CN104860587A - Double-layer structure flexible finishing material and preparation method thereof - Google Patents
Double-layer structure flexible finishing material and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a double-layer structure flexible finishing material and a preparation method thereof. The double-layer structure flexible finishing material comprises a substrate layer and a paste interface layer, wherein the substrate layer is formed by rolling, is 1-5 mm in thickness, and comprises the following components in part by weight: 65-80 parts of modified soil, 8-10 parts of flexible agent, 0.05-0.1 part of ultraviolet absorbent, 2-3 parts of flame retardant, 0.1-0.5 part of short fiber, 12-15 parts of water and 0.3-0.5 part of defoamer; the paste interface layer is directly sprayed on the back of the substrate layer by using a spraying method, is 0.3-0.5 mm in thickness, and comprises the following components in part by weight: 25-30 parts of inorganic cementitious material, 8-10 parts of auxiliary cementitious material, 25-60 parts of fine sand, 2-3 parts of flexible agent, 0.5-1 part of inorganic thickener, 0.1-0.2 part of water reducing agent, 0.25-0.3 part of early strength agent, 0.25-0.3 part of alkali inhibitor, 0.2-0.5 part of waterproofing agent, 15-20 parts of water and 0.3-0.5 part of defoamer; the substrate layer and the paste interface layer are dried at 50-70 DEG C to obtain the double-layer structure flexible finishing material. The double-layer structure flexible finishing material prepared by using the method disclosed by the invention can be pasted directly by using the inorganic cementitious material, and has the advantages of high wall bonding strength, low comprehensive cost, convenient construction and the like.
Description
Technical field
The present invention relates to a kind of architecture inside and outside decoration material and preparation method thereof, particularly flexible finishing material of a kind of bilayer structure and preparation method thereof.
Background technology
Flexible finishing material is main raw material by modified inorganic filler, and high molecular polymer is auxiliary agent, uses that special temperature control moulding system is shaping, baking, a kind of of cross-linking radiation have flexible building decoration plane materiel.The power consumption of its manufacturing processed is low, and raw material, based on various waste (urban construction rubbish, industrial solid castoff, mud, mud etc.), is a kind of New Building Materials of environmental protection.The building decoration sheet material of the effects such as various brick, timber, stone material, leather, pottery, embossment can be showed.Compared with ceramic tile, stone material, it has the features such as light, thin, soft, ventilative, expressive force strong, prevent fires, construct simply, decorative effect is good with traditional finishing material, and thoroughly solve ceramic tile, the stone material potential safety hazard in Highrise buildings, greatly reduce construction cost and construction period simultaneously.
The flexible finishing material circulated in the market and body of wall are pasted and be there is technical bottleneck, mainly flexible finishing material itself is containing certain organic high molecular polymer, if directly paste with inorganic coagulation material such as cement system phenomenons such as easily occurring alice, come off.If a kind of flexible finishing material being applicable to pure inorganic coagulation material and directly pasting can be developed, not only greatly can reduce construction cost, and significantly can also improve the cohesive strength of flexible finishing material and metope, the security of General Promotion material.At present, there is no the relevant report being directly applied for the flexible finishing material that pure inorganic coagulation material is pasted both at home and abroad.
Summary of the invention
For above-mentioned already present problem, the invention discloses flexible finishing material of a kind of bilayer structure and preparation method thereof, the flexible finishing material utilizing the method to obtain can with inorganic coagulation material as cement system be directly pasted.
The flexible finishing material of described a kind of bilayer structure is made up of base layer and adhesion interface layer, wherein base layer passes through roll forming, thickness is 1 ~ 5 millimeter, comprise: with mass parts number scale, Modified soil 65 ~ 80 parts, soft agent 8 ~ 10 parts, uv-absorbing agent 0.05 ~ 0.1 part, fire retardant 2 ~ 3 parts, 0.1 ~ 0.5 part, staple fibre, 12 ~ 15 parts, water, defoamer 0.3 ~ 0.5 part; Adhesion interface layer adopts the mode of spraying to coat base layer, thickness is 0.3 ~ 0.5 millimeter, comprise: with mass parts number scale, inorganic coagulation material 25 ~ 30 parts, supplementary cementitious material 8 ~ 10 parts, fine sand 25 ~ 60 parts, soft agent 2 ~ 3 parts, inorganic thickening agent 0.5 ~ 1 part, water reducer 0.1 ~ 0.2 part, hardening accelerator 0.25 ~ 0.3 part, press down alkaline agent 0.25 ~ 0.3 part, water-resisting agent 0.2 ~ 0.5 part, 15 ~ 20 parts, water, defoamer 0.3 ~ 0.5 part.
