CN104873446B - A kind of toothpaste containing cinnamon oil - Google Patents
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Abstract
The present invention relates to technical field of toothpaste, and in particular to a kind of toothpaste containing cinnamon oil, includes the raw material of following weight percentage：Cinnamon oil 0.2%~1.5%；Precipitated calcium carbonate 20%~30%；Silica 20%~30%；Peppermint oil 0.1%~0.7%；NMF 20%~30%；Foaming agent 1.5%~2.5%；Thickener 1.2%~2.7%；Xylitol 0.03%~0.15%；Saccharin 0.01%；Propolis 0.02%~0.05%；Methyl p-hydroxybenzoate 0.05%~0.15%；Distilled water surplus.The present invention also further adds traditional Chinese medicine ingredients; the toothpaste that preparation method of the present invention obtains is clearing heat and detoxicating; anti-inflammation; heat-clearing and fire-reducing can be played a part of, suppress oral cavity harmful bacteria, take care of one's teeth, energy effectively preventing treats the mouth diseases such as canker sore, gingival swelling and pain, alveolar abscess, tooth age inflammation, periodontitis, pulpitis.
Description
Technical field
The present invention relates to technical field of toothpaste, and in particular to a kind of toothpaste containing cinnamon oil.
Background technology
Toothpaste is commonly used in people's daily life, is improved and is formed by tooth powder, and the tooth powder of early stage mainly uses carbonic acid
Calcium as rubbing agent, using soap as surfactant.With developing rapidly for science and technology, toothpaste industry also obtains very big improvement,
On the one hand it is the development and application of new rubbing agent, NMF, thickener and surfactant, tooth paste product quality is constantly risen
Level is regenerated；On the other hand, toothpaste also turns into the oral hygiene use of preventing and treating odontopathy from the common function development that cleans the teeth for addition medicine
Product, most prominent is to add fluorine toothpaste, greatly reduces the dental caries incidence of disease.
The firm tooth of a bite, pure and fresh implication, everybody wants to possess.But into manhood, the morbidity of periodontal disease
Rate is gradually increasing, and with advancing age, its order of severity is also constantly deepened.Gum, periodontium are protected, for adult
People seems more urgent.Part Chinese herbal toothpaste can really play a part of taking care of one's teeth comprehensively, tooth age, periodontium.For example,
Mica filled polypropylene, it can prevent the oral problem such as tooth age bleeding, prevention tooth age inflammation, periodontitis, tooth age atrophy rapidly.Certainly,
This depends on the active component of Yunnan Baiyao in toothpaste, can effectively improve tooth age, periodontium and oral cavity and be followed with regard to the blood of film
Ring, improve the supply of periodontium and oral cavity mucous membrane tissue nutrient, the disease-resistant energy of enhancing tooth age, periodontal, tooth and oral cavity with regard to film
Power.
Retrieve be related to toothpaste patent it is as follows：
1st, Chinese patent, title：Chinese medicinal toothpaste application number 03159651.7 is applied（Patent right）People:Liuzhou Radix zanthoxyli
Limited company makes a summary：The present invention relates to Chinese medicinal toothpaste technical field, and its Chinese herbal medicine composite is in its lotion of toothpaste
Content is 0.05-1.5%, and the murraya paniculata concrete for having 10% is comprised at least in the Chinese herbal medicine composite；The murraya paniculata concrete be by
Kamuning pulverizing medicinal materials to 0.1-l0 mm in size granule materials；Using 40-90% ethanol as solvent, with diacolation speed
For l-l00 milliliters seepage pressure effects per minute, percolate through ethanol is recovered under reduced pressure, be concentrated into relative density be 1.0-1.3 it is clear
After cream, acid-base value is adjusted, it is 7-l0 to make pH value, and controls the obtained thing that yield is 50-150%.This toothpaste has in use
There are stronger subdhing swelling and detoxicating, promoting qi circulation and relieving pain, dissipating bind by blood stasis and smoothing collaterals wind-dispelling, the effect of sharp water desinsection, to toothache, tooth age bleeding, tooth
Age inflammation, the oral cavity such as periodontal abscess, pericoronitis, canker sore, sphagitis and dental disorders have more significant prophylactic-therapeutic effect, and
Can chronically it use safely.
2nd, Chinese patent, title：A kind of toothpaste containing Chinese medical extract and preparation method and application；Application number
03128352.7 application（Patent right）People:Make a summary Beijing Jiangzhong High-Tech Investment Limited Liability Company：The present invention relates to one kind
Toothpaste containing Chinese medical extract, the especially toothpaste containing root tuber of aromatic turmeric class Chinese medical extract, and preparation method thereof and whitening control tooth
Application.Can be 0.1-the 10% of toothpaste gross weight as the addition for the Chinese medical extract that root tuber of aromatic turmeric class is used as medicine.The traditional Chinese medicine extraction
Thing is especially suitable for except korron, tea spot, the tooth paste product being made from it, appearance luster is light, and product quality is stable, the whitening that cleans the teeth effect
Fruit is obvious.
3rd, Chinese patent, title：Toothpaste for auxiliary treatment gingivitis and preparation method thereof；Application number
2013lOll3804.8 application（Patent right）People:Liu Bingtian makes a summary：The invention provides one kind to be used for auxiliary treatment gingivitis
Toothpaste, the toothpaste includes the traditional Chinese medicine composition extract liquid of 20% one 30% auxiliary treatment gingivitis, 2% one 4% bondings
Agent, 18% one 28% rubbing agents, 40% one 50% NMFs, 1% one 3% surfactants, 1% one 2% sweeteners, O.5%
The water of one 1.5% stabilizer, 1.5% one 2.5% antiseptics and surplus.Toothpaste provided by the invention can be effectively improved gum and refer to
Number and plaque index, mitigate gingivitis degree, have to treatment gingivitis and help effect well.
