-uridine monophosphate disodium or potassium four kinds of 5 '-mixed nucleotides or sylvite; Deoxynucleoside hydrochlorate refers to: 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium,, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite.The source of nucleosides hydrochlorate and deoxynucleoside hydrochlorate is take nucleic acid as raw material, mainly the nucleic acid of dry method or wet production is adopted to be raw material from the mycelium after fermentation plant fermentation, this kind of nucleic acid is a small amount of thymus nucleic acid (DNA) of main mixing with Yeast Nucleic Acid (RNA), makes with alkali lye hydrolysis.
Beneficial effect of the present invention:
Because the present invention is not sugary or/and amino acid, decrease composition activeconstituents, so more economize in raw materials and cost.
Nucleosides hydrochlorate and deoxynucleoside hydrochlorate is coordinated, reasonable ratio, more targeted specifically because the present invention contains trace element
Promote the growth of fruit and seed class medicinal plant.
Although the present invention decreases activeconstituents, its effect does not still subtract and even produces better effect.
The present invention is not particularly containing glucose, and glucose easily absorbs moisture deliquescence, and the nutrient substance containing glucose is generally
Place the deliquescence that namely absorbs water more than a year under condition of storage, occur that product lumps, make nucleosides hydrochlorate and the further water of deoxynucleoside hydrochlorate
Separate, cause quality product to reduce and even lost efficacy, so, the invention solves the problem of the not easily standing storage of nutrient substance.
Because the present invention also comprises weighting agent: starch, dextrin, Mierocrystalline cellulose, polyvidone, Magnesium Stearate, calcium sulfate or sulphur
One or more of acid magnesium etc., adding of weighting agent has adapted to generally be not less than 20 as the foliage fertilizer minimum package of merchandise sales
Gram relevant regulations; Filler starch, dextrin, Mierocrystalline cellulose etc. also possess certain viscosity, make nutrient substance be attached to leaf after spraying
Face and the plant surface time longer, make its action effect better; Weighting agent polyvidone, Magnesium Stearate, calcium sulfate or magnesium sulfate etc.
Etc. having dispersiveness and oilness, the quality guaranteed period of nutrient substance can be extended.
Due to preparation method of the present invention: (1), can from fermentation plant (Gourmet Powder Factory, brew-house, antibiotics plant, yeast
Active sludge after factory, Amino Acid Factory, paper mill, sewage disposal, petroleum fermentation etc.) byproduct (tankage) mycelium after fermentation adopts the nucleic acid of dry method or wet production to be raw material, and its price of this nucleic acid is low, is easy to cost-saving; (2), can adopt the preparation method be hydrolyzed for raw material with commercially available nucleic acid, products pure degree is high, and the proportioning of Yeast Nucleic Acid and thymus nucleic acid can adjust, product suitability and better effects if; (3), also can directly with commercially available 5 '-adenylic acid (AMP) disodium or potassium, 5 '-Sodium guanylate or potassium, 5 '-cytidylic acid disodium or potassium, 5 '-uridine monophosphate disodium or potassium and 5 '-Desoxyadenosine acid disodium or potassium, 5 '-deoxidation bird adenylic acid (AMP) disodium or potassium, 5 '-Deoxyribose cytidine acid disodium or potassium, 5 '-deoxyuridine acid disodium, the sodium salt of 5 '-deoxythymidine acid disodium or potassium five kinds of 5 '-deoxidation mixed nucleotides or sylvite preparation; Add trace element again, form the present invention, be therefore suitable for more flexible, technique is simpler.
Purposes of the present invention is: as fertilizer particularly as foliage fertilizer or nutrient substance or plant-growth regulator in promotion
Application in the growth of fruit and seed class medicinal plant; Or be applied to fruit and seed class medicinal plant produce can improve its produce
Amount, quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
The present invention is applied to the growth promoting fruit and seed class medicinal plant, with strong points, can improve its Yield and quality, quality, enhancing resistance, uniformity coefficient, reduce nuisance content, cost-saving, increase income, synergy.
