CN104789109B - A kind of environment-friendly water-based lacquer as woodenware finish and preparation method thereof - Google Patents
A kind of environment-friendly water-based lacquer as woodenware finish and preparation method thereof Download PDFInfo
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- CN104789109B CN104789109B CN201510238350.6A CN201510238350A CN104789109B CN 104789109 B CN104789109 B CN 104789109B CN 201510238350 A CN201510238350 A CN 201510238350A CN 104789109 B CN104789109 B CN 104789109B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/47—Levelling agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of environment-friendly water-based lacquer as woodenware finish, it is related to water paint technical field, it is composed of the following components by weight：78.5 83.5 parts of acrylic acid modified polyurethane, 3.5 6.5 parts of coalescents, 0.3 0.6 parts of wetting agent, 0.1 0.4 parts of aqueous defoamer, aqueous 0.3 1 parts of slip agent, 0.5 0.75 parts of levelling agent, 0.2 1.5 parts of sterilization antiseptic, 58 parts of Anti-moth-eating powder, 0.2 0.6 parts of PH conditioning agents, 10 15 parts of water, the Anti-moth-eating powder is the mixture of 2 3.5 parts of azedarach powder and 3 4.5 parts of Celastrus angulatus pulvis.Beneficial effects of the present invention：Using environment-friendly water-based lacquer as woodenware finish made from special formulation of the present invention and method, with good anti-moth and insect prevention result, scratch resistance capability is strong, wear-resisting, hardness is high, substantially increases the service life of product, meanwhile, other performances also comply with relevant national standard.
Description
Technical field
The present invention relates to water paint technical field, more particularly to a kind of environment-friendly water-based lacquer as woodenware finish and preparation method thereof.
Background technology
With the development and the enhancing of people's environmental consciousness of society, the environmental regulation that various countries are formulated is all to volatility in coating
Organic compound (VOC) has strict limitation, such as standard GB/T 1851-2009《Interior decoration material, solvent wood coatings
Middle limits of harmful substances》、GB24410-2009《Limits of harmful substances in indoor decorating and refurnishing materials, water-borne wood coating》, it is right
VOC limitation, which is proposed, in indoor coating is distinctly claimed.
Woodcare paint can assign timber, rattan articles color, gloss, and it can also be helped to resist caused by humidity, chemical attack etc.
Destruction, but the mothproof effect of current woodcare paint insect prevention is poor, and not wear-resisting, scratch resistance capability is not strong, and hardness is not high.
The content of the invention
In view of this, an object of the present invention is to provide a kind of environment-friendly water-based lacquer as woodenware finish, with insect prevention, anti-zoned
The high advantage of wound, wear-resisting, hardness.
The present invention solves above-mentioned technical problem by following technological means：
It is composed of the following components by weight the invention provides a kind of environment-friendly water-based lacquer as woodenware finish：It is acrylic acid modified poly-
78.5-83.5 parts of urethane, 3.5-6.5 parts of coalescents, 0.3-0.6 parts of wetting agent, 0.1-0.4 parts of aqueous defoamer is aqueous to increase
0.3-1 parts of lubrication prescription, 0.5-0.75 parts of levelling agent, 0.2-1.5 parts of sterilization antiseptic, 5-8 parts of Anti-moth-eating powder, pH adjusting agent 0.2-
0.6 part, 10-15 parts of water, the Anti-moth-eating powder is the mixture of 2-3.5 parts of azedarach powder and 3-4.5 parts of Celastrus angulatus pulvis.
One kind that acrylic acid and polyurethane polyureas are combined by aforesaid propylene acid modified polyurethane by polymerizations such as core-shell structure copolymers
New type resin, it not only has weatherability chemical resistance of acrylic resin and the wetability to pigment and inherits polyurethane
The performances such as the high adhesion force wearability and high rigidity of resin.
Wetting agent uses non-ionic wetting agent, mainly contains simple function group, oleoyl alkylene oxide block copolymer, right
Color stuffing peptizaiton, and improve color developing.
Aqueous defoamer is one kind in nonionic defoamer, molecular antifoaming agent, with good compatibility and can
Principal characteristic.
Levelling agent use can promote coating to form a smooth, smooth, uniform film during drying and forming-film.Can have
Liquid surface tension is covered with paint, lacquer, colour wash, etc. in effect reduction, improves its levelability and a class material of uniformity, can be improved the permeability for covering with paint, lacquer, colour wash, etc. liquid, can be subtracted
The possibility of spot and spot is produced when brushing less, increases spreadability, makes film forming uniform, natural.