The mouth diseases such as periodontitis, toothache, hemodia annoying the life of people always；Chinese herbal toothpaste species at present
A lot, its effective component both is from greatly natural animal-plant, small with excitant compared to other chemical synthetic drugs, toxic side effect
The characteristics of small, accepted extensively by people；It mainly adds corresponding Chinese medicine in the blind body matrix of toothpaste of composition toothpaste
Composition forms Chinese medicinal toothpaste, although these compositions prevent and treat periodontitis, anti-inflammatory analgesic with certain suppression oral cavity harmful bacteria
Effect；But possessing multi-efficiency at present, the toothpaste of comprehensive solution mouth disease is actually rare.
The content of the invention
It is an object of the invention to provide a kind of toothpaste containing cinnamon oil, cinnamon oil is added in toothpaste, plays killing
The effect of harmful levels of pathogens in skin and oral cavity, the toothpaste that is prepared of the present invention have heat-clearing and fire-reducing, suppress oral cavity harmful bacteria,
Fresh breath, the effect to take care of one's teeth, moreover it is possible to which effectively preventing treats canker sore, gingival swelling and pain, alveolar abscess, tooth age inflammation, tooth
The mouth diseases such as Zhou Yan, pulpitis.
In order to realize the purpose of the present invention, the present invention adopts the following technical scheme that：
A kind of toothpaste containing cinnamon oil, it is characterised in that include the raw material of following weight percentage：
Cinnamon oil 0.2%~1.5%；Precipitated calcium carbonate 20%~30%；Silica 20%~30%；Peppermint oil 0.1%~
0.7%；NMF 20%~30%；Foaming agent 1.5%~2.5%；Thickener 1.2%~2.7%；Xylitol 0.03%~0.15%；Sugar
Essence 0.01%；Propolis 0.02%~0.05%；Methyl p-hydroxybenzoate 0.05%~0.15%；Distilled water surplus.
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that traditional Chinese medicine ingredients, its weight score are also further added in toothpaste
Number is 5%~10%.
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that described traditional Chinese medicine ingredients include the component of following parts by weight：
10~17 parts of wintercherry fruit or calyx, 10~15 parts of indigo naturalis, 12~18 parts of asarum, 6~10 parts of dandelion, 2~5 parts of fimbriatestipulate begonia herb, balloonflower root 3~5
Part, 5~8 parts of the root bark of tree peony.
Above-mentioned propolis is the propolis powder for being ground into 100~120 mesh.
Above-mentioned NMF is the one or more in glycerine, propane diols and sorbierite；Described foaming agent is dioctyl
Sodium sulfosuccinate or lauroyl sulfoacetic acid sodium；Described thickener be sodium alginate, xanthans, guar gum, carrageenan,
One or more in deer horn pectin and carragheen.
The preparation method step of the above-mentioned toothpaste containing cinnamon oil is as follows：
（1）Each component in traditional Chinese medicine ingredients is ground into 50~80 mesh respectively with pulverizer, then taken in parts by weight
The each component crushed is sufficiently mixed uniformly, obtains mixture, and it is 80%~90% ethanol that determining alcohol is added into mixture, second
The addition of alcohol is 2~3 times of volume of mixture, is flowed back 4~7 hours at 60~85 DEG C, filters, obtains phegma；
（2）Phegma is evaporated under reduced pressure, removes ethanol, solid fraction object is obtained, then solid fraction object is dried
Powder
Powder is broken into, obtains the traditional Chinese medicine ingredients for preparing the toothpaste containing cinnamon oil；
（3）By obtained traditional Chinese medicine ingredients according to proportioning and silica；Precipitated calcium carbonate；Cinnamon oil；Peppermint oil；Moisturizing
Agent；Foaming agent；Thickener；Xylitol；Saccharin；Propolis；Methyl p-hydroxybenzoate is sufficiently mixed, and then adds distilled water, is used
Mixer strong stirring is uniform, is formed with the lotion of certain viscosity；
（4）Obtained lotion is ground twice with grinder, grinding 1~2 hour, then carries out second again for the first time
Secondary grinding, second of grinding 1 hour, vacuum outgas is carried out after second of grinding, untill vacuum reaches -0.097Mpa,
The vacuum outgas time is about 40~45 minutes；A period of time is stood after lotion degassing, obtains product.
Above-mentioned cinnamon oil is canella Chinese cassia tree Cinnamomum cassia Presl drying branch, leaf through vapor
The volatile oil that distillation obtains.Cinnamon oil is widely used in medicine, food and light industry industry.Top grade is classified as in history tree, it is believed that
There is the effect such as mends fire supporing yang, let the fire back to its origin, eliminating cold to stop pain, invigorate blood circulation.The traditional Chinese medical science is used as and controls impotence, Gong Leng, waist and knee crymodynia, kidney deficiency
Breathe heavily, dizziness due to yang deficiency, hot eyes pharyngalgia, trusted subordinate's crymodynia, cold of insufficiency type vomiting and diarrhea, cold hernia, run quickly globefish, Amenorrhea, emmenagogue uses.Modern study shows
Show, Chinese cassia tree has a variety of effects such as antibacterial, antitumor, antiulcer, antipyretic, analgesia spasmolysis, establishing-Yang, desinsection.Cinnamon oil has day
The effect of right expelling parasite desinsection, killing fungus, again will not contaminated food.Cinnamon oil is to common bacteria（It is Escherichia coli, salmonella, withered
Careless bacillus, Dipel etc.）, saccharomycete（Brewer's yeast, Saccharomyces cerevisiae etc.）, mould（Aspergillus niger, aspergillus oryzae, Huang Qu
Mould, mould, trichoderma, Mucor, head mold etc.）Very strong inhibitory action is respectively provided with, cinnamon oil is added in toothpaste, has and kills skin
The effect of harmful levels of pathogens in skin and oral cavity.
