CN104940530A - External preparation for treating alopecia and preparing method thereof - Google Patents
External preparation for treating alopecia and preparing method thereof Download PDFInfo
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Abstract
The invention discloses an external preparation for treating alopecia. The external preparation is mainly prepared from, by weight, 8-16 parts of tribulus terrestris, 10-15 parts of lilac daphne flower buds, 12-18 parts of moutan bark, 9-16 parts of brooklet anemone roots, 7-13 parts of safflower carthamus, 10-16 parts of radix paeoniae alba, 8-14 parts of prepared rehmannia roots, 11-16 parts of fresh sesame flowers, 9-14 parts of notopterygium roots, 8-15 parts of tengyuch euonymus bark, 11-17 parts of lotus leaves, 10-18 parts of codonopsis pilosula, 8-14 parts of dioscorea collettii hooks, 6-13 parts of cayratia trifolia roots, 10-14 parts of rhizoma alismatis and 9-17 parts of royal jelly. Selected materials are traditional Chinese medicine materials, and through syndrome differentiation and medicine compatibility, the external preparation has the advantages of being excellent in curative effect, free of side effects, easy to prepare, economical and convenient; effective components are stable and long in shelf life and act for a long time; medicine herbs are easy to obtain and low in cost, and therefore burdens of patients can be relieved.
Description
Technical field
The present invention relates to traditional Chinese medicine field.Particularly relate to a kind of external preparation and method for making thereof of hair growth.
Background technology
Along with the fast development of society and the continuous quickening of rhythm of life, huge pressure is brought to the life of people, many youngsters are because the pressure of life and the irregular of work and rest cause a large amount of alopecias, also a large amount of alopecia of the women in puerperal is had, nervous alopecia, hereditary alopecia etc. have all brought worried and puzzlement.
The traditional Chinese medical science is thought, alopecia is relevant with the liver,kidney,spleen in human five internal organs and QI and blood.Sending out is the honor of blood, not have full blood, and hair is then difficult nourishing; Blood stored in the liver, main catharsis, the liver failing to maintain the normal flow of QI is functional activity of QI being not smooth then, and blood can not moisten foster skin with gas, and pore diastole is then dealt with; Kidney governing bones, its honor is being sent out; The spleen has the function to transport and transform nutrients, and cardiopulmonary defeated on essence of water and grain are turned to the important living matters such as QI and blood.So, when any change occurs their function, all coming off of hair can be caused.Modern medicine thinks that alopecia is due to endocrine disturbance, immunity degradation, and alimentation does not go up, because hemotrophic nutrition, moisten hair, what cause loses hair.
Application publication number CN 103720900 A(application number 201210390427.8) Chinese invention patent document disclose a kind of Chinese medicine of hair growth, be prepared from by the crude drug of following weight proportion: Radix Rehmanniae 30-50, Cortex Phellodendri 10-20, Fructus Lycii 10-20, Radix Angelicae Sinensis 5-10, Radix Astragali 50-100, Herba Ecliptae 20-30, Rhizoma Chuanxiong 10-20, Radix Rubiae 20-40.Application publication number CN104225172A(application number 201310607348.2) Chinese invention patent document disclose a kind of Chinese medicine of hair growth, be prepared from by the crude drug of following weight proportion: Caulis Polygoni Multiflori 8-12 gram, Radix Ginseng Rubra 15-25 gram, Fructus Ligustri Lucidi 6-12 gram, Semen Cuscutae 8-10 gram, Semen Sesami Nigrum 8-10 gram, Poria 6-20 gram, Rohdea japonica Roth 2-5 gram, Cortex Ailanthi 10-25 gram.Application publication number CN 103690649 A(application number 201310723842.5) Chinese invention patent document disclose a kind of Chinese medicine formula of hair growth, be prepared from by the crude drug of following weight proportion: Radix Astragali 8-25 gram, Radix Ginseng 5-20 gram, Radix Angelicae Sinensis 5-20 gram, Rhizoma Atractylodis Macrocephalae 5-20 gram, Fructus Arctii 0-15 gram, Caulis Sesami 5-25 gram, Poria 0-15 gram, Fructus Aurantii 0-15 gram, Ramulus Cinnamomi 0-15 gram, Radix Glycyrrhizae 0-7 gram.
The medicine of the symptoms such as current hair growth, is mostly Western medicine, can bring certain toxic and side effects in patient's use procedure, therapeutic effect is not good, fundamentally can not solve the disease of patient, and drug dependence is larger, long-term taking easily causes body damage, immunity degradation.The prescription for the treatment of by Chinese herbs primary disease nourishes blood the side of enriching blood; Nourishing the liver and kidney side; Strong liver QI invigorating side; Yin nourishing removing heat from blood side; Liver-smoothing, qi-regulating side; Admittedly decorations dredging collateral side etc.The clinical effectiveness of these medicines or prescription is all undesirable, or function singleness, or toxic and side effects is large; And some medical materials used costly, adds the financial burden of common people.