Anti-moth-eating powder is the mixture of azedarach powder and Celastrus angulatus pulvis, and azedarach powder is shone by the bark and root skin of China tree
Dry grinds, bitter；It is cold in nature；It is poisonous；There is desinsection and tinea is treated.The active insecticidal components of Celastrus angulatus are from Celastrus angulatus
The compound separated, Celastrus angulatus has the active insecticidal components of anesthesia, food refusal and stomach poison function.Celastrus angulatus pulvis
It is made up of Celastrus angulatus, the mixture of azedarach powder and Celastrus angulatus pulvis is vegetable insecticide, and environmental protection is harmless.
Further, it is composed of the following components by weight：79-82 parts of acrylic acid modified polyurethane, coalescents 4-5.5
Part, 0.45-0.5 parts of wetting agent, 0.2-0.35 parts of aqueous defoamer, aqueous slip agent 0.5-0.7 parts, levelling agent 0.55-0.65
Part, 0.4-1.3 parts of sterilization antiseptic, 6-7 parts of Anti-moth-eating powder, 0.3-0.5 parts of pH adjusting agent, 12-14 parts of water, the Anti-moth-eating powder
For 2-3 parts of azedarach powder and the mixture of 3.5-4 parts of Celastrus angulatus pulvis.
Further, it is composed of the following components by weight：81 parts of acrylic acid modified polyurethane, 4 parts of coalescents, wetting agent
0.5 part, 0.3 part of aqueous defoamer, aqueous 0.7 part of slip agent, 0.6 part of levelling agent, 1.1 parts of sterilization antiseptic, Anti-moth-eating powder 7
Part, 0.4 part of pH adjusting agent, 13 parts of water, the Anti-moth-eating powder is the mixture of 3 parts of azedarach powder and 4 parts of Celastrus angulatus pulvis.
Further, described coalescents are Lauryl Alcohol ester, contribute to film forming matter film forming at low temperature.
Further, the sterilization antiseptic uses the isothiazolinone disinfecting agent without VOC, with heat resistance, rises simultaneously
Sterilization and anticorrosion is acted on.
Further, the levelling agent is polyether polyester azo polyether polyeste levelling agent, with polyethers, polyester modification siloxanes
Be greatly improved with the compatibility of resin, reduce surface tension, control surface flowing ability, increase slip, nonshrink hole,
The effect of resist blocking and that is also all fine.
A kind of preparation method of environment-friendly water-based lacquer as woodenware finish of the present invention, specifically includes following steps：
A. feeding is standby according to a formula；
B. wetting agent and water are added into mixer, it is scattered 7 minutes with 800 revs/min of speed mixing；
C. aqueous defoamer is added in the dispersion liquid obtained to step B, it is scattered 4 minutes with 600 revs/min of speed mixing；
D. keep rotating speed constant, acrylic acid modified polyurethane, coalescents, aqueous increasing are sequentially added into the dispersion liquid
Lubrication prescription, modified polyorganosiloxane levelling agent, sterilization antiseptic and Anti-moth-eating powder；
E. pH adjusting agent is added into the dispersion liquid, the acid-base value scope for adjusting the dispersion liquid is 8~9, with 600
Rev/min scattered 15 minutes of speed mixing.
Beneficial effects of the present invention：Using environment-friendly water-based woodenware face made from special formulation of the present invention and method
Paint, with good anti-moth and insect prevention result, scratch resistance capability is strong, wear-resisting, hardness is high, substantially increases the service life of product,
Meanwhile, other performances also comply with relevant national standard.
Embodiment
Embodiment 1
Environment-friendly water-based lacquer as woodenware finish, it is composed of the following components by weight：Acrylic acid modified polyurethane is had using Weng Kaier
The product of limit company, model H-40, weight is 78.5Kg, coalescents 3.5Kg, wetting agent 0.3Kg, aqueous defoamer
0.4Kg, aqueous slip agent 1Kg, polyether polyester azo polyether polyeste levelling agent 0.5Kg, isothiazolinone disinfecting agent 0.5Kg,
Anti-moth-eating powder 5Kg, pH adjusting agent 0.3Kg, water 11Kg, Anti-moth-eating powder are the mixing of 2Kg azedaraches powder and 3Kg Celastrus angulatus pulvis
Thing.Azedarach powder dries grinds, bitter by the bark and root skin of China tree；It is cold in nature；It is poisonous；There is desinsection and tinea is treated.
The compound that the active insecticidal components of Celastrus angulatus are separated from Celastrus angulatus, with having anesthesia, food refusal and stomach poison function.It is bitter
Skin rattan element pulvis is made up of Celastrus angulatus, and the mixture of azedarach powder and Celastrus angulatus pulvis is vegetable insecticide, and environmental protection is to people
Body is harmless, adds azedarach powder in environment-friendly water-based lacquer as woodenware finish and Celastrus angulatus pulvis makes it have the mothproof effect of good insect prevention
Really.The acrylic acid modified polyurethane of use, its feature adds wear-resisting and anti-chemistry in addition to the characteristics of adhering to acrylic paint, again
Property it is strong the characteristics of, make hardness of paint film preferably, the examination of pencil rule is 1H, richness is preferable.Coalescents are Lauryl Alcohol ester, also may be used
Arbitrarily to be mixed with the one or two kinds of in dipropylene and dipropylene glycol methyl ether, contribute to film forming matter at low temperature into
Film.