So product of the present invention: saving, environmental protection (nontoxic, harmless, noresidue, without any adverse side effect), comprehensive to fruit and seed class medicinal plant purposes, increase production, increase income, synergy, strengthen resistance, improve quality effective.
The present invention and 201010514241.X patent, traditional product and method contrast table 1
The present invention and 201010514241.X patent, traditional product and method contrast table 2
The present invention implements to spray agency part effect in table 3 to concrete crop
Note: content's index detection method is carried out with reference to national standard or industry standard, content is pressed dry product and is calculated
embodiment:
Embodiment 1: get 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams, pulverizes Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element, sieves, mix.
Embodiment 2: get 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt trace element 4 grams, by Nucleotide sylvite
Pulverize with deoxynucleoside acid potassium salt, trace element, sieve, mix, obtain nutrient substance.
Embodiment 3: take 7 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt (or sodium salt), trace element 5
Gram, mixing, pulverizing, sieve, obtain nutrient substance.
Embodiment 4: get commercially available Nucleotide potassium or sodium salt and deoxynucleotide potassium or sodium salt 10 grams, trace element 10 grams,
W-Gum 50 grams, Magnesium Stearate 30 grams, mix.
Embodiment 5: get Nucleotide potassium or sodium salt 90 grams, deoxynucleotide potassium or sodium salt 10 grams, mixing; Get trace element 100 grams again, Xylo-Mucine 800 grams, remix, pulverizing, excessively 90 mesh sieves.
Embodiment 6: by the crude product Yeast Nucleic Acid obtained from the mycelium of fermentation plant's byproduct by dry method or wet method
(RNA) 100 grams, be dissolved in the sodium hydroxide solution of 3 liters of 6.3N, under 37 DEG C of conditions, stir 12 hours, obtain and mainly refer to contain: 5 '-adenylic acid (AMP) disodium, 5 '-bird adenylic acid (AMP) disodium, 5 '-cytidylic acid disodium, the sodium salt of 5 '-uridine monophosphate disodium, four kinds of 5 '-mixed nucleotides (also has deoxynucleoside hydrochlorate: 5 '-Desoxyadenosine acid disodium, 5 '-deoxidation bird adenylic acid (AMP) disodium, 5 '-Deoxyribose cytidine acid disodium, 5 '-deoxyuridine acid disodium, , the sodium salt of 5 '-deoxythymidine acid disodium, five kinds of 5 '-deoxidation mixed nucleotides and the solution of impurity), filter, filtrate is neutralized to pH8-8.5, be evaporated to appropriate, concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 15%, nearly dry new-nucleo and Sodium Deoxyribomuleotide is dissolved by proper amount of clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, about obtain 85-90 grams, white core thuja acid salt and deoxynucleoside hydrochlorate and water soluble mixt impurity, get 90 grams of trace elements again to mix with it, mixture is pulverized, cross 100 mesh sieves.
Embodiment 7: by the crude product Yeast Nucleic Acid obtained from the mycelium of fermentation plant's byproduct by dry method or wet method
(RNA) 100 grams, be dissolved in the potassium hydroxide solution of 2.5 liters of 6N, under 40 DEG C of conditions, stir 10 hours, obtain and mainly refer to contain: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, the sylvite of 5 '-uridylic acid dipotassium, four kinds of 5 '-mixed nucleotides, also has deoxynucleoside hydrochlorate: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, , the sylvite of 5 '-deoxythymidylic acid dipotassium, five kinds of 5 '-deoxidation mixed nucleotides and impurity (amino acid, sugar part and nitrogen, phosphorus, potassium, iron, calcium, magnesium, zinc, copper, manganese etc.) solution, filter, filtrate is neutralized to pH8-8.5, be evaporated to appropriate, concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume to 20%, nearly dry Nucleotide potassium and deoxynucleotide potassium is dissolved by proper amount of clear water, its solution adds alcohol and separates out, crystallization suction filtration is dry, about 88-93 grams of white core thuja acid sylvite and deoxynucleoside acid potassium salt and water soluble mixt impurity, get 80 grams of trace elements again to mix with it, mixture is pulverized, cross 80 mesh sieves.
