CN104856032A - Method for preparing honeysuckle beverage concentrate through recycled solvent - Google Patents
Method for preparing honeysuckle beverage concentrate through recycled solvent Download PDFInfo
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- CN104856032A CN104856032A CN201510289761.8A CN201510289761A CN104856032A CN 104856032 A CN104856032 A CN 104856032A CN 201510289761 A CN201510289761 A CN 201510289761A CN 104856032 A CN104856032 A CN 104856032A
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to a comprehensive processing method for preparing honeysuckle beverage concentrate and series of products through a recycled solvent. The method is characterized in that edible materials mainly comprising honeysuckle are extracted through a 40-90% ethanol solution; the extraction solution is distilled to obtain ethyl alcohol which can be reutilized and obtain corresponding beverage concentrate and series of processed products at the same time. According to the invention, functional components and flavor substances can be extracted through the ethanol solution more safely and effectively; the obtained beverage concentrate has the advantage of being convenient for raw material storage and fast production; ethyl alcohol is recycled, so that the influence caused by ethyl alcohol remaining in the beverage concentrate and the discharge of the ethyl alcohol to the environment can be reduced; the method can be used for preparing the beverage concentrate, while producing instant beverage, solid electuary, dietary fiber and other series of products. Besides, through the comprehensive processing method, various health beverages having the conditioning function or the function of assisting curative effect can be prepared.
Description
Technical field
The invention belongs to food processing technology field, comprise the extraction to active ingredient in the property of medicine food materials based on honeysuckle, the host product of preparation honeysuckle series beverage and the comprehensive process of the aspect such as health food and beverage.Particularly relate to recycling design, recycle alcohol extract and prepare beverage host, carry out many effects, multi-flavour medicine food processing technology and processing method.
Background technology
Honeysuckle is the plant food materials that the food medicine of Chinese tradition is taken into account.As Chinese herbal medicine honeysuckle, there is antiviral, effect such as anti inflammation and heat resolution, antitumor raising immunity; Also be refrigerant, relieving summer-heat, pest of dispelling heat tea-drinking food simultaneously.No matter honeysuckle, as important industrial production raw material, is in food use or processing of crude drugs scope substantially all adopts and carries out solvent extraction mode to honeysuckle, to obtain the nucleus wherein with treatment, health properties.Chlorogenic acid is one of component substances of wherein the most representative and feature effect.For improving the outstanding utilization of extraction to active ingredient in honeysuckle (be characteristic component mainly with chlorogenic acid) and property of medicine material thereof, many pharmacy corporations and associated production unit thereof all adopt alcohol solvent honeysuckle to extract.By obtaining maximum extracted rate, then extraction product is obtained the processing mode (CN1199728, CN103288644A, CN102443619A, CN1616403, CN102285885A, CN1439410) of medicine.Merely from the viewpoint of Raw material processing, select edible ethanol extraction honeysuckle not only safety, extraction efficiency is high but also can retain original special flavor, should belong to good food processing processing method.But, numerous food product enterprise but because of undue residual (in the soft drink alcohol must not more than 0.5%) of scruple ethanol easily in beverage/food and to problems such as the exhaust emissions of production environment, has to select the mode (201310239133X, CN102485068A, CN103315201A) of high temperature (90 ~ 100 DEG C) extracting in boiling water to carry out the functional component obtained wherein.It is too low and cause the waste of honeysuckle raw material that the result of process operation like this is not only aqueous extraction rate, and hot conditions very easily destroys chlorogenic acid in honeysuckle and flavor components; Simultaneously its highly energy-consuming and height extraction consuming time too increase production cycle and processing cost.In recent years, many manufacturing enterprises and research unit are in food processing, improve honeysuckle functional component productive rate and value, have done much effort research and experiment discussion.Comprise and select the supplementary means such as ultrasonic wave, microwave to improve extraction effect (CN103655667A, CN102824396A, CN102001946A, CN103190676A).From practical function analysis, though there is certain progress, its industrialization effect is not still given prominence to.In addition, honeysuckle raw material is very easily damaged by worms when normal temperature storage and is occurred the phenomenon of going mouldy, and also has and needs honeysuckle price when producing all can annoying relevant processing and manufacturing enterprise far above the raw material problem that waits of harvest time at beverage.