In above-mentioned traditional Chinese medicine ingredients, described wintercherry fruit or calyx Classification system is：Physalis alkekengi L.var.franchetiiAlso known as：Franchet groundcherry persistent calyx or fruit, cape gooseberry, red lantern, Miss, golden Miss, golden lamp, aunt grind youngster, cluck bird；Wintercherry fruit or calyx
For Solanaceae Physalis perennial herb plant, medicinal fruit, there are clearing heat and detoxicating, relieving sore-throat, resolving sputum, diuresis, soothing the liver and antibechic
The function of diuresis.Cure mainly liver-qi depression, ephritis, hepatitis；Scurvy, phlegm-heat cough.Wintercherry fruit or calyx plant is as Chinese medicine, alcohol containing wintercherry
（physanol）A、B；Sterol containing grass in seed（gramisterol）, obtusifoliol（obtusifoliol）, cycloartanol
（cycloartanol）, cycloartenol（cycloartenol）Etc. chemical composition.It is cold in nature, bitter, cure mainly lung heat laryngalgia, lung
Disease, parotitis, hot hernia, blood strangury；Control skin sore swells, pemphigus, swelling and aching of gum outside.Have clearing heat and detoxicating a, relieving sore-throat, resolving sputum, diuresis it
Effect.Seedling, leaf, stem, root can be used as medicine, and bitter, tremble with fear, be nontoxic.Seedling, leaf, stem A0.02% containing physagulin, B0.002%, C are (de-
Oxygen physagulin A).It is sour, bitter, it is cold in nature, there is clearing heat and detoxicating, diuresis function.Can control cough, jaundice, malaria, oedema, furunculosis,
Erysipelas etc..It is root bitter, cold in nature, there are heat-clearing, sharp water function.Can preventing and curing malaria disease, jaundice, hernia.Seed is sour, flat, nontoxic.That expands harbors
Calyx can be used as medicine, and have the effect of refrigerant, resolving sputum, antibechic, diuresis.Fruity is sour-sweet, slightly bitter taste, and pericarp taste is extremely bitter, and both can all enter
Medicine, bright and beautiful lamp fruit claim " I " on Chinese medicine, can clearing heat and detoxicating, clearing phlegm and relieving cough, treat chronic bronchitis.
Described indigo naturalis：For acanthaceous vegetable acanthaceous indigoBaphicacanthus cusia (Nees) Bremek.Polygonaceae plant
Indigo plantPolygonum tinctorium AitOr cruciferae isatisIsatis indigotica Fort.Leaf or stem
Leaf processed obtained dried powder, agglomerate or particle.Also known as：Indigo flower, clam powder, blue or green cylinder flower, Lan Lu, the flower that forms sediment, indigo foam flower；Property
Taste is salty-cold, there is clearing heat and detoxicating, blood cooling and ecchymoses removing, purging intense heat arresting convulsion and other effects.It is mainly used in warm disease excess heat, macula, spits blood, spitting of blood,
Pharyngalgia aphtha, pediatric epilepsy scared, sore swells, erysipelas, snake bite and insect sting etc..《Kaibao Bencao》：" all medicine poison of principal solution, infantile pyretic diseases, hair of fainting from fear
Heat, pestilent headache fever and chills, pan-fried water, which is ground, takes it.Also rub the poison such as swollen deposited herpes simplex, evil, metal-inflicted wound, lower blood, snake dog.4《Book on Chinese herbal medicine covers bamboo fish trap》：" rush down
Liver, only diarrhea, phlegm water on the diaphragm that disappears, epidemic disease headache is driven, holds back the red spot of typhoid fever, water is taken after mixing with liquid it.”
《Compendium of Materia Medica》：" reduce phlegm and internal heat tired, spit blood, spitting of blood, spot sore, the erosion of vulva, kill and dislike worm.”《Book on Chinese herbal medicine is stated》：" control apoplexy, intermittent headache,
Hypochondriac pain, Chi, flutter, dizziness, cough, cough, vomit long, tongue nosebleed, cough blood, cold hernia." indigo naturalis is to microsporum lanosum, disconnected hair
Tinea, Microsporum gypseum, purple tinea bacterium, trichophyton gypseum, red mentagrophytes, acrothesium floccosum etc. have stronger suppression to make
With gingivitis can be treated.
Described asarum, alias：Asarum sieboldii, basin grass asarum, Latin literary fame：Asarum sieboldii Miq.Birthwort
Section, asarum perennial herb；Asarum is as medicinal plant, Shi Zai Qin Han《Sheng Nong's herbal classic》,《Sheng Nong's herbal classic》Arranged
For top grade.HERBA ASARI from Liaoning of China root is thin, color sallow, leaf color are green, the peppery numb tongue of acrid flavour.It is warm-natured, it is slightly poisonous.The thoughts of returning home, lung, kidney channel.There is wind-dispelling, dissipate
It is cold, warm lung, water-filling, have one's ideas straightened out, the effect of antipyretic-antalgic, there is the curative effects such as antibacterial, anti-inflammatory, hemostasis, analgesia.Control anemofrigid headache, nose
Deep pool, dentalgia, phlegm and retained fluid cough is inverse, arthralgia pain due to rheumatism.In addition, asarum also has anti inflammatory immunity, local anaesthesia, improves metabolism, antibacterial
Effect, also available for Chemotherapy of Tumor Patients and the Neuroleptic Leukocytopenia of caused by radiation.Calm, analgesic activity Herba Asari volatile oil has substantially
Central inhibitory action, low dose can make that animal is quiet, taming, autonomic activities is reduced；Heavy dose can make animal sleep, and have bright
Aobvious anticonvulsant action.Asarum decoction, which gavages, also analgesic activity.Its stronger analgesic activity is its treatment head bodily pain, toothache etc.
