CN102942349B - Manufacturing method of inorganic dolomite magnesia fireproof gel material - Google Patents
Manufacturing method of inorganic dolomite magnesia fireproof gel material Download PDFInfo
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- CN102942349B CN102942349B CN201210459606.2A CN201210459606A CN102942349B CN 102942349 B CN102942349 B CN 102942349B CN 201210459606 A CN201210459606 A CN 201210459606A CN 102942349 B CN102942349 B CN 102942349B
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Abstract
The invention relates to a manufacturing method of an inorganic dolomite magnesia fireproof gel material, which comprises the following step that 100 to 200 parts by weight of dolomite powder, 20 to 100 parts by weight of dilute sulphuric acid, 25 to 56 parts by weight of light calcined magnesia, 10 to 15 parts by weight of magnesium sulfate, 1 to 3 parts by weight of auxiliary additives waterproofing agent, 0.2 to 18 parts by weight of water-based foaming agent, 2 to 3 parts by weight of catalyst, 0.15 parts by weight of inhibitor, 20 to 100 parts by weight of lightweight filler plant fiber powder, 6 to 24 parts by weight of perlite, 3 to 12 parts by weight of polystyrene granule, 10 to 45 parts by weight of clean water and 15 to 65 parts by weight of equipment washing water slurry are prepared in accordance with manufacturing procedures. The invention aims to provide the novel inorganic dolomite magnesia fireproof gel material which has the advantages of high strength, no chloride ion, A-level fire protection, water resistance, high frost resistance, energy saving, heat preservation, excellent comprehensive performance and low cost.
Description
Technical field
The invention belongs to relevant fire proof construction decoration material field class, particularly a kind of making method of inorganic dolomite magnesia fireproof gel material.
Background technology
Also magnesium cement or Sorel cement is claimed, since Sorel invention in 1867, the history of existing more than 100 year. it has many performances to be better than portland cement: do not need wet curing, and fire resistance is good, and thermal conductivity is little, and wear resistance is good, and early strength is high, oil resistant, anti-organic solvent, the performance that anti-ordinary salt and sulfide corrode is also fairly good. and therefore, in the world, some countries are successfully applied to light roof, light fire-proof body of wall, cell floor, upholstery, a lot of aspect such as racecourse and tennis court. China, from the SO age, just starts the exploitation of goods, research work, have developed packaging boxboard in succession, top ceiling, partition plate, wood wool board, ventilator trunk, pantile, bathtub, grinding tool, furniture, agricultural dish canopy, grape trellis, cattle and sheep hutch, a lot of goods such as lightweight wall block. but the main source giobertite of the major ingredient MgO of this cement is mainly distributed in Liaoning Province's (accounting for 85%) in China, Shandong Province's (accounting for 10%) and Hebei one with. owing to transporting the difficulty caused, very big inconvenience is brought to its application. and extremely abundant in China as the dolomite resources in one of tago source, the place of production spreads all over each province. at present, the main raw material of national major part all using rhombspar as production active MgO that much magnesite is few, magnesium oxysulfide concrete is fired to rhombspar and has done systematic research, be that preparation of raw material has become the magnesium oxysulfide concrete of excellent property with caustic dolomite, almost also a blank in China. therefore develop dolomite resources, will very high economic benefit and social benefit be had.
At present, China's materials for wall industry is also very backward, in product, about 90% is solid clay brick, about 7,000 hundred million pieces every year, bakes bricks every year and ruins about 100,000 mu, field, a large amount of breaking-up farmland, have a strong impact on agriculture development, therefore, accelerate the paces of materials for wall reform and Building Energy-saving Work, very urgent, country is greatly developing insulation, the novel wall material that heat insulation, fire-proof light is high-strength and operating efficiency is high.
The building block of light dolomite light internal wall, that rhombspar is calcined under rational temperature and time, with the ground dolomite after calcining for main raw material(s), be equipped with blender, and various admixture, material modified, through foaming agent foam, make light fire-proof material, there is investment little, with low cost, the advantages such as high-strength light and wide market.