(e.g., 1. alcohol extract easily remains to the present invention be directed to normal some problems existed in honeysuckle drink processing; 2. water extraction efficiency is low, active ingredient is easily destroyed, precipitation easily appears in beverage products put procedure; 3. honeysuckle cost of material is directly stored high), analyze by experiment and study and structure adjusting is carried out to existing honeysuckle beverage production.By on the basis of preparation of drinks host, with the effective component in ethanolic solution extraction honeysuckle and flavor substance.Realize extracting arranged side by side, the comprehensive production model that ethanol recycled, rapidly and efficiently extracted, prepares for shelf-stable, the beverage host just processed and beverage series product.
Summary of the invention
The object of the invention is to overcome the technical deficiency part in original honeysuckle beverage processing process, there is provided a kind of and extract flos lonicerae effect composition and flavor substance safe, fast, efficiently, obtained resistance to accumulating, the honeysuckle beverage host being convenient to processing and relevant series of products, and can extraction ethanol be carried out recovery and be recycled, reduce production cost, decreasing pollution, realize the comprehensive process to honeysuckle, recycle the production method that solvent pattern prepares honeysuckle beverage host and series of products.
The technical scheme that technical solution problem of the present invention adopts is:
Utilize circulating solvent to prepare a method for honeysuckle beverage host, step is as follows:
(1), according to function and the products characteristics of different beverage raw material, select to comprise the different performance of honeysuckle, the raw material of food medicine dual-purpose carry out combination and compatibility, to meet the basic demand of food processing;
(2) raw material are after finishing, require to carry out cleaning, the treatment step such as stoning and pulverizing according to fabrication design, mixed particle uniformly;
(3) particle is loaded in and extracts in cylinder mould or mesh bag and guarantee that particle is not scattered, then inserts in extractor by cylinder mould or mesh bag;
(4) being undertaken adding concentration by the feed liquid mass ratio of 1:5 ~ 20 in extractor is the ethanolic solution of 40% ~ 90%, makes circulation dynamic soaking and extract 1 ~ 3h under 50 ~ 70 DEG C of conditions.Drained by cylinder mould after completing extraction, obtain extract and particle respectively, particle proceeds to residue treatment link, obtains corresponding edible fiber products through processing further;
(5) extract carries out decompression distillation after filtration and concentrates, and the ethanol steamed again does new raw material again and extracts solution use (recycling) after allotment; Extract obtains different honeysuckle beverage host after concentrated.
And described step (4) middle ethanolic solution is the ethanolic solution of 50% ~ 90%.
And, described step (4), (5) in the condition of distillation and concentration be: by after filtration, the extract that is separated carries out decompression distillation, to obtain the host product that solid content is 20% ~ 60% correspondence under lower than 80 DEG C of conditions.
And, described step (5) in the solid quality content of honeysuckle beverage host control 20% ~ 60%.
And, described step (5) in obtain different honeysuckle beverage host and directly can pack and be in store for or transport outward.
And, described step (5) in obtain different honeysuckle beverage host can with suitably prepare burden carry out composite, granulation, drying after obtain solid beverage agent; Or above-mentioned host is after allotment, homogeneous, sterilization, embedding, and juice product drunk by obtained i.e. drink.
And, described step (5) in obtain different honeysuckle beverage host and can carry out the processing of multiple remedy diet, production health-care beverage series and food with suitably prepare burden.