Valuable pharmacological basis.Anti-inflammatory, immunosupress and antiallergic action Herba Asari volatile oil, which are gavaged or injected, obvious anti-inflammatory
Effect.Antibacterial, antivirus action kakuol preserved material, volatile oil etc. have necessarily to gram positive bacteria, hay bacillus and typhoid bacillus
In-vitro Inhibitory Effect, decoction also has inhibitory action to tubercle bacillus and typhoid bacillus.Herba Asari volatile oil is to a variety of fungies such as Huang
Aspergillus, black-koji mould, Candida albicans etc. have inhibitory action, and the active ingredient of antibacterial is safrole.α-asarone has suppression
The effect of Respiratory Syncytial Virus(RSV) propagation processed.
Described dandelion（Classification system：Taraxacum mongolicum Hand.-Mazz.）Composite family,
Dandelion herbaceos perennial.Dandelion alias dandelion, Po Poding, Hua Hualang etc..Major function：Clearly
Thermal detoxification, diuresis dissipating bind.Control acute mastitis, adenolymphitis, scrofula, boil poisonous soreness, acute conjunctivitis, cold, fever is acute
Tonsillitis, acute bronchitis, gastritis, hepatitis, cholecystitis, urinary tract infections.Contain taraxol, Pu in dandelion plant
A variety of health-nutrition compositions such as public English element, choline, organic acid, synanthrin.Containing taraxol, taraxerol, ψ-Portugal's public affairs English in root
Sterol, taraxasterol, β-amyrin, stigmasterol, cupreol, choline, organic acid, fructose, sucrose, glucose, grape
Glucoside and resin, rubber etc..Leaf is containing lutein, violaxanthin, phylloquinone, vitamin C（50~70 milligrams/100 grams）With
Vitamin D（5~9 milligrams/100 grams）.Nature and flavor are sweet, slight bitter, tremble with fear.Return liver, stomach.There are the work(such as diuresis, laxative, removing jaundice subcutaneous ulcer, cholagogic
Effect.Control heat toxin, carbuncle swells, sore, internal carbuncle, red eye, swell pain, damp and hot, jaundice, the puckery pain of dribbling urination, furuncle swelling toxin, acute mastitis, scrofula,
Toothache, hot eyes, pharyngalgia, lung carbuncle, acute appendicitis, jaundice with damp-heat pathogen, puckery pain of heat gonorrhea.Control acute mastitis, adenolymphitis, scrofula, serious case of furuncle sore
It is swollen, acute conjunctivitis, cold, fever, acute tonsillitis, acute bronchitis, gastritis, hepatitis, cholecystitis, urinary tract infections etc..
Dandelion is raw-eaten, stir-fries and eats, cooks soup, is the plant of dietotherapeutic.
Described fimbriatestipulate begonia herb（Scientific name：Begonia fimbristipula）Also known as Gynura bicolor, red autumnal leaves, scattered blood, dragon and tiger
Leaf, night cross red, red water certain herbaceous plants with big flowers, are a kind of Chinese medicines.Bulb or complete stool for Begoniaceae plant Gynura bicolor.Function cures mainly heat-clearing
Cool blood, promoting blood circulation and detoxication.Control hot summer weather high fever, cough with lung heat, spitting of blood, bruises and sprains, blood stasis pain, sore mange, scald.
Property sweet-puckery flavor, it is cool, it is nontoxic.Guangzhou army《Conventional Chinese herbal medicine handbook》：" it is clearing heat and detoxicating, moisten dryness and relieve cough, eliminating stasis to subdue swelling.Control diseases caused by external factors
High fever.Heatstroke is had a fever, cough with lung heat, treating swelling and pain by traumatic injury.Fresh goods is mashed, and can apply malignant sore serious case of furuncle."《Conventional Chinese herbal medicine color atlas》："
Control pneumonia cough, spitting of blood, chronic bronchitis."《Guangxi practicality Chinese herbal medicine newly selects》：" cooling and activating blood, anti-inflammatory analgetic.Cure mainly and cough up
Blood, abdominal pain due to blood stasis, bruise, fracture, burn, tinea scabies ".
Described balloonflower root, Classification system：Platycodon grandiflorus (Jacq.) A. DCAlias burden
Flower, small bell flower, mitral flower, are herbaceos perennials, major function：Facilitaing lung, relieving sore-throat, eliminating the phlegm, apocenosis.For coughing with a lot of sputum,
Uncomfortable in chest not smooth, pharyngalgia, sound is mute, lung carbuncle pyemesis, and sore purulence is not into bursting.Pharmacological action：1. eliminating the phlegm and antitussive effect, contained by balloonflower root
Stimulation to a certain degree is caused when saponin is oral to mucosa and gastric mucosa, causes respiratory mucosa hypersecretion reflectingly,
Sputum is diluted, promotes its discharge, rough platycodoside has antitussive effect；2. hypoglycemic effect；3. antiinflammatory action：Thick balloonflower root soap
Glucoside has antiinflammatory action, and balloonflower root is without direct antibacterial action, but its water extract can strengthen macrophage phagocytic function, strengthens neutral white
The sterilizing power of cell.Improve the activity of lysozyme.4. suppress gastric secretion and antiulcer action；5. other effects：Thick balloonflower root soap
Glucoside has calm, analgesia and refrigeration function.
