CN104150853B - A kind of environmental protection composite fire-proof body of wall material and preparation method thereof - Google Patents

A kind of environmental protection composite fire-proof body of wall material and preparation method thereof Download PDF

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Publication number
CN104150853B
CN104150853B CN201410367281.4A CN201410367281A CN104150853B CN 104150853 B CN104150853 B CN 104150853B CN 201410367281 A CN201410367281 A CN 201410367281A CN 104150853 B CN104150853 B CN 104150853B
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China
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parts
proof
environmental protection
protection composite
fire
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CN201410367281.4A
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Chinese (zh)
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CN104150853A (en
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胡刚
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泗阳县弘达新型墙体材料有限公司
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Publication of CN104150853A publication Critical patent/CN104150853A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

Abstract

The invention discloses a kind of environmental protection composite fire-proof body of wall material and preparation method thereof, environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 35-60 part, phosphogypsum 25-45 part, flyash 15-35 part, clay 12-25 part, resin 10-30 part, fire retardant 5-25 part, coupling agent 2-15 part, thermo-stabilizer 1-10 part, softening agent 2-15 part, waste glass powder 5-25 part, rock wool waste material 2-15 part, useless ceramic tile powder 2-15 part, water 35-55 part.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, then itself and cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder, water are made environmental protection composite fire-proof body of wall material through being uniformly mixed.