The advantage that the present invention obtains and good effect are:
1, the inventive method utilizes 40% ~ 90% ethanolic solution to extract the food plants such as honeysuckle, produce honeysuckle beverage host through concentration and recovery ethanol simultaneously, in method, use the ethanolic solution of 40 ~ 60 DEG C can safety, high efficiency extraction active ingredient wherein and flavor substance; The beverage host that the method prepares is more conducive to deposit fortune and quick preparation of drinks as raw material; The method adopts the mode of recycle and reuse ethanol can reduce its remaining influence in the beverage and the exhaust emission to environment; The method can be produced i.e. drink and be drunk the series of products such as juice, solid granules and dietary fiber while preparing beverage host, improves the comprehensive processing and utilization to honeysuckle.
2, the beverage host that prepared by the inventive method is more conducive to the deposit of raw material, without the need to considering the mothproof storage of honeysuckle; Beverage host is utilized to be conducive to directly adjusting converting and producing honeysuckle beverage; Honeysuckle beverage is produced in the convenient transport of beverage host and strange land allotment, saves raw material deposit and extracts link; The host that the method obtains directly can complete the production of solid granules by batch mixing, granulation, drying; The residue produced in the method preparation process can directly carry out refinement and kiss-coating process, makes dissimilar diet fiber product.
3, the inventive method utilizes the ethanolic solution under medium temperature (40 ~ 70 DEG C) condition to extract honeysuckle, at utmost can obtain, protect wherein active ingredient and flavor substance, makes beverage products can retain original feature local flavor and drink effect; Utilize the feed liquid mass ratio of ethanolic solution and 1:5 ~ 20 can complete extraction (1 ~ 3h) to honeysuckle fast; Utilize the honeysuckle beverage host that (40% ~ 90%) ethanolic solution can obtain containing certain moisture, be beneficial to dilution that processing further needs and composite; Utilize ethanolic solution to extract and can reduce colloid and protein component stripping in raw material, to reduce the deposited phenomenon that drink juice put procedure occurs.
4, the inventive method is done the utilization of extraction solution again by concentrated extracting solution recovery ethanol and reduces production cost and cost of material; Contribute to reducing ethanol residual quantity in the beverage (in soft drink alcohol must not more than 0.5%) by reclaiming ethanol, in beverage host, residual ethanol in proper amount is conducive to store the protection of active ingredient in beverage host and product, but in beverage production process by dilution on final beverage granules, i.e. product such as drink drink juice and dietary fiber etc. all without affecting; In addition, be conducive to reducing the discharge to environment and pollution by closed extraction and recovery ethanol.
5, the inventive method is by utilizing comprehensive process pattern, selects different properties food to make raw material, produce tasty drink and processed food that series has health-care efficacy in different medicine food resource area.
6, the present invention is in the process of soft drink raw material, utilizes ethanolic solution effectively to improve extraction to effective ingredient of honeysuckle and utilization; Residual and the pollution of ethanol in soft drink product is decreased by Distillation recovery; Producing the concentrated honeysuckle beverage host of series, to have corrosion resistant mothproof, the original advantage that easy storage is just produced; The extraction residue that sealing lixiviate Continuous maching obtains directly processing can become consumable products, to avoid secondary pollution; Be more convenient for the production of non-season of picking flowers, strange land beverage by the honeysuckle beverage host of producing, be conducive to the processing cost and the raw materials consumption that reduce beverage; By the comprehensive process pattern in the present invention, do function compatibility in conjunction with the food material that different supplemental treatment is selected in drug food of TCM prompting, nurse one's health health properties, obtain the health drink that different series has conditioning functions or auxiliary curative effect.
Accompanying drawing explanation
Fig. 1 is preparation technology's flow chart of the inventive method.
Fig. 2 is the effect tendency of extraction temperature of the present invention to chlorogenic acid yield;
Fig. 3 is the effect tendency of extraction time of the present invention to chlorogenic acid yield.
Detailed description of the invention
For content of the present invention, Characteristic can be understood further, hereby exemplify following examples, and coordinate accompanying drawing to be described in detail as follows.It should be noted that, the present embodiment is descriptive, is not determinate, can not limit protection scope of the present invention thus.