The described root bark of tree peony, also known as moutan bark, Chinese medicine name.For ranunculaceae peony（Classification system：Paeonia
suffruticosa Andr.）Dry root skin.《Compendium of Materia Medica》：" nourishing Yin and falling fire, solution spot poison, throat, diuresis
Stasis.Descendant is specially to control mutually fire with amur cork tree, does not know that the work(of the root bark of tree peony more wins.Red colored person's profit, white flower person mend, and people also seldom realizes, preferably divided
Not it." modern study, contained paeonol and its glucosides constituents in addition have antiinflammatory action；The methanolic extract of moutan bark
There is suppression Platelet；Paeonol has the central inhibitory actions such as calmness, cooling, antipyretic, analgesia, spasmolysis and anti-atherogenic hard
Change, diuresis, antiulcer etc. act on.It is cold in nature, bitter；It is cool；It is slightly cold.The thoughts of returning home；Liver；Kidney；Lung channel.Root bark of tree peony water decoction Carrageenan
Various inflammatory reactions caused by edema, adjuvant-induced arthritis and Arthus reactions etc. are inhibited, and moutan bark is to the anesthetized dog heart
Coronary blood flow can be increased, cardiac output is reduced, reduce the effect of left room work done.Moutan bark decoction is to hay bacillus, large intestine bar
Bacterium, typhoid bacillus, paratyphosum Bacterium, proteus, Pseudomonas aeruginosa, staphylococcus, hemolytic streptococcus, pneumococcus, cholera
Vibrios etc. has stronger antibacterial action, and tree peony leaf decoction has significantly to shigella dysenteriae, Pseudomonas aeruginosa and staphylococcus aureus
Antibacterial action, its effective ingredient are gallic acid.
Described propolis is the resin that honeybee gathers from plant gemma or trunk, is mixed into palatine gland, wax thereon
A kind of colloidal solid thing with aromatic odor that the secretion of gland is process.Classification system is：Colla
Apis, it is the stickum that Apidae animal apis cerana etc. repairs yellowish-brown or dark brown secreted by honeycomb, can be used as medicine.Its
It is cold in nature, it is bitter, pungent, there is the effect of moisturizing myogenic, anti-inflammatory analgetic, gastric ulcer, canker sore, burn and scald, skin Tearing Pain can be treated,
The illnesss such as radiation proof；The mcg/ml concentration of propolis ethanol soluble extraction 100 is to 25 kinds in 39 kinds of bacteriums and 39 kinds of plant epiphytes
In 20 kinds have inhibitory action, it is most sensitive to gram-positive bacterium and acid fast bacteria.1% -10% propolis alcohol or ether
The extract fungi common to the mankind, tinea bacterium, floccus mentagrophyte, red mentagrophytes, Microsporum ferrugineum, Microsporum gypseum,
Microsporum lanosum, brain shape tinea bacterium, trichophyton gypseum, trichophyton tonsurans, purple tinea bacterium etc. have inhibitory action.To cucumber
Mosaic virus, tobacco mottle virus, tobacco necrosis virus and influenza A have preferable killing action.Blister sore can be suppressed
The breeding of poison and the infection for significantly mitigating vaccinia virus；It is external just successfully to have been treated again using propolis ointment early in the fifties
The mouth diseases such as hair property aphtha, oral cavity anabrosis, ulcer.Abundant and unique bioactive substance contained by propolis, makes its tool
There are the multiple functions such as antibacterial, anti-inflammatory, antipruritic, anti-oxidant, immune, the hypoglycemic, reducing blood lipid of enhancing, antitumor, have to human body extensively
General medical treatment, health-care effect.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, cinnamon oil is added in toothpaste by the present invention, and cinnamon oil has the effect of natural insect-repelling desinsection, killing fungus, and not
Can contaminated food；Cinnamon oil is to common bacteria（Escherichia coli, salmonella, bacillus subtilis, Dipel etc.）, yeast
Bacterium（Brewer's yeast, Saccharomyces cerevisiae etc.）, mould（Aspergillus niger, aspergillus oryzae, aspergillus flavus, mould, trichoderma, Mucor, head mold etc.）Have
There is very strong inhibitory action, cinnamon oil is added in toothpaste, have the function that to kill harmful levels of pathogens in skin and oral cavity.Toothpaste
In also further add traditional Chinese medicine ingredients, and add peppermint oil, the peppermint oil of addition, which can not only play antibacterial action, to be had
The taste of traditional Chinese medicine of the comprehensive traditional Chinese medicine ingredients added of effect, subtracts taste of traditional Chinese medicine light, improves the smell of toothpaste so that toothpaste has a kind of light
Light peppermint delicate fragrance, play a part of fresh breath during using toothpaste；Adding propolis can be strengthened the antibacterial action of toothpaste,
And propolis has good therapeutic action to mouth disease.
2nd, the traditional Chinese medicine ingredients that the present invention uses combine wintercherry fruit or calyx, indigo naturalis, asarum, dandelion, fimbriatestipulate begonia herb, balloonflower root and the root bark of tree peony
The effective component of this several Chinese medicinal material, clearing heat and detoxicating, anti-inflammation, heat-clearing and fire-reducing can be played, suppresses oral cavity harmful bacteria, protect
Protect the effect of tooth, moreover it is possible to which effectively preventing treats canker sore, gingival swelling and pain, alveolar abscess, tooth age inflammation, periodontitis, pulpitis
Etc. mouth disease.
3rd, toothpaste produced by the present invention has stronger subdhing swelling and detoxicating, anti-inflammation, and the effect of anti-inflammatory and antalgic can be more preferable
Control halitosis and patch formation, bleeding gums, inflamed, pain, the symptom of canker sore can be played effective slow
Solution acts on, and has more significant prophylactic-therapeutic effect to dental disorders, and Chinese medicine is lightly seasoned, can chronically use safely.