Summary of the invention
In order to overcome the above-mentioned shortcoming of prior art, a kind of novel high-strength of the present invention, to reach the making method of A level, water-fast, high frost resistance, dolomite magnesia fireproof gel material that energy-saving heat preserving excellent combination property cost is low without chlorion, fire prevention.
The technical solution adopted for the present invention to solve the technical problems is: a kind of making method of inorganic dolomite magnesia fireproof gel material, wherein: by ground dolomite 100-200 weight part, dilute sulphuric acid 20-100 weight part, light calcined magnesia 25-56 weight part, magnesium sulfate 10-15 weight part, supplementary additive water-resisting agent 1-3 weight part, aqueous foaming agent 0.2-18 weight part, catalyzer 2-3 weight part, inhibitor 0.15 weight part, light filler plant fiber powder 20-100 weight part, perlite 6-24 weight part, granules of polystyrene 3-12 weight part and clear water 10-45 weight part, equipment washing aqueous slurry 15-65 weight part forms through manufacturing procedure.
As a further improvement on the present invention: described ground dolomite for being ground to 300-400 order rhombspar magnesium powder, preferably containing calcium carbonate quantity higher than 30% oxidation magnesium amount higher than 20% rhombspar magnesium slag; Light calcined magnesia is active quantities is that 58-65 calcines powder, auxiliary solidification in earlier stage; It is 18% low concentrated acid that sulfuric acid dilutes content for industry; Magnesium sulfate is industrial magnesium sulfate monohydrate or magnesium sulfate heptahydrate, auxiliary solidification in earlier stage; But the broken powder of vegetable fibre sawdust, powdered rice hulls or other plant; Granules of polystyrene is 3-6# particle; Water-resisting agent is silicon class water-proofing powder or poly-methyl silicon class I liquid I water-resisting agent; Aqueous foaming agent is water-based nonionic class composite fluid whipping agent; Catalyzer is orthophosphoric acid salt system, preferred acidic aluminium dihydrogen phosphate powder or liquid type, for accelerating system reactivity; Inhibitor is acid fog inhibitor, prevents diluted acid in the generation of use procedure and initial reaction stage acid mist, is beneficial to environmental protection.; Equipment washing aqueous slurry is by being stayed sulfur acid calcium and magnesia slurry washing lotion with cleaning equipment in this gel product production process, and recycling is without discharge, and energy-conserving and environment-protective are pollution-free.
As a further improvement on the present invention: described manufacturing procedure step adds ground dolomite for being joined by catalyzer in stirred vessel after in 18% dilute sulphuric acid, stirring question response bubble stops after vulcanization acid magnesium to stir, then add light calcined magnesia and stir 1-2 minute, with appropriate equipment washing aqueous slurry and part clear water adjusting viscosity, last foundation production product type adds different light filler, and add whipping agent or through sending out foam that machine is suppressed and stirring blanking after 2 minutes, with Dual-layer or multilayer glass-fiber-fabric and the face roll forming of nonwoven interlining end liner on fire-proof board molding device, about insulation 25-30 degree, the aftershaping demoulding in 18-48 hour.
Compared with prior art, the invention has the beneficial effects as follows: be beneficial to natural ground dolomite in conjunction with light-burning magnesium powder be generated as intensity high, to reach A level, high frost resistance, water-fast, energy-saving heat preserving excellent combination property and the low dolomite magnesia fireproof gel material of cost without chlorion, fire prevention, utilize this gel material by the various building materials product of technological forming, and the recycle of all manufacture course of products rinse water, zero release, energy-conserving and environment-protective.
Embodiment
Application principle of the present invention is as follows:
React under calcium carbonate in ground dolomite and magnesium oxide and sulfuric acid and catalyst action, generate calcium sulfate and fluid sulphuric acid magnesium, after fluid sulphuric acid magnesium and additional sulfuric acid magnesium combine, air-setting magnesium oxysulfide concrete is generated with light-burning magnesium powder reaction, magnesium oxysulfide concrete and calcium sulfate are combined into the fire prevention jello of high strength, and additional sulfuric acid magnesium and light-burning magnesium powder play Curing effect in early stage.According to desired product type, by this jello and the different matched combined of material such as light filler, water-resisting agent and whipping agent, by the dissimilar fire proof construction building material product of technological forming.