Summary of the invention
For the deficiencies in the prior art, add oral drugs and be rich in hormone more, easily cause body metabolism disorderly, even Secondary cases fungus, viral infection, and hair transplant all can cause the deep lesions of hair follicle to a certain extent, cortex is totally disrupted, and cannot repair.An object of the present invention be to provide a kind of can the external preparation of effective hair growth, adopt medical material comparatively common in the localities as raw material, with low cost.Another object of the present invention is just to provide the preparation method of the external preparation of above-mentioned hair growth.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
The external preparation of hair growth, is prepared from by the primary raw material of following weight proportioning: Fructus Tribuli 8-16; Flos Genkwa 10-15; Cortex Moutan 12-18; Radix Anemones Rivularis 9-16; Flos Carthami 7-13; Radix Paeoniae Alba 10-16; Radix Rehmanniae Preparata 8-14; Fresh Flos Sesami indici 11-16; Rhizoma Et Radix Notopterygii 9-14; Cortex Biotae Radicis 8-15; Folium Nelumbinis 11-17; Radix Codonopsis 10-18; Nine sons are not from female 8-14; Cayratia trifolia (L.) Domin 6-13; Rhizoma Alismatis 10-14; Lac regis apis 9-17.
In preferred scheme, Fructus Tribuli 10-14; Flos Genkwa 11.5-13.5; Cortex Moutan 14-16; Radix Anemones Rivularis 11-14; Flos Carthami 9-11; Radix Paeoniae Alba 12-14; Radix Rehmanniae Preparata 10-12; Fresh Flos Sesami indici 12.5-14.5; Rhizoma Et Radix Notopterygii 10.5-12.5; Cortex Biotae Radicis 10-13; Folium Nelumbinis 12.5-15.5; Radix Codonopsis 12-16; Nine sons are not from female 10-12; Cayratia trifolia (L.) Domin 8-11; Rhizoma Alismatis 11-13; Lac regis apis 11-15.
Be more preferably, Fructus Tribuli 12; Flos Genkwa 12.5; Cortex Moutan 15; Radix Anemones Rivularis 12.5; Flos Carthami 10; The Radix Paeoniae Alba 13; Radix Rehmanniae Preparata 11; Fresh Flos Sesami indici 13.5; Rhizoma Et Radix Notopterygii 11.5; Cortex Biotae Radicis 11.5; Folium Nelumbinis 14; Radix Codonopsis 14; Nine sons are not from female 11; Cayratia trifolia (L.) Domin 9.5; Rhizoma Alismatis 12; Lac regis apis 13.
The preparation method of the external preparation of hair growth, step is as follows:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing of ethanol and soak, obtain medicinal liquid for subsequent use;
(3) by Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis are placed in crock, the deionized water adding 6-10 times amount infiltrates (deionized water preferably adding 7-9 times amount infiltrates), then big fire is heated to boil, turn little fire and decoct three times slowly, first time decocts 28-46 minute (preferably first time decocts 34-40 minute), second time decocts 16-34 minute (preferably second time decocts 22-28 minute), third time decocts 8-14 minute (preferably third time decocts 10-12 minute), the deionized water (adding the deionized water of 5.5-6.5 times amount before preferred second time and for the third time decoction respectively) of 4.5-7.5 times amount is added respectively before second time and for the third time decoction, merge three decocting liquids, filter, filtrate is for subsequent use,
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, add wetting agent and scalp irritation element simultaneously, stir, through microporous filter membrane filtration, to obtain final product.
The preparation method of the external preparation of above-mentioned hair growth, preferred scheme is, in step (2), the mass concentration of ethanol is the mass concentration of the preferred ethanol of 50%-70%(is 55%-65%, and the mass concentration of the ethanol be more preferably is 60%).
The preparation method of the external preparation of above-mentioned hair growth, preferred scheme is, the time that step (2) is soaked is 3-7 days (the preferred time of soaking is 4-6 days, and the time of the immersion be more preferably is 5 days).
The preparation method of the external preparation of above-mentioned hair growth, preferred scheme is, the time infiltrated in step (3) is 2-5 hour (the preferred time infiltrated is 3-4 hour, and the time of the infiltration be more preferably is 3.5 hours).
The preparation method of the external preparation of above-mentioned hair growth, preferred scheme is, wetting agent described in step (4) is one in glycerol, propylene glycol and Sorbitol (preferred described wetting agent is the one in propylene glycol and Sorbitol, and the described wetting agent be more preferably is propylene glycol).
The preparation method of the external preparation of above-mentioned hair growth, preferred scheme is, the element of scalp irritation described in step (4) is the one (preferred described scalp irritation is plain is the one in nicotinic acid acyl and Mylabris tincture, and the described scalp irritation element be more preferably is nicotinic acid acyl) in nicotinic acid acyl, capsicum tincture and Mylabris tincture.
The preparation method of the external preparation of above-mentioned hair growth, preferred scheme is, the aperture of micropore filtering film described in step (4) is 0.05-0.1 μm (aperture of preferred described micropore filtering film is 0.06-0.09 μm, and the aperture of the described micropore filtering film be more preferably is 0.08 μm).
The pharmacological effect of each crude drug is respectively:
Fructus Tribuli: base is former: be the fruit of zygophyllaceae plant Fructus Tribuli.Chemical analysis: fruit is containing nimbecetin, nimbecetin 3-glycoside, nimbecetin 3-rutinoside, Fructus Tribuli glycoside, peroxidase.Dry fruit fatty oily 3.5% and a small amount of volatile oil, tannin, resin, sterol, potassium salt, Alkaloid etc.; Again containing Saponin 1.47%.Seed, containing alkaloid 3-methyl-4-carboline and harmine, does not contain Saponin.Pharmacological action: 1. reduce blood pressure effect; 2. diuresis.Nature and flavor: toil, temperature.Gui Jing: enter liver, lung meridian.Function cures mainly: loose wind, improving eyesight, the therapeutic method to keep the adverse QI flowing downwards, promoting the circulation of blood.Control headache, itching over the body, conjunctival congestion swells nebula, fullness in the chest, cough with dyspnea, lump in the abdomen, and breast is difficult, carbuncle, scrofula.