Embodiment
Embodiment 1
A kind of toothpaste containing cinnamon oil, it is characterised in that include the raw material of following weight percentage：
Cinnamon oil 0.2%；Precipitated calcium carbonate 20%；Silica 20%；Peppermint oil 0.1%；NMF glycerine 20%；Foaming agent
Dioctyl sodium sulphosuccinate 1.5%；Thickener sodium alginate 1.2%；Xylitol 0.03%；Saccharin 0.01%；Propolis 0.02%；It is right
Methyl hydroxybenzoate 0.05%；Distilled water surplus；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that traditional Chinese medicine ingredients, its weight score are also further added in toothpaste
Number is 5%；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that described traditional Chinese medicine ingredients include the component of following parts by weight：
10 parts of wintercherry fruit or calyx, 10 parts of indigo naturalis, 12 parts of asarum, 6 parts of dandelion, 2 parts of fimbriatestipulate begonia herb, 3 parts of balloonflower root, 5 parts of the root bark of tree peony；
Above-mentioned propolis is the propolis powder for being ground into 100~120 mesh；
The preparation method step of the above-mentioned toothpaste containing cinnamon oil is as follows：
（1）Each component in traditional Chinese medicine ingredients is ground into 50~80 mesh respectively with pulverizer, then taken in parts by weight
The each component crushed is sufficiently mixed uniformly, obtains mixture, and it is 80%~90% ethanol that determining alcohol is added into mixture, second
The addition of alcohol is 2~3 times of volume of mixture, is flowed back 7 hours at 60 DEG C, filters, obtains phegma；
（2）Phegma is evaporated under reduced pressure, removes ethanol, solid fraction object is obtained, then solid fraction object is dried
Powder
Powder is broken into, obtains the traditional Chinese medicine ingredients for preparing the toothpaste containing cinnamon oil；
（3）By obtained traditional Chinese medicine ingredients according to proportioning and silica；Precipitated calcium carbonate；Cinnamon oil；Peppermint oil；NMF
Glycerine；Foaming agent dioctyl sodium sulphosuccinate；Thickener sodium alginate；Xylitol；Saccharin；Propolis；P-hydroxybenzoic acid first
Ester is sufficiently mixed, and then adds distilled water, uniform with mixer strong stirring, is formed with the lotion of certain viscosity；
（4）Obtained lotion is ground twice with grinder, excessively thick, really up to the mark particle is levigate, make lotion it is fine and smooth,
Uniformly, stably, grind 1~2 hour for the first time, then carry out second of grinding again, second of grinding 1 hour, the
Vacuum outgas is carried out after secondary grinding, untill vacuum reaches -0.097Mpa, the vacuum outgas time is about 40 minutes；Cream
A period of time is stood after body degassing, obtains product.
Embodiment 2
A kind of toothpaste containing cinnamon oil, it is characterised in that include the raw material of following weight percentage：
Cinnamon oil 0.7%；Precipitated calcium carbonate 23%；Silica 24%；Peppermint oil 0.3%；NMF 23%；Foaming agent
1.7%；Thickener 1.7%；Xylitol 0.07%；Saccharin 0.01%；Propolis 0.03%；Methyl p-hydroxybenzoate 0.08%；Distilled water
Surplus；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that traditional Chinese medicine ingredients, its weight score are also further added in toothpaste
Number is 6%；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that described traditional Chinese medicine ingredients include the component of following parts by weight：
Described traditional Chinese medicine ingredients include the component of following parts by weight：13 parts of wintercherry fruit or calyx, 11 parts of indigo naturalis, 14 parts of asarum, 7 parts of dandelion,
3 parts of fimbriatestipulate begonia herb, 3.5 parts of balloonflower root, 6 parts of the root bark of tree peony；
Above-mentioned propolis is the propolis powder for being ground into 100~120 mesh；
Above-mentioned NMF is the one or more in glycerine, propane diols and sorbierite；Described foaming agent is dioctyl
Sodium sulfosuccinate or lauroyl sulfoacetic acid sodium；Described thickener be sodium alginate, xanthans, guar gum, carrageenan,
One or more in deer horn pectin and carragheen；
The preparation method step of the above-mentioned toothpaste containing cinnamon oil is as follows：
（1）Each component in traditional Chinese medicine ingredients is ground into 50~80 mesh respectively with pulverizer, then taken in parts by weight
The each component crushed is sufficiently mixed uniformly, obtains mixture, and it is 80%~90% ethanol that determining alcohol is added into mixture, second
The addition of alcohol is 2~3 times of volume of mixture, is flowed back 6 hours at 70 DEG C, filters, obtains phegma；
（2）Phegma is evaporated under reduced pressure, removes ethanol, solid fraction object is obtained, then solid fraction object is dried
Powder is ground into, obtains the traditional Chinese medicine ingredients for preparing the toothpaste containing cinnamon oil；
（3）By obtained traditional Chinese medicine ingredients according to proportioning and silica；Precipitated calcium carbonate；Cinnamon oil；Peppermint oil；Moisturizing
Agent；Foaming agent；Thickener；Xylitol；Saccharin；Propolis；Methyl p-hydroxybenzoate is sufficiently mixed, and then adds distilled water, is used
Mixer strong stirring is uniform, is formed with the lotion of certain viscosity；
（4）Obtained lotion is ground twice with grinder, excessively thick, really up to the mark particle is levigate, make
Lotion is fine and smooth, uniformly, stably, and grinding 1~2 hour, then carries out second of grinding again for the first time, grinds for second
1 hour, vacuum outgas is carried out after second of grinding, untill vacuum reaches -0.097Mpa, the vacuum outgas time is about 42
Minute；A period of time is stood after lotion degassing, obtains product.