Below in conjunction with embodiment, the present invention is further described.
Specific embodiments, but example data does not do the present invention's constraint and restriction, and all data are weight part unit.
embodiment one: building decorative plates concrete steps are as follows:
1, inorganic gel material:
300 order dolomite powders 150;
18% dilute sulphuric acid 32;
Light calcined magnesia 50;
Magnesium sulfate 26;
2, supplementary additive
Water-resisting agent 2.2;
Aqueous foaming agent 0.4;
Catalyzer 2.5;
Inhibitor 0.15;
3, light filler:
Plant fiber powder 65;
Perlite 12;
4, other
Clear water 15;
Equipment washing aqueous slurry 25;
5, sheet for architectural decoration flow process is manufactured:
In stirred vessel, catalyzer is joined after in 18% dilute sulphuric acid and add ground dolomite, stirring reaction;
Add magnesium sulfate to stir, then add light calcined magnesia and stir 1-2 minute, with the equipment washing aqueous slurry measured and clear water adjusting viscosity, finally add light filler, and add whipping agent and stir blanking after 2 minutes, with Dual-layer or multilayer glass-fiber-fabric and the face roll forming of nonwoven interlining end liner on fire-proof board molding device, about insulation 25-30 degree, the aftershaping demoulding in 18-48 hour.
embodiment two: building decoration lightweight ceilings concrete steps are as follows:
1, inorganic gel material:
300 order dolomite powders 150;
18% dilute sulphuric acid 32;
Light calcined magnesia 50;
Magnesium sulfate 26;
2, supplementary additive
Water-resisting agent 3;
Whipping agent 18;
Catalyzer 2.5;
Inhibitor 0.15;
3, light filler:
Plant fiber powder 35;
Perlite 24;
4, other
Clear water 15;
Equipment washing aqueous slurry 45;
Operation steps illustrates:
In stirred vessel, catalyzer is joined after in 18% dilute sulphuric acid and add ground dolomite, stirring question response bubble stops after vulcanization acid magnesium to stir, then add light calcined magnesia and stir 1-2 minute, with the equipment washing aqueous slurry measured and clear water adjusting viscosity, finally add light filler, and add the foam suppressed through foaming machine and stir blanking after 2 minutes, with Dual-layer or multilayer glass-fiber-fabric and the face roll forming of nonwoven interlining end liner on fire-proof board molding device, about insulation 25-30 degree, the aftershaping demoulding in 18-48 hour.
embodiment three: building external application warming plate concrete steps are as follows:
1, inorganic gel material:
300 order dolomite powders 150;
18% dilute sulphuric acid 32;
Light calcined magnesia 50;
Magnesium sulfate 26;
2, supplementary additive
Water-resisting agent 3;
Whipping agent 18;
Catalyzer 2.5;
Inhibitor 0.15;
3, light filler:
Granules of polystyrene 12;
4, other
Clear water 10;
Equipment washing aqueous slurry 45;
Operation steps illustrates:
In stirred vessel, catalyzer is joined after in 18% dilute sulphuric acid and add ground dolomite, stir question response.Add magnesium sulfate to stir, add light calcined magnesia and stir 1-2 minute, with the equipment washing aqueous slurry measured and clear water adjusting viscosity, add light filler, and add the foam suppressed through foaming machine stir 2 minutes after blanking on fire-proof board molding device, use Dual-layer roll forming, about insulation 25-30 degree, the aftershaping demoulding in 8-16 hour.
embodiment four: architecture indoor light partition board concrete steps are as follows:
1, inorganic gel material:
300 order dolomite powders 150;
18% dilute sulphuric acid 32;
Light calcined magnesia 50;
Magnesium sulfate 26;
2, supplementary additive
Water-resisting agent 3;
Whipping agent 12;
Catalyzer 2.5;
Inhibitor 0.15;
3, light filler:
Plant fiber powder 35;
Granules of polystyrene 12;
4, other
Clear water 15;
Equipment washing aqueous slurry 60;
Operation steps illustrates:
In stirred vessel, catalyzer is joined after in 18% dilute sulphuric acid and add ground dolomite, stir question response.Add magnesium sulfate to stir, add light calcined magnesia and stir 1-2 minute, with the equipment washing aqueous slurry measured and clear water adjusting viscosity, add light filler, and add the foam suppressed through foaming machine and to stir after 2 minutes blanking at 30000*600*90(120) on hollow aperture combined pressure mould on form or fire-proof board molding device with Dual-layer or multilayer glass-fiber-fabric and the face roll forming of nonwoven interlining end liner, about 25-30 degree, the aftershaping demoulding in 8-16 hour.
