CN105029702A - Glycerol triacetate extract of fructus chebulae immaturus and application of glycerol triacetate extract to cigarettes - Google Patents
Glycerol triacetate extract of fructus chebulae immaturus and application of glycerol triacetate extract to cigarettes Download PDFInfo
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- CN105029702A CN105029702A CN201510337057.5A CN201510337057A CN105029702A CN 105029702 A CN105029702 A CN 105029702A CN 201510337057 A CN201510337057 A CN 201510337057A CN 105029702 A CN105029702 A CN 105029702A
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- glycerol triacetate
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Abstract
The invention discloses glycerol triacetate extract of fructus chebulae immaturus and application of the glycerol triacetate extract to cigarettes. Fructus chebulae immaturus particles with the water contents of 6-8% and the particle sizes of 20-40 meshes are used as raw materials, glycerol triacetate is used as an extracting agent, and the glycerol triacetate extract of the fructus chebulae immaturus is extracted and prepared by the aid of ultrasonic waves in a heating reflux mode; the glycerol triacetate extract of the fructus chebulae immaturus is prepared by the aid of a solvent, namely, the glycerol triacetate to obtain liquor with the concentration of 1-4%, the liquor is uniformly sprayed on tow according to a proportion of 7-8% of the weight of the acetate fiber tow to obtain cigarette filter rods, and the cigarettes with the filter rods containing effective constituents of the fructus chebulae immaturus can be manufactured by the aid of conventional cigarette making procedures. The glycerol triacetate extract and the application have the advantages that salivation promoting properties and sweet after-taste of smoke can be obviously enhanced by the extract, irritation to the mouths and the throats of users can be relieved, remaining taste is clean and comfortable, and cigarette flavor is fresh and natural; the glycerol triacetate extract is simple in manufacturing process, high in operability and standardization, low in cost and convenient to industrially manufacture and has an excellent application prospect, and the raw materials are easy to obtain.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract.Meanwhile, the invention still further relates to the described application of FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract in cigarette.
Background technology
FRUCTUS TERMINALIAE IMMATURUS, also known as myrobalan, is the young fruit of gentleman section myrobalan platymiscium.Pharmacopeia is recorded: its bitter and puckery flavor, micro-sweet, and property is flat partially cold, has the effect of clearing heat and promoting fluid, liyan jiedu and preventing phlegm from forming and stopping coughing, can be used for acute and chronic sphagitis, abscess of throat, the symptom such as hoarseness and dry throat.The bioactivator of FRUCTUS TERMINALIAE IMMATURUS is mainly divided into four classes, i.e. tannin class, triterpenes, phenolic acid and aliphatic category compound.Study based on to the biochemical activity of large molecule phenolic acid class, FRUCTUS TERMINALIAE IMMATURUS, except having inhibiting bacteria and diminishing inflammation, the effect such as clearing heat and detoxicating, also has stronger radicals scavenging effect.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of FRUCTUS TERMINALIAE IMMATURUS extract prepared using triacetyl glycerine as extractant is provided, this extract is applied to the sweet sense of promoting the production of body fluid back that cigarette effectively can strengthen cigarette, and smoke alcohol and fine and smooth, fragrant of cigarette, excitant and assorted gas alleviate.
The present invention also aims to provide the described application of FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract, is obtained by the method for following steps:
(1) first by FRUCTUS TERMINALIAE IMMATURUS coarse crushing, under 50 ~ 70 DEG C of conditions, be dried to moisture is 6 ~ 8%, then is crushed to 20 ~ 40 orders further, for subsequent use;
(2) take 1 ~ 5 part of FRUCTUS TERMINALIAE IMMATURUS particle according to weight portion and be placed in round-bottomed flask, add 7 ~ 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature, after 3 ~ 8 hours, carries out refluxing extraction under 70 ~ 130 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 300 ~ 500W, 40kHZ condition, extract 20 ~ 55 minutes, cross the settled solution obtained after filtering filter residue and be required FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract.
Described FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is applied in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 4%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that FRUCTUS TERMINALIAE IMMATURUS exists by prior art when filter stick additive is mixed and is fitted in plasticizer.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in FRUCTUS TERMINALIAE IMMATURUS fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract effectively can give prominence to sweet sense of promoting the production of body fluid back, thoroughly the hai roll cigarette nature fragrance of cigarette, has the effect reducing flue gas excitant, improve pleasant impression simultaneously.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
First by FRUCTUS TERMINALIAE IMMATURUS coarse crushing, under 70 DEG C of conditions, be dried to moisture is 6%, be crushed to 40 orders further again, take 2 parts of FRUCTUS TERMINALIAE IMMATURUS particles according to weight portion and be placed in round-bottomed flask, add 7 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 90 DEG C of conditions, extraction time is 8 hours, to be cooled to room temperature, FRUCTUS TERMINALIAE IMMATURUS after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (300W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains FRUCTUS TERMINALIAE IMMATURUS active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette of adding above-mentioned FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract promotes the production of body fluid back sweet sense obviously, and cigarette is fragrant fine and smooth, fresh and clean, and flue gas excitant obviously reduces, and oral cavity is residual to alleviate.