The preparation method of environment-friendly water-based lacquer as woodenware finish, mixer is added by wetting agent and water, mixed with 800 revs/min of speed
Close scattered 7 minutes；Aqueous defoamer is added into above-mentioned dispersion liquid again, it is scattered 4 minutes with 600 revs/min of speed mixing；Keep
Rotating speed is constant, and acrylic acid modified polyurethane is sequentially added into the dispersion liquid, and Lauryl Alcohol ester, aqueous slip agent, polyethers gathers
Ester modified organosiloxane levelling agent, isothiazolinone disinfecting agent, azedarach powder and Celastrus angulatus pulvis；It is last to disperse to above-mentioned
PH adjusting agent is added in liquid, the acid-base value scope of regulation dispersion liquid is 8~9, it is scattered 15 minutes with 600 revs/min of speed mixing
It can be made into product.
Embodiment 2
Environment-friendly water-based lacquer as woodenware finish, composed of the following components by weight, acrylic acid modified polyurethane 83.5Kg, film forming is helped
Agent 6.5Kg, wetting agent 0.45Kg, aqueous defoamer 0.3Kg, aqueous slip agent 0.7Kg, polyether polyester azo polyether polyeste stream
Flat agent 0.6Kg, isothiazolinone disinfecting agent 1.1Kg, pH adjusting agent 0.4Kg, water 13Kg, Anti-moth-eating powder be 3Kg azedaraches powder and
The mixture of 4Kg Celastrus angulatus pulvis.
The preparation method be the same as Example 1 of above-mentioned environment-friendly water-based lacquer as woodenware finish.
Embodiment 3
Environment-friendly water-based lacquer as woodenware finish, composed of the following components by weight, acrylic acid modified polyurethane 81Kg, coalescents
4Kg, wetting agent 0.5Kg, aqueous defoamer 0.1Kg, aqueous slip agent 0.6Kg, polyether polyester azo polyether polyeste levelling agent
0.75Kg, isothiazolinone disinfecting agent 0.8Kg, pH adjusting agent 0.35Kg, water 12Kg, Anti-moth-eating powder be 2.5Kg azedaraches powder and
The mixture of 4.5Kg Celastrus angulatus pulvis.
The preparation method be the same as Example 1 of above-mentioned environment-friendly water-based lacquer as woodenware finish.
In above three example, acrylic acid modified polyurethane uses the product of Weng Kaier Co., Ltds, model H-40, water
Property defoamer the product of Fine Chemical Co., Ltd is entered using Dongguan City Gauss, product type is GSK-713 defoamers, pH regulations
Agent uses the product of the credible Chemical Co., Ltd. of Yixing City, and product type is KX-pH pH adjusting agent.
As carrying out performance detection to environment-friendly water-based lacquer as woodenware finish obtained by above-described embodiment, property indices see the table below：
As can be seen from the above table, environment-friendly water-based lacquer as woodenware finish of the invention has relative to common environment-friendly water-based lacquer as woodenware finish
There is extraordinary anti-moth and insect prevention result, scratch resistance capability is strong, and abrasion resistant effect is good, and hardness is 3H, and other indexs meet GB1851-
2009 and GB24410-2009 standard.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to compared with
The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to skill of the invention
Art scheme is modified or equivalent, and without departing from the objective and scope of technical solution of the present invention, it all should cover at this
Among the right of invention.
Claims (7)
1. a kind of environment-friendly water-based lacquer as woodenware finish, it is characterised in that：It is composed of the following components by weight：Acrylic acid modified polyurethane
78.5-83.5 parts, 3.5-6.5 parts of coalescents, 0.3-0.6 parts of wetting agent, 0.1-0.4 parts of aqueous defoamer, aqueous slip agent
0.3-1 parts, 0.5-0.75 parts of levelling agent, 0.2-1.5 parts of sterilization antiseptic, 5-8 parts of Anti-moth-eating powder, 0.2-0.6 parts of pH adjusting agent,
10-15 parts of water, the Anti-moth-eating powder is the mixture of 2-3.5 parts of azedarach powder and 3-4.5 parts of Celastrus angulatus pulvis.