Flos Genkwa: base is former: be the alabastrum of Isolated From Thymelaeaceae Species Flos Genkwa.Pharmacological action: 1. diuresis; 2. antitussive, phlegm-dispelling functions; 3. the effect of couple central nervous system; 4. the effect of pair digestive system; 5. antifertility action; 6. the inhibitory action of pair xanthine oxidase (XO); 7. leukemia resisting action; 8. antibacterial action.Nature and flavor: pungent; Bitter; Warm in nature; Poisonous.Gui Jing: lung; Spleen; Kidney; Urinary bladder channel.Function cures mainly: removing fluid-retention by purgation; Expelling phlegm for arresting cough; Removing toxic substances parasite killing.Main edema; Expand; Phlegm retention breast water; Breath with cough; Carbuncle furuncle tinea.
Cortex Moutan: base is former: be the root bark of ranunculaceae peony.Chemical analysis: root is containing paeonol, paeonolide, paeonolide, paeoniflorin.Still containing volatile oil 0.15 ~ 0.4% and plant sterol etc.Nature and flavor: arduous, cool.Gui Jing: enter the heart, liver, kidney channel.Function cures mainly: heat clearing away, removing heat from blood, and blood, repercussive.Control the pathogenic heat attacking blood system in febrile diseases, send out speckle, infantile convulsion, tells, is defeated in battle, has blood in stool, hectic fever due to YIN-deficiency consumptive fever, amenorrhea, lump in the abdomen, and carbuncle and ulcer, flutters damage.
Radix Anemones Rivularis: base is former: be the root of the grass that ranunculaceae plant Radix Anemones Rivularis and little Hua tiger slap.Chemical analysis: Radix Anemones Rivularis root contains betulic acid, Herba Veronicastri Sibirici Saponin, Radix Anemones Rivularis Saponin A, B, C, D and Saponin AR-1, AR-3.Pharmacological action: 1. antitussive action; 2. phlegm-dispelling functions.Nature and flavor: bitter; Pungent; Temperature; Mild toxicity.Gui Jing: lung; Stomach; Liver Channel.Function cures mainly: heat-clearing and toxic substances removing; Relaxing muscles and tendons to promote blood circulation; Reducing swelling and alleviating pain.Main laryngopharynx swelling and pain; Mumps; Scrofula tuberculosis; Swollen ulcer drug; Malaria; Cough; Jaundice due to damp-heat; Rheumatalgia; Stomachache; Toothache; Traumatic injury.
Flos Carthami: base is former: this product is the dried floral of feverfew Flos Carthami.Character: this product is the tubular flower not with ovary.Surface red is yellow or red.Tube is elongated, and tip 5 splits, and sliver is slat shape; Flower pesticide aggregates into tubular, yellow-white; Stigma elongated cylindrical, top differential is pitched.Matter is soft.Nature and flavor: pungent, temperature.Gui Jing: GUIXIN, Liver Channel.Effect: promoting blood circulation to restore menstrual flow, eliminating stasis to stop pain.Cure mainly: for amenorrhea, dysmenorrhea, lochia ， mass in the abdomen mass in the abdomen, injury from falling down, skin infection swells and ache.
The Radix Paeoniae Alba: base is former: this product is the dry root of ranunculaceae plant Radix Paeoniae.Chemical analysis: root contains paeoniflorin, paeonol, paeoniflorin, benzoic acid about 1.07%, volatile oil, fatty oil, resin, tannin, sugar, starch, phlegmatic temperament, protein, cupreol and triterpenes.Nature and flavor: bitter, sour, are slightly cold.Gui Jing: return liver, spleen channel.Effect: suppressing the hyperactive liver pain relieving, nourishing blood for regulating menstruation, astringing YIN to stop sweating.Cure mainly: dizzy for having a headache, hypochondriac pain, stomachache, limb pain twin, blood deficiency and yellow complexion, menoxenia, spontaneous perspiration, night sweat.
Radix Rehmanniae Preparata: base is former: this product is the Preparation process product of Radix Rehmanniae.Character: this product is irregular piece of sheet, fragment, and size, thickness differ.Surface corvinus, glossy, stickiness is large.Matter is soft and be with toughness, not frangibility, section corvinus, glossy.Feeble QI, taste is sweet.Nature and flavor: sweet, tepor.Gui Jing: return liver, kidney channel.Effect: nourishing YIN and supplementing blood, beneficial essence fills out marrow.Cure mainly: for the hepatic and renal YIN deficiency, soreness of the waist and knees, osteopyrexia and fever, night sweat is passed out semen, and interior-heat is quenched one's thirst, blood deficiency and yellow complexion, severe palpitation, menoxenia, and metrostaxis is dizzy, tinnitus, early whitening of beard and hair.
Rhizoma Et Radix Notopterygii: base is former: this product is dry rhizome and the root of samphire Rhizoma Et Radix Notopterygii or Radix et Rhizoma Notopterygii.Chemical analysis: Radix et Rhizoma Notopterygii is containing volatilization wet goods.Nature and flavor: pungent, bitter, temperature.Gui Jing: return bladder, kidney channel.Effect: cold expelling, dispels the wind, dehumidifying, pain relieving.Cure mainly: for anemofrigid cold headache, rheumatic arthralgia, aching pain in should and back.
Cortex Biotae Radicis: base is former: for Cupressaceae plant Cacumen Platycladi removes the root bark of cork the sixth of the twelve Earthly Branches.Nature and flavor: bitter; Property is put down.Function cures mainly: removing heat from blood; Removing toxic substances; Sore; Hair growth promoting.Main scald; Post-moxibustion sore; Skin infection festers; Alopecia.