Preparation method's concrete steps of the flexible finishing material of described a kind of bilayer structure are as follows.
Step 1: with mass parts number scale, the soft agent of 8 ~ 10 parts is added in the water of 12 ~ 15 parts, Modified soil 65 ~ 80 parts, uv-absorbing agent 0.1 ~ 0.2 part, fire retardant 2 ~ 3 parts, 0.1 ~ 0.5 part, staple fibre, defoamer 0.3 ~ 0.5 part is added sequentially respectively after abundant dispersed with stirring is even, admixtion 1 is obtained after stirring, for subsequent use.
Step 2: by admixtion 1 compression moulding in roller head machine obtained in step 1, obtained thickness is the flexible finishing material base layer idiosome of 1 ~ 5 millimeter, obtains flexible finishing material base layer after 50 ~ 70 degrees Celsius of lower drying and dewaterings.
Step 3: with mass parts number scale, the soft agent of 2 ~ 3 parts is joined in the water of 15 ~ 20 parts, add inorganic coagulation material 25 ~ 30 parts, supplementary cementitious material 8 ~ 10 parts, inorganic thickening agent 0.5 ~ 1 part, water reducer 0.05 ~ 0.1 part, hardening accelerator 0.25 ~ 0.3 part after abundant dispersed with stirring is even sequentially respectively, press down alkaline agent 0.25 ~ 0.3 part, water-resisting agent 0.2 ~ 0.5 part, defoamer 0.3 ~ 0.5 part, fine sand 25 ~ 60 parts is added while stirring after being uniformly dispersed, admixtion 2 is obtained after stirring, for subsequent use.
Step 4: join in spraying machine by admixtion 2 obtained in step 3, the base layer back side that spraying is obtained in step 2, coating thickness is 0.3 ~ 0.5 millimeter, forms adhesion interface layer.
Step 5: material obtained in step 4 is dried under 50 ~ 70 degrees Celsius, the i.e. flexible finishing material of obtained bilayer structure.
Further, described Modified soil is by silane coupler modified clay, flyash, silicon dirt and at least one in the building waste of fragmentation.
Further, described soft agent is one or more mixing in acrylate and vinyl acetate emulsion, benzene emulsion, pure-acrylic emulsion, organosilicon crylic acid latex.
Further, described staple fibre is polypropylene fibre or the glass fibre of 3 ~ 6 millimeters.
Further, described inorganic coagulation material be hydraulic cementing materials as silicate cement, aluminate cement, aluminosulfate cement etc., air hardening cementitious materials as lime, gypsum, water glass etc. and in alkali-activated carbonatite gelling material any one or a few mixing.
Further, described supplementary cementitious material is at least one in flyash, slag, gypsum.
Further, described fine sand is natural or machine-processed siliceous, the calcareous or magnesia fine sands of 40 ~ 120 objects.
Further, described inorganic thickening agent is at least one in natural clay, wilkinite, Attapulgite, polynite.
Further, described hardening accelerator is any one in villaumite, organic amine, complex accelerator.
Further, described water reducer is at least one in high performance water reducing agent of polyocarboxy acid, Ppolynuclear aromatic sulfonate, sulfonated lignin.
Further, described water-resisting agent is silicone based water-resisting agent.
Further, described fire retardant is at least one in aluminium hydroxide, magnesium hydroxide, weisspiessglanz, red phosphorus.
Further, described uv-absorbing agent is BP-4 or benzotriazole category uv-absorbing agent.
Further, the described alkaline agent that presses down is the mixture containing unsetting highly reactive form of oxygen SiClx and high sorbent material.
Further, described defoamer is water insoluble defoamer.
The invention has the beneficial effects as follows: 1, mold temperature of the present invention only have 50 ~ 70 degrees Celsius shaping, greatly saved the energy consumption in moulding process, meet country advocate green production; 2, the flexible finishing material that the present invention obtains can adopt common inorganic coagulation material such as cement system to complete secure bond, its technique is simple, with low cost, the flexible finishing material adhesive special that producer need not be adopted to provide is bonding, can effectively prevent layman from occurring the flexible finishing material adhesive special not adopting cost higher coming off, the phenomenon such as rake angle.
Embodiment
For describing the present invention in detail, below in conjunction with specific embodiment, the present invention will be further described.
Embodiment 1.