Embodiment 8: by commercially available nucleosides hydrochlorate 90 grams, deoxynucleoside hydrochlorate 10 grams, mixing, be dissolved in the potassium hydroxide solution of 2.5 liters of 6N, under 40 DEG C of conditions, stir 10 hours, must contain: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, the sylvite of 5 '-uridylic acid dipotassium, four kinds of 5 '-mixed nucleotides, also has deoxynucleoside hydrochlorate: 5-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, , the solution of the sylvite of 5 '-deoxythymidylic acid dipotassium, five kinds of 5 '-deoxidation mixed nucleotides, filter, filtrate is neutralized to pH8-8.5, be evaporated to appropriate, concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume to 20%, nearly dry Nucleotide potassium and deoxynucleotide potassium is dissolved by proper amount of clear water, its solution adds alcohol and separates out, and crystallization suction filtration is dry, about obtains 95-98 grams of white core thuja acid sylvite and deoxynucleoside acid potassium salt, get 120 grams of trace elements again to mix with it, mixture is pulverized, cross 120 mesh sieves.
Embodiment 9: snakegourd: perennial herbaceous stem rattan wood, after cultivation, Second Year sprays three times every year, and first time, at stem climing length 30 cm, with 4 grams of nutrient substances, is watered 20 liters, evenly sprays on snakegourd rattan leaf; Second time, at the plant blossom initial stage, is filled a prescription by embodiment 3, is watered 30 liters, evenly spray on one mu of snakegourd, and third time, at full-bloom stage, fills a prescription by embodiment 2, is watered 40 liters, evenly spray on one mu of snakegourd.Snakegourd can increase production 20%-30%, and the root (Snakegourd Root) of snakegourd also can increase production more than 30% simultaneously.
Embodiment 10: cape jasmine: respectively spray once at initial bloom stage and full-bloom stage, fill a prescription by embodiment 1, be watered 30 liters, evenly sprays on one mu of cape jasmine; Respectively spray once again at fruit development period and fruit expanding period: fill a prescription by embodiment 2, convert 30 premium on currency, evenly spray on one mu of cape jasmine; Can reduce shedding 60-80%, stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size evenly, jasminoidin and crocin content is respectively higher than existing standards of pharmacopoeia 20-36%.
Claims (4)
1. the purposes of the nutrient substance of fruit and seed class medicinal plant, is characterized in that: described nutrient substance is in order to the standby nutrient substance of below legal system:
Step is: a. gets 2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams;
B. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Or:
C. 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt is got, trace element 4 grams;
D. Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element are pulverized, sieve, mix;
Described trace element refers to: manganous sulfate, borax, ferrous sulfate, zinc sulfate, copper sulfate, ammonium molybdate; The weight ratio of trace element is: Mn::B:Fe: Zn::Cu: Mo=5:3:3:3:2:1;
Described Nucleotide sylvite refers to: 5 '-adenylic acid (AMP) dipotassium, 5 '-bird adenylic acid (AMP) dipotassium, 5 '-cytidylic acid dipotassium, 5 '-uridylic acid dipotassium, the di-potassium of four kinds of 5 '-mixed nucleotides; Described deoxynucleoside acid potassium salt refers to: 5 '-deoxyadenylic acid dipotassium, 5 '-deoxidation bird adenylic acid (AMP) dipotassium, 5 '-deoxycytidylic acid(dCMP) dipotassium, 5 '-deoxyuridylic acid dipotassium, 5 '-deoxythymidylic acid dipotassium, the di-potassium of five kinds of 5 '-deoxidation mixed nucleotides;
The application in the growth promoting fruit and seed class medicinal plant cape jasmine as fertilizer or plant-growth regulator of this nutrient substance;
Or be applied to fruit and seed class medicinal plant cape jasmine produce make described cape jasmine:
Determination of Gardenoside is greater than 2.1%;
Jasminoidin and crocin content are respectively higher than existing standards of pharmacopoeia 20-36%;
Cape jasmine can reduce shedding 60-80%, and stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size is even;
Cape jasmine extracting effective components yield can reach 149% of the cape jasmine than produced in conventional processes.