Folium Nelumbinis: base is former: this product is the dried leaves of nymphaeaceae plant lotus.Chemical analysis: leaf is containing nuciferine, nuciferine, miltanthin, armepavine, pronuciferine (+)-Pronuciferine, N-demethyl nuciferine, D-N-methyl coclaurine, anonaine, liriodendrin, Quercetin, Isoquercitrin, lotus glycoside, tartaric acid, citric acid, malic acid, gluconic acid, oxalic acid, succinic acid, tannin.Also containing the alkaline components of resisting mitosis effect.Nature and flavor: bitter are flat.Gui Jing: return liver, spleen, stomach warp.Effect: clearing away summer-heat, sending up the lucid YANG, cooling blood for hemostasis.Cure mainly: for multiple hemorrhage and puerperal blood faints.
Radix Codonopsis: base is former: the dry root that this product is Campanulaceae Radix Codonopsis, element spends Radix Codonopsis or radix codonpsis tangshen.Chemical analysis: Radix Codonopsis root is containing Saponin, Alkaloid, sucrose, glucose, inulin, starch, mucus and resin etc.Nature and flavor: sweet are flat.Gui Jing: return spleen, lung meridian.Effect: invigorating the spleen and replenishing QI, spleen invigorating lung benefiting.Cure mainly: for deficiency of the spleen and lung, cardiopalmus of breathing hard, anorexia and loose stool, dyspnea due to deficiency is coughed, and interior-heat is quenched one's thirst.
Nine sons are not from mother: base is former: be the rhizome of Dioscoreaceae plant Rhizoma Dioscoreae Hypoglaucae.Chemical analysis: tuber contains diosgenin, Yamogenin.Rhizome is containing steroid, except diosgenin and Yamogenin, also have: △,-deoxidation Tigogenin, △-deoxidation neotigogenin, diosgenin palmitate, Yamogenin cetylate, different narthogenin, Yamogenin-3-O-β-D-Glucose glycoside, cupreol, smilagenin ketone, chinaroot greenbrier sapogenin ketone, table smilagenin, table chinaroot greenbrier sapogenin, Yamogenin 3-O-[α-L-rhamnopyranosyl (1 → 4) β-D-glucopyanoside].Nature and flavor: bitter; Micro-pungent; Be slightly cold.Function cures mainly: expelling wind and removing dampness; Removing obstruction in the collateral to relieve pain; Heat-clearing and toxic substances removing.Main air pain of dampness syndrome; Contracture is numb; Peratodynia; Jaundice due to damp-heat; Nebulousurine; Drench pain; Leucorrhea; Traumatic pain; Eczema toxic swelling; Rubella; Eczema; Venom.
Cayratia trifolia (L.) Domin: base is former: be the root of vitaceae Caulis et Folium cayratiae trifoliae.Nature and flavor: pungent; Flat.Function cures mainly: expelling wind and removing dampness; Eliminating stasis to stop pain.Main air pain of dampness syndrome; Traumatic injury; Eczema; Tinea alba.
Rhizoma Alismatis: base is former: be the tuber of Notes On Alism At Aceae Rhizoma Alismatis.Chemical analysis: separate five kinds of triterpenoid compound in tuber: Alisol A, alisol B, acetic acid Alisol A ester, acetic acid alisol B ester and epialisol A; Another containing volatile oil (including furfural), in a small amount alkaloid, asparagine, a plant sterols, a kind of phytosterolin, fatty acid (Palmic acid, stearic acid, oleic acid, linoleic acid); Also resinous, protein and volume starch.Nature and flavor: sweet, cold.Gui Jing: return kidney, urinary bladder channel.Effect: diuresis, clearing away damp-heat.Cure mainly: for dysuria. edema distension, oliguria of having loose bowels, dizziness due to fluid-retention, the puckery pain of pyretic stranguria; Hyperlipidemia.
Lac regis apis: base is former: be the worker bee glandulae pharyngeae of Apidae animal apis cerana etc. and the milky jelly of the rear glandular secretion of pharynx.Chemical analysis: the special foods royal jelly of young queen bee, average moisture content 66%, ash 0.82%, protein 12.2%, fat rib 5.46%, reducing substances total amount 12.49%, unknown materials 2.84%, its composition as the larvae grow phase and different.Royal jelly is containing 5 kinds of sugar, and wherein 4 kinds is fructose, grape sugar, sucrose and ribose.In its fats, have special fat acid ω-hydroxyl △ 2-decylenic acid, content is quite high.Pharmacological action: 1. strengthen Abwehrkraft des Koepers and growth promoting effects.2. the impact of Endocrine: external report royal jelly can make atrophy of thymus gland, has the effect of thyroliberin sample.3. on the impact of blood circulation: containing two kinds of similar acetylcholine sample materials in royal jelly, blood pressure is caused to decline rapidly to after cat, dog intravenous injection, drawdown curve is similar to acetylcholine, the hypotensive effect of lml royal jelly, be equivalent to l μ g acetylcholine, this effect can be atropine and resisted, and is strengthened by physostigmine, serum choline zymase can destroy it, on the boosting of epinephrine and ephedrine then without impact.4. on the impact of hemopoietic organ: royal jelly can reduce mice because of the mortality rate caused by six mercaptopurine, life-saving, and alleviates its bone marrow inhibition, oral or injection can increase the diameter of human red blood cell and the hemoglobin of reticulocyte, and blood iron content shows to be increased.5. on the impact of blood glucose: royal jelly can reduce the blood glucose of rat of normal rat, mice and alloxan diabetes, in addition can also partial agonistic epinephrine to the blood glucose increasing effect of normal mouse.6. antitumaous effect: the ether insoluble portion of royal jelly.W-hydroxyl-△ 2 decylenic acid has the effect of strong inhibition transplantability AKR from growth of cancer cells such as disorders of blood, 6C3HED lymphatic cancer, TA3 breast carcinoma and multiple ascitic type ehrlich carcinomas.7. antibacterial action: W-hydroxyl-△ 2-decylenic acid is about little by 1/4 compared with penicillium sp rope to pyococcus inhibitory action, about little by 1/5 compared with chlortetracycline to colibacillary inhibitory action, to the inhibitory action of staphylococcus aureus not as good as penicillin, and humble room temperature holding time and reducing, to 2 times that act as negative bacterium of gram positive bacteria.Nature and flavor: sweet in the mouth; Acid; Property is put down.Gui Jing: liver; Spleen channel.Function cures mainly: nourishing; Strong; The liver benefiting; Spleen invigorating.Main weak after being ill; Infantile malnutrition; Old asthenia; Leukopenia; Unresolved and chronic hepatitis; Duodenal ulcer; Bronchial asthma; Diabetes; Hematopathy; Psychosis; Anovulatory dysfunctional uterine hemorrhage; Menoxenia; Functional sterility and alopecia etc.