Embodiment 2
First by FRUCTUS TERMINALIAE IMMATURUS coarse crushing, under 50 DEG C of conditions, be dried to moisture is 7%, be crushed to 20 orders further again, take 5 parts of FRUCTUS TERMINALIAE IMMATURUS particles according to weight portion and be placed in round-bottomed flask, add 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 8 hours, refluxing extraction is carried out under 120 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, FRUCTUS TERMINALIAE IMMATURUS after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (300W, 40kHZ), extract 50 minutes, cross after filtering filter residue and obtain settled solution, required FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is mixed with the solution that concentration is 4%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains FRUCTUS TERMINALIAE IMMATURUS active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract promotes the production of body fluid back sweet, and flue gas excitant reduces, entrance is smooth and easy, and pleasant impression is totally comfortable, and cigarette perfume (or spice) is fresh and clean.
Embodiment 3
First by FRUCTUS TERMINALIAE IMMATURUS coarse crushing, under 70 DEG C of conditions, be dried to moisture is 8%, be crushed to 40 orders further again, take 2 parts of FRUCTUS TERMINALIAE IMMATURUS particles according to weight portion and be placed in round-bottomed flask, add 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 6 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 8 hours, to be cooled to room temperature, FRUCTUS TERMINALIAE IMMATURUS after described refluxing extraction and triacetyl glycerine are placed in ultrasonic extractor (500W, 40kHZ), extract 30 minutes, cross after filtering filter residue and obtain settled solution, required FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is mixed with the solution that concentration is 1%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains FRUCTUS TERMINALIAE IMMATURUS active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette mouthfeel of adding above-mentioned FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is obviously improved, and the excitant of flue gas alleviates, and promotes suction comfort level.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract, is obtained by the method for following steps:
(1) first by FRUCTUS TERMINALIAE IMMATURUS coarse crushing, under 50 ~ 70 DEG C of conditions, be dried to moisture is 6 ~ 8%, then is crushed to 20 ~ 40 orders further, for subsequent use;
(2) take 1 ~ 5 part of FRUCTUS TERMINALIAE IMMATURUS particle according to weight portion and be placed in round-bottomed flask, add 7 ~ 10 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature, after 3 ~ 8 hours, carries out refluxing extraction under 70 ~ 130 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 300 ~ 500W, 40kHZ condition, extract 20 ~ 55 minutes, cross the settled solution obtained after filtering filter residue and be required FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract.
2. FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract according to claim 1 is applied in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described FRUCTUS TERMINALIAE IMMATURUS triacetyl glycerine extract is mixed with the solution that concentration is 1 ~ 4%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| CN102144808A (en) * | 2011-05-17 | 2011-08-10 | 何金星 | Preparation method of cigarette additive and application thereof |
| CN103054189A (en) * | 2012-12-29 | 2013-04-24 | 广东中烟工业有限责任公司 | Ternary tobacco fiber paper filter stick of composite moistening plants and preparation method thereof |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
| CN104450192A (en) * | 2014-09-30 | 2015-03-25 | 云南中烟工业有限责任公司 | Tobacco flavor prepared by taking fructus terminaliae immaturus, dendrobium nobile, tobacco and the like as raw materials and application thereof |
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2015
- 2015-06-17 CN CN201510337057.5A patent/CN105029702A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101053447A (en) * | 2006-04-14 | 2007-10-17 | 钱玉章 | Liquid compound for eliminating smoke harm and preparing method thereof |
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN102144808A (en) * | 2011-05-17 | 2011-08-10 | 何金星 | Preparation method of cigarette additive and application thereof |
| CN103054189A (en) * | 2012-12-29 | 2013-04-24 | 广东中烟工业有限责任公司 | Ternary tobacco fiber paper filter stick of composite moistening plants and preparation method thereof |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
| CN104450192A (en) * | 2014-09-30 | 2015-03-25 | 云南中烟工业有限责任公司 | Tobacco flavor prepared by taking fructus terminaliae immaturus, dendrobium nobile, tobacco and the like as raw materials and application thereof |
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Application publication date: 20151111 |