Step 1: with mass parts number scale, the pure-acrylic emulsion of 8.5 parts is added in the water of 14 parts, modified coal ash 75 parts, BP-4 0.1 part, 2 parts, aluminium hydroxide, 3 millimeters long polypropene staple 0.1 part, defoamer 0.3 part is added sequentially respectively after abundant dispersed with stirring is even, admixtion 1 is obtained after stirring, for subsequent use.
Step 2: by admixtion 1 compression moulding in roller head machine obtained in step 1, obtained thickness is the flexible finishing material base layer idiosome of 1.5 millimeters, obtains flexible finishing material base layer at 50 c after drying and dewatering.
Step 3: with mass parts number scale, the pure-acrylic emulsion of 2 parts is joined in the water of 15 parts, add silicate cement 25 parts, 10 parts, flyash, wilkinite 0.5 part, water reducer 0.05 part, calcium formiate 0.3 part after abundant dispersed with stirring is even sequentially respectively, press down alkaline agent 0.3 part, water-resisting agent 0.4 part, defoamer 0.45 part, 80 ~ 120 order natural quartz fine sand 46 parts is added while stirring after being uniformly dispersed, admixtion 2 is obtained after stirring, for subsequent use.
Step 4: join in spraying machine by admixtion 2 obtained in step 3, the base layer back side that spraying is obtained in step 2, coating thickness is 0.3 millimeter, forms adhesion interface layer.
Step 5: material obtained in step 4 is dried under 55 degrees Celsius, the i.e. flexible finishing material of obtained bilayer structure.
Embodiment 2.
Step 1: with mass parts number scale, the organosilicon crylic acid latex of 9 parts is added in the water of 15 parts, abundant dispersed with stirring evenly after add modified silicon ashes 72 parts, BP-4 0.2 part, magnesium hydroxide 3 parts, 5 millimeters of polypropene staples 0.4 part, defoamer 0.4 part sequentially respectively, admixtion 1 is obtained after stirring, for subsequent use.
Step 2: by admixtion 1 compression moulding in roller head machine obtained in step 1, obtained thickness is the flexible finishing material base layer idiosome of 2.5 millimeters, obtains flexible finishing material base layer after 55 degrees Celsius of lower drying and dewaterings.
Step 3: with mass parts number scale, the benzene emulsion of 3 parts is joined in the water of 18 parts, add 27 parts, lime, wollastonite powder 8 parts, wilkinite 0.8 part, water reducer 0.1 part, compound hardening accelerator 0.25 part after abundant dispersed with stirring is even sequentially respectively, press down alkaline agent 0.25 part, water-resisting agent 0.2 part, defoamer 0.4 part, 60 ~ 100 order mechanism Wingdale fine sand 42 parts is added while stirring after being uniformly dispersed, admixtion 2 is obtained after stirring, for subsequent use.
Step 4: join in spraying machine by admixtion 2 obtained in step 3, the base layer back side that spraying is obtained in step 2, coating thickness is 0.4 millimeter, forms adhesion interface layer.
Step 5: material obtained in step 4 is dried at 60 c, the i.e. flexible finishing material of obtained bilayer structure.
Embodiment 3.
Step 1: with mass parts number scale, the benzene emulsion of 10 parts is added in the water of 12 parts, abundant dispersed with stirring evenly after add modified coal ash 75 parts, BP-4 0.2 part, 2 parts, aluminium hydroxide, 0.3 part, 4 millimeters of glass fibre, defoamer 0.5 part sequentially respectively, admixtion 1 is obtained after stirring, for subsequent use.
Step 2: by admixtion 1 compression moulding in roller head machine obtained in step 1, obtained thickness is the flexible finishing material base layer idiosome of 5 millimeters, obtains flexible finishing material base layer at 60 c after drying and dewatering.
Step 3: with mass parts number scale, the pure-acrylic emulsion of 2.5 is joined in the water of 20 parts, add alkali-activated carbonatite gelling material 30 parts, 9 parts, flyash, polynite 0.8 part, water reducer 0.1 part, organic ammonium 0.3 part after abundant dispersed with stirring is even sequentially respectively, press down alkaline agent 0.3 part, water-resisting agent 0.5 part, defoamer 0.5 part, 40 ~ 80 order mechanism rhombspar fine sand 36 parts is added while stirring after being uniformly dispersed, admixtion 2 is obtained after stirring, for subsequent use.
Step 4: join in spraying machine by admixtion 2 obtained in step 3, the base layer back side that spraying is obtained in step 2, coating thickness is 0.5 millimeter, forms adhesion interface layer.
Step 5: material obtained in step 4 is dried under 65 degrees Celsius, the i.e. flexible finishing material of obtained bilayer structure.