The reagent used in the present invention, if no special requirements, is the conventional reagent of this area; The method used in the present invention, if no special requirements, is the conventional method of this area.
Embodiment 1 (clearing heat, relieving sore-throat)
Honeysuckle beverage host: raw material selects honeysuckle 3 parts, chrysanthemum 3 parts, 2 parts, lotus leaf, reed rhizome 2 parts, raw material adds 80 part of 70% ethanolic solution after chopping, be separated residue after 60 DEG C of extraction 2hr, the extract after filtration obtains the beverage host of solid content about 30% after reclaiming ethanol.
Embodiment 2 (driving away summer heat antipyretic)
Dark plum beverage host: raw material selects honeysuckle 3 parts, dark plum 4 parts, the sterculia seed 2 parts, green tea 1 part, raw material adds 150 part of 50% ethanolic solution (if residue is for the preparation of dietary fiber after chopping, dark plum needs to remove hard core), be separated residue after 70 DEG C of extraction 3hr, the extract after filtration obtains the beverage host of solid content about 40% after reclaiming ethanol.
Embodiment 3 (clear pest improving eyesight)
Cassia seed beverage host, raw material selects honeysuckle 1 part, matrimony vine 3 parts, cassia seed 4 parts, chrysanthemum 2 parts of raw materials to add 70 part of 60% ethanolic solution after chopping, be separated residue after 70 DEG C of extraction 2hr, the extract after filtration obtains the beverage host of solid content about 50% after reclaiming ethanol.
Embodiment 4 (relieve summer heating Detoxication)
Bamboo leaf beverage host and drink juice: raw material selects honeysuckle 2 parts, 4 parts, the leaf of bamboo, dried peppermint leaf 2 parts, lotus leaf 2 parts of raw materials to add 80 part of 60% ethanolic solution after chopping, be separated residue after 60 DEG C of extraction 2hr, the extract after filtration obtains beverage host after reclaiming ethanol.
Add appropriate citric acid, HFCS, sweetener, thickener etc. in above-mentioned beverage host, obtain drink juice product through operation links such as homogeneous, sterilization, specifications.
Embodiment 5 (appetizingization silt)
Hawthorn beverage host and electuary: raw material comprises honeysuckle 2 parts, dark plum 3 parts, hawthorn 4 parts, reed rhizome 2 parts, raw material adds 120 part of 50% ethanolic solution (if residue is for the preparation of dietary fiber after chopping, dark plum needs to remove hard core), be separated residue after 70 DEG C of extraction 3hr, the extract after filtration obtains beverage host after reclaiming ethanol.
Directly add the operations such as the batching such as acid, sweetener, maltodextrin carries out mixing, granulation, drying in above-mentioned beverage host, obtain solid beverage agent product.
Embodiment 6 (warm stomach is calmed the nerves)
Jujube tea host and electuary: raw material comprises honeysuckle 2 parts, reed rhizome 2 parts, 5 parts, date, black tea 1 part, raw material adds 100 part of 60% ethanolic solution (if residue is for the preparation of dietary fiber after chopping, date needs to remove hard core), be separated residue after 70 DEG C of extraction 3hr, the extract after filtration obtains beverage host after reclaiming ethanol.
Directly add the operations such as the batching such as acid, sweetener, maltodextrin carries out mixing, granulation, drying in above-mentioned beverage host, obtain solid beverage agent product.
(beverage has heat-clearing and relieves the effect of alcohol embodiment 7; Capsule then has defaecation gut purge effect)
Kudzu root beverage host and dietary fiber capsule: raw material selects honeysuckle 2 parts, the root of kudzu vine 3 parts, reed rhizome 2 parts, chrysanthemum 3 parts, raw material adds 80 part of 70% ethanolic solution after chopping, filter extract after 70 DEG C of extraction 1hr and obtain residue simultaneously, after reclaiming ethanol, obtain beverage host.