2. the purposes of the nutrient substance of fruit and seed class medicinal plant, is characterized in that: described nutrient substance is in order to the standby nutrient substance of below legal system:
2 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 2 grams; Or: 5 grams of Nucleotide sylvite and deoxynucleoside acid potassium salt, trace element 4 grams; Get commercially available nucleosides hydrochlorate and deoxynucleoside hydrochlorate, mixing; Get commercially available trace element again, remix, pulverize, sieve;
The application in the growth promoting fruit and seed class medicinal plant cape jasmine as fertilizer or plant-growth regulator of this nutrient substance;
Or be applied to fruit and seed class medicinal plant cape jasmine produce make described cape jasmine:
Determination of Gardenoside is greater than 2.1%;
Jasminoidin and crocin content are respectively higher than existing standards of pharmacopoeia 20-36%;
Cape jasmine can reduce shedding 60-80%, and stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size is even;
Cape jasmine extracting effective components yield can reach 149% of the cape jasmine than produced in conventional processes.
3. the purposes of the nutrient substance of fruit and seed class medicinal plant, is characterized in that: described nutrient substance is made up of nucleosides hydrochlorate and deoxynucleoside hydrochlorate 2 grams, trace element 2 grams; Or by: 5 grams of nucleosides hydrochlorates and deoxynucleoside hydrochlorate, trace element 4 grams of compositions; Not comprising glucose or/and amino acid in ideal nutrient composition, its preparation, take nucleic acid as raw material:
1., the hydrolysis of nucleic acid: the ratio mixed nucleus bronsted lowry acids and bases bronsted lowry liquid according to nucleic acid, buck weight ratio being 1:20-30, alkali lye is
5.5-7N, under 30-45 DEG C of condition, stirs 10-14 hours, obtains nucleosides hydrochlorate and deoxynucleoside hydrochlorate is molten
Liquid, filters, and filtrate adjusts pH8-8.5, concentrating under reduced pressure;
2., decolouring, dry concentrated solution is added activated carbon decolorizing, suction filtration it, filtrate reduced in volume is to moisture 10-25%;
3., crystallization with clear water dissolve dry after nucleosides hydrochlorate and deoxynucleoside hydrochlorate, its solution adds alcohol and separates out, and crystallization is taken out
Be filtered dry dry, obtain white core thuja acid salt and deoxynucleoside hydrochlorate;
4., trace element is got; Nucleosides hydrochlorate and deoxynucleoside hydrochlorate are mixed with trace element, pulverize, sieves;
The application in the growth promoting fruit and seed class medicinal plant cape jasmine as fertilizer or plant-growth regulator of this nutrient substance; Or be applied to fruit and seed class medicinal plant cape jasmine produce make described cape jasmine:
Determination of Gardenoside is greater than 2.1%;
Jasminoidin and crocin content are respectively higher than existing standards of pharmacopoeia 20-36%;
Cape jasmine can reduce shedding 60-80%, and stimulation ratio reaches more than 36%, and cape jasmine fruit 80%-90% size is even;
Cape jasmine extracting effective components yield can reach 149% of the cape jasmine than produced in conventional processes.
4. the purposes of the nutrient substance of fruit and seed class medicinal plant according to claim 3, it is characterized in that, in described nucleic acid hydrolysis process, alkali lye used is sodium hydroxide or potassium hydroxide solution.
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