Embodiment 3
A kind of toothpaste containing cinnamon oil, it is characterised in that include the raw material of following weight percentage：
Cinnamon oil 1.1%；；Precipitated calcium carbonate 26%；Silica 27%；Peppermint oil 0.5%；NMF sorbierite 27%；Hair
Infusion lauroyl sulfoacetic acid sodium 2.1%；Thickener carrageenan 2.3%；Xylitol 0.11%；Saccharin 0.01%；Propolis 0.04%；
Methyl p-hydroxybenzoate 0.12%；Distilled water surplus；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that traditional Chinese medicine ingredients, its weight score are also further added in toothpaste
Number is 8%；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that described traditional Chinese medicine ingredients include the component of following parts by weight：
15 parts of wintercherry fruit or calyx, 13 parts of indigo naturalis, 16 parts of asarum, 8 parts of dandelion, 4 parts of fimbriatestipulate begonia herb, 4 parts of balloonflower root, 7 parts of the root bark of tree peony；
Above-mentioned propolis is the propolis powder for being ground into 100~120 mesh；
The preparation method step of the above-mentioned toothpaste containing cinnamon oil is as follows：
（1）Each component in traditional Chinese medicine ingredients is ground into 50~80 mesh respectively with pulverizer, then taken in parts by weight
The each component crushed is sufficiently mixed uniformly, obtains mixture, and it is 80%~90% ethanol that determining alcohol is added into mixture, second
The addition of alcohol is 2~3 times of volume of mixture, is flowed back 5 hours at 80 DEG C, filters, obtains phegma；
（2）Phegma is evaporated under reduced pressure, removes ethanol, solid fraction object is obtained, then solid fraction object is dried
Powder
Powder is broken into, obtains the traditional Chinese medicine ingredients for preparing the toothpaste containing cinnamon oil；
（3）By obtained traditional Chinese medicine ingredients according to proportioning and silica；Precipitated calcium carbonate；Cinnamon oil；Peppermint oil；NMF
Sorbierite；Foaming agent lauroyl sulfoacetic acid sodium；Thickener carrageenan；Xylitol；Saccharin；Propolis；P-hydroxybenzoic acid first
Ester is sufficiently mixed, and then adds distilled water, uniform with mixer strong stirring, is formed with the lotion of certain viscosity；
（4）Obtained lotion is ground twice with grinder, excessively thick, really up to the mark particle is levigate, make lotion it is fine and smooth,
Uniformly, stably, grind 1~2 hour for the first time, then carry out second of grinding again, second of grinding 1 hour, the
Vacuum outgas is carried out after secondary grinding, untill vacuum reaches -0.097Mpa, the vacuum outgas time is about 43 minutes；Cream
A period of time is stood after body degassing, obtains product.
Embodiment 4
A kind of toothpaste containing cinnamon oil, it is characterised in that include the raw material of following weight percentage：
Cinnamon oil 1.5%；Precipitated calcium carbonate 30%；Silica 30%；Peppermint oil 0.7%；NMF 30%；Foaming agent 2.5%；
Thickener 2.7%；Xylitol 0.15%；Saccharin 0.01%；Propolis 0.05%；Methyl p-hydroxybenzoate 0.15%；Distilled water surplus；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that traditional Chinese medicine ingredients, its weight score are also further added in toothpaste
Number is 10%；
The above-mentioned toothpaste containing cinnamon oil, it is characterised in that described traditional Chinese medicine ingredients include the component of following parts by weight：
17 parts of wintercherry fruit or calyx, 15 parts of indigo naturalis, 18 parts of asarum, 10 parts of dandelion, 5 parts of fimbriatestipulate begonia herb, 5 parts of balloonflower root, 8 parts of the root bark of tree peony；
Above-mentioned propolis is the propolis powder for being ground into 100~120 mesh；
Described NMF is propane diols and sorbierite；Described foaming agent is dioctyl sodium sulphosuccinate or lauroyl
Base sulfoacetic acid sodium；Described thickener is sodium alginate and xanthans；
The preparation method step of the described toothpaste containing cinnamon oil is as follows：
（1）Each component in traditional Chinese medicine ingredients is ground into 50~80 mesh respectively with pulverizer, then taken in parts by weight
The each component crushed is sufficiently mixed uniformly, obtains mixture, and it is 80%~90% ethanol that determining alcohol is added into mixture, second
The addition of alcohol is 2~3 times of volume of mixture, is flowed back 4 hours at 85 DEG C, filters, obtains phegma；
（2）Phegma is evaporated under reduced pressure, removes ethanol, solid fraction object is obtained, then solid fraction object is dried
Powder is ground into, obtains the traditional Chinese medicine ingredients for preparing the toothpaste containing cinnamon oil；
（3）By obtained traditional Chinese medicine ingredients according to proportioning and silica；Precipitated calcium carbonate；Cinnamon oil；Peppermint oil；Moisturizing
Agent；Foaming agent；Thickener；Xylitol；Saccharin；Propolis；Methyl p-hydroxybenzoate is sufficiently mixed, and then adds distilled water, is used
Mixer strong stirring is uniform, is formed with the lotion of certain viscosity.
（4）Obtained lotion is ground twice with grinder, excessively thick, really up to the mark particle is levigate, make lotion it is fine and smooth,
Uniformly, stably, grind 1~2 hour for the first time, then carry out second of grinding again, second of grinding 1 hour, grind for the second time
After carry out vacuum outgas, untill vacuum reaches -0.097Mpa, the vacuum outgas time is about 45 minutes；After lotion degassing
A period of time is stood, obtains product.
Application effect：
Mouth disease is played a part of for the Chinese medicinal toothpaste that further the checking present invention is protected, below through overtesting
Further illustrate the good result of the present invention.It is specific as follows：
Select voluntarily to participate in suffers from canker sore, gingival swelling and pain, alveolar abscess, tooth age inflammation, periodontitis, pulpitis oral cavity
The volunteer of disease, the Chinese medicinal toothpaste obtained by Example 1-4, to be tested, test method is：The daily morning and evening each one
Secondary, dosage is the half of ordinary toothpaste, after 5-7 days, observes result.Clinical statisticses standard is as shown in table l, curative effect clinic number
It is as shown in table 2 according to statistics.