Description

A kind of environmental protection composite fire-proof body of wall material and preparation method thereof
Technical field
The present invention relates to materials for wall, particularly relate to a kind of environmental protection composite fire-proof body of wall material and preparation method thereof.
Background technology
Novel wall material is energy saving building, the important support of green building and basis.The object of materials for wall innovation not only will reduce with soil, forbid that breaking-up is ploughed, make full use of various local resources and waste is turned waste into wealth, also have important goal will realize exactly economizing on resources, save energy, saving material, limited resources by advanced technology and rational distributing style, be that materials for wall becomes the building consolidated structures with multi-functional unification and high-effect utilization.
In recent years, along with the deep development of energy-saving and emission-reduction particularly building energy conservation, novel wall material development is very fast, wherein insulation and structure-integrated technology have also been obtained wide popularization and application, but really meet modernization of architecture, industrialization and the high quality of architectural structure system needs, multi-functional, energy-conservation, green materials for wall still slower development.The product proportion such as various light composite wallboards, self-thermal insulation material particularly representing materials for wall developing direction is also lower.Therefore, the future development of materials for wall industry must meet higher levels of challenge: the development of novel wall material must adhere to high-strength light, product high-quality, ensure construction industry progress and project of vital and lasting importance, the criterion that quality first; The requirement of process of producing product, architectural process and the comprehensive energy-conserving and environment-protective of buildings use procedure must be met; The requirement of process of producing product, architectural process and the comprehensive energy-conserving and environment-protective of buildings use procedure must be met; The requirement of modern architecture to multi-functional unifications such as materials for wall sound insulation, insulation, fire prevention, waterproof, antidetonation, decoration and self-heat conservings must be met; Must adapt with building industrialization, housing industrialization and building system, with architectural design and construction application consistent, embody market orientation, consumer uppermost requirement.Here it is materials for wall industry transition and upgrade facing challenges.
Summary of the invention
the technical problem solved:
The present invention, in order to realize materials for wall environmental protection, fp high request, provides a kind of environmental protection composite fire-proof body of wall material and preparation method thereof.
technical scheme:
The invention discloses a kind of environmental protection composite fire-proof body of wall material, environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 35-60 part, phosphogypsum 25-45 part, flyash 15-35 part, clay 12-25 part, resin 10-30 part, fire retardant 5-25 part, coupling agent 2-15 part, thermo-stabilizer 1-10 part, softening agent 2-15 part, waste glass powder 5-25 part, rock wool waste material 2-15 part, useless ceramic tile powder 2-15 part, water 35-55 part.
As preferably, the resin that the present invention adopts is thermoplastic resin.
A kind of preparation method of environmental protection composite fire-proof body of wall material, being that resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture, then itself and cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder, water being made environmental protection composite fire-proof body of wall material through being uniformly mixed.
As a preferred technical solution of the present invention, resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed granular mixture by the present invention, and the particle diameter of each particle is at 150-280 micron.
As a preferred technical solution of the present invention, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder are pulverized by the present invention, spray waterside, limit is stirred, and rotating speed is 650-1100 rev/min, and the time is 45-90 minute.
As a preferred technical solution of the present invention, in the present invention, all materials mix rear standing 2.5-4.5 hour, and through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 184.5-212.5 DEG C, pressure range controls at 8-19atm, and the time is 4-9 hour.
beneficial effect
Compared to the prior art a kind of environmental protection composite fire-proof body of wall material of the present invention and preparation method thereof adopts above technical scheme, and have following technique effect: oxygen index reaches 56-87%, fire resistance is strong.
Embodiment
Embodiment 1:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 35 parts, phosphogypsum 25 parts, 15 parts, flyash, clay 12 parts, resin 10 parts, fire retardant 5 parts, coupling agent 2 parts, thermo-stabilizer 1 part, 2 parts, softening agent, waste glass powder 5 parts, 2 parts, rock wool waste material, useless ceramic tile powder 2 parts, 35 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 150 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 650 revs/min, and the time is 90 minutes; Leave standstill 2.5 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 184.5 DEG C, and pressure range controls at 8atm, and the time is 9 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 56% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 2:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 40 parts, phosphogypsum 30 parts, 20 parts, flyash, clay 15 parts, resin 12 parts, fire retardant 8 parts, coupling agent 5 parts, thermo-stabilizer 2 parts, 5 parts, softening agent, waste glass powder 10 parts, 5 parts, rock wool waste material, useless ceramic tile powder 5 parts, 40 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 180 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 700 revs/min, and the time is 85 minutes; Leave standstill 3 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 186.5 DEG C, and pressure range controls at 10atm, and the time is 8.5 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 65% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 3:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 45 parts, phosphogypsum 35 parts, 20 parts, flyash, clay 18 parts, resin 15 parts, fire retardant 10 parts, coupling agent 8 parts, thermo-stabilizer 4 parts, 8 parts, softening agent, waste glass powder 13 parts, 8 parts, rock wool waste material, useless ceramic tile powder 7 parts, 45 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 190 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 750 revs/min, and the time is 80 minutes; Leave standstill 3 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 191.5 DEG C, and pressure range controls at 11atm, and the time is 7.5 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 72% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 4:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 50 parts, phosphogypsum 35 parts, 25 parts, flyash, clay 20 parts, resin 20 parts, fire retardant 14 parts, coupling agent 10 parts, thermo-stabilizer 6 parts, 10 parts, softening agent, waste glass powder 15 parts, 11 parts, rock wool waste material, useless ceramic tile powder 9 parts, 50 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 200 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 800 revs/min, and the time is 80 minutes; Leave standstill 3.5 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 193.5 DEG C, and pressure range controls at 13atm, and the time is 7.5 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 77% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 5:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 50 parts, phosphogypsum 35 parts, 30 parts, flyash, clay 20 parts, resin 20 parts, fire retardant 18 parts, coupling agent 12 parts, thermo-stabilizer 6 parts, 12 parts, softening agent, waste glass powder 17 parts, 12 parts, rock wool waste material, useless ceramic tile powder 11 parts, 50 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 220 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 900 revs/min, and the time is 80 minutes; Leave standstill 3.5 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 195.5 DEG C, and pressure range controls at 13atm, and the time is 7.5 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 81% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 6:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 55 parts, phosphogypsum 40 parts, 30 parts, flyash, clay 20 parts, resin 25 parts, fire retardant 20 parts, coupling agent 12 parts, thermo-stabilizer 6 parts, 12 parts, softening agent, waste glass powder 17 parts, 12 parts, rock wool waste material, useless ceramic tile powder 11 parts, 50 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 240 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 950 revs/min, and the time is 85 minutes; Leave standstill 4 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 198.5 DEG C, and pressure range controls at 15atm, and the time is 8 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 83% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 7:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 55 parts, phosphogypsum 45 parts, 30 parts, flyash, clay 25 parts, resin 27 parts, fire retardant 22 parts, coupling agent 12 parts, thermo-stabilizer 8 parts, 12 parts, softening agent, waste glass powder 20 parts, 12 parts, rock wool waste material, useless ceramic tile powder 11 parts, 50 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 260 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 1050 revs/min, and the time is 90 minutes; Leave standstill 4 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 205.5 DEG C, and pressure range controls at 17atm, and the time is 8 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 87% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.
Embodiment 8:
Environmental protection composite fire-proof body of wall material is made by following raw material weight number proportioning: cement 60 parts, phosphogypsum 45 parts, 35 parts, flyash, clay 25 parts, resin 30 parts, fire retardant 25 parts, coupling agent 15 parts, thermo-stabilizer 10 parts, 15 parts, softening agent, waste glass powder 25 parts, 15 parts, rock wool waste material, useless ceramic tile powder 15 parts, 55 parts, water.Resin, fire retardant, coupling agent, thermo-stabilizer, softening agent heating and melting are formed mixture by preparation method, and the particle diameter of each particle is at 280 microns; Then, after cement, phosphogypsum, flyash, clay, waste glass powder, rock wool waste material, useless ceramic tile powder being pulverized, spray waterside, limit is stirred, and rotating speed is 1100 revs/min, and the time is 90 minutes; Leave standstill 4.5 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 212.5 DEG C, and pressure range controls at 19atm, and the time is 9 hours, namely can be made into environmental protection composite fire-proof body of wall material.
According to reaching 87% by the obtained materials for wall oxygen index of technique means, fire resistance is strong.