Embodiment one decorative panel for building physicals table:
| Thickness mm | Proportion kg/m 3 | Fire-protection rating | Folding strength MPa | Volume water absorption rate % | Contract with dry rate % | The wet rate % that rises | Nail-holding ability N/mm |
| 9 | 993 | A1 | 12 | 6 | 1.0 | 2.3 | 21 |
Embodiment two building decoration lightweight ceilings physicals table:
| Thickness mm | Proportion kg/m 3 | Fire-protection rating | Folding strength MPa | Volume water absorption rate % | Contract with dry rate % | The wet rate % that rises | Nail-holding ability N/mm |
| 8 | 551 | A1 | 8.3 | 6 | 1.0 | 2.3 | 22 |
Embodiment three builds external application light thermal insulation board plate physicals table:
| Thickness mm | Proportion kg/m 3 | Fire-protection rating | Thermal conductivity W/ (M/K) | 30 freeze-thaw-circulation mass loss rate % | Cohesive strength MPa | Folding strength MPa | Resistance to compression hit intensity MPa | Volume water absorption rate % |
| 30 | 221 | A2 | 0.058 | 1 | 0.12 | 0.27 | 0.43 | 6 |
Embodiment four architecture indoor light partition board physicals:
| Thickness mm | The heavy kg/m2 of plate | Fire-protection rating | Sound-damping qualities db | Erosion-resisting characteristics time | Single-point hanging force N | Resistance to compression hit intensity MPa |
| 90 | 32 | A2 | 49 | 7 | 1300 | 12 |
Claims (1)
1. a making method for inorganic dolomite magnesia fireproof gel material, is characterized in that: building decorative plates concrete steps are as follows:
(1) inorganic gel material:
300 order dolomite powder 150 weight parts;
18% dilute sulphuric acid 32 weight part;
Light calcined magnesia 50 weight part;
Magnesium sulfate 26 weight part;
(2) supplementary additive:
Water-resisting agent 2.2 weight part;
Aqueous foaming agent 0.4 weight part;
Catalyzer 2.5 weight part;
Inhibitor 0.15 weight part;
(3) light filler:
Plant fiber powder 65 weight part;
Perlite 12 weight part;
(4) other:
Clear water 15 weight part;
Equipment washing aqueous slurry 25 weight part;
(5) sheet for architectural decoration flow process is manufactured:
In stirred vessel, catalyzer is joined after in 18% dilute sulphuric acid and add ground dolomite, stirring reaction;
Add magnesium sulfate to stir, then add light calcined magnesia and stir 1-2 minute, with the equipment washing aqueous slurry measured and clear water adjusting viscosity, finally add light filler, and add whipping agent and stir blanking after 2 minutes, with the fine cloth of upper and lower layer glass and the face roll forming of nonwoven interlining end liner on fire-proof board molding device, insulation 25-30 degree, the aftershaping demoulding in 18-48 hour.