Be separated residue to carry out colloid mill refinement, mix with glucan, inulin etc. again, drying, powder process, filling, obtained dietary fiber capsule product.
(beverage has appetizing of quenching one's thirst to embodiment 8; Chewable tablets then has desilting defaecation effect)
Chinese wolfberry fruit drink host and fiber chewable tablets: raw material selects honeysuckle 1 part, matrimony vine 4 parts, hawthorn 3 parts, witloof 2 parts, raw material adds 100 part of 60% ethanolic solution after chopping, be separated residue after 70 DEG C of extraction 3hr, the extract after filtration obtains beverage host after reclaiming ethanol.
Separation residue carried out colloid mill refinement, prepare burden with glucan, inulin, xanthans, acid, sweetener, essence etc. and mix again, drying, powder process, compressing tablet, obtained dietary fiber chewable tablets product.
The related test results of the different honeysuckle beverage host that the method that the present invention utilizes circulating solvent to prepare honeysuckle beverage host prepares:
Honeysuckle as its functional component of property of medicine food materials and flavor substance kind more complicated, and outstanding characteristic component material is chlorogenic acid.Substantially be analyze the technical indicator with assessment with the recovery rate of its Content of Chlorogenic Acid (%) and productive rate (mg/g) when relating to honeysuckle extraction effect in the present invention.
First the present invention prepares by utilizing ethanolic solution to extract honeysuckle comprehensive production model and the method that honeysuckle beverage host carries out relevant serial Product processing simultaneously, as shown in Figure 1.
Present invention utilizes the principle (as table 1) of the easier stripping of the more simple aqueous phase of ethanolic solution and protection chlorogenic acid, ethanol water then remains and proposes the reservation of its submember compound sugar.
The different extractant of table 1 is to the extraction effect table of chlorogenic acid
After complete lixiviate being carried out to honeysuckle or auxiliary material by ethanol water, obtain the most high extraction of wherein active ingredient and maximum productive rate.Simultaneously after completing extraction, ethanol used is then recycled by distillation and concentration, then makees the extract of new raw material.Ethanol prepare non-volatile in beverage host and product, do not remain, do not discharge, constantly recycle.For checking invention effect, again investigating ethanolic solution affects the contrast of honeysuckle under different extraction temperature and extraction time condition from simple aqueous phase.Investigate result and indicate ethanolic solution to the advantage of honeysuckle extraction effect and feature simultaneously, the results are shown in Figure shown in 2 and Fig. 3.
Ethanolic solution is being extracted in the investigation that can reduce and reduce the generation of beverage products deposited phenomenon, the stripping that can be reduced protein because of residual in extract or polysaccharide material by the extraction of ethanolic solution can be seen, thus effectively avoid or and reduce the deposited phenomenon that the beverage products made displays in process (table 2) occurs.
The precipitation degree table of the different extract of table 2 in put procedure
Symbol implication :+/+: precipitation is significantly; +: cotton-shaped suspension;-/+: slightly thread suspension;-: clarity is poor;-/-be clear completely.
Claims (7)
1. utilize circulating solvent to prepare a method for honeysuckle beverage host, it is characterized in that: step is as follows:
(1), according to different beverage functional characteristics, select to comprise the different performance of honeysuckle, the raw material of food medicine dual-purpose carry out combination and compatibility, to meet food processing basic demand;
(2) raw material are after finishing, require to carry out cleaning, the treatment step such as stoning and pulverizing according to fabrication design, mixed particle uniformly;
(3) particle is loaded in and extracts in cylinder mould or mesh bag and guarantee that particle is not scattered, then inserts in extractor by cylinder mould or mesh bag;
(4) being undertaken adding concentration by the feed liquid mass ratio of 1:5 ~ 20 in extractor is the ethanolic solution of 40% ~ 90%, makes circulation dynamic soaking and extract 1 ~ 3h under 50 ~ 70 DEG C of conditions.Drained by cylinder mould after completing extraction, obtain extract and particle respectively, particle proceeds to residue treatment link, obtains corresponding edible fiber products through processing further;
(5) extract carries out decompression distillation after filtration and concentrates, and the ethanol steamed again does new raw material again and extracts solution use (recycling) after allotment; Extract obtains different honeysuckle beverage host after concentrated.