Above embodiment is only good embodiment of the present invention, but and is not used to retrain the present invention, but in order to easy understand implementation of the present invention.The technician of any building material field, is not departing under disclosed spiritual prerequisite, and the equivalent variations made part details, replacement, all within the scope of protection of the invention.
Claims (12)
1. flexible finishing material of bilayer structure and preparation method thereof, it comprises the steps:
Step 1: with mass parts number scale, the soft agent of 8 ~ 10 parts is added in the water of 12 ~ 15 parts, Modified soil 65 ~ 80 parts, uv-absorbing agent 0.1 ~ 0.2 part, fire retardant 2 ~ 3 parts, 0.1 ~ 0.5 part, staple fibre, defoamer 0.3 ~ 0.5 part is added sequentially respectively after abundant dispersed with stirring is even, admixtion 1 is obtained after stirring, for subsequent use;
Step 2: by admixtion 1 compression moulding in roller head machine obtained in step 1, obtained thickness is the flexible finishing material base layer idiosome of 1 ~ 5 millimeter, obtains flexible finishing material base layer after 50 ~ 70 degrees Celsius of lower drying and dewaterings;
Step 3: with mass parts number scale, the soft agent of 2 ~ 3 parts is joined in the water of 15 ~ 20 parts, add inorganic coagulation material 25 ~ 30 parts, supplementary cementitious material 8 ~ 10 parts, inorganic thickening agent 0.5 ~ 1 part, water reducer 0.05 ~ 0.1 part, hardening accelerator 0.25 ~ 0.3 part after abundant dispersed with stirring is even sequentially respectively, press down alkaline agent 0.25 ~ 0.3 part, water-resisting agent 0.2 ~ 0.5 part, defoamer 0.3 ~ 0.5 part, fine sand 25 ~ 60 parts is added while stirring after being uniformly dispersed, admixtion 2 is obtained after stirring, for subsequent use;
Step 4: admixtion 2 obtained in step 3 is joined in spraying machine, the base layer back side that spraying is obtained in step 2, coating thickness is 0.3 ~ 0.5 millimeter, forms adhesion interface layer;
Step 5: material obtained in step 4 is dried under 50 ~ 70 degrees Celsius, the i.e. flexible finishing material of obtained bilayer structure;
Described Modified soil is by silane coupler modified clay, flyash, silicon dirt and at least one in the building waste of fragmentation;
Described soft agent is one or more mixing in acrylate and vinyl acetate emulsion, benzene emulsion, pure-acrylic emulsion, organosilicon crylic acid latex;
Described inorganic thickening agent is at least one in natural clay, wilkinite, Attapulgite, polynite.
2. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described staple fibre is polypropylene fibre or the glass fibre of 3 ~ 6 millimeters.
3. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, it is characterized in that: described inorganic coagulation material be hydraulic cementing materials as silicate cement, aluminate cement, aluminosulfate cement etc., air hardening cementitious materials as lime, gypsum, water glass etc. and in alkali-activated carbonatite gelling material any one or a few mixing.
4. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described supplementary cementitious material is at least one in flyash, slag, gypsum.
5. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described fine sand is natural or machine-processed siliceous, the calcareous or magnesia fine sands of 40 ~ 120 objects.
6. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described hardening accelerator is any one in villaumite, organic amine, complex accelerator.
7. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described water reducer is at least one in high performance water reducing agent of polyocarboxy acid, Ppolynuclear aromatic sulfonate, sulfonated lignin.
8. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described water-resisting agent is silicone based water-resisting agent.
9. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described fire retardant is at least one in aluminium hydroxide, magnesium hydroxide, weisspiessglanz, red phosphorus.
10. flexible finishing material of a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described uv-absorbing agent is BP-4 or benzotriazole category uv-absorbing agent.
Flexible finishing material of 11. a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: the described alkaline agent that presses down is the mixture containing unsetting highly reactive form of oxygen SiClx and high sorbent material.
Flexible finishing material of 12. a kind of bilayer structure according to claim 1 and preparation method thereof, is characterized in that: described defoamer is water insoluble defoamer.
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| CN106084600A (en) * | 2016-06-23 | 2016-11-09 | 合肥奇腾农业科技有限公司 | A kind of light sound-proof environment-protection ground panel material and preparation method thereof |
| CN108609963A (en) * | 2018-06-15 | 2018-10-02 | 海安南京大学高新技术研究院 | Build porcelain tendre material and preparation method thereof |
| CN109336428A (en) * | 2018-10-26 | 2019-02-15 | 安徽理工大学 | Layered fabric type cement and the double gelling system material preparation methods of MSWI bottom ash alkali-activated carbonatite |
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