From above-mentioned clinical data, the present invention is for treatment canker sore, gingival swelling and pain, alveolar abscess, tooth age inflammation, tooth
The mouth diseases such as Zhou Yan, pulpitis have the effect of fine.
Claims (1)
1. a kind of toothpaste containing cinnamon oil, it is characterised in that include the raw material of following weight percentage：
Cinnamon oil 0.2%~1.5%；Precipitated calcium carbonate 20%~30%；Silica 20%~30%；Peppermint oil 0.1%~
0.7%；NMF 20%~30%；Foaming agent 1.5%~2.5%；Thickener 1.2%~2.7%；Xylitol 0.03%~
0.15%；Saccharin 0.01%；Propolis 0.02%~0.05%；Methyl p-hydroxybenzoate 0.05%~0.15%；More than distilled water
Amount；
The described toothpaste containing cinnamon oil, also further adds traditional Chinese medicine ingredients, and its weight is 5%~10% than fraction；In described
Medicine composition includes the component of following parts by weight：10~17 parts of wintercherry fruit or calyx, 10~15 parts of indigo naturalis, 12~18 parts of asarum,
6~10 parts of dandelion, 2~5 parts of fimbriatestipulate begonia herb, 3~5 parts of balloonflower root, 5~8 parts of the root bark of tree peony；
Described propolis is the propolis powder for being ground into 100~120 mesh；
Described NMF is the one or more in glycerine, propane diols and sorbierite；Described foaming agent is dioctyl sulfo group
Sodium succinate or lauroyl sulfoacetic acid sodium；Described thickener is in sodium alginate, xanthans, guar gum and carragheen
It is one or more；
The preparation method step of the described toothpaste containing cinnamon oil is as follows：
（1）Each component in traditional Chinese medicine ingredients is ground into 50~80 mesh respectively with pulverizer, then takes powder in parts by weight
Broken each component is sufficiently mixed uniformly, obtains mixture, and it is 80%~90% ethanol that determining alcohol is added into mixture, ethanol
Addition be 2~3 times of volume of mixture, flow back 4~7 hours at 60~85 DEG C, filtering, obtains phegma；
（2）Phegma is evaporated under reduced pressure, removes ethanol, obtains solid fraction object, solid fraction object is dried and then crushed
Into powder, the traditional Chinese medicine ingredients for preparing the toothpaste containing cinnamon oil are obtained；
（3）By obtained traditional Chinese medicine ingredients according to proportioning and silica；Precipitated calcium carbonate；Cinnamon oil；Peppermint oil；NMF；Hair
Infusion；Thickener；Xylitol；Saccharin；Propolis；Methyl p-hydroxybenzoate is sufficiently mixed, and then adds distilled water, uses mixer
Strong stirring is uniform, is formed with the lotion of certain viscosity；
（4）Obtained lotion is ground twice with grinder, for the first time grinding 1~2 hour, then carried out again second
Grinding, second of grinding 1 hour, vacuum outgas is carried out after second of grinding, is until vacuum reaches -0.097Mpa
Only, the vacuum outgas time is 40~45 minutes；A period of time is stood after lotion degassing, obtains product.
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| CN105726443A (en) * | 2016-03-21 | 2016-07-06 | 王跃华 | Fructus crataegi healthcare toothpaste |
| RU2637432C1 (en) * | 2016-11-07 | 2017-12-04 | федеральное государственное бюджетное образовательное учреждение высшего образования "Башкирский государственный медицинский университет" Министерства здравоохранения Российской Федерации | Dental pin for periodontitis treatment |
| TWI730287B (en) * | 2019-01-31 | 2021-06-11 | 楊曉婷 | Preparation method and usage of oral composition |
| TWI730286B (en) * | 2019-01-31 | 2021-06-11 | 楊曉婷 | Preparation method and usage of oral composition |
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|---|---|---|---|---|
| CN101327175A (en) * | 2007-06-21 | 2008-12-24 | 温州医学院 | Zedoary turmeric oil dental health article |
| CN102824286A (en) * | 2012-09-07 | 2012-12-19 | 广州安德生物科技有限公司 | Soft capsule oral care agent and preparation method thereof |
| CN103520578A (en) * | 2013-10-25 | 2014-01-22 | 李佃场 | Traditional Chinese medicine composition for treating oral ulcer and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101327175A (en) * | 2007-06-21 | 2008-12-24 | 温州医学院 | Zedoary turmeric oil dental health article |
| CN102824286A (en) * | 2012-09-07 | 2012-12-19 | 广州安德生物科技有限公司 | Soft capsule oral care agent and preparation method thereof |
| CN103520578A (en) * | 2013-10-25 | 2014-01-22 | 李佃场 | Traditional Chinese medicine composition for treating oral ulcer and preparation method thereof |
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| 《中草药在牙膏中应用的回顾与展望》;徐春生;《口腔护理用品工业》;20120229;1-6页 * |
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Inventor after: Mo Mingxin Inventor before: He Junlin |
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Effective date of registration: 20180115 Address after: Hengxian Heng Zhou Zhen Liu Ming 530300 Nanning Road, the Guangxi Zhuang Autonomous Region No. 80 Applicant after: Mo Mingxin Address before: Hengxian Heng Zhou Zhen Liu Ming 530300 Nanning Road, the Guangxi Zhuang Autonomous Region No. 80 Applicant before: Bi Bingchun |
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Effective date of registration: 20210513 Address after: No. 86, Zhenhua North Road, Shenshan Industrial Park, Jianggao Town, Baiyun District, Guangzhou, Guangdong 510450 Patentee after: GUANGZHOU CHINA HAN ORAL PRODUCTS Co.,Ltd. Address before: 530300 No.80, Liuming Road, Hengzhou Town, Heng County, Nanning City, Guangxi Zhuang Autonomous Region Patentee before: Mo Mingxin |