Technical advantage of the present invention is also embodied in:
1,this product, on the basis of summing up forefathers' experience, adopts pure natural draft Chinese medicine unique formula and technique to refine and forms, by scalp irritation acupuncture point, can play and regulate meridians, promoting flow of QI and blood, nourishing the liver and kidney, the diseases such as hair growth, can play again and improve cerebral blood flow supply, the effect of immunity moderation.
2,selected materials is all Chinese medicine material, and through dialectical compatibility, curative effect is remarkable, has no side effect, and has and prepares simple, economy feature easily; Active ingredient is stablized, persistent, long shelf-life.
3,medicine source is easy to get, with low cost, can relieve patient ' s burden.
Detailed description of the invention
Describe technical scheme of the present invention in detail below in conjunction with embodiment and experimental example, but protection domain is not by this restriction.
embodiment 1the external preparation of hair growth, is prepared from (65g/ part) by the primary raw material of following weight proportioning: Fructus Tribuli 8 parts; Flos Genkwa 10 parts; Cortex Moutan 12 parts; Radix Anemones Rivularis 9 parts; 7 parts, Flos Carthami; The Radix Paeoniae Alba 10 parts; Radix Rehmanniae Preparata 8 parts; 11 parts, fresh Flos Sesami indici; Rhizoma Et Radix Notopterygii 9 parts; Cortex Biotae Radicis 8 parts; 11 parts, Folium Nelumbinis; Radix Codonopsis 10 parts; Nine sons are not from female 8 parts; Cayratia trifolia (L.) Domin 6 parts; Rhizoma Alismatis 10 parts; Lac regis apis 9 parts.
The preparation method of the external preparation of hair growth is:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing immersion of ethanol 3 days that mass concentration is 50%, obtain medicinal liquid for subsequent use;
(3) Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not placed in crock from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis, the deionized water adding 6-10 times amount infiltrates 2 hours, then big fire is heated to boil, and turn little fire and decoct three times slowly, first time decocts 28 minutes, second time decocts 16 minutes, third time decocts 8 minutes, adds the deionized water of 4.5 times amount respectively, merge three decocting liquids before second time and third time decoct, filter, filtrate is for subsequent use;
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, adds wetting agent glycerol and scalp irritation element Mylabris tincture simultaneously, stirs, via hole diameter is 0.05 μm of microporous filter membrane filtration, to obtain final product.
The using method of the external preparation of gained hair growth of the present invention is: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.
Model case: Song XX, man, 19 years old, people from Zhou village, Zibo.Patient is a student at school, deeply affects for many years by alopecia, and treated coldly by classmate around.Household seeks medical advice and medicine everywhere and wishes to allow patient break away from the puzzlement of alopecia early, but has not sought real effective skilful doctor's secret recipe always.Surprisingly afterwards learnt my institute's hair growth Be very effective, it is to our hospital in December in 2011 22 days that patient and household thereof have the attitude of trying in arms.Check: have cephalagra before patient's alopecia, then alopecia, and with insomnia and dreamful sleep symptom, tongue is dark, yellow and thin fur, thready and rapid pulse.
Use the external preparation of the present embodiment gained hair growth, using method: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.After treating a course for the treatment of, patient's alopecia symptom takes a turn for the better gradually, and insomnia and dreamful sleep symptom liquid significantly improves; After treating two courses for the treatment of, patient's alopecia director goes out tiny fine hair, and more and more, and hair quality is more and more closeer.After treating three courses for the treatment of, new sending out has been covered with in alopecia place, and hair quality is thicker, blackening, and alopecia symptom disappears completely.Drug withdrawal is paid a return visit after half a year, and patient's hair is dense, and without alopecia symptom, self-induction is fully recovered.
embodiment 2the external preparation of hair growth, is prepared from (25g/ part) by the primary raw material of following weight proportioning: Fructus Tribuli 16 parts; Flos Genkwa 15 parts; Cortex Moutan 18 parts; Radix Anemones Rivularis 16 parts; 13 parts, Flos Carthami; The Radix Paeoniae Alba 16 parts; Radix Rehmanniae Preparata 14 parts; 16 parts, fresh Flos Sesami indici; Rhizoma Et Radix Notopterygii 14 parts; Cortex Biotae Radicis 15 parts; 17 parts, Folium Nelumbinis; Radix Codonopsis 18 parts; Nine sons are not from female 14 parts; Cayratia trifolia (L.) Domin 13 parts; Rhizoma Alismatis 14 parts; Lac regis apis 17 parts.
