CN104910813A - 一种精制油茶果壳栲胶的制备方法 - Google Patents
一种精制油茶果壳栲胶的制备方法 Download PDFInfo
- Publication number
- CN104910813A CN104910813A CN201510203982.9A CN201510203982A CN104910813A CN 104910813 A CN104910813 A CN 104910813A CN 201510203982 A CN201510203982 A CN 201510203982A CN 104910813 A CN104910813 A CN 104910813A
- Authority
- CN
- China
- Prior art keywords
- oil
- tannin extract
- processing units
- tea camellia
- camellia husks
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000001648 tannin Substances 0.000 title claims abstract description 50
- 235000018553 tannin Nutrition 0.000 title claims abstract description 50
- 229920001864 tannin Polymers 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 235000013399 edible fruits Nutrition 0.000 title abstract description 6
- 241001122767 Theaceae Species 0.000 title abstract description 5
- 239000000463 material Substances 0.000 claims abstract description 41
- 239000011344 liquid material Substances 0.000 claims abstract description 29
- 238000001914 filtration Methods 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 16
- 238000002386 leaching Methods 0.000 claims abstract description 15
- 238000003756 stirring Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000008367 deionised water Substances 0.000 claims abstract description 12
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 12
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical class Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims abstract description 9
- 239000012535 impurity Substances 0.000 claims abstract description 9
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000007605 air drying Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 7
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims abstract description 7
- 240000001548 Camellia japonica Species 0.000 claims description 44
- 235000018597 common camellia Nutrition 0.000 claims description 44
- 239000010903 husk Substances 0.000 claims description 43
- 238000000034 method Methods 0.000 claims description 24
- 238000007670 refining Methods 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 14
- JXAZAUKOWVKTLO-UHFFFAOYSA-L sodium pyrosulfate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)OS([O-])(=O)=O JXAZAUKOWVKTLO-UHFFFAOYSA-L 0.000 claims description 14
- 238000003828 vacuum filtration Methods 0.000 claims description 12
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 9
- 239000012141 concentrate Substances 0.000 claims description 6
- 238000002203 pretreatment Methods 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 229960003280 cupric chloride Drugs 0.000 claims description 2
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims description 2
- 238000000605 extraction Methods 0.000 abstract description 3
- 239000002244 precipitate Substances 0.000 abstract 4
- 238000001816 cooling Methods 0.000 abstract 1
- 230000007423 decrease Effects 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 239000003643 water by type Substances 0.000 description 8
- 150000001298 alcohols Chemical class 0.000 description 4
- 244000147058 Derris elliptica Species 0.000 description 3
- 239000010495 camellia oil Substances 0.000 description 3
- 210000004027 cell Anatomy 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 235000006667 Aleurites moluccana Nutrition 0.000 description 1
- 241000283690 Bos taurus Species 0.000 description 1
- 240000004957 Castanea mollissima Species 0.000 description 1
- 235000018244 Castanea mollissima Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 229930185884 camellianin Natural products 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 229960004232 linoleic acid Drugs 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
Landscapes
- Tea And Coffee (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510203982.9A CN104910813B (zh) | 2015-04-27 | 2015-04-27 | 一种精制油茶果壳栲胶的制备方法 |
Applications Claiming Priority (1)
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CN201510203982.9A CN104910813B (zh) | 2015-04-27 | 2015-04-27 | 一种精制油茶果壳栲胶的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN104910813A true CN104910813A (zh) | 2015-09-16 |
CN104910813B CN104910813B (zh) | 2017-06-23 |
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CN201510203982.9A Expired - Fee Related CN104910813B (zh) | 2015-04-27 | 2015-04-27 | 一种精制油茶果壳栲胶的制备方法 |
Country Status (1)
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CN (1) | CN104910813B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106867408A (zh) * | 2017-03-24 | 2017-06-20 | 广西壮族自治区林业科学研究院 | 一种利用板栗苞提取栲胶和制备复合材料的方法 |
CN106893493A (zh) * | 2017-03-24 | 2017-06-27 | 广西壮族自治区林业科学研究院 | 利用油茶壳提取栲胶的方法及其在制备复合材料的应用 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040137093A1 (en) * | 2003-01-13 | 2004-07-15 | Luis-Henrique Lamb | Process for the provision of a plant extract containing condensed tannins, with astringent characteristics, modified by copolymerization, for use in tanning and retainning of skins, a plant extract with astringent characteristics, modified by copolymerization, and use of a modified plant extract containing tannings |
CN101870849A (zh) * | 2009-04-22 | 2010-10-27 | 中国科学院过程工程研究所 | 一种超声强化提取板栗苞生产栲胶的新方法 |
CN102757543A (zh) * | 2011-09-30 | 2012-10-31 | 江西省林业科学院 | 油茶果壳液化树脂胶粘剂的制备方法 |
-
2015
- 2015-04-27 CN CN201510203982.9A patent/CN104910813B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040137093A1 (en) * | 2003-01-13 | 2004-07-15 | Luis-Henrique Lamb | Process for the provision of a plant extract containing condensed tannins, with astringent characteristics, modified by copolymerization, for use in tanning and retainning of skins, a plant extract with astringent characteristics, modified by copolymerization, and use of a modified plant extract containing tannings |
CN101870849A (zh) * | 2009-04-22 | 2010-10-27 | 中国科学院过程工程研究所 | 一种超声强化提取板栗苞生产栲胶的新方法 |
CN102757543A (zh) * | 2011-09-30 | 2012-10-31 | 江西省林业科学院 | 油茶果壳液化树脂胶粘剂的制备方法 |
Non-Patent Citations (1)
Title |
---|
邹礼根: "《农产品加工副产物综合利用技术》", 31 March 2013, 浙江大学出版社 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106867408A (zh) * | 2017-03-24 | 2017-06-20 | 广西壮族自治区林业科学研究院 | 一种利用板栗苞提取栲胶和制备复合材料的方法 |
CN106893493A (zh) * | 2017-03-24 | 2017-06-27 | 广西壮族自治区林业科学研究院 | 利用油茶壳提取栲胶的方法及其在制备复合材料的应用 |
CN106867408B (zh) * | 2017-03-24 | 2020-03-24 | 广西壮族自治区林业科学研究院 | 一种利用板栗苞提取栲胶和制备复合材料的方法 |
CN106893493B (zh) * | 2017-03-24 | 2020-12-25 | 广西壮族自治区林业科学研究院 | 利用油茶壳提取栲胶的方法及其在制备复合材料的应用 |
Also Published As
Publication number | Publication date |
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CN104910813B (zh) | 2017-06-23 |
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Inventor after: Chen Xisheng Inventor before: Chen Chen |
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Effective date of registration: 20170602 Address after: 212000, 97, Cheng Cheng Road, new town, Zhenjiang, Jiangsu Applicant after: Jiangsu all state Mstar Technology Ltd Address before: 239300 Tianchang, Anhui, West Gate Street, No. 33, No. Applicant before: Chong Xishan |
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