Claims (1)

1. an environmental protection composite fire-proof body of wall material, is characterized in that, obtained by following methods: resin 30 parts, fire retardant 25 parts, coupling agent 15 parts, thermo-stabilizer 10 parts, softening agent 15 parts of heating and meltings are formed mixture, and the particle diameter of each particle is at 280 microns; Then, after cement 60 parts, phosphogypsum 45 parts, 35 parts, flyash, clay 25 parts, waste glass powder 25 parts, 15 parts, rock wool waste material, useless ceramic tile powder 15 parts being pulverized, spray waterside, limit is stirred, and rotating speed is 1100 revs/min, and the time is 90 minutes; Leave standstill 4.5 hours after mixing above-mentioned material, through steam press maintenance process, in steam press maintenance process, vapor temperature scope control is at 212.5 DEG C, and pressure range controls at 19atm, and the time is 9 hours, namely can be made into environmental protection composite fire-proof body of wall material.
CN201410367281.4A 2014-07-30 2014-07-30 A kind of environmental protection composite fire-proof body of wall material and preparation method thereof CN104150853B (en)

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CN105175958A (en) * 2015-07-15 2015-12-23 常州市武进金阳光电子有限公司 Non-asbestos-fiber oil-resistant and high-temperature-resistant calcium silicate plate and preparation method thereof
CN104962007A (en) * 2015-07-15 2015-10-07 常州市武进金阳光电子有限公司 Ultraviolet-resistant waste glass powder polyethylene external wall panel and production method thereof
CN105016712A (en) * 2015-07-16 2015-11-04 常州市武进凯利达电子有限公司 Waste brick residue sintered brick and preparation method thereof
CN105060767A (en) * 2015-07-16 2015-11-18 常州市武进凯利达电子有限公司 Outer ultraviolet-resistant polyethylene wallboard prepared from waste brick dregs and production method of wallboard
CN105060766A (en) * 2015-07-29 2015-11-18 苏州科淼新材料有限公司 Novel heat-insulation sound-insulation building material and preparation method thereof
CN107032697A (en) * 2017-03-30 2017-08-11 合肥金同维低温科技有限公司 A kind of fire-retardant heat-insulation material and preparation method thereof
CN108996957A (en) * 2018-08-27 2018-12-14 南京奥新可工程科技有限公司 A kind of impervious building mortar of cracking resistance and its preparation method and application

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CN102746591B (en) * 2011-04-22 2016-08-17 北京恒通创新赛木科技股份有限公司 A kind of materials for wall compositions and preparation method thereof
CN103664222A (en) * 2012-09-11 2014-03-26 西安润丰电子科技有限责任公司 Energy-saving environment-friendly building wall material
CN103011747B (en) * 2012-12-28 2014-06-11 怀方林 Poly-silicon biomass phenolic aldehyde foaming heat-preservation fireproof material and manufacturing method thereof

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