The preparation method of the external preparation of hair growth is:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing immersion of ethanol 7 days that mass concentration is 70%, obtain medicinal liquid for subsequent use;
(3) Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not placed in crock from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis, the deionized water adding 10 times amount infiltrates 5 hours, then big fire is heated to boil, and turn little fire and decoct three times slowly, first time decocts 46 minutes, second time decocts 34 minutes, third time decocts 14 minutes, adds the deionized water of 7.5 times amount respectively, merge three decocting liquids before second time and third time decoct, filter, filtrate is for subsequent use;
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, adds wetting agent Sorbitol and scalp irritation element capsicum tincture simultaneously, stirs, via hole diameter is 0.1 μm of microporous filter membrane filtration, to obtain final product.
The using method of the external preparation of gained hair growth of the present invention is: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.
embodiment 3the external preparation of hair growth, is prepared from (55g/ part) by the primary raw material of following weight proportioning: Fructus Tribuli 10 parts; Flos Genkwa 11.5 parts; Cortex Moutan 14 parts; Radix Anemones Rivularis 11 parts; 9 parts, Flos Carthami; The Radix Paeoniae Alba 12 parts; Radix Rehmanniae Preparata 10 parts; 12.5 parts, fresh Flos Sesami indici; Rhizoma Et Radix Notopterygii 10.5 parts; Cortex Biotae Radicis 10 parts; 12.5 parts, Folium Nelumbinis; Radix Codonopsis 12 parts; Nine sons are not from female 10 parts; Cayratia trifolia (L.) Domin 8 parts; Rhizoma Alismatis 11 parts; Lac regis apis 11 parts.
The preparation method of the external preparation of hair growth is:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing immersion of ethanol 4 days that mass concentration is 55%, obtain medicinal liquid for subsequent use;
(3) Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not placed in crock from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis, the deionized water adding 7 times amount infiltrates 3 hours, then big fire is heated to boil, and turn little fire and decoct three times slowly, first time decocts 34 minutes, second time decocts 22 minutes, third time decocts 10 minutes, adds the deionized water of 5.5 times amount respectively, merge three decocting liquids before second time and third time decoct, filter, filtrate is for subsequent use;
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, adds wetting agent glycerol and scalp irritation element Mylabris tincture simultaneously, stirs, via hole diameter is 0.06 μm of microporous filter membrane filtration, to obtain final product.
The using method of the external preparation of gained hair growth of the present invention is: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.
embodiment 4the external preparation of hair growth, is prepared from (35g/ part) by the primary raw material of following weight proportioning: Fructus Tribuli 14 parts; Flos Genkwa 13.5 parts; Cortex Moutan 16 parts; Radix Anemones Rivularis 14 parts; 11 parts, Flos Carthami; The Radix Paeoniae Alba 14 parts; Radix Rehmanniae Preparata 12 parts; 14.5 parts, fresh Flos Sesami indici; Rhizoma Et Radix Notopterygii 12.5 parts; Cortex Biotae Radicis 13 parts; 15.5 parts, Folium Nelumbinis; Radix Codonopsis 16 parts; Nine sons are not from female 12 parts; Cayratia trifolia (L.) Domin 11 parts; Rhizoma Alismatis 13 parts; Lac regis apis 15 parts.
The preparation method of the external preparation of hair growth is:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing immersion of ethanol 6 days that mass concentration is 65%, obtain medicinal liquid for subsequent use;
(3) Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not placed in crock from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis, the deionized water adding 9 times amount infiltrates 4 hours, then big fire is heated to boil, and turn little fire and decoct three times slowly, first time decocts 240 minutes, second time decocts 28 minutes, third time decocts 12 minutes, adds the deionized water of 6.5 times amount respectively, merge three decocting liquids before second time and third time decoct, filter, filtrate is for subsequent use;
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, adds wetting agent propylene glycol and scalp irritation element nicotinic acid acyl simultaneously, stirs, via hole diameter is 0.09 μm of microporous filter membrane filtration, to obtain final product.
The using method of the external preparation of gained hair growth of the present invention is: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.
Model case: Wei XX, female, 32 years old, people from Yuncheng, Heze.Patient is in the raw girl of natural labor on April 19th, 2012, and puerperal, the unexpected alopecia in partial below, the crown appearred in one and a half months, ovalize, area 2.5cm × 3.5cm, and alopecia district skin Lightening, there is the hair of frangibility at edge.In certain First Academy local treatment, because worrying that Western medicine side effect is large, have influence on anemia of pregnant woman's health, give the treatment of oral medicinal herb decoction, after taking three courses for the treatment of, patient's baldness shape is not eased.Introduced through colleague afterwards, carried out my institute's treatment on August 9th, 2012.Check: patient's alopecia district scurf is greasy, set is comparatively tight, and hypotrichosis comes off, with indigestion and loss of appetite insomnia, and red tongue, yellow and greasy fur, soft pulse.