2. utilization circulation Extraction solvent according to claim 1 prepares the method for honeysuckle beverage host, it is characterized in that: described step (4) middle ethanolic solution is the edible ethanol solution of 50% ~ 90%.
3. the method utilizing circulating solvent to prepare honeysuckle beverage host according to claim 1, it is characterized in that: described step (4), (5) in the condition of distillation and concentration be: by after filtration, the extract that is separated carries out decompression distillation, to obtain the host product that solid content is 20% ~ 60% correspondence under lower than 80 DEG C of conditions.
4. the circulating solvent that utilizes according to any one of claims 1 to 3 prepares the method for honeysuckle beverage host, it is characterized in that: described step (5) in the solid quality content of honeysuckle beverage host control 20% ~ 60%.
5. the circulating solvent that utilizes according to any one of claims 1 to 3 prepares the method for honeysuckle beverage host, it is characterized in that: described step (5) in obtain different honeysuckle beverage host and directly can pack and be in store for or transport outward.
6. the circulating solvent that utilizes according to any one of claims 1 to 3 prepares the method for honeysuckle beverage host, it is characterized in that: described step (5) in obtain different honeysuckle beverage host can with suitably prepare burden carry out composite, granulation, drying after obtain solid beverage agent; Or above-mentioned host is after allotment, homogeneous, sterilization, embedding, and juice product drunk by obtained i.e. drink.
7. the circulating solvent that utilizes according to any one of claims 1 to 3 prepares the method for honeysuckle beverage host, it is characterized in that: described step (5) in can to multiple health giving quality food materials and batching compatibility extract and comprehensive process, to obtain health drink and the processed food of different honeysuckle series beverage host and correspondence.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199728A (en) * | 1997-05-15 | 1998-11-25 | 中国人民武装警察部队湖北省总队医院 | Chlorogenic acid extracting process from honeysuckle |
| CN101288485A (en) * | 2008-05-26 | 2008-10-22 | 北京市科威华食品工程技术有限公司 | Honeysuckle health-care beverage |
| CN101999493A (en) * | 2010-12-08 | 2011-04-06 | 费维来 | Preparation method of plant health-care cool tea |
| US20140141082A1 (en) * | 2012-11-16 | 2014-05-22 | Song Gao | Compositions Containing Enriched Natural Crocin and/or Crocetin, and Their Therapeutic or Nutraceutical Uses |
| CN104069150A (en) * | 2014-07-18 | 2014-10-01 | 鲁南制药集团股份有限公司 | Preparation method for honeysuckle extract |
-
2015
- 2015-06-01 CN CN201510289761.8A patent/CN104856032A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199728A (en) * | 1997-05-15 | 1998-11-25 | 中国人民武装警察部队湖北省总队医院 | Chlorogenic acid extracting process from honeysuckle |
| CN101288485A (en) * | 2008-05-26 | 2008-10-22 | 北京市科威华食品工程技术有限公司 | Honeysuckle health-care beverage |
| CN101999493A (en) * | 2010-12-08 | 2011-04-06 | 费维来 | Preparation method of plant health-care cool tea |
| US20140141082A1 (en) * | 2012-11-16 | 2014-05-22 | Song Gao | Compositions Containing Enriched Natural Crocin and/or Crocetin, and Their Therapeutic or Nutraceutical Uses |
| CN104069150A (en) * | 2014-07-18 | 2014-10-01 | 鲁南制药集团股份有限公司 | Preparation method for honeysuckle extract |
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