2. environment-friendly water-based lacquer as woodenware finish as claimed in claim 1, it is characterised in that：It is composed of the following components by weight：Third
79-82 parts of olefin(e) acid modified polyurethane, 4-5.5 parts of coalescents, 0.45-0.5 parts of wetting agent, 0.2-0.35 parts of aqueous defoamer,
Aqueous slip agent 0.5-0.7 parts, 0.55-0.65 parts of levelling agent, 0.4-1.3 parts of sterilization antiseptic, 6-7 parts of Anti-moth-eating powder, pH is adjusted
Save 0.3-0.5 part of agent, 12-14 part of water, the Anti-moth-eating powder mixes for 2-3 parts of azedarach powder and 3.5-4 parts of Celastrus angulatus pulvis
Compound.
3. environment-friendly water-based lacquer as woodenware finish as claimed in claim 1, it is characterised in that：It is composed of the following components by weight：Third
81 parts of olefin(e) acid modified polyurethane, 4 parts of coalescents, 0.5 part of wetting agent, 0.3 part of aqueous defoamer, aqueous 0.7 part of slip agent, stream
Flat 0.6 part of agent, 1.1 parts of sterilization antiseptic, 7 parts of Anti-moth-eating powder, 0.4 part of pH adjusting agent, 13 parts of water, the Anti-moth-eating powder is 3 parts
The mixture of azedarach powder and 4 parts of Celastrus angulatus pulvis.
4. the environment-friendly water-based lacquer as woodenware finish as described in one of claim 1-3, it is characterised in that：Described coalescents are 12 carbon
Alcohol ester.
5. the environment-friendly water-based lacquer as woodenware finish as described in one of claim 1-3, it is characterised in that：The sterilization antiseptic is used and is free of
VOC isothiazolinone disinfecting agent.
6. the environment-friendly water-based lacquer as woodenware finish as described in one of claim 1-3, it is characterised in that：The levelling agent changes for polyether polyester
Property organosiloxane levelling agent.
7. the preparation method of the environment-friendly water-based lacquer as woodenware finish according to one of claim 1-3, it is characterised in that：Include successively
Following steps：
A. feeding is standby according to a formula；
B. wetting agent and water are added into mixer, it is scattered 7 minutes with 800 revs/min of speed mixing；
C. aqueous defoamer is added in the dispersion liquid obtained to step B, it is scattered 4 minutes with 600 revs/min of speed mixing；
D. keep rotating speed constant, acrylic acid modified polyurethane is sequentially added into the dispersion liquid, coalescents, aqueous increasing is slided
Agent, polyether polyester azo polyether polyeste levelling agent, isothiazolinone disinfecting agent and Anti-moth-eating powder；
E. pH adjusting agent is added into the dispersion liquid, the acid-base value scope for adjusting the dispersion liquid is 8~9, with 600 revs/min
Scattered 15 minutes of speed mixing.
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105315882A (en) * | 2015-11-16 | 2016-02-10 | 北京展辰新材料有限公司 | Water-based scratch-resistant transparent finishing coat as well as preparation method and application thereof |
| CN105602428A (en) * | 2016-02-02 | 2016-05-25 | 宁波美代进出口有限公司 | Antimicrobial mildewproof mothproof finish paint for furniture and preparation method thereof |
| CN106634554A (en) * | 2017-01-10 | 2017-05-10 | 大连佳秀百隆新材料股份有限公司 | Water-based wood finish formula |
| CN107418424A (en) * | 2017-09-08 | 2017-12-01 | 肇庆高新区恒泰信息服务有限公司 | A kind of novel high-performance acrylic acid modified polyurethane aqueous woodware paint |
| CN111234619A (en) * | 2018-11-09 | 2020-06-05 | 上饶市中科化工有限责任公司 | Formula of water-soluble air-drying finish paint |
| CN112300683A (en) * | 2019-07-30 | 2021-02-02 | 董智慧 | Multifunctional water-based woodware high-gloss finish paint and preparation method thereof |
| CN111978811A (en) * | 2020-08-07 | 2020-11-24 | 珠海展辰新材料股份有限公司 | Water-based single-component top-coat paint and preparation method thereof |
| CN114574102A (en) * | 2022-03-15 | 2022-06-03 | 尚品本色智能家居有限公司 | Plant extraction environment-friendly paint and production process thereof |
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| CN103262868B (en) * | 2013-05-23 | 2014-09-10 | 洛阳早春大樱桃种植农民专业合作社 | Biological insecticide for cherry trees and preparation method thereof |
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| US6001915A (en) * | 1994-10-20 | 1999-12-14 | Basf Coating Ag | Polyurethane-modified polyacrylate |
| CN104341990A (en) * | 2013-07-31 | 2015-02-11 | 徐州居叶香家具有限公司 | Mildew and moth resistant woodenware paint |
| CN103385261A (en) * | 2013-08-09 | 2013-11-13 | 邹飞剑 | Efficient green pesticide and production method thereof |
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| CN104449336A (en) * | 2014-12-11 | 2015-03-25 | 广东朗法博涂装新材料科技有限公司 | Self-repairing waterborne woodware finishing coat |
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