Use the external preparation of the present embodiment gained hair growth, using method: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.After treatment one and a half months, alopecia district hair all grows new sending out.All the other all diseases disappear.Advise and continue to use, with after treatment, patient's self-induction recovery from illness after three months.Through repeatedly following up a case by regular visits to, so far without recurrence.
embodiment 5the external preparation of hair growth, is prepared from (45g/ part) by the primary raw material of following weight proportioning: Fructus Tribuli 12 parts; Flos Genkwa 12.5 parts; Cortex Moutan 15 parts; Radix Anemones Rivularis 12.5 parts; 10 parts, Flos Carthami; The Radix Paeoniae Alba 13 parts; Radix Rehmanniae Preparata 11 parts; 13.5 parts, fresh Flos Sesami indici; Rhizoma Et Radix Notopterygii 11.5 parts; Cortex Biotae Radicis 11.5 parts; 14 parts, Folium Nelumbinis; Radix Codonopsis 14 parts; Nine sons are not from female 11 parts; Cayratia trifolia (L.) Domin 9.5 parts; Rhizoma Alismatis 12 parts; Lac regis apis 13 parts.
The preparation method of the external preparation of hair growth is:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing immersion of ethanol 5 days that mass concentration is 60%, obtain medicinal liquid for subsequent use;
(3) Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not placed in crock from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis, the deionized water adding 8 times amount infiltrates 3.5 hours, then big fire is heated to boil, and turn little fire and decoct three times slowly, first time decocts 37 minutes, second time decocts 25 minutes, third time decocts 11 minutes, adds the deionized water of 6 times amount respectively, merge three decocting liquids before second time and third time decoct, filter, filtrate is for subsequent use;
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, adds wetting agent propylene glycol and scalp irritation element nicotinic acid acyl simultaneously, stirs, via hole diameter is 0.08 μm of microporous filter membrane filtration, to obtain final product.
The using method of the external preparation of gained hair growth of the present invention is: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.
test example:the clinical practice of the preparation method (embodiment 5) of the external preparation of invention gained hair growth:
In July ,-2013 in March, 2010, screen in 4 hospitals the patient that 346 examples suffer from alopecia in various degree.Wherein alopecia totalis 230 example, alopecia universalis 116 example.Male patient is totally 232 examples, and female patient is totally 114 examples.Age, 42.5 ± 1.5 years old mean age, the course of disease was the shortest in half a year, the longest 11 years in 18-59 year.All Patients Patients are divided into matched group and experimental group randomly, and two groups all have comparability in sex, age, the course of disease and the state of an illness.Experimental group uses the external preparation of gained hair growth of the present invention, using method: dip appropriate this product uniform application in hair loss area with absorbent cotton.Every day 3-5 time, 30 days courses for the treatment of.Matched group with experimental group under identical time and environment, use the product of other treatment alopecia (as ancient prescription hair growth liquor, reach fall thick and fast glad, reinforce the kidney hair-growth ballet etc.).Treat three courses for the treatment of altogether, and observe simultaneously, record the natural on-off cycles of hair growth situation of every group patient.Curative effect situation criterion: recovery from illness: alopecia district all grows new hair, and Xin Faseze, hardness are all normal.Effective: alopecia district hair grows more than 60%, and hair no longer comes off; Take a turn for the better: alopecia district hair grows more than 35%.Invalid: alopecia district hair grows less than 15%, or grow without new sending out.Wherein effective percentage adds effective in recovery from illness.Result is as shown in table 1:
Table 1: the therapeutic outcome of experimental group and matched group patient
Therapeutic outcome: experimental group is fully recovered 166 examples (73.5%), and effective 56 examples (24.8%), 3 examples that take a turn for the better (1.3%), invalid 1 example (0.4%), effective percentage is 98.3%.And matched group effective percentage is 70%.From result, experimental group successful is better than matched group.
The present invention select Fructus Tribuli, Flos Genkwa, Cortex Moutan, Radix Anemones Rivularis, Flos Carthami, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii and Cortex Biotae Radicis etc. totally 16 taste primary raw material medicines be prepared from.Fang Zhong, Cortex Moutan heat clearing away, removing heat from blood, and blood; Radix Anemones Rivularis heat-clearing and toxic substances removing; Relaxing muscles and tendons to promote blood circulation; Flos Carthami promoting blood circulation to restore menstrual flow, eliminating stasis to stop pain; Radix Rehmanniae Preparata nourishing YIN and supplementing blood, beneficial essence fills out marrow; Radix Codonopsis invigorating the spleen and replenishing QI, spleen invigorating lung benefiting; Lac regis apis nourishing, strong, the liver benefiting, spleen invigorating.All medicines share to be had good blood circulation promoting and blood stasis dispelling, promotion of blood circulation, improves hair follicle nutrition, hair follicle stimulating growth, promote new effect sending out regeneration, has good therapeutic effect to alopecia.
Finally it should be noted that, embodiment is the detailed description of the invention of optimum of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. the external preparation of hair growth, is characterized in that, is prepared from by the primary raw material of following weight proportioning: Fructus Tribuli 8-16; Flos Genkwa 10-15; Cortex Moutan 12-18; Radix Anemones Rivularis 9-16; Flos Carthami 7-13; Radix Paeoniae Alba 10-16; Radix Rehmanniae Preparata 8-14; Fresh Flos Sesami indici 11-16; Rhizoma Et Radix Notopterygii 9-14; Cortex Biotae Radicis 8-15; Folium Nelumbinis 11-17; Radix Codonopsis 10-18; Nine sons are not from female 8-14; Cayratia trifolia (L.) Domin 6-13; Rhizoma Alismatis 10-14; Lac regis apis 9-17.