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| CN201210459606.2A CN102942349B (en) | 2012-11-15 | 2012-11-15 | Manufacturing method of inorganic dolomite magnesia fireproof gel material |
Applications Claiming Priority (1)
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| CN201210459606.2A CN102942349B (en) | 2012-11-15 | 2012-11-15 | Manufacturing method of inorganic dolomite magnesia fireproof gel material |
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| CN102942349A CN102942349A (en) | 2013-02-27 |
| CN102942349B true CN102942349B (en) | 2015-01-07 |
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| CN103834219B (en) * | 2014-01-24 | 2016-09-21 | 徐国清 | A kind of production method of novel environment friendly sealing paint filling |
| CN105859244A (en) * | 2016-03-28 | 2016-08-17 | 北京中晶环境科技股份有限公司 | Solid partition wall plate |
| CN105859243A (en) * | 2016-03-28 | 2016-08-17 | 北京中晶环境科技股份有限公司 | Magnesium oxysulfate cement foamed bricks and preparation method therefor |
| CN106626597A (en) * | 2016-12-05 | 2017-05-10 | 张维满 | Pressure-resistant fireproof plate and manufacturing method thereof |
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| CN106626621A (en) * | 2017-01-04 | 2017-05-10 | 张爱英 | Double-sided decorative waterproof plate and production method thereof |
| CN107619300A (en) * | 2017-09-15 | 2018-01-23 | 上海福精特金属装饰材料有限公司 | The preparation method of fire proofing material composition and its fire-proof board |
| CN108729619A (en) * | 2018-04-08 | 2018-11-02 | 佛山市欣中茂节能建材科技有限公司 | A kind of installation method of raised flooring system and its production method and the floor |
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| CN1098394A (en) * | 1994-07-01 | 1995-02-08 | 薛耀民 | Magnesite cementing material and its use |
| US6395084B1 (en) * | 1999-02-16 | 2002-05-28 | James L. Priest | Platelet/flake magnesium oxide, methods of making the same, and magnesium oxychloride/oxysulfate ceramic materials |
| CN102070353A (en) * | 2010-11-22 | 2011-05-25 | 中国科学院青海盐湖研究所 | Light-burned dolomite foam light partition board |
| CN102515824A (en) * | 2011-11-30 | 2012-06-27 | 南京航空航天大学 | Super-light foam cement concrete and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5604801B2 (en) * | 2009-03-17 | 2014-10-15 | 吉澤石灰工業株式会社 | Soil solidifying material and soil solidifying method |
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Patent Citations (4)
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|---|---|---|---|---|
| CN1098394A (en) * | 1994-07-01 | 1995-02-08 | 薛耀民 | Magnesite cementing material and its use |
| US6395084B1 (en) * | 1999-02-16 | 2002-05-28 | James L. Priest | Platelet/flake magnesium oxide, methods of making the same, and magnesium oxychloride/oxysulfate ceramic materials |
| CN102070353A (en) * | 2010-11-22 | 2011-05-25 | 中国科学院青海盐湖研究所 | Light-burned dolomite foam light partition board |
| CN102515824A (en) * | 2011-11-30 | 2012-06-27 | 南京航空航天大学 | Super-light foam cement concrete and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| JP特开2010-215821A 2010.09.30 * |
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Owner name: DANDONG KINGKANG MINING CO., LTD. Free format text: FORMER OWNER: DANDONG KINGKANG BUILDING MATERIAL CO., LTD. Effective date: 20140627 |
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Effective date of registration: 20140627 Address after: 118200 Liaoning city of Dandong province Kuandian Yongdian Gunzi Village Applicant after: DANDONG KINGKANG BUILDING MATERIAL CO., LTD. Address before: 118200 Liaoning city of Dandong province Kuandian Manchu Autonomous County Gunzi Village Applicant before: Dandong Kingkang Building Material Co., Ltd. |
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Owner name: DANDONG KINGKANG BUILDING MATERIAL CO., LTD. Free format text: FORMER OWNER: DANDONG KINGKANG MINING CO., LTD. Effective date: 20150528 |
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Effective date of registration: 20150528 Address after: 118200, Dandong County, Liaoning province Kuandian County Green Chair Hill Industrial Park Patentee after: Dandong Kingkang Building Material Co., Ltd. Address before: 118200 Liaoning Province, Dandong Kuandian Yongdian Gunzi Village Patentee before: DANDONG KINGKANG BUILDING MATERIAL CO., LTD. |
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Effective date of registration: 20160614 Address after: 321200 Zhejiang city of Jinhua province Wuyi County Lake Street King Village Road Patentee after: Wuyi County magnesium refractories Co., Ltd. Address before: 118200, Dandong County, Liaoning province Kuandian County Green Chair Hill Industrial Park Patentee before: Dandong Kingkang Building Material Co., Ltd. |
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Granted publication date: 20150107 Termination date: 20161115 |