2. the external preparation of hair growth as claimed in claim 1, is characterized in that, be prepared from by the primary raw material of following weight proportioning: Fructus Tribuli 10-14; Flos Genkwa 11.5-13.5; Cortex Moutan 14-16; Radix Anemones Rivularis 11-14; Flos Carthami 9-11; Radix Paeoniae Alba 12-14; Radix Rehmanniae Preparata 10-12; Fresh Flos Sesami indici 12.5-14.5; Rhizoma Et Radix Notopterygii 10.5-12.5; Cortex Biotae Radicis 10-13; Folium Nelumbinis 12.5-15.5; Radix Codonopsis 12-16; Nine sons are not from female 10-12; Cayratia trifolia (L.) Domin 8-11; Rhizoma Alismatis 11-13; Lac regis apis 11-15.
3. the external preparation of hair growth as claimed in claim 1, is characterized in that, be prepared from by the primary raw material of following weight proportioning: Fructus Tribuli 12; Flos Genkwa 12.5; Cortex Moutan 15; Radix Anemones Rivularis 12.5; Flos Carthami 10; The Radix Paeoniae Alba 13; Radix Rehmanniae Preparata 11; Fresh Flos Sesami indici 13.5; Rhizoma Et Radix Notopterygii 11.5; Cortex Biotae Radicis 11.5; Folium Nelumbinis 14; Radix Codonopsis 14; Nine sons are not from female 11; Cayratia trifolia (L.) Domin 9.5; Rhizoma Alismatis 12; Lac regis apis 13.
4. the preparation method of the external preparation of the hair growth as described in claim 1-3, is characterized in that, step is as follows:
(1) fresh Flos Sesami indici is smashed to pieces, gets its juice, for subsequent use; Fructus Tribuli is placed in parch container, slow fire parching to brown, takes out, for subsequent use;
(2) Fructus Tribuli step (1) processed and Flos Genkwa, Cortex Moutan, Flos Carthami and Folium Nelumbinis are together placed in hermetic container, add the In Shade sealing of ethanol and soak, obtain medicinal liquid for subsequent use;
(3) by Radix Anemones Rivularis, the Radix Paeoniae Alba, Radix Rehmanniae Preparata, Rhizoma Et Radix Notopterygii, Cortex Biotae Radicis, Radix Codonopsis, nine sons are not from mother, Cayratia trifolia (L.) Domin and Rhizoma Alismatis are placed in crock, the deionized water adding 6-10 times amount infiltrates (deionized water preferably adding 7-9 times amount infiltrates), then big fire is heated to boil, turn little fire and decoct three times slowly, first time decocts 28-46 minute (preferably first time decocts 34-40 minute), second time decocts 16-34 minute (preferably second time decocts 22-28 minute), third time decocts 8-14 minute (preferably third time decocts 10-12 minute), the deionized water (adding the deionized water of 5.5-6.5 times amount before preferred second time and for the third time decoction respectively) of 4.5-7.5 times amount is added respectively before second time and for the third time decoction, merge three decocting liquids, filter, filtrate is for subsequent use,
(4) step (2) gained medicinal liquid is joined in above-mentioned filtrate, reclaim ethanol, be cooled to room temperature, add the fresh Flos Sesami indici liquid of step (1) gained and Lac regis apis, mixing, add wetting agent and scalp irritation element simultaneously, stir, through microporous filter membrane filtration, to obtain final product.
5. the preparation method of the external preparation of hair growth according to claim 4, it is characterized in that, in step (2), the mass concentration of ethanol is the mass concentration of the preferred ethanol of 50%-70%(is 55%-65%, and the mass concentration of the ethanol be more preferably is 60%).
6. the preparation method of the external preparation of hair growth according to claim 4, is characterized in that, the time that step (2) is soaked is 3-7 days (the preferred time of soaking is 4-6 days, and the time of the immersion be more preferably is 5 days).
7. the preparation method of the external preparation of hair growth according to claim 4, is characterized in that, the time infiltrated in step (3) is 2-5 hour (the preferred time infiltrated is 3-4 hour, and the time of the infiltration be more preferably is 3.5 hours).
8. the preparation method of the external preparation of hair growth according to claim 4, it is characterized in that, wetting agent described in step (4) is one in glycerol, propylene glycol and Sorbitol (preferred described wetting agent is the one in propylene glycol and Sorbitol, and the described wetting agent be more preferably is propylene glycol).
9. the preparation method of the external preparation of hair growth according to claim 4, it is characterized in that, the element of scalp irritation described in step (4) is the one (preferred described scalp irritation is plain is the one in nicotinic acid acyl and Mylabris tincture, and the described scalp irritation element be more preferably is nicotinic acid acyl) in nicotinic acid acyl, capsicum tincture and Mylabris tincture.
10. the preparation method of the external preparation of hair growth according to claim 4, it is characterized in that, the aperture of micropore filtering film described in step (4) is 0.05-0.1 μm (aperture of preferred described micropore filtering film is 0.06-0.09 μm, and the aperture of the described micropore filtering film be more preferably is 0.08 μm).
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|---|---|---|---|---|
| JP2007051075A (en) * | 2005-08-16 | 2007-03-01 | Keio Gijuku | Method for preparing plant extract, plant extract and its application |
| CN101983693A (en) * | 2010-08-26 | 2011-03-09 | 葛德钜 | Drug for treating alopecia and preparation method thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007051075A (en) * | 2005-08-16 | 2007-03-01 | Keio Gijuku | Method for preparing plant extract, plant extract and its application |
| CN101983693A (en) * | 2010-08-26 | 2011-03-09 | 葛德钜 | Drug for treating alopecia and preparation method thereof |
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| 罗和古等: "《经方验方巧治皮肤病.下册》", 30 September 2007, 中国医药科